CN106511144B - A kind of lip makeup remover and preparation method thereof - Google Patents
A kind of lip makeup remover and preparation method thereof Download PDFInfo
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- CN106511144B CN106511144B CN201611169680.5A CN201611169680A CN106511144B CN 106511144 B CN106511144 B CN 106511144B CN 201611169680 A CN201611169680 A CN 201611169680A CN 106511144 B CN106511144 B CN 106511144B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention provides a kind of lip makeup remover and preparation method thereof.In terms of the weight percent of the eye lip makeup remover, the eye lip makeup remover includes following components: PEG-8 caprylic/capric glyceride: 1-15%, preferably 5-10%；Yeast extract: 0.5-10%, preferably 3-7%；Palmityl tripeptides -5:0.5-5%, preferably 1-3%；Sea lettuce extract: 0.5-5%, preferably 0.8-2%；Moisturizer: 1-15%；Preferably 2-8%；Water: 50-90%；Preferably 70-85%.Contain PEG-8 caprylic/capric glyceride in eye lip makeup remover of the invention, can be realized mild makeup removing, and can quickly remove ornaments and formal dress to eye shadow, mascara, informer, lipstick, lip line, lip oil, moreover, no longer need to be cleaned after makeup removing, it is easy to use；Also contain yeast extract and palmityl tripeptides -5, eye microgroove and cheilogramma is enabled to be improved.
Description
Technical field
The present invention relates to a kind of lip makeup removers and preparation method thereof, belong to cosmetic field.
Background technique
Makeup removing is the basis of skin care, and residual adornment is oily dirt, and meeting blocked pore breathes cell from smooth, interferes skin
Skin is normally metabolic, so that skin becomes coarse gradually, pore is coarse, colour of skin yellowing, also breeds dark grain, acne.At present
Cleansing product in the market has: makeup remover, makeup removing breast, makeup remover, make-up remover.
Wherein, the ingredient that uses of makeup remover and make-up remover is emulsifier and grease, can be merged with color make-up greasy dirt on the face,
Again thoroughly dissolving color make-up in a manner of water emulsification.And the water content of makeup removing breast is more compared to makeup remover and make-up remover, it is same
Sample is that the more difficult color make-up pigmentolysis removed with water is washed with water product and is removed grease using grease.But makeup removing breast,
Makeup remover or make-up remover are not used to remove the mascara of waterproof, if accidentally pleasing to the eye, there is a great harm for eyes.And it is excessive
When using makeup removing breast, makeup remover or make-up remover, it may appear that the phenomenon that skin aging.
In recent years makeup remover because its mildness, ease of use and price it is less expensive by consumer welcome.But it is existing
There is the makeup remover in technology that can not solve the problems, such as that eye skin is easy to appear the cheilogramma of wrinkle and lip.Patent application document
CN104288027A provides a kind of eye lip makeup removing liquid and preparation method thereof, uses plant extraction liquid, grease and inorganic salts as master
Want ingredient；Patent application document CN105708733A provides a kind of makeup remover and preparation method thereof for being exclusively used in a lip, Yi Boluo
Husky nurse 184, ring five dimethyl silicone polymer, polyaminopropyl biguanide, isohexadecane, agent of releiving, propylene glycol, hexylene glycol, benzene oxygen second
Alcohol, water are as main component.But these patents can not solve the problems, such as that a lip skin is easy to appear wrinkle.
Patent application document CN105581928A provides that a kind of food grade is crease-resistant, anti-aging makeup remover, with crease-resistant function
Can, it is with smilax, semen coicis, rhizoma atractylodis, benzyl alcohol, natural phosphatidyl choline, amino acid, lauryl sodium sulfate, alcohol, natural olive
Olive oil is main component, and still, Surfactant SDS therein is irritant to eye lip skin, and discomfort shares
In eye and lip.
