CN107737028A - A kind of three layers of gentle make up remover and preparation method thereof - Google Patents
A kind of three layers of gentle make up remover and preparation method thereof Download PDFInfo
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- CN107737028A CN107737028A CN201711110938.9A CN201711110938A CN107737028A CN 107737028 A CN107737028 A CN 107737028A CN 201711110938 A CN201711110938 A CN 201711110938A CN 107737028 A CN107737028 A CN 107737028A
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- layers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/33—Free of surfactant
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
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- Birds (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The present invention proposes a kind of three layers of gentle make up remover, including the plant oil phase on upper strata, the silicone oil phase in middle level and the aqueous phase of lower floor, and based on the gross weight of three layers of described make up remover, the plant oil phase is 10 ~ 30%；The silicone oil is mutually 20 ~ 30%；The aqueous phase includes the water of 20 ~ 30% polyalcohol, 0.05 ~ 1% inorganic salts and surplus, and each component sum is 100%.The present invention also proposes the preparation method of described three layers of gentle make up remover.Three layers of make up remover of the present invention, without surfactant and traditional preservatives, and possess high cleaning power, the skin moisturizing after washing, and both without tight feeling, are also remained without obvious greasy feeling, it is smaller to skin irritation the advantages that.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of three layers of gentle make up remover and preparation method thereof.
Background technology
Makeup removal products mainly have the types such as makeup remover, makeup remover, double-deck make up remover.Wherein makeup remover is by without oil institute
Poor with the ability of removing ornaments and formal dress, some makeup removers are also added into table work composition, and the stimulation to skin is larger.Makeup remover and double-deck make up remover
Due to containing a large amount of mineral oil component, obvious stimulation sense slightly having been stopped after makeup removing, the greasy feeling of skin is remained after being cleaned
Also it is relatively strong, and tight discomfort, need to further it be cleaned with cleaning supplies such as mildy wash, and the normal skin of skin can be influenceed by repeatedly cleaning
Adipose gland is secreted, and destroys the natural protective barrier of skin.In addition, makeup removal products contain preservative, and it is big to the excitant of skin, it is right
Be not suitable for long-term use in the more fragile position of eye lip skin or sensitive flesh user.
The content of the invention
The defects of to overcome prior art, it is an object of the invention to provide a kind of three layers of gentle make up remover, without table
Face activating agent and traditional preservatives, and possess high cleaning power, the skin moisturizing after washing, both without tight feeling, also without obvious greasy feeling
Residual is smaller to skin irritation.
It is another object of the present invention to propose the preparation method of upper described three layers of gentle make up remover.
The present invention proposes a kind of three layers of gentle make up remover, including the plant oil phase on upper strata, the silicone oil phase in middle level and lower floor
Aqueous phase, based on the gross weight of three layers of described make up remover, the plant oil phase be 10~30%；The silicone oil mutually for 20~
30%；The aqueous phase includes the water of 20~30% polyalcohol, 0.05~1% inorganic salts and surplus, and each component sum is
100%.
In the one or more embodiments of the present invention, the density of the plant oil phase is 0.8~0.9g/mL, and saponification number is
90~200mg KOH/g.The vegetable oil phase density is smaller, and decolouring of the plant oil phase on upper strata, preferably water white transparency can be achieved
Vegetable oil, it is easy to toning to form aesthetic appearances.The plant oil phase chooses plant of the saponification number in the range of 90~200mg KOH/g
Thing oil, helps to be formed and stablizes three layers of outward appearance, therefore system stability is had a certain impact.
In the one or more embodiments of the present invention, the plant oil phase includes macadimia nut oil, gardenia flower oil, Jojoba
One or both of seed oil, olive oil, sweet almond oil are a variety of.
In the one or more embodiments of the present invention, the silicone oil is mutually dimethyl silicone polymer.
In the one or more embodiments of the present invention, the polyalcohol includes DPG, glycerine, isoprene, 1,3-
One or both of butanediol and propane diols are a variety of.
In the one or more embodiments of the present invention, the inorganic salts include sodium chloride, potassium chloride, sodium citrate, phosphoric acid
One or both of potassium, magnesium sulfate are a variety of.
The present invention also proposes a kind of preparation method of above-mentioned three layers of gentle make up remover, comprises the following steps：
S1：Each raw material of aqueous phase is weighed, polyalcohol and inorganic salts are dispersed in water, is heated to about 85~90 DEG C, insulation 20
~40min, it is well mixed to obtain mixture；
S2：S1 mixture is cooled to room temperature, obtains the aqueous phase of lower floor；
S3：Silicone oil phase, vegetable oil are added into S2 lower floor's aqueous phase successively, obtain upper strata be vegetable oil, middle level be
Silicone oil, the product that lower floor is aqueous phase.
Compared with prior art, three layers of make up remover of the invention have advantages below：
1st, oil phase accounting is up to 30%-60% in three layers of make up remover of the invention, the color make-up stronger to film formings such as informers
Also there is good dissolubility；Contain plant oil phase and silicone oil phase in three layers of make up remover simultaneously, to silicone oil system and vegetable oils
It is that cosmetics have preferable dissolubility, therefore three layers of make up remover have high cleaning power.
