CN108030764A - A kind of bilayer make up remover and preparation method thereof - Google Patents
A kind of bilayer make up remover and preparation method thereof Download PDFInfo
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- CN108030764A CN108030764A CN201711454006.6A CN201711454006A CN108030764A CN 108030764 A CN108030764 A CN 108030764A CN 201711454006 A CN201711454006 A CN 201711454006A CN 108030764 A CN108030764 A CN 108030764A
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of double-deck make up remover, it is characterised in that by weight percentage, including following components：30 50wt% of grease；1 10wt% of alcohols moisturizer；0.01 2wt% of nonionic surface active agent；0.5 3wt% of natural moisturizing factor；There is 0.1 0.4wt% of non-preservative of bacteriostasis；0.001 0.1wt% of pH adjusting agent；0.001 1wt% of chelating agent；Water is supplemented to 100wt%.One or more of the nonionic surface active agent of the present invention in polysorbate20,7 glyceryl cocoates of PEG, Plantacare 818, poloxamer, 40 rilanit specials of PEG, 6 caprylic/capric glyceride of PEG.The present invention double-deck makeup remover have the advantages that it is pleasing to the eye it is non-stimulated, cleaning effect is good, without preservative.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of double-deck make up remover and preparation method thereof.
Background technology
As the improvement of people's living standards, everybody increasingly follows the fashion and beauty, the use of color make-up are also more and more wider
General, especially eye make-up and lipstick are most important two parts of a dressing.But after making up, especially eye make-up and lip adornment, if
Do not know thoroughly, remaining cosmetics can damage fragile eye and skin of lip.
Existing makeup removing class cosmetics, mainly based on the products such as makeup remover or makeup remover.Makeup remover be using grease it
Between the similar characteristic to mix, the grease between dissolving color make-up the oil-soluble film forming agent and pigment that include, and human skin secretion
Grease, helps the pigment in color make-up to be removed from skin by the action of massage.The makeup removing ability of makeup remover is stronger, in makeup removing
The sebum film of skin in itself can also be shed at the same time, eye part skin and skin of lip are all relatively thin, are not suitable for this using makeup remover
The stronger makeup removal products of cleaning force；And the makeup removing principle of makeup remover is to add surfactant in formula to reach clean work
With, makeup remover quality is salubriouser, have while moisten, while the sensation removed ornaments and formal dress, water security of removing ornaments and formal dress is gently, small to skin irritation, fits
Large area makeup removing is closed, but the main component of general eye color make-up and lip Cosmetics is grease, using relatively mild makeup remover, that is, is matched somebody with somebody
The poor makeup remover makeup removing power of Fang Zhongbiao work is inadequate, it is more difficult to thoroughly cleaning eye and lip Cosmetics；It is stronger using makeup removing power
Makeup remover, the i.e. few makeup remover of surfactant addition can cause to stimulate to eye again.
Double-deck make up remover is the mixing of water phase and oil phase, and being rocked before use makes water oil phase be sufficiently mixed emulsification, and bilayer unloads
Adornment liquid combines the two-fold advantage of makeup remover and makeup remover, non-greasy salubriouser than makeup remover, removes ornaments and formal dress than makeup remover more thorough, again
Removal eye and lip Cosmetics that can be more efficient.But removal eye make-up and the double-deck make up remover of lip adornment on the market is generally all very
Makeup removing effect and pleasing to the eye non-stimulated is difficult to guarantee, and is had in double-deck eye lip makeup removing liquid on the market plus some preservatives, is made for a long time
With the risk that might have accumulation injury eyes.
The content of the invention
It is an object of the present invention to provide a kind of double-deck make up remover, have it is gentle, non-stimulated to skin, pleasing to the eye it is non-stimulated,
The advantages that cleaning effect is good, without preservative.
Another object of the present invention is to, there is provided a kind of preparation method of above-mentioned double-deck make up remover.
The present invention is achieved by the following technical solutions：
A kind of bilayer make up remover, by weight percentage, including following components：
Grease 30-50wt%；
Alcohols moisturizer 1-10wt%；
Nonionic surface active agent 0.01-2wt%；
Natural moisturizing factor 0.5-3wt%；
There is the non-preservative 0.1-0.4wt% of bacteriostasis；
PH adjusting agent 0.001-0.1wt%；
Chelating agent 0.001-1wt%；
Water is supplemented to 100wt%.