Summary of the invention
Problems to be solved by the invention
The purpose of the present invention is to provide a kind of lip makeup removers and preparation method thereof.The eye lip makeup remover has mild
The function of makeup removing and anti-wrinkle can supplement the moisture that a lip skin is lost, can also realize quick makeup removing, no longer need to after makeup removing
It is cleaned.
The solution to the problem
The present invention provides a kind of lip makeup remover, in terms of the weight percent of the eye lip makeup remover, including following components:
PEG-8 caprylic/capric glyceride: 1-15%, preferably 5-10%；
Yeast extract: 0.5-10%, preferably 3-7%；
Palmityl tripeptides -5:0.5-5%, preferably 1-3%；
Sea lettuce extract: 0.5-5%, preferably 0.8-2%；
Moisturizer: 1-15%, preferably 2-8%；
Water: 50-90%, preferably 70-85%.
Eye lip makeup remover according to the present invention, group sequence possessed by the palmityl tripeptides -5 rely for palmityl -
Propylhomoserin-valine-lysine-hydroxyl.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: bladder-wrack extract, with described
The weight percent meter of eye lip makeup remover, the additional amount of the bladder-wrack extract are 0.5-5%, preferably 0.8-2%.
Eye lip makeup remover according to the present invention, wherein the moisturizer includes: 1,3-PD, butanediol, dipropyl two
The combination of one or more of alcohol, methyl propanediol, 1,2- pentanediol, glycerol.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: pentanediol is unloaded with the eye lip
The weight percent meter of adornment water, the additional amount of the pentanediol are 0.5-5%, preferably 1-3%.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: Sodium Hyaluronate, with the eye
The weight percent meter of lip makeup remover, the additional amount of the Sodium Hyaluronate are 0.005-0.05%, preferably 0.01-
0.03%.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: Cremophor RH40, with
The weight percent meter of the eye lip makeup remover, the additional amount of the Cremophor RH40 are 0.01-1%, preferably
0.3-0.7%.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: one of preservative, essence
Or two kinds of combination；Preferably, in terms of the weight percent of the eye lip makeup remover, the additional amount of the preservative is 0.1-
0.8%, preferably 0.3-0.6%；The additional amount of the essence is 0.01-0.3%, preferably 0.03-0.1%.
The present invention also provides a kind of preparation methods of eye lip makeup remover according to the present invention, which is characterized in that including by institute
The step of stating each component mixing of a lip makeup remover.
The effect of invention
Eye lip makeup remover of the invention may be implemented mildly to remove ornaments and formal dress, and to eye shadow, mascara, informer, lipstick, lip line,
Lip oil can quickly remove ornaments and formal dress, moreover, no longer need to be cleaned after makeup removing, it is easy to use；Eye lip makeup remover of the invention can be with
So that eye microgroove and cheilogramma are improved.In addition, eye lip makeup remover of the invention can also realize eye and lip and surrounding
The quick moisturizing of skin.
Specific embodiment
The present invention provides a kind of lip makeup remover, in terms of the weight percent of the eye lip makeup remover, including following components:
PEG-8 caprylic/capric glyceride, yeast extract, palmityl tripeptides -5, sea lettuce extract, moisturizer, water.
Wherein, PEG-8 caprylic/capric glyceride is the main makeup removing ingredient of eye lip makeup remover of the invention, utilizes fat
Acid glyceride is formed by micella group, to obtain deep layer cleaning ability.Specifically, due to fatty glyceride and ion table
Face activating agent is different, can exactly match with the phospholipid bilayer structure of Skin Cell wall, when the fatty glyceride in liquid reaches
When certain critical concentration, a globular macromolecule, as micella group will form, micella group has the ability of deep layer cleaning.