2nd, three layers of make up remover of the invention contain oil phase and aqueous phase simultaneously, and makeup removing is realized by oil phase solubilising, water oil separation,
Remained without oil, therefore available clear water is cleaned completely, is remained without obvious greasy feeling.
3rd, plant oil phase is contained in three layers of make up remover of the invention, crude vegetal can dissolve oil-soluble dirt, while right
Skin has certain moist and nursing efficacy so that washes rear skin moisturizing, no tight feeling.
4th, surfactant is free of in three layers of make up remover of the invention, thus it is gentleer to skin, and excitant is relatively small,
It is equally applicable in the sensitive skin such as eye and lip.
5th, more than 20% polyalcohol is contained in three layers of make up remover of the invention, the polyalcohol of high content has double action：
The polyalcohol of one side high content has from antiseptic property, can avoid adding traditional preservatives, further reduce to skin
Excitant；Another aspect polyalcohol has certain dissolubility to oil-soluble dirt, can further enhance makeup removing ability.
6th, the inorganic salts included in the aqueous phase of three layers of make up remover of the invention, have the function that to be demulsified, three layers of make up remover are same
Shi Hanyou oil phases and aqueous phase, makeup removing is realized by oil phase solubilising, water oil separation, emulsifiable shape under the conditions of shaking in use
Into emulsification system, the inorganic salts of addition can promote emulsification system fast hierarchical, realize water oil separation, further enhance makeup removing power.
Embodiment
With reference to specific embodiment, the present invention is described further：
Embodiment 1-5 and comparative example 1-3：
First, the preparation of make up remover composition
1st, the component proportion of embodiment 1-5 in table 1 is prepared according to the following steps respectively：
S1：Each raw material of aqueous phase is weighed, polyalcohol and inorganic salts are dispersed in water, is heated to about 85~90 DEG C, insulation 20
~40min, it is well mixed to obtain mixture；
S2：S1 mixture is cooled to room temperature, obtains the aqueous phase of lower floor；
S3：Silicone oil phase, vegetable oil are added into S2 lower floor's aqueous phase successively, obtain upper strata be vegetable oil, middle level be
Silicone oil, the transparent three layer make up remover composition that lower floor is aqueous phase.
Table 1
2nd, the component proportion of the comparative example 1-3 in table 2 is mixed to get corresponding make up remover composition respectively.
Table 2
2nd, antiseptic property and stability test
Table 3
Embodiment 1-5 three layers of make up remover are tested according to the detection project and detection method of table 3, assay is equal
Meet above-mentioned test stone requirement.
3rd, measure of merit
By make up remover composition made from Tables 1 and 2, carry out residuing in the greasy feeling of skin after makeup removing power, washing, wash
The assessment test of the excitement to eyes when the tight feeling of skin, eye makeup removing afterwards.
1st, makeup removing power
Cosmetic agent has used red lipstick, and the make up remover composition dosage for cleaning cosmetic agent is 2mL, uses during cleaning
Water be 400mL.
Assessment mode：
Most preferably：Cosmetic agent residual rate is less than 10%；
Preferably：Cosmetic agent residual rate is 10%~15%；
Typically：Cosmetic agent residual rate is 15%~25%；
Difference：Cosmetic agent residual rate is more than 25%.
2nd, the greasy feeling of skin is residued in after washing
For " greasy feeling for residuing in skin after being rinsed with clear water ", 20 participants are asked to be assessed.Every participant
Used make up remover composition dosage is 2mL, and the water used during flushing is 400mL.
Assessment mode：
Most preferably：There are more than 15 answers " no greasy feeling " in 20；
Preferably：There are 10~14 answers " no greasy feeling " in 20；
Typically：There are 6~9 answers " no greasy feeling " in 20；
Difference：There are less than 5 answers " no greasy feeling " in 20.
3rd, the tight feeling of skin after washing
For " tight feeling of skin after being rinsed with clear water ", 20 participants are asked to be assessed.Every participant is used
Make up remover composition dosage be 2mL, the water used during flushing is 400mL.
Assessment mode：
Most preferably：There are more than 15 answers " no tight feeling " in 20；
Preferably：There are 10~14 answers " no tight feeling " in 20；
Typically：There are 6~9 answers " no tight feeling " in 20；
Difference：There are less than 5 answers " no tight feeling " in 20.
4th, the excitement to eyes when eye is removed ornaments and formal dress
For " when eye is removed ornaments and formal dress to the excitement of eyes ", 20 participants are asked to be assessed.Every participant is made
Make up remover composition dosage is 2mL, and the water used during flushing is 400mL.
Assessment mode：
Most preferably：There are more than 15 answers " excitement is smaller " in 20；
Preferably：There are 10~14 answers " excitement is smaller " in 20；
Typically：There are 6~9 answers " excitement is smaller " in 20；
Difference：There are less than 5 answers " excitement is smaller " in 20.
