CN109602792A - A kind of trollflower broken wall medicine materical crude slice and preparation method thereof - Google Patents
A kind of trollflower broken wall medicine materical crude slice and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A61K2236/10—Preparation or pretreatment of starting material
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The present invention relates to Chinese medicine wall cell disruption medicine materical crude slice technical field, a kind of trollflower broken wall medicine materical crude slice and preparation method thereof is disclosed.Method includes the following steps: dry globeflower medicinal materials precomminution is the particle of 40-100 mesh by (1), then impregnated, filtered with ethanol water, obtained filter cake is freeze-dried；(2) trollius chinensis granular that step (1) obtains is placed under vacuum condition and carries out microwave treatment, then pulverized, then mix obtained micropowders with ethanol water, pelletized, it is dry.The higher trollflower broken wall medicine materical crude slice of broken wall ratio can be made using method of the present invention.
Description
Technical field
The present invention relates to Chinese medicine wall cell disruption medicine materical crude slice technical fields, and in particular to a kind of trollflower broken wall medicine materical crude slice and its preparation side
Method.
Background technique
Chinese medicine wall cell disruption medicine materical crude slice be with modern superfine communication technique by traditional medicine materical crude slice be process it is a kind of in powder form
The prepared slices of Chinese crude drugs being used as medicine.Chinese medicine wall cell disruption medicine materical crude slice is that full ingredient is used as medicine, and medical substance basis is constant, meets the intension of the prepared slices of Chinese crude drugs,
The nature and flavor of medicine materical crude slice and channel tropism after broken wall, function keep consistent with the tradition property of medicine materical crude slice with curing mainly etc., and broken wall medicine materical crude slice can be straight
It connects to brew and take, can be taken together with the dregs of a decoction.But medicine materical crude slice manufacturing enterprise applies not broken wall medicine materical crude slice technology at home at present
Extensively, real industry standard is not formed yet.Therefore, a kind of preparation method of Chinese medicine wall cell disruption medicine materical crude slice is researched and developed, sufficiently
The advantage that the full ingredient of Chinese medicine wall cell disruption medicine materical crude slice is used as medicine is played, whole effective components of traditional Chinese medicine are retained by broken wall, and then more sharp
In absorption of the user to effective component, is extracted with alleviating after existing Chinese medicine particle adds water to be concentrated, Chinese medicine part can only be extracted
The problem of effective component, becomes very necessary and urgent.
Trollflower (Trollius chinensis Bunge) is the plant of Ranunculaceae Trollius.Its chemical component is main
There are veratric acid (veratric acid), orientoside (orientin), vitexin (vitexin), Li Lu amide
(veratramide), palmitinic acid (palmitic acid) etc.., can be clearing heat and detoxicating with medicinal function, cure mainly tonsillitis, in
Otitis.For acute and chronic tonsillitis, otitis media acuta, acute myringitis, acute conjunctivitis, acute lymphangitis.However,
There is presently no the reports about trollflower broken wall medicine materical crude slice and its preparation process.
Summary of the invention
The object of the present invention is to provide a kind of trollflower broken wall medicine materical crude slice and preparation method thereof.
The present invention provides a kind of preparation methods of trollflower broken wall medicine materical crude slice, method includes the following steps:
(1) it is the particle of 40-100 mesh by dry globeflower medicinal materials precomminution, is then impregnated with ethanol water, mistake
Obtained filter cake is freeze-dried by filter；
(2) trollius chinensis granular that step (1) obtains is placed under vacuum condition and carries out microwave treatment, then carry out Ultramicro-powder
It is broken, obtained micropowders are mixed with ethanol water then, are pelletized, it is dry.
The present invention also provides the trollflower broken wall medicine materical crude slice prepared by the above method.
According to the preparation method of trollflower broken wall medicine materical crude slice of the present invention, globeflower medicinal materials are subjected to precomminution first,
Then it successively impregnated, be freeze-dried and microwave treatment, a whole set for the treatment of process in this way can be to the cell wall of trollflower
Embrittlement is carried out, then can easily make trollflower breaking-wall cell by pulverizing, to obtain the higher gold of broken wall ratio
Lotus flower broken wall medicine materical crude slice.Moreover, the product composition consistency of the trollflower broken wall medicine materical crude slice prepared according to the method described in the present invention compared with
Good, quality is stable, controllable.
Specific embodiment
Detailed description of the preferred embodiments below.It should be understood that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to restrict the invention.