PEG-8 caprylic/capric glyceride in the present invention is a kind of the three sweet of the middle chain produced with coconut oil and palm oil
The ethoxylate of grease is the water-soluble liquid with surface-active, mild non-stimulated, suitable for sensitive eye and lip
Portion's makeup removing.Its molecular weight is larger, milder to eye and lip and surrounding skin, can be realized mild makeup removing, and
It can quickly remove ornaments and formal dress to eye shadow, mascara, informer, lipstick, lip line, lip oil, moreover, no longer needing to be cleaned after makeup removing, use
It is convenient.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the PEG-8 caprylic/capric glyceride is 1-
15%, preferably 5-10%；If the additional amount of PEG-8 caprylic/capric glyceride is less than 1%, it is difficult to form micella group, remove ornaments and formal dress
Effect is poor；If the additional amount of PEG-8 caprylic/capric glyceride is greater than 15%, irritation can be generated, and with the increase of content
Irritation also will increase.
Yeast extract (yeast extract) in the present invention is that yeast will wherein protein, nucleic acid, dimension after broken wall
The extractings such as raw element, then the active skull cap components such as the amino acid rich in small molecule, peptide, nucleotide, vitamin through biological enzymolysis
Substance.Wherein amino acid content is 30% or more, and total protein content is 50% or more, and nucleotide content is 10% or more.Therefore
Yeast extract is easy to be absorbed by the skin, and so that the epidermis of aging is restored elasticity, delays the aging of eye and lip surrounding skin.And
And can boost metabolism, improve the effects of protein aggregate velocity, enhancing immunity function, enhancement of SOD activity improve eye
And the antiradical activities of lip surrounding skin.In addition, the nutrients such as vitamin and mineral a small amount of in yeast extract
Sufficient nutrition can also be provided for skin, to play crease-resistant effect.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the yeast extract is 0.5-10%, preferably
For 3-7%；If the additional amount of yeast extract is less than 0.5%, anti-wrinkle effect is unobvious；If the additional amount of yeast extract
Greater than 10%, cost is too high.
There are three types of amino acid for tool in palmityl tripeptides -5 in the present invention, can substantially reduce the wrinkle of eye and lip,
Enhance the elasticity of eye and lip and its surrounding skin.Palmityl tripeptides -5 can also promote cell activity, and it is aqueous to improve skin
Amount improves the colour of skin.Group sequence possessed by the palmityl tripeptides -5 is palmitoyl-lys-valine-lysine -
Hydroxyl, can be by the synthesis of collagen and elastin laminin in promotion skin corium, so that the depth of wrinkle, roughness, wrinkle
Closeness etc. can significantly improve, additionally it is possible to prevent the appearance of crow's feet and cheilogramma, and safe and non-stimulating in use process.
Palmityl tripeptides -5 in the present invention are used in compounding with yeast extract, can generate synergistic effect, further increase crease-resistant effect
Fruit.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the palmityl tripeptides -5 is 0.5-5%, preferably
For 1-3%；If the additional amount of palmityl tripeptides -5 is less than 0.5%, anti-wrinkle effect is unobvious；If palmityl tripeptides -5 add
Enter amount greater than 5%, cost is too high.
In sea lettuce extract in the present invention based on ulvan component, while amino acid also rich in, dimension life
Element and microelement isoreactivity ingredient.Contain a large amount of uronic acid in ulvan, monosaccharide component is similar to hyaluronic acid, therefore
With good moisture-keeping functions.Ulvan does not only have toxicity to cell proliferation, but also may additionally facilitate cell growth and new old
Metabolism, while also having stronger resistance to oxidation and bacteriostasis, can remove free radical, improve elastin laminin skin histology,
Wrinkle is reduced, and can be inhibited tyrosinase activity, the generation of melanin is reduced, there is certain white-skinned face function, to subtract
The generation of few circumference of eyes melanin.
Sea lettuce extract in the present invention can be commercial product, can also be prepared using conventional method.Citing and
Speech, the preparation method of sea lettuce extract of the invention the following steps are included:
Sea lettuce seaweed crushed material is immersed in the aqueous solution of alcohol, soak is obtained；
Microwave abstracting is carried out to the soak, obtains liquid sea lettuce extract.
Specifically, the alcohol is 1,3-BDO, and in the aqueous solution of the alcohol, the mass ratio of water and alcohol is 1:1-1:3, institute
The solid-liquid ratio for stating sea lettuce seaweed crushed material and 1,3 butylene glycol aqueous solution is 1:10-1:30.
