CN101461852A - Method for preparing super fine powder of rose - Google Patents
Method for preparing super fine powder of rose Download PDFInfo
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- CN101461852A CN101461852A CNA2007101591066A CN200710159106A CN101461852A CN 101461852 A CN101461852 A CN 101461852A CN A2007101591066 A CNA2007101591066 A CN A2007101591066A CN 200710159106 A CN200710159106 A CN 200710159106A CN 101461852 A CN101461852 A CN 101461852A
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Abstract
The invention relates to a method for preparing rose superfine powder, which comprises: taking medicinal and edible fresh rose as a raw material, and performing impurity removal, cleaning and vacuum freeze-drying; and coarsely crushing the dried rose raw material, applying fluidized bed pneumatic milling technology for superfine processing, and preparing superfine powder products with water content between 6 and 8 and granularity between 1,000 and 3,000 meshes. The products produced by the method have the characteristics of uniform granularity, good dispersity, no processing pollution, capability of reserving bioactive compositions and thermosensitive compositions to the maximum degree, and not only can be quick to take health care effect and complete to absorb and digest but also can reduce the dosage and greatly improve the utilization rate of nutritive compositions of the rose.
Description
Technical field
The present invention relates to the superfine powder process technology of the biomaterial of nourishing healthy, medical treatment, daily cosmetics, specifically a kind of preparation method of Flos Rosae Rugosae micropowder.
Background technology
Flos Rosae Rugosae (Rosa rugosa Thumb.) is a Rosaceae, the machaka of Rosa.Flos Rosae Rugosae originates in China, plant with a long history, as far back as the Han dynasty just relevant for the literature record of Flos Rosae Rugosae.The Flos Rosae Rugosae resource distribution is wide, and south gets Guangdong, Shenyang, Liaoning is arrived in north, Shanghai, Jiangsu, Zhejiang, Shandong from the east of the coastal area, and generally all there is cultivation in the west to landlocked Henan, Gansu, Xinjiang.Wherein based on Gansu, Sichuan, Jiangsu, Shandong, Beijing, Henan, Hebei, Liaoning, Heilungkiang, Taiwan, Shanxi and Xinjiang and other places.
Its advantage of Flos Rosae Rugosae of Liaoning areas of Shenyang plantation is: cold-resistant, impoverishment tolerant, disease-resistant, drought resisting, adaptability are strong, manageability, and growth is fast, and at the florescence long (May-October), full-bloom stage can maintain more than 15 years.Not only started big flowering plant and normally survived the winter, also improved Flos Rosae Rugosae afforestation use value simultaneously, more enriched the biological value of Flos Rosae Rugosae in Shenyang.
Flos Rosae Rugosae can not only be beautified, afforest the city and also be collected medicinal, edible for one, is widely used in chemical industry, food, wine brewing, medicine and other fields.Chinese Ancient Books pharmacopeia " detailed outline is picked up any lost article from the road " is carried: the effect of " Flos Rosae Rugosae and blood, promoting the circulation of blood regulating QI to promote menstruation, looks skin care ".The traditional Chinese medical science thinks, Flos Rosae Rugosae is warm in nature, sweet in the mouth, little hardship, returns liver, kidney channel, can pass through resolving depression, promoting blood circulation to remove blood stasis.Be used for dysentery traumatic injury etc. under stomachache due to hyperactive liver-QI attacking the stomach, mastalgia toxic swelling, menorrhagia, leucorrhea with red and white discharge, the enteritis.
It is sweet and refreshing that Flos Rosae Rugosae contains the fragrance of abundant vitamin C, glucose, xylose, sucrose, citric acid, malic acid, food, and it is refreshing to make us the spacious god of the heart.This shows that along with development of modern science and technology and people's health care consciousness enhancing, nutritive value of Flos Rosae Rugosae and health care are worth the favor that more and more is subjected to people, the bioavailability with nutrition receives much attention especially.
At present, the product of domestic extract except that Flos Rosae Rugosae, the processing technique of Flos Rosae Rugosas pollen is much more extensive, and drying mode or program can cause the loss of Flos Rosae Rugosae active ingredient; Or its goods fineness only reaches 70～90 orders, fails to make the nutritive value of Flos Rosae Rugosae to obtain more effective absorbing.
Lyophilisation claims drying bu sublimation again, its principle be with the quick-freezing of material elder generation to below the eutectic point of contained solution, under vacuum condition, make ice crystal be converted into water vapour (being called distillation) then and remove, thus the acquisition dried product.The goods of lyophilisation have the advantage that many other methods can not be reached: as keep biological activity, be suitable for the processing of temperature-sensitive article and readily oxidizable substance product (Wang Yiqiang etc., vacuum lyophilization is to the influence of food quality, the Laiyang Agricultural College journal, 2003,20 (2): 149-153); Product volume is constant, has avoided material to concentrate and makes goods rotten; Form the structure of porosity and looseness, goods have extremely strong rehydration; Dehydration thoroughly, can be under sealing or room temperature long preservation, (Jia Mingsheng, Freeze Drying Technique is in Application in Food Processing, food research and development, 1996,17 (2): 51-54) and the nutritive value loss is few.Therefore, the application of Lyophilisation technique for making in biological medicine and food service industry more and more widely, the feasibility of goods processing and economy depend on that then working process parameter selects and the produce market orientation.
To the powder body material between the nanometer, ultra-fine powder technology comprises preparation, separation, drying, conveying, mixing and the homogenizing technology of micropowder to the space scale that superfine powder is meant object particle at micron, and process for modifying surface detects and application technology etc.Micropowder is because its fine size, narrow diameter distribution, quality are even, thereby has specific surface area is big, surface activity is high, chemical reaction velocity is fast, fusing speed is fast, sintered body intensity is big and unique electricity, magnetic, optical characteristics etc.At present, micropowder is widely used in many high-technology fields, as material, chemical industry, electronics, castoff regenerative and biological medicine etc., especially the application of micropowder in Chinese medicine and health food, expanded human medical-care health food source, make nutritious or effective in cure but discharge slow, moving of absorption difference, plant product has become high-grade trophism health food, promptly take effect after 9 days really as superfine pumpkin powder feed artificial diabetes rabbit, (that opens is good etc. and common Fructus Cucurbitae moschatae powder needs just to see more than 15 days curative effect, superfine pumpkin powder is to the research of rabbit experiment diabetes effect, China's grain and oil journal, 1998,13 (2): 52-56).The dissolution rate and the utilization rate of effective ingredient have been improved greatly through the Chinese crude drug of superfine grinding, their taking conveniences, avoided numerous and diverse decoction, improved surplus in the of 20% than gastrodia tuber dispensing granule as the particulate gastrodine dissolution of Rhizoma Gastrodiae micropowder, and in 5 minutes gastrodine stripping (World Science technology-Chinese medicine is integrated for Zhang Xiaojuan etc., Chinese medicine superfine powder and the application in Chinese medicine western language granule thereof more than 70%, 2002,4 (1): 47-49).
In using the numerous ultra-fine Chinese medicine of above-mentioned technology processing, health food source, the preparation of Flos Rosae Rugosae micropowder yet there are no relevant report at home.
Summary of the invention
The object of the present invention is to provide the efficiently stripping of a kind of its nutritional labeling, release, thereby improve the preparation method of the Flos Rosae Rugosae micropowder of bioavailability.
To achieve these goals, the technical solution adopted in the present invention is:
A kind of preparation method of super fine powder of rose:
1) be raw material with fresh Flos Rosae Rugosae, remove impurity, water