Including following components preferably, by weight percentage,：
Grease 30-50wt%；
Alcohols moisturizer 1-8wt%；
Nonionic surface active agent 0.01-1wt%；
Natural moisturizing factor 1-3wt%；
There is the non-preservative 0.1-0.4wt% of bacteriostasis；
PH adjusting agent 0.001-0.1wt%；
Chelating agent 0.001-1wt%wt%；
Water is supplemented to 100wt%.
The grease is selected from grape-kernel oil, evening primrose oil, Queensland nut seed oil, hydrogenated rapeseed oil, hydrogenation Jojoba
Shepherd's purse seed oil, cotmar, Malus spectabilis fruit seed oil, avocado oil, hydrogenated olive oil, palm are saved in oil, rice bran oil, peanut oil, deep-sea two
Oil, rust Red Rosebush seed oil, hydrogenated palm oil, Sweet Almond Oil, sesame seed oil, wheat-germ oil, castor oil, sweet almond are oily, bright red
Tangerine peel oil, deep-sea two save shepherd's purse seed oil, wineberry seed oil, redwood seed oil, sunflower seed oil, Wild soybean oil, saualane, pungent
Acid/Triglyceride DDD, ethylhexyl palmitate, isopropyl myristate, isopropyl palmitate, isononyl isononanoate, hydrogenation
Polyisobutene, isohexadecane, carbonic acid dioctyl ester, Permethyl 99A, dimethyl silicone polymer, phenyl trimethicone, ring five
One or more in dimethyl silicone polymer, cyclohexasiloxane.
The alcohols moisturizer is selected from polyethylene glycol-8,1,2- propane diols, 1,3 butylene glycol, glycerine, sorbierite, corn
One or more in propane diols, diglycerol.
The one kind or more of the natural moisturizing factor in Anjidew NL50, sodium lactate, ceramide, glycine betaine, amino acid
Kind.
The nonionic surface active agent is selected from polysorbate -20, PEG-7 glyceryl cocoates, decyl glucose
One or more in glycosides, poloxamer, Cremophor RH40, PEG-6 caprylic/capric glyceride.
The non-preservative with bacteriostasis refers to being not included in《Cosmetics safety technical specification（2015
Version）》Specified in mutatis mutandis preservative list, but have the function that to inhibit bacteria the cosmetic material with fungi；The tool
Have bacteriostasis non-preservative be selected from 1,2- hexylene glycols, 1,2- pentanediols, 1,2- isoprenes, decoyl hydroximic acid, silver oxide,
One or more in PCA cocounut oil acyl arginine ethyl esters salt, glycerol caprylate, Sensiva SC50, the smooth caprylate of sorb；It is preferred that
For decoyl hydroximic acid and PCA cocounut oil acyl arginine ethyl ester salt weight ratio 2：1.
By weight percentage, the plant extracts of 0-5wt% is further included；The plant extracts is carried selected from rice plumule
Take thing, saccharomycete/rice bran tunning, purslane extract, flat peach Cactus Flower extract, Thymus serpyllum extract, soap
One or more in careless extract, Crithmum maritimum extract, peppery mint extract, Pseudoalteromonas tunning extract.
The pH adjusting agent is in citric acid, sodium citrate, disodium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium glycyrrhizinate
One or more.
One or more of the chelating agent in disodium ethylene diamine tetraacetate, tetrasodium ethylenediamine tetraacetate.
By weight percentage, the conditioner of 0-3wt% is further included；The conditioner is selected from bee milk albumen, vitamin
E, the one or more in lactic acid, beta glucan, zinc gluconate, batyl alcohol, bisabolol；By weight percentage, further include
The sodium chloride or potassium chloride of 0-2wt%.