The endpoint of disclosed range and any value are not limited to the accurate range or value herein, these ranges or
Value should be understood as comprising the value close to these ranges or value.For numberical range, between the endpoint value of each range, respectively
It can be combined with each other between the endpoint value of a range and individual point value, and individually between point value and obtain one or more
New numberical range, these numberical ranges should be considered as specific open herein.
The preparation method of trollflower broken wall medicine materical crude slice of the present invention the following steps are included:
(1) it is the particle of 40-100 mesh by dry globeflower medicinal materials precomminution, is then impregnated with ethanol water, mistake
Obtained filter cake is freeze-dried by filter；
(2) trollius chinensis granular that step (1) obtains is placed under vacuum condition and carries out microwave treatment, then carry out Ultramicro-powder
It is broken, obtained micropowders are mixed with ethanol water then, are pelletized, it is dry.
In step (1), after precomminution, the size for the particle that the globeflower medicinal materials obtain after crushing is 40-
100 mesh.By carrying out precomminution to the globeflower medicinal materials, the specific surface area of globeflower medicinal materials is improved, thus after being more advantageous to
Embrittlement of the processes such as continuous immersion, freezing and microwave treatment to trollflower cell wall.In the present invention, the work of the precomminution
Sequence is implemented using the grinding device of this field routine, and details are not described herein.
In step (1), the concentration for carrying out impregnating the ethanol water used to trollius chinensis granular can be 20-40
Weight %.In the preferred case, the concentration of the ethanol water is 30-40 weight %.In the present invention, using above-mentioned concentration
Ethanol water trollius chinensis granular is impregnated, be conducive to trollflower cell wall carry out embrittlement, to help to obtain
The trollflower broken wall medicine materical crude slice of high sporoderm-broken rate.
In step (1), the condition of immersion may include: that temperature is 40-60 DEG C, and the time is 0.5-2 hours.In the present invention
In, by impregnating trollius chinensis granular at a relatively high temperature, freezing processing is then carried out at very low temperature,
So that trollflower cell is exposed under the larger temperature difference, be conducive to carry out embrittlement to trollflower cell wall in this way, to be conducive to
Obtain the trollflower broken wall medicine materical crude slice of high sporoderm-broken rate.
In step (1), during the immersion, the volume ratio of trollius chinensis granular and ethanol water can be 1:
2-10, preferably 1:3-8, more preferably 1:3-5.
In step (1), the condition of freeze-drying may include: that temperature is -5 DEG C~-30 DEG C, vacuum degree 5-30Pa.
Herein, vacuum degree refers to absolute pressure.
In step (1), filtering can use the strainer filtering of this field routine.In a particular embodiment, described
Strainer can be the stainless steel cloth that mesh size is 200 mesh.
In step (2), the condition of microwave treatment may include: that temperature is 10-40 DEG C, time 20-40min, microwave
Power be 10-20kW, vacuum degree 5-30Pa.
In step (2), it is preferable that it is 40 microns or less that the process of the ultramicro grinding, which crushes the trollius chinensis granular,
The micropowders of (preferably 5-40 microns, more preferably 5-30 microns).Equipment used in pulverizing can be wall cell disruption powder
Broken machine, such as CW5-100QA broken wall micronizer.
In step (2), the concentration of ethanol water used can be 50-70 weight %.
In step (2), the mixing mass ratio of the micropowders and the ethanol water is 1:0.5-0.8, preferably
For 1:0.6-0.7.
In step (2), the method for the drying can be contact drying, pneumatic conveying drying, tunnel type baking oven drying, vacuum
Drying, fluidized drying, freeze-drying, far-infrared ray drying or microwave drying.In the preferred case, the method for the drying is freezing
It is dry.
The present invention also provides the trollflower broken wall medicine materical crude slice prepared by the above method.
The present invention will be described in detail by way of examples below.
Embodiment 1
1.0kg globeflower medicinal materials are taken, precomminution to granularity is the particle of 80 mesh, is subsequently added into 5 times of volumes of trollius chinensis granular
30 weight % ethanol solution, impregnated 1 hour at 50 DEG C, with the stainless steel wire net filtration of 200 mesh, the filter cake that will be obtained
It is freeze-dried at -20 DEG C, under 20Pa vacuum degree.Obtained trollius chinensis granular is placed under vacuum condition and is carried out at microwave
Reason, the condition of microwave treatment are as follows: temperature is 25 DEG C, time 30min, and the power of microwave is 15kW, vacuum degree 20Pa.With
CW5-100QA broken wall micronizer pulverizes obtained trollius chinensis granular, obtain granularity be 5-30 micron surpass
Fine powder.With the ethanol water that concentration is 60 weight % it is that 1:0.6 is mixed with weight ratio by the micropowders, squeezes out
Granulation, is then freeze-dried at -20 DEG C, under 20Pa vacuum degree, so that trollflower broken wall medicine materical crude slice sample A1 be made.