Specifically, the time of the immersion is 4-10 hours, and the time of the microwave abstracting is 5-20 minutes, the microwave
The temperature of extraction is 30-80 DEG C, and the power of the microwave abstracting is 200-1000W.
Furthermore it is possible to which liquid sea lettuce extract is filtered and is concentrated again, sea lettuce extract is obtained.
The sea lettuce extract is dispersed in spare in cosmetics-stage glycerol, propylene glycol or 1,3-BDO, can be added suitable
Quantization cosmetic often uses auxiliary anticorrosion agent such as Sensiva SC50, pungent glycol etc..
In terms of the weight percent of the eye lip makeup remover, the additional amount of the sea lettuce extract is 0.5-5%；Preferably
0.8-2%；If the moistening effect that the additional amount of sea lettuce extract less than 0.5%, can not obtain；If sea lettuce extract
Additional amount is greater than 5%, and cost is excessively high, and skin sense is more thick and heavy, influences using effect.
Moisturizer in the present invention can permeate skin bottom, and compact skin restores moist elasticity, hence it is evident that improve lip or
Eye is dry and astringent, it is dry itch or weather caused by skin split, shouting pain, prevent skin ageing, lock moisture for skin, restore natural water profit
Gloss and elasticity prevent and repair dry and external environment to stimulation damage caused by skin.
Moisturizer of the invention include: 1,3- propylene glycol, butanediol, dipropylene glycol, methyl propanediol, 1,2- pentanediol,
The combination of one or more of glycerol.Wherein, butanediol is small molecule moisturizing ingredient.Glycerol has strong hygroscopicity,
The speed that distributes for the moisture that can be allowed on skin slows down, and can suitably absorb water from air.1,2- pentanediol is good
Good moisturizer, additionally it is possible to so that reducing preservative usage amount in cosmetics, and the irritation of protective system be effectively reduced, fit
Share the nursing in sensitive delicate skin and aging dry skin.1,3-PD is natural products, will not cause skin irritatin
Or allergy, product performance of keeping humidity can be enhanced.Methyl propanediol has good moistening effect, while providing salubrious skin sense.Dipropyl
Glycol is the moisturizer small to skin irritation.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the moisturizer is 1-15%；Preferably 2-
8%；If the additional amount of moisturizer is less than 1%, moistening effect is unobvious；If the additional amount of moisturizer is greater than 15%, skin sense
It is more sticky, influence using effect.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the water is 50-90%；Preferably 70-85%.
Eye lip makeup remover according to the present invention, the eye lip makeup remover further include: bladder-wrack extract, in the present invention,
Bladder-wrack extract can improve elastin laminin skin histology, glabrous skin, with high security, anti-oxidant, anti-aging, crease-resistant
And the effect of water conservation moisturizing.In terms of the weight percent of the eye lip makeup remover, the additional amount of the bladder-wrack extract is
0.5-5%, preferably 0.8-2%；If the additional amount of bladder-wrack extract less than 0.5%, cannot further function as smoothly
The effect of wrinkle；If the additional amount of bladder-wrack extract is greater than 5%, skin sense is more sticky, influences using effect.
Bladder-wrack extract in the present invention can be commercial product, can also be prepared using conventional method.Citing
For, the preparation method of bladder-wrack extract of the invention the following steps are included:
Bladder-wrack crushed material is immersed in the aqueous solution of alcohol, soak is obtained；
Microwave abstracting is carried out to the soak, obtains liquid ink angle algae extract.
Specifically, the alcohol is 1,3-BDO, and in the aqueous solution of the alcohol, the mass ratio of water and alcohol is 1:1-1:3, institute
The solid-liquid ratio for stating bladder-wrack crushed material and 1,3 butylene glycol aqueous solution is 1:10-1:30.