The preparation method of double-deck make up remover, comprises the following steps：
(1) the non-preservative of bacteriostasis is weighed in proportion, is dissolved by heating at 40 DEG C, sequentially adds alcohols moisturizing
Agent, nonionic surface active agent, natural moisturizing factor, conditioner, plant extracts, chelating agent, pH adjusting agent, sodium chloride or
The raw materials such as potassium chloride, water, are added in agitated kettle, and stirring at room temperature is mixed thoroughly it, obtains mixed liquor A phase； (2)
Grease has been weighed in proportion, has been added in agitated kettle, and stirring at room temperature is mixed thoroughly it, obtains oil phase mixed liquid B；
(3) oil phase mixed liquid B is slowly added into water to mix in liquid A；
(4) discharging is stirred after detecting.
The present invention has the advantages that：
The present invention double-deck makeup remover be for eye, lip makeup removing and design, have it is gentle, non-stimulated to skin, enter
The advantages that eye is non-stimulated, cleaning effect is good, without preservative；The present invention uses nonionic surface active agent, compares formula
It is non-stimulated to eyes, skin in ionic surfactant milder；The present invention is also using the non-anti-corrosion with bacteriostasis
Agent, has more used decoyl hydroximic acid and PCA cocounut oil acyl arginine ethyl ester salt weight ratio 2：1 formula and dosage is optimized,
Stimulation of the make up remover to eyes and skin is effectively reduced, and eliminates potential hazard of the preservative long-time service to eyes.
Embodiment
The present invention is further illustrated below by embodiment, and following embodiments are the preferable embodiment party of the present invention
Formula, but embodiments of the present invention and from the limitation of following embodiments.
Raw material used derives from commercially available in the specific embodiment of the invention.
The preparation method of embodiment 1-3 and comparative example 1-4：The non-preservative of bacteriostasis is weighed in proportion, 40
Dissolved by heating at DEG C, sequentially add alcohols moisturizer, surfactant, natural moisturizing factor, conditioner, plant extracts,
The raw material such as chelating agent, pH adjusting agent, sodium chloride or potassium chloride, water, is added in agitated kettle, and stirring at room temperature is thoroughly mixed it
Uniformly, mixed liquor A phase is obtained；Grease has been weighed in proportion, has been added in agitated kettle, and stirring at room temperature is thoroughly mixed it
Uniformly, oil phase mixed liquid B is obtained；Oil phase mixed liquid B is slowly added into water to mix in liquid A；Discharging is stirred after detection.
Table 1：Embodiment and comparative formulation（Percentage by weight）
The above-mentioned non-preservative for having bacteriostasis is decoyl hydroximic acid and PCA cocounut oil acyl arginine ethyl ester salt weight ratio 2：1.
Each performance test methods：
（1）Trial effect is evaluated：
Tested material：Embodiment 1-3 comparative examples 1-4；
Subject：Totally 30 people, women, age 18-57 Sui, meets the selected mark of subject's aspiration；
Test method：It is required that participating in subject on probation is intended to picture informer and waterproof mascara or common mascara, to trier
Respectively makeup removing operation is carried out using the double-deck make up remover of embodiment 1-3, comparative example 1-4；During makeup removing, first by above and below double-deck make up remover
Under rocking 10, pour out 2g or so and applied 15 seconds on eyes or lip on makeup removing cotton, then slightly firmly wipe.Allow subject after on probation
Give a mark according to item is investigated；
Contrast item：Spreadability, greasy degree, makeup removing effect, mildness, beaten with rear skin sense, layered effect, general impression
Point.Common 1-5 points, outside oil removal degree, remaining investigates item fraction closer to 5, illustrates that evaluation is more excellent；Greasy degree scoring is got over
It is low, illustrate that evaluation is more excellent；
Evaluation information is fed back：Fraction in table 2 is the average mark after collecting to trial state；
Table 2：Embodiment 1-3 and comparative example 1-4 trial effect evaluation scores
（2）Patch test and result：
Tested material：Embodiment 1-3, comparative example 1-4；
Negative control：Water；
Subject：Totally 30 people, male 5 people, 25 people of female, age 18-57 Sui, meets subject and volunteers inclusion criteria；
Test method：Qualified spot examination device is selected, in closed patch test method, tested material 0.03ml is applied to spot examination device
Interior, external application special adhesive tape is pasted on subject back, 24 it is small when after remove tested material, 0.5,24,48 after patch test
Hour observation change of skin, is pressed《Cosmetics safety technical specification》（2015 editions）Middle dermoreaction class criteria records its result.