Embodiment 2
1.0kg globeflower medicinal materials are taken, precomminution to granularity is the particle of 40 mesh, is subsequently added into 5 times of volumes of trollius chinensis granular
20 weight % ethanol solution, impregnated 2 hours at 40 DEG C, with the stainless steel wire net filtration of 200 mesh, the filter cake that will be obtained
It is freeze-dried at -20 DEG C, under 20Pa vacuum degree.Obtained trollius chinensis granular is placed under vacuum condition and is carried out at microwave
Reason, the condition of microwave treatment are as follows: temperature is 25 DEG C, time 30min, and the power of microwave is 15kW, vacuum degree 20Pa.With
CW5-100QA broken wall micronizer pulverizes obtained trollius chinensis granular, obtain granularity be 5-30 micron surpass
Fine powder.With the ethanol water that concentration is 70 weight % it is that 1:0.5 is mixed with weight ratio by the micropowders, squeezes out
Granulation, is then freeze-dried at -20 DEG C, under 20Pa vacuum degree, so that trollflower broken wall medicine materical crude slice sample A2 be made.
Embodiment 3
1.0kg globeflower medicinal materials are taken, precomminution to granularity is the particle of 100 mesh, is subsequently added into 5 times of volumes of trollius chinensis granular
40 weight % ethanol solution, impregnated 0.5 hour at 60 DEG C, with the stainless steel wire net filtration of 200 mesh, the filter cake that will be obtained
It is freeze-dried at -20 DEG C, under 20Pa vacuum degree.Obtained trollius chinensis granular is placed under vacuum condition and is carried out at microwave
Reason, the condition of microwave treatment are as follows: temperature is 25 DEG C, time 30min, and the power of microwave is 15kW, vacuum degree 20Pa.With
CW5-100QA broken wall micronizer pulverizes obtained trollius chinensis granular, obtain granularity be 5-30 micron surpass
Fine powder.With the ethanol water that concentration is 50 weight % it is that 1:0.8 is mixed with weight ratio by the micropowders, squeezes out
Granulation, is then freeze-dried at -20 DEG C, under 20Pa vacuum degree, so that trollflower broken wall medicine materical crude slice sample A3 be made.
Embodiment 4
1.0kg globeflower medicinal materials are taken, precomminution to granularity is the particle of 50 mesh, is subsequently added into 3 times of volumes of trollius chinensis granular
25 weight % ethanol solution, impregnated 2 hours at 45 DEG C, with the stainless steel wire net filtration of 200 mesh, the filter cake that will be obtained
It is freeze-dried at -20 DEG C, under 20Pa vacuum degree.Obtained trollius chinensis granular is placed under vacuum condition and is carried out at microwave
Reason, the condition of microwave treatment are as follows: temperature is 25 DEG C, time 30min, and the power of microwave is 15kW, vacuum degree 20Pa.With
CW5-100QA broken wall micronizer pulverizes obtained trollius chinensis granular, obtain granularity be 5-30 micron surpass
Fine powder.With the ethanol water that concentration is 55 weight % it is that 1:0.8 is mixed with weight ratio by the micropowders, squeezes out
Granulation, is then freeze-dried at -20 DEG C, under 20Pa vacuum degree, so that trollflower broken wall medicine materical crude slice sample A4 be made.
Embodiment 5
1.0kg globeflower medicinal materials are taken, precomminution to granularity is the particle of 100 mesh, is subsequently added into 4 times of volumes of trollius chinensis granular
35 weight % ethanol solution, impregnated 2 hours at 55 DEG C, with the stainless steel wire net filtration of 200 mesh, the filter cake that will be obtained
It is freeze-dried at -20 DEG C, under 20Pa vacuum degree.Obtained trollius chinensis granular is placed under vacuum condition and is carried out at microwave
Reason, the condition of microwave treatment are as follows: temperature is 25 DEG C, time 30min, and the power of microwave is 15kW, vacuum degree 20Pa.With
CW5-100QA broken wall micronizer pulverizes obtained trollius chinensis granular, obtain granularity be 5-30 micron surpass
Fine powder.With the ethanol water that concentration is 65 weight % it is that 1:0.5 is mixed with weight ratio by the micropowders, squeezes out
Granulation, is then freeze-dried at -20 DEG C, under 20Pa vacuum degree, so that trollflower broken wall medicine materical crude slice sample A5 be made.