Specifically, the time of the immersion is 4-10 hours, and the time of the microwave abstracting is 5-20 minutes, the microwave
The temperature of extraction is 30-80 DEG C, and the power of the microwave abstracting is 200-1000W.
Furthermore it is possible to which liquid ink angle algae extract is filtered and is concentrated again, bladder-wrack extract is obtained.
The bladder-wrack extract is dispersed in spare in cosmetics-stage glycerol, propylene glycol or 1,3-BDO, can be added
Appropriate cosmetics often use auxiliary anticorrosion agent such as Sensiva SC50, pungent glycol etc..
Eye lip makeup remover according to the present invention, the eye lip makeup remover further include: Sodium Hyaluronate, ambient enviroment it is opposite
Influence of the humidity to the moisture retention of Sodium Hyaluronate is smaller, hygroscopic capacity of the Sodium Hyaluronate under low relative humidity (33%) compared with
Height, and the hygroscopic capacity under high relative humidity is minimum, can further such that eye lip makeup remover of the invention in Various Seasonal, no
With using under humidity environment, the moisture that supplement eye lip skin is lost while makeup removing is realized.Particularly, Sodium Hyaluronate often with
Other moisturizer (such as: glycerol) it is used cooperatively, to obtain better moistening effect.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the Sodium Hyaluronate is 0.005-0.05%,
Preferably 0.01-0.03%；If the additional amount of Sodium Hyaluronate less than 0.005%, cannot further function as better moisturizing
Effect；If the additional amount of Sodium Hyaluronate is greater than 0.05%, skin sense is more sticky in eye lip makeup remover of the invention, influences to make
Use effect.
Eye lip makeup remover according to the present invention, the eye lip makeup remover further include: pentanediol.Pentanediol of the invention is not only
Have the function of moisturizing, while also there is antisepsis, the product of preservative free can be prepared, reduces allergy caused by preservative.
In addition, the active constituent of pentanediol dissolution indissoluble.In terms of the weight percent of the eye lip makeup remover, the addition of the pentanediol
Amount is 0.5-5%, preferably 1-3%；If the additional amount of pentanediol, less than 0.5%, the effect of anti-corrosion synergy is unobvious；If
The additional amount of pentanediol is greater than 5%, can generate fever sense, and using effect is bad.
Eye lip makeup remover according to the present invention, wherein the eye lip makeup remover further include: one of preservative, essence
Or two kinds of combination；Preferably, in terms of the weight percent of the eye lip makeup remover, the additional amount of the preservative is 0.1-
0.8%, preferably 0.3-0.6%；The additional amount of the essence is 0.01-0.3%, preferably 0.03-0.1%.
Preferably, the preservative include Chlorphenesin, pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, it is a kind of in benzyl alcohol or
Two or more combinations.
Eye lip makeup remover according to the present invention, the eye lip makeup remover further include: Cremophor RH40 is a kind of normal
Efficient solubilizing agents, can by oily matters such as essence, essential oils, be evenly dispersed into water, formed stablize, transparent solution.
In terms of the weight percent of the eye lip makeup remover, the additional amount of the Cremophor RH40 is 0.01-1%, preferably
0.3-0.7%.
In addition, eye lip makeup remover of the invention can without containing to eye lip skin compound excitatory, such as: can be with
Without containing to eye lip skin lauryl sodium sulfate excitatory etc..
The present invention also provides a kind of preparation methods of eye lip makeup remover according to the present invention, including by the eye lip makeup remover
Each component mixing the step of.
Specifically, the preparation method of eye lip makeup remover of the invention, comprising the following steps:
(1) it adds water in emulsion pot, glycerol, pentanediol and Sodium Hyaluronate is soluble in water, it is heated to 75-90 DEG C,
Stirring and dissolving is complete, it is preferred to use homogenizer auxiliary dissolution continues insulated and stirred 10-15 minutes.
(2) emulsion pot is added in PEG-8 caprylic/capric glyceride, maintains 75-90 DEG C of temperature to continue stirring 10-15 minutes,
Then cool down while stirring.