Table 3：The human skin patch result of embodiment 1
Human body patch test results show that 0 skin adverse reaction occurs in 30 people.
Table 4：The human skin patch result of embodiment 2
Human body patch test results show that 0 skin adverse reaction occurs in 30 people.
Table 5：The human skin patch result of embodiment 3
Human body patch test results show that 0 skin adverse reaction occurs in 30 people.
Table 6：The human skin patch result of comparative example 1
Human body patch test results show that 0 skin adverse reaction occurs in 30 people.
Table 7：The human skin patch result of comparative example 2
Human body patch test results show that 6 skin adverse reaction occur in 30 people.
Table 8：The human skin patch result of comparative example 3
Human body patch test results show that 8 skin adverse reaction occur in 30 people.
Table 9：The human skin patch result of comparative example 4
Human body patch test results show that 0 skin adverse reaction occurs in 30 people.
（3）Lagophthalmos urgency skin is taken aback test
According to《Cosmetics safety technical specification》（2015 editions）Specified in standard method carry out anxious skin and be taken aback test, it, which is tested, ties
Fruit such as table 10：
Table 10：Embodiment 1-3 lagophthalmos urgency skins are taken aback test result
It is non-stimulated to skin to can be seen that the double-deck make up remover of the present invention from embodiment 1-3, it is even more non-stimulated to eye, also have
The features such as layered velocity is fast, mildness is good, greasy degree is low, makeup removing effect is good；From comparative example 1 as can be seen that excessive has suppression
The dosage of the non-preservative of bacterium effect, can reduce mildness and improve greasy degree, be deteriorated using skin sense, but stingless to skin
Swash；From comparative example 2 as can be seen that using ionic surfactant laureth sodium sulfovinate, using rear skin sense and gently
Property declines to a great extent, larger to skin irritatin；From comparative example 3 as can be seen that using preservative methyl hydroxybenzoate, mildness is further
Decline, the stimulation to skin is also maximum；From comparative example 4 as can be seen that in the case of being added without sodium chloride, layered velocity and gentle
Property decline, greasy degree is substantially increased.
Claims (12)
- A kind of 1. bilayer make up remover, it is characterised in that by weight percentage, including following components：Grease 30-50wt%；Alcohols moisturizer 1-10wt%；Nonionic surface active agent 0.01-2wt%；Natural moisturizing factor 0.5-3wt%；There is the non-preservative 0.1-0.4wt% of bacteriostasis；PH adjusting agent 0.001-0.1wt%；Chelating agent 0.001-1wt%；Water is supplemented to 100wt%.
- 2. bilayer make up remover according to claim 1, it is characterised in that by weight percentage, including following components：Grease 30-50wt%；Alcohols moisturizer 1-8wt%；Nonionic surface active agent 0.01-1wt%；Natural moisturizing factor 1-3wt%；There is the non-preservative 0.1-0.4wt% of bacteriostasis；PH adjusting agent 0.001-0.1wt%；Chelating agent 0.001-1wt%wt%；Water is supplemented to 100wt%.
- 3. bilayer make up remover according to claim 1 or 2, it is characterised in that the grease is selected from grape-kernel oil, sees the moon Shepherd's purse seed oil, hydrogenation are saved in careless oil, Queensland nut seed oil, hydrogenated rapeseed oil, hydrogenated jojoba oil, rice bran oil, peanut oil, deep-sea two Cottonseed oil, Malus spectabilis fruit seed oil, avocado oil, hydrogenated olive oil, palm oil, rust Red Rosebush seed oil, hydrogenated palm oil, Sweet Almond Oil, Sesame seed oil, wheat-germ oil, castor oil, sweet almond be oily, shepherd's purse seed oil is saved at big red tangerine peel oil, deep-sea two, wineberry seed oil, Redwood seed oil, sunflower seed oil, Wild soybean oil, saualane, caprylic/capric triglyceride, ethylhexyl palmitate, myristic acid It is isopropyl ester, isopropyl palmitate, isononyl isononanoate, Parleam, isohexadecane, carbonic acid dioctyl ester, Permethyl 99A, poly- One or more in dimethyl siloxane, phenyl trimethicone, ring five dimethyl silicone polymer, cyclohexasiloxane.