Comparative example 1
Trollflower broken wall medicine materical crude slice is prepared according to the method for embodiment 1, the difference is that not implementing ethanol water immersion
Process, so that trollflower broken wall medicine materical crude slice sample D1 be made.
Comparative example 2
Trollflower broken wall medicine materical crude slice is prepared according to the method for embodiment 1, the difference is that being replaced with the mode of natural air drying cold
Be lyophilized it is dry, thus be made trollflower broken wall medicine materical crude slice sample D2.
Comparative example 3
Trollflower broken wall medicine materical crude slice is prepared according to the method for embodiment 2, the difference is that not implementing ethanol water immersion
Process, so that trollflower broken wall medicine materical crude slice sample D3 be made.
Comparative example 4
Trollflower broken wall medicine materical crude slice is prepared according to the method for embodiment 2, the difference is that being replaced with the mode of natural air drying cold
Be lyophilized it is dry, thus be made trollflower broken wall medicine materical crude slice sample D4.
Test case
The non-broken cells limit of trollflower broken wall medicine materical crude slice is tested with the following method: taking trollflower broken wall medicine materical crude slice
0.1g adds chloraldurate aqueous solution (volume ratio of chloraldurate test solution and water is 1:1) 10ml to be placed on glass slide, and load is set
In microscopically observation, under 10 × 10 times of visuals field, greater than 100 microns and the powder number of complete cell is 0-5.Test
As a result as shown in table 1 below.
Table 1
| Embodiment number | Non- broken cells limit (a) |
| Embodiment 1 | 1 |
| Embodiment 2 | 0 |
| Embodiment 3 | 3 |
| Embodiment 4 | 2 |
| Embodiment 5 | 1 |
| Comparative example 1 | 8 |
| Comparative example 2 | 7 |
| Comparative example 3 | 9 |
| Comparative example 4 | 8 |
Can be seen that by the result of table 1 can be made the higher lily feet of broken wall ratio using method of the present invention
Flower broken wall medicine materical crude slice.
The preferred embodiment of the present invention has been described above in detail, and still, the present invention is not limited thereto.In skill of the invention
In art conception range, can with various simple variants of the technical solution of the present invention are made, including each technical characteristic with it is any its
Its suitable method is combined, and it should also be regarded as the disclosure of the present invention for these simple variants and combination, is belonged to
Protection scope of the present invention.
Claims (9)
1. a kind of preparation method of trollflower broken wall medicine materical crude slice, which is characterized in that method includes the following steps:
(1) it is the particle of 40-100 mesh by dry globeflower medicinal materials precomminution, is then impregnated with ethanol water, is filtered, it will
Obtained filter cake freeze-drying；
(2) trollius chinensis granular that step (1) obtains is placed under vacuum condition and carries out microwave treatment, then pulverized,
Then obtained micropowders are mixed with ethanol water, is pelletized, it is dry.
2. the method according to claim 1, wherein it is 40- that soaking conditions described in step (1), which include: temperature,
60 DEG C, the time is 0.5-2 hours.
3. the method according to claim 1, wherein the condition of freeze-drying described in step (1) includes: temperature
It is -5 DEG C~-30 DEG C, vacuum degree 5-30Pa.
4. method described in any one of -3 according to claim 1, which is characterized in that the ethyl alcohol used in step (1)
The concentration of aqueous solution is 20-40 weight %.
5. the method according to claim 1, wherein the process of ultramicro grinding described in step (2) is by the gold
It is 40 microns of micropowders below that lotus flower particle, which crushes,.
6. the method according to claim 1, wherein the condition of microwave treatment described in step (2) includes: temperature
It is 10-40 DEG C, time 20-40min, the power of microwave is 10-20kW, vacuum degree 5-30Pa.
7. the method according to claim 1, wherein the concentration of the ethanol water used in step (2)
For 50-70 weight %.
8. method according to claim 1 or claim 7, which is characterized in that in step (2), the micropowders and the second
The mixing mass ratio of alcohol solution is 1:0.5-0.8.
9. the trollflower broken wall medicine materical crude slice of the preparation of the method as described in any one of claim 1-8.
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Application publication date: 20190412 |
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