(3) Cremophor RH40 and essence are added in another reactor, is uniformly mixed, when emulsification pot temperature
Be down to 40-50 DEG C of addition mixed liquor, add sea lettuce extract, bladder-wrack extract, yeast extract, palmityl tripeptides -5 and
Preservative, continuation are cooled to 28-35 DEG C while stirring, stop stirring, obtain a lip makeup remover.
In preparation method of the invention, between 20-50r/min, rate when homogenizer auxiliary dissolves is stirring rate
1500-2500r/min。
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is not specified in embodiment specific
Condition person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer is
It can be with conventional products that are commercially available.
Palmityl tripeptides -5: manufacturer: DSM, trade name:
Yeast extract: manufacturer: BASF, trade name:LS 8430。
Sea lettuce method for preparing extractive in the application: after sea lettuce seaweed high pressure abrasive 30 minutes, sea lettuce seawood meal is obtained
It minces, sea lettuce seaweed crushed material is put into reactor, and 1,3-BDO aqueous solution is added, wherein sea lettuce seaweed crushed material
Mass ratio with 1,3-BDO aqueous solution is 1:20, and the mass ratio of water and 1,3-BDO is 1 in 1,3-BDO aqueous solution:
2, stirring is impregnated 5 hours, obtains soak.Then soak is transferred in extractor and carries out microwave abstracting, extraction process is taken
Temperature programming, microwave abstracting time are 10 minutes, and microwave abstracting temperature is 60 DEG C, microwave abstracting power 500W, then will extraction
Take liquid by obtaining sea lettuce extract after membrane filtration, concentration.
Bladder-wrack method for preparing extractive in the application: after bladder-wrack high pressure abrasive 30 minutes, by the black angle after grinding
Algae is put into reactor, and 1,3-BDO aqueous solution is added, wherein the matter of bladder-wrack crushed material and 1,3-BDO aqueous solution
Amount is than being 1:20, and the mass ratio of water and 1,3-BDO is 1:2 in 1,3-BDO aqueous solution, and stirring is impregnated 5 hours, soaked
Steep liquid.Then soak is transferred in extractor and carries out microwave abstracting, extraction process takes temperature programming, and the microwave abstracting time is
10 minutes, microwave abstracting temperature was 60 DEG C, microwave abstracting power 500W, and microwave abstracting liquid is then passed through membrane filtration, dense
Bladder-wrack extract is obtained after contracting.
Embodiment 1-10
According to the content (number) of each component in the following table 1 and table 2, and a lip makeup removing is prepared as steps described below
Water.
The preparation step of eye lip makeup remover is as follows:
(1) it adds water in emulsion pot, A phase (glycerol, pentanediol, Sodium Hyaluronate) is soluble in water, 80 DEG C are heated to,
It is complete to stir (35r/min) dissolution, it is preferred to use homogenizer (2000r/min) auxiliary dissolution continues insulated and stirred (35r/min)
10 minutes.
(2) emulsion pot is added in B phase (PEG-8 caprylic/capric glyceride), maintains 80 DEG C of temperature to continue to stir (35r/
Min) 10 minutes, then (35r/min) Bian Jiangwen was stirred on side.
(3) C phase (Cremophor RH40 and essence) is added in another reactor, stirring (35r/min) mixing is equal
Even, when emulsification pot temperature is down to 45 DEG C of addition mixed liquors, adding D phase, (sea lettuce extract, bladder-wrack extract, yeast are extracted
Object, palmityl tripeptides -5 and preservative), continuation is cooled to 30 DEG C when stirring (35r/min), stops stirring, obtains a lip and unload
Adornment water.
Table 1
Table 2
Comparative example 1-6
According to the content (number) of each component in the following table 3, and it is prepared according to the step similar to embodiment 1-10
The eye lip makeup remover of comparative example 1-6.
