CN107019718A - A kind of preparation method of Radix Codonopsis broken wall medicine materical crude slice - Google Patents
A kind of preparation method of Radix Codonopsis broken wall medicine materical crude slice Download PDFInfo
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/34—Campanulaceae (Bellflower family)
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- A61K35/644—Beeswax; Propolis; Royal jelly; Honey
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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Abstract
The invention discloses a kind of preparation method of Radix Codonopsis broken wall medicine materical crude slice, including herein below:First codonopsis pilosula is soaked by soak, then Radix Codonopsis medicine materical crude slice is dried, then the medicinal material coarse powder of 80 120 mesh is made after the crushing of the pulverizer through 100 mesh sieves;Then in turn through microwave drying, grinding superfine powder, then further by ethanol water wet granulation, and the extrusion forming under certain rotating speed, dry, thus obtained Radix Codonopsis broken wall medicine materical crude slice;The Radix Codonopsis broken wall medicine materical crude slice of the present invention is first soaked using soak, improve the nutritive value of Radix Codonopsis, just process, then further by ethanol water wet granulation, obtained Radix Codonopsis broken wall medicine materical crude slice particle type is preferable, elasticity is moderate, stability is strong, disintegrative is good, while relatively conventional super-micro wall-broken breaking method, the present invention greatly improves the sporoderm-broken rate of Radix Codonopsis, nutriment has obtained maximized reservation, realizes sporoderm-broken rate height and nutritional ingredient preserves comprehensive beneficial effect.
Description
Technical field
The present invention relates to a kind of preparation method of medicine materical crude slice, and in particular to a kind of preparation method of Radix Codonopsis broken wall medicine materical crude slice.
Background technology
Distribution in the cell, can only release part active ingredient during conventional medicine materical crude slice decoction mostly for active ingredient in Chinese medicine
Release, utilization rate of active components 10-30%;And broken wall crushing technology is used, the prepared slices of Chinese crude drugs are such as crushed to 300 mesh or so, carefully
Born of the same parents' sporoderm-broken rate is up to 86.7%, improves the dissolution of active ingredient in medicinal material, greatly enhances its drug effect, utilization rate of active components
More than 90%, reduction medicinal material usage amount and protection herb resource are reached, while can also improve the quality increase drug effect of medicine.But
It is that current main superfine communication technique remains in the stage that traditional Chinese medicine powder is broken to superfine formulation.Because superfine formulation is thin
, there is the product increase of broken wall dosage surface, in irregular shape, mobility, bad dispersibility, it is easy to moisture absorption are stable in the increase of born of the same parents' sporoderm-broken rate
Property the inherent characteristicses such as difference, pelletized, improve the stability of product.
Radix Codonopsis, its active ingredient includes triterpene compound, phytosterol, choline nitrogen-containing compound, a large amount of carbohydrates
Material and volatile oil etc., using traditional decocting method, are easily destroyed its heat-sensitive ingredients, another aspect active ingredient is decocted not
Completely, the loss of active ingredient is caused.Radix Codonopsis is prepared into Radix Codonopsis superfine powder, is conducive to improving the utilization rate of active ingredient,
But simultaneously because the increase of powder specific-surface area detection, produces the shortcoming for being easy to the moisture absorption, oxidation, rotten etc..
The content of the invention
In order to alleviate the deficiencies in the prior art, it is an object of the invention to provide a kind of making side of Radix Codonopsis broken wall medicine materical crude slice
Method.
The present invention is adopted the following technical scheme that:
The preparation method of Radix Codonopsis broken wall medicine materical crude slice, including herein below:
(1)Medicinal material processing:Then selection is soaked by picking clean, medicinal material drying Radix Codonopsis medicine materical crude slice 1.8-2.2kg with 0.1-0.2kg
Immersion bubble is steeped, 40-50 DEG C is heated to, constant temperature is cooked 30-40 minutes, 80-90 DEG C is continuously heating to, constant temperature cooks 15-20
Minute, it is finally heated to be cooked 10-15 minutes to seething with excitement, room temperature is cooled to, Radix Codonopsis piece is taken out;The composition of described soak is former
Expect that parts by weight are:Yellow rice wine 55-70, fresh milk 12-15, refined honey 8-10, mulberry juice 20-25, plantain seed 3-4, fry cattail pollen 2-4, process
Radix glycyrrhizae 4-5, Folium eriobotryae 3-4, Radix Astragali 1-2;Plantain seed is weighed by weight, cattail pollen, honey-fried licorice root, Folium eriobotryae and the Radix Astragali is fried, and is added water
Decocted, be cooked by slow fire 20-25 minutes after changing after boiling water, decoction filters off the dregs of a decoction, concoction and yellow rice wine, fresh ox after finishing
Milk, refined honey, mulberry juice mixing, you can;
(2)80- is made after the above-mentioned Radix Codonopsis medicine materical crude slice drying after soak is handled, then the pulverizer through 100 mesh sieves are crushed
The medicinal material coarse powder of 120 mesh;
(3)The Radix Codonopsis coarse powder of above-mentioned crushing is placed under vacuum condition, microwave treatment 10~30 minutes, controls the middle temperature of microwave process
Spend for 20-35 DEG C, the microwave device for the 5KW-20KW that described microwave treatment is used carries out microwave treatment;
(4)Radix Codonopsis coarse powder after the processing of above-mentioned vacuum microwave is ground into superfine powder;
(5)Softwood processed:Superfine powder made from broken wall is placed in mixer, the second that ethanol mass fraction is 60-75% is added
Alcohol-water solution softwood;The mass ratio of ultrafine powder and ethanol-water solution is 1:0.5-0.7;
(6)By above-mentioned steps(5)In softwood extruding obtain wet grain;Wet grain, which is dried, obtains Radix Codonopsis broken wall medicine materical crude slice.