- 4. bilayer make up remover according to claim 1 or 2, it is characterised in that the alcohols moisturizer is selected from poly- second two One or more in alcohol -8,1,2- propane diols, 1,3 butylene glycol, glycerine, sorbierite, corn propane diols, diglycerol.
- 5. bilayer make up remover according to claim 1 or 2, it is characterised in that the natural moisturizing factor is selected from PCA One or more in sodium, sodium lactate, ceramide, glycine betaine, amino acid.
- 6. bilayer make up remover according to claim 1 or 2, it is characterised in that the nonionic surface active agent choosing From polysorbate -20, PEG-7 glyceryl cocoates, Plantacare 818, poloxamer, Cremophor RH40, PEG-6 One or more in caprylic/capric glyceride.
- 7. bilayer make up remover according to claim 1 or 2, it is characterised in that the non-anti-corrosion with bacteriostasis Agent refers to being not included in《Cosmetics safety technical specification（Version in 2015）》Specified in mutatis mutandis preservative list, but have Inhibit bacteria the cosmetic material with the effect of fungi；The non-preservative with bacteriostasis be selected from 1,2- hexylene glycols, 1,2- pentanediols, 1,2- isoprenes, decoyl hydroximic acid, silver oxide, PCA cocounut oil acyl arginine ethyl esters salt, glycerol caprylate, second One or more in base hexyl glycerine, the smooth caprylate of sorb；Preferably decoyl hydroximic acid and PCA cocounut oil acyl arginine ethyl esters Salt weight ratio 2：1.
- 8. bilayer make up remover according to claim 1 or 2, it is characterised in that by weight percentage, further include 0-5wt% Plant extracts；The plant extracts is selected from rice germ extracts, saccharomycete/rice bran tunning, purslane extraction Thing, flat peach Cactus Flower extract, Thymus serpyllum extract, Saponaria officinalis extract, Crithmum maritimum extract, peppery mint extract, One or more in Pseudoalteromonas tunning extract.
- 9. bilayer make up remover according to claim 1 or 2, it is characterised in that the pH adjusting agent is selected from citric acid, lemon One or more in lemon acid sodium, disodium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium glycyrrhizinate.
- 10. bilayer make up remover according to claim 1 or 2, it is characterised in that the chelating agent is selected from ethylenediamine tetrem One or more in acid disodium, tetrasodium ethylenediamine tetraacetate.
- 11. bilayer make up remover according to claim 1 or 2, it is characterised in that by weight percentage, further include 0- The conditioner of 3wt%；The conditioner is selected from bee milk albumen, vitamin E, lactic acid, beta glucan, zinc gluconate, shark liver One or more in alcohol, bisabolol；By weight percentage, the sodium chloride or potassium chloride of 0-2wt% is further included.
- 12. the preparation method of claim 1-11 any one of them bilayer make up remover, it is characterised in that comprise the following steps：(1) the non-preservative of bacteriostasis is weighed in proportion, is dissolved by heating at 40 DEG C, sequentially adds alcohols moisturizing Agent, nonionic surface active agent, natural moisturizing factor, conditioner, plant extracts, chelating agent, pH adjusting agent, sodium chloride or The raw materials such as potassium chloride, water, are added in agitated kettle, and stirring at room temperature is mixed thoroughly it, obtains mixed liquor A phase； (2) Grease has been weighed in proportion, has been added in agitated kettle, and stirring at room temperature is mixed thoroughly it, obtains oil phase mixed liquid B； (3) oil phase mixed liquid B is slowly added into water to mix in liquid A；(4) discharging is stirred after detecting.
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| CN114788804B (en) * | 2021-06-04 | 2024-01-26 | 广州一一生物技术有限公司 | Moisturizing double-layer water and preparation method thereof |
| CN113274302A (en) * | 2021-07-06 | 2021-08-20 | 广州集妍化妆品科技有限公司 | Composition, safe and refreshing cleansing water and preparation method thereof |
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| CN116509775A (en) * | 2023-07-05 | 2023-08-01 | 科妍生物工程研究(天津)有限公司 | Rosewood seed skin care lotion and preparation method and application thereof |
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