Table 3
Makeup removing effect assessment
The eye lip makeup remover that the eye lip makeup remover and comparative example 1-2 being prepared using embodiment 3 are prepared is right respectively
10 women testers of health carry out test assessment, and using ten point system, 10 points are best for makeup removing effect, 9 gradation, and 1
Divide makeup removing effect worst.As a result as shown in table 4 below:
Table 4
In terms of test result, the eye lip makeup remover that the embodiment of the present invention 3 is prepared is right compared to comparative example 1 and comparative example 2
Lipstick, eye shadow, mascara have very strong makeup removing ability.In addition, the embodiment of the present invention 1-2 and embodiment 4-10 also counterpart
Red, eye shadow, mascara have stronger makeup removing ability.
Wrinkling resistance assessment
The eye lip makeup remover that the eye lip makeup remover and comparative example 3-6 being prepared using embodiment 3 are prepared is right respectively
10 women testers of health carry out test assessment, and using ten point system, 10 points are best for anti-wrinkle effect, 9 gradation, and 1
Divide anti-wrinkle effect worst.Continuous use 4 weeks twice is used daily, as a result as shown in table 5 below:
Table 5
In terms of test result, eye lip of the eye lip makeup remover compared to comparative example 3-6 that the embodiment of the present invention 3 is prepared is removed ornaments and formal dress
Water has apparent anti-wrinkle effect to crow's feet, eye circumference wrinkle, cheilogramma.In addition, the embodiment of the present invention 1-2 and embodiment 4-10
Also there is stronger wrinkling resistance to crow's feet, eye circumference wrinkle, cheilogramma.
Moistening effect measurement
The eye lip makeup remover that the eye lip makeup remover and comparative example 1-5 being prepared using embodiment 3 are prepared is right respectively
10 women testers of health carry out test assessment, use 2 times daily, are used continuously 4 weeks, test skin moisture content
Variation.Test method uses Germany referring to light industry professional standard QB/T4256-2011 " cosmetics moisture-keeping efficacy evaluation guide "
The variation of CK company moisture of skin test probe Corneometer CM825 test skin moisture content, as a result such as the following table 6 institute
Show:
Table 6
In terms of test result, eye lip of the eye lip makeup remover compared to comparative example 1-5 that the embodiment of the present invention 3 is prepared is removed ornaments and formal dress
Water has preferably moisturizing immediately and lasting moistening effect, and can also improve and keep the moisture in skin.In addition, this hair
Bright embodiment 1-2 and embodiment 4-10 also has instant moisturizing and lasting moistening effect.
Claims (13)
1. a kind of lip makeup remover, which is characterized in that in terms of the weight percent of the eye lip makeup remover, including following components:
PEG-8 caprylic/capric glyceride: 1-15%；
Yeast extract: 0.5-10%；
Palmityl tripeptides -5:0.5-5%；
Sea lettuce extract: 0.5-5%；
Bladder-wrack extract: 0.5-5%；
Sodium Hyaluronate, 0.005-0.05%；
Moisturizer: 1-15%；
Water: 50-90%；
The moisturizer include: one or both of 1,3- propylene glycol, butanediol, dipropylene glycol, methyl propanediol, glycerol with
On combination.
2. according to claim 1 lip makeup remover, which is characterized in that with the weight percent of the eye lip makeup remover
Meter, the additional amount of the PEG-8 caprylic/capric glyceride are 5-10%；The additional amount of the yeast extract is 3-7%；Institute
The additional amount for stating palmityl tripeptides -5 is 1-3%；The additional amount of the sea lettuce extract is 0.8-2%；The moisturizer adds
Entering amount is 2-8%；The additional amount of the water is 70-85%.
3. according to claim 1 lip makeup remover, which is characterized in that group sequence possessed by the palmityl tripeptides -5
It is classified as palmitoyl-lys-valine-lysine-hydroxyl.
4. according to claim 1-3 lip makeup remover, which is characterized in that with the weight of the eye lip makeup remover
Percentages, the additional amount of the bladder-wrack extract are 0.8-2%.