4th, measure of merit result
By make up remover composition made from Tables 1 and 2, carry out residuing in the greasy feeling of skin after makeup removing power, washing, wash
The assessment test of the excitement to eyes when the tight feeling of skin, eye makeup removing afterwards, it is as a result as shown in table 4 below.
Table 4
In summary, the mainly vegetable oil of comparative example 1 and the double-deck make up remover of polyalcohol compounding, gentle but makeup removing effect one
As；Comparative example 2 is mainly the double-deck make up remover of silicone oil and polyalcohol compounding, makeup removing effect it is general and after washing skin have it is tight
Sense；Comparative example 3 is mainly the makeup remover that table is lived with polyalcohol compounding, due to without oil, without greasy feeling after washing, but power one of removing ornaments and formal dress
As and have excitement to eye part skin.
Three layers of make up remover in embodiment 1-5, it is made up of upper strata plant oil phase, middle level silicone oil phase, lower floor's aqueous phase, without table
Face activating agent and traditional preservatives, it is provided simultaneously with high cleaning power, and the skin moisturizing after washing, both without tight feeling, also without obvious
Greasy feeling remains, and gentle to skin, excitant is smaller, and resultant effect is better than each comparative example.In addition, antiseptic effect and stability are equal
Reach standard requirement.
It is that above-mentioned preferred embodiment should be regarded as application scheme embodiment for example, all with application scheme thunder
Same, approximation or the technology deduction made based on this, replacement, improvement etc., it is regarded as the protection domain of this patent.
Claims (7)
1. a kind of three layers of gentle make up remover, it is characterised in that the silicone oil phase of plant oil phase, middle level including upper strata and lower floor
Aqueous phase, based on the gross weight of three layers of described make up remover,
The plant oil phase is 10~30%；
The silicone oil is mutually 20~30%；
The aqueous phase includes the water of 20~30% polyalcohol, 0.05~1% inorganic salts and surplus, and each component sum is
100%.
2. three layers of gentle make up remover according to claim 1, it is characterised in that the density of the plant oil phase is 0.8
~0.9g/mL, saponification number are 90~200mg KOH/g.
3. three layers of gentle make up remover according to claim 2, it is characterised in that the plant oil phase includes Queensland nut
One or both of oil, gardenia flower oil, jojoba seed oil, olive oil, sweet almond oil are a variety of.
4. three layers of gentle make up remover according to claim 1, it is characterised in that the silicone oil is mutually polydimethylsiloxanes
Alkane.
5. three layers of gentle make up remover according to claim 1, it is characterised in that the polyalcohol include DPG,
One or both of glycerine, isoprene, 1,3-BDO and propane diols are a variety of.
6. three layers of gentle make up remover according to claim 1, it is characterised in that the inorganic salts include sodium chloride, chlorine
Change one or both of potassium, sodium citrate, potassium phosphate, magnesium sulfate or a variety of.
A kind of 7. preparation method of three layers of gentle make up remover described in claim 1-6 any one, it is characterised in that including
Following steps：
S1：Each raw material of aqueous phase is weighed, polyalcohol and inorganic salts are dispersed in water, is heated to about 85~90 DEG C, insulation 20~
40min, it is well mixed to obtain mixture；
S2：S1 mixture is cooled to room temperature, obtains the aqueous phase of lower floor；
S3：Silicone oil phase, vegetable oil are added into S2 lower floor's aqueous phase successively, obtain upper strata be vegetable oil, middle level be silicone oil,
Lower floor is the product of aqueous phase.
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| CN201711110938.9A CN107737028A (en) | 2017-11-10 | 2017-11-10 | A kind of three layers of gentle make up remover and preparation method thereof |
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| CN201711110938.9A CN107737028A (en) | 2017-11-10 | 2017-11-10 | A kind of three layers of gentle make up remover and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108774609A (en) * | 2018-08-23 | 2018-11-09 | 安庆枝梅化工有限责任公司 | A kind of preparation method of skin care scented soap |
| CN109453069A (en) * | 2018-11-26 | 2019-03-12 | 广州博科健康科技集团有限公司 | Sparkling and crystal-clear makeup removing essence composition of one kind and preparation method thereof |
| CN111686025A (en) * | 2020-04-24 | 2020-09-22 | 丽鑫生技化妆品（上海）有限公司 | Three-layer cleansing lotion and preparation method thereof |
| US11975094B2 (en) * | 2021-06-07 | 2024-05-07 | L'oreal | Three-part makeup remover compositions |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108774609A (en) * | 2018-08-23 | 2018-11-09 | 安庆枝梅化工有限责任公司 | A kind of preparation method of skin care scented soap |
| CN109453069A (en) * | 2018-11-26 | 2019-03-12 | 广州博科健康科技集团有限公司 | Sparkling and crystal-clear makeup removing essence composition of one kind and preparation method thereof |
| CN111686025A (en) * | 2020-04-24 | 2020-09-22 | 丽鑫生技化妆品（上海）有限公司 | Three-layer cleansing lotion and preparation method thereof |
| US11975094B2 (en) * | 2021-06-07 | 2024-05-07 | L'oreal | Three-part makeup remover compositions |
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Application publication date: 20180227 |