Described step(3)Sterilization treatment first can be carried out to Radix Codonopsis coarse powder after microwave treatment, superfine powder is then carried out again
Crush.
Described sterilizing methods use ultraviolet radiation method, are that Radix Codonopsis medicine materical crude slice tiles to deploy, uviol lamp radiation treatment
10-30 minutes;During ultra violet lamp, using wavelength 240-270nm ultraviolet light source.
Beneficial effects of the present invention:
The Radix Codonopsis broken wall medicine materical crude slice of the present invention is first soaked using soak, improves the nutritive value of Radix Codonopsis, just process, Ran Houzai
Further by alcohol-water wet granulation, and the extrusion forming under certain rotating speed, dry, thus obtained Radix Codonopsis broken wall drink
Preferably, elasticity is moderate, and stability is strong, disintegrative is good, while relatively conventional super-micro wall-broken breaking method, this hair for piece particle type
The bright sporoderm-broken rate for greatly improving Radix Codonopsis, effectively protect triterpene compound, phytosterol, choline nitrogen-containing compound,
A large amount of active ingredients such as glucide and volatile oil are not damaged, and nutriment has obtained maximized reservation, realizes broken wall
Rate is high and nutritional ingredient preserves comprehensive beneficial effect.
Embodiment
Embodiment 1:The preparation method of Radix Codonopsis broken wall medicine materical crude slice, including herein below:
(1)Medicinal material processing:Then selection soaks immersion by picking clean, medicinal material drying Radix Codonopsis medicine materical crude slice 2.0kg with 0.15kg
Bubble, is heated to 45 DEG C, constant temperature is cooked 35 minutes, is continuously heating to 85 DEG C, constant temperature is cooked 18 minutes, finally heated to boiling
Rise, cook 12 minutes, be cooled to room temperature, take out Radix Codonopsis piece;The constitutive material parts by weight of described soak are:It is yellow rice wine 60, fresh
Milk 13, refined honey 9, mulberry juice 22, plantain seed 3.5, stir-fry cattail pollen 3, honey-fried licorice root 4.5, Folium eriobotryae 3.5, the Radix Astragali 1.5;By weight
Weigh plantain seed, fry cattail pollen, honey-fried licorice root, Folium eriobotryae and the Radix Astragali, add water and decocted, 25 points are cooked by slow fire after changing after boiling water
Clock, decoction filters off the dregs of a decoction after finishing, and concoction is mixed with yellow rice wine, fresh milk, refined honey, mulberry juice, you can;
(2)100 are made after the above-mentioned Radix Codonopsis medicine materical crude slice drying after soak is handled, then the pulverizer through 100 mesh sieves are crushed
Purpose medicinal material coarse powder;
(3)The Radix Codonopsis coarse powder of above-mentioned crushing is placed under vacuum condition, microwave treatment 20 minutes, controls the temperature in microwave process to be
20-35 DEG C, the microwave device for the 5KW-20KW that described microwave treatment is used carries out microwave treatment;
(4)Radix Codonopsis coarse powder after the processing of above-mentioned vacuum microwave is ground into superfine powder;
(5)Softwood processed:Superfine powder made from broken wall is placed in mixer, the second that ethanol mass fraction is 60-75% is added
Alcohol-water solution softwood;The mass ratio of ultrafine powder and ethanol-water solution is 1:0.5-0.7;
(6)By above-mentioned steps(5)In softwood extruding obtain wet grain;Wet grain, which is dried, obtains Radix Codonopsis broken wall medicine materical crude slice.
Described step(3)Sterilization treatment first can be carried out to Radix Codonopsis coarse powder after microwave treatment, superfine powder is then carried out again
Crush.
Described sterilizing methods use ultraviolet radiation method, are that Radix Codonopsis medicine materical crude slice tiles to deploy, uviol lamp radiation treatment
10-30 minutes;During ultra violet lamp, using wavelength 240-270nm ultraviolet light source.
Claims (3)
1. a kind of preparation method of Radix Codonopsis broken wall medicine materical crude slice, it is characterised in that including herein below:
(1)Medicinal material processing:Then selection is soaked by picking clean, medicinal material drying Radix Codonopsis medicine materical crude slice 1.8-2.2kg with 0.1-0.2kg
Immersion bubble is steeped, 40-50 DEG C is heated to, constant temperature is cooked 30-40 minutes, 80-90 DEG C is continuously heating to, constant temperature cooks 15-20
Minute, it is finally heated to be cooked 10-15 minutes to seething with excitement, room temperature is cooled to, Radix Codonopsis piece is taken out;The composition of described soak is former
Expect that parts by weight are:Yellow rice wine 55-70, fresh milk 12-15, refined honey 8-10, mulberry juice 20-25, plantain seed 3-4, fry cattail pollen 2-4, process
Radix glycyrrhizae 4-5, Folium eriobotryae 3-4, Radix Astragali 1-2;Plantain seed is weighed by weight, cattail pollen, honey-fried licorice root, Folium eriobotryae and the Radix Astragali is fried, and is added water
Decocted, be cooked by slow fire 20-25 minutes after changing after boiling water, decoction filters off the dregs of a decoction, concoction and yellow rice wine, fresh ox after finishing
Milk, refined honey, mulberry juice mixing, you can;
(2)80- is made after the above-mentioned Radix Codonopsis medicine materical crude slice drying after soak is handled, then the pulverizer through 100 mesh sieves are crushed
The medicinal material coarse powder of 120 mesh;
(3)The Radix Codonopsis coarse powder of above-mentioned crushing is placed under vacuum condition, microwave treatment 10~30 minutes, in control microwave process
Temperature is 20-35 DEG C, and the microwave device for the 5KW-20KW that described microwave treatment is used carries out microwave treatment;
(4)Radix Codonopsis coarse powder after the processing of above-mentioned vacuum microwave is ground into superfine powder;
(5)Softwood processed:Superfine powder made from broken wall is placed in mixer, the second that ethanol mass fraction is 60-75% is added
Alcohol-water solution softwood;The mass ratio of ultrafine powder and ethanol-water solution is 1:0.5-0.7;
(5)By above-mentioned steps(5)In softwood extruding obtain wet grain;Wet grain, which is dried, obtains Radix Codonopsis broken wall medicine materical crude slice.
2. the preparation method of Radix Codonopsis broken wall medicine materical crude slice according to claim 1, it is characterised in that described step(3)Microwave
Sterilization treatment first can be carried out to Radix Codonopsis coarse powder after processing, superfine powder crushing is then carried out again.
3. the preparation method of Radix Codonopsis broken wall medicine materical crude slice according to claim 2, it is characterised in that described sterilizing methods are used
Ultraviolet radiation method, is that Radix Codonopsis medicine materical crude slice tiles to deploy, uviol lamp radiation treatment 10-30 minutes;Ultra violet lamp process
In, using wavelength 240-270nm ultraviolet light source.
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CN109602792A (en) * | 2018-12-11 | 2019-04-12 | 江西赣隆药业有限公司 | A kind of trollflower broken wall medicine materical crude slice and preparation method thereof |
CN109528778A (en) * | 2018-12-17 | 2019-03-29 | 江西赣隆药业有限公司 | It is a kind of for increasing the monkey mushroom broken wall medicine materical crude slice and preparation method thereof of immunity and anti-aging |
CN109528903A (en) * | 2018-12-17 | 2019-03-29 | 江西赣隆药业有限公司 | The preparation method of dye yam broken wall medicine materical crude slice with regulating qi-flowing for relieving pain and heat-clearing toxin-expelling functions and the dye yam broken wall medicine materical crude slice prepared by this method |
CN109846833A (en) * | 2018-12-17 | 2019-06-07 | 江西赣隆药业有限公司 | It is a kind of for treating the ilex pubescens broken wall medicine materical crude slice and preparation method thereof of anemopyretic cold and dyspnea and cough due to lung-heat |
CN109846832A (en) * | 2018-12-17 | 2019-06-07 | 江西赣隆药业有限公司 | For treat the lance asiabell root broken wall medicine materical crude slice of spiritlessness and weakness and dizziness headache preparation method and lance asiabell root broken wall medicine materical crude slice prepared therefrom |
CN109692192A (en) * | 2018-12-17 | 2019-04-30 | 江西赣隆药业有限公司 | The broken wall medicine materical crude slice for having effects that the preparation method of clearing heat and detoxicating, promoting blood circulation to remove blood stasis alangium broken wall medicine materical crude slice and being prepared by this method |
CN109646473A (en) * | 2018-12-17 | 2019-04-19 | 江西赣隆药业有限公司 | For treating abundant expectoration, panting, not well, overstrain cough hemoptysis hempleaf groundsel herb broken wall medicine materical crude slice and preparation method thereof of coughing up phlegm |
CN109602801A (en) * | 2018-12-17 | 2019-04-12 | 江西赣隆药业有限公司 | Have effects that the preparation method of the five fingers mandarin orange broken wall medicine materical crude slice of liver-smoothing, qi-regulating protecting the stomach and relieve the pain and the five fingers mandarin orange broken wall medicine materical crude slice prepared therefrom |
CN109568356A (en) * | 2018-12-18 | 2019-04-05 | 江西赣隆药业有限公司 | For treat the hyperici,herba broken wall medicine materical crude slice of rheumatism and dysentery preparation method and hyperici,herba broken wall medicine materical crude slice prepared therefrom |
CN109528872A (en) * | 2018-12-19 | 2019-03-29 | 江西赣隆药业有限公司 | Have effects that the preparation method of the cayropteris incana broken wall medicine materical crude slice of antibacterial and cough-relieving and cayropteris incana broken wall medicine materical crude slice prepared therefrom |
CN109528787A (en) * | 2018-12-19 | 2019-03-29 | 江西赣隆药业有限公司 | It is a kind of for curing cold, the HERBA BUPLEURI broken wall medicine materical crude slice of parotitis, tonsillitis and preparation method thereof |
CN109549962A (en) * | 2018-12-20 | 2019-04-02 | 江西赣隆药业有限公司 | The preparation method of Siberian cocklebur grass broken wall medicine materical crude slice with antispastic and analgesic efficacy and Siberian cocklebur grass broken wall medicine materical crude slice prepared therefrom |
CN109846837A (en) * | 2018-12-21 | 2019-06-07 | 江西赣隆药业有限公司 | A kind of rabdosia lophanthide broken wall medicine materical crude slice and preparation method thereof for treating acute icteric hepatitis, acute cholecystitis and dysentery |
CN109528794A (en) * | 2018-12-21 | 2019-03-29 | 江西赣隆药业有限公司 | For treat the Cynanchum otophyllum Schneid broken wall medicine materical crude slice of epilepsy and chronic hepatitis preparation method and Cynanchum otophyllum Schneid broken wall medicine materical crude slice prepared therefrom |
CN109528873A (en) * | 2018-12-25 | 2019-03-29 | 江西赣隆药业有限公司 | For treat the Manyflower Gueldenstaedtid Herb broken wall medicine materical crude slice of jaundice, enteritis and dysentery preparation method and Manyflower Gueldenstaedtid Herb broken wall medicine materical crude slice prepared therefrom |
CN109528828A (en) * | 2018-12-25 | 2019-03-29 | 江西赣隆药业有限公司 | The preparation method of Cortex Cinnamomi broken wall medicine materical crude slice with calm, cooling and antihypertensive effect and Cortex Cinnamomi broken wall medicine materical crude slice prepared therefrom |
CN109528826A (en) * | 2018-12-25 | 2019-03-29 | 江西赣隆药业有限公司 | For treat the salvia bowleyana Dunn broken wall medicine materical crude slice of thoracic obstruction colic pain and epigastric pain preparation method and salvia bowleyana Dunn broken wall medicine materical crude slice prepared therefrom |
CN109528797A (en) * | 2018-12-25 | 2019-03-29 | 江西赣隆药业有限公司 | Have effects that the preparation method of clearing heat and detoxicating and inducing diuresis to remove edema elephants-foot broken wall medicine materical crude slice and elephants-foot broken wall medicine materical crude slice prepared therefrom |
CN109528907A (en) * | 2018-12-25 | 2019-03-29 | 江西赣隆药业有限公司 | It is a kind of for treating the preparation method for curing mainly the careless river vehicle broken wall medicine materical crude slice of carbuncle swells tuberculosis chronic cough and careless river vehicle broken wall medicine materical crude slice prepared therefrom |
CN109846838A (en) * | 2018-12-25 | 2019-06-07 | 江西赣隆药业有限公司 | Have effects that the preparation method of the wallich swallowwort root broken wall medicine materical crude slice of Bu Shen Zhuang waist and strengthening the bones and muscles and wallich swallowwort root broken wall medicine materical crude slice prepared therefrom |
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