5. according to claim 1-3 lip makeup remover, which is characterized in that the eye lip makeup remover further include:
Pentanediol, in terms of the weight percent of the eye lip makeup remover, the additional amount of the pentanediol is 0.5-5%.
6. according to claim 5 lip makeup remover, which is characterized in that with the weight percent of the eye lip makeup remover
Meter, the additional amount of the pentanediol are 1-3%.
7. according to claim 1-3 lip makeup remover, which is characterized in that with the weight of the eye lip makeup remover
Percentages, the additional amount of the Sodium Hyaluronate are 0.01-0.03%.
8. according to claim 1-3 lip makeup remover, which is characterized in that the eye lip makeup remover further include:
Cremophor RH40, in terms of the weight percent of the eye lip makeup remover, the additional amount of the Cremophor RH40
For 0.01-1%.
9. according to claim 8 lip makeup remover, which is characterized in that with the weight percent of the eye lip makeup remover
Meter, the additional amount of the Cremophor RH40 are 0.3-0.7%.
10. according to claim 1-3 lip makeup remover, which is characterized in that the eye lip makeup remover further include:
The combination of one or both of preservative, essence.
11. according to claim 10 lip makeup remover, which is characterized in that with the weight percent of the eye lip makeup remover
Meter, the additional amount of the preservative are 0.1-0.8%；The additional amount of the essence is 0.01-0.3%.
12. according to claim 11 lip makeup remover, which is characterized in that with the weight percent of the eye lip makeup remover
Meter, the additional amount of the preservative are 0.3-0.6%；The additional amount of the essence is 0.03-0.1%.
13. a kind of preparation method of -12 described in any item lip makeup removers according to claim 1, which is characterized in that including inciting somebody to action
The step of each component mixing of the eye lip makeup remover.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611169680.5A CN106511144B (en) | 2016-12-16 | 2016-12-16 | A kind of lip makeup remover and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611169680.5A CN106511144B (en) | 2016-12-16 | 2016-12-16 | A kind of lip makeup remover and preparation method thereof |
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| CN106511144A CN106511144A (en) | 2017-03-22 |
| CN106511144B true CN106511144B (en) | 2019-08-06 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108192091B (en) * | 2018-01-08 | 2018-12-07 | 广州科罗德新材料科技有限公司 | A kind of PEG glycerin ether isomer fatty acids ester, preparation method and its application |
| CN110585035B (en) * | 2019-08-29 | 2022-09-13 | 广州市科能化妆品科研有限公司 | Makeup removing composition containing bamboo charcoal powder |
| CN111358730B (en) * | 2020-03-17 | 2022-09-23 | 广东芭薇生物科技股份有限公司 | Double-layer cleansing lotion and preparation method thereof |
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| CN104398467A (en) * | 2014-11-10 | 2015-03-11 | 广州市博卡利生物科技有限公司 | Makeup removing mask |
| CN104918603A (en) * | 2012-12-27 | 2015-09-16 | 株式会社林原 | Skin-exterior anti-ageing composition and production method therefor |
| JP2015199694A (en) * | 2014-04-07 | 2015-11-12 | 孝男 中村 | skin conditioning agent |
| CN105878108A (en) * | 2016-04-14 | 2016-08-24 | 广州丹奇日用化工厂有限公司 | Special makeup remover for minimizing pores and moistening skin as well as preparation method of makeup remover |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104918603A (en) * | 2012-12-27 | 2015-09-16 | 株式会社林原 | Skin-exterior anti-ageing composition and production method therefor |
| JP2015199694A (en) * | 2014-04-07 | 2015-11-12 | 孝男 中村 | skin conditioning agent |
| CN104398467A (en) * | 2014-11-10 | 2015-03-11 | 广州市博卡利生物科技有限公司 | Makeup removing mask |
| CN105878108A (en) * | 2016-04-14 | 2016-08-24 | 广州丹奇日用化工厂有限公司 | Special makeup remover for minimizing pores and moistening skin as well as preparation method of makeup remover |
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| CN106511144A (en) | 2017-03-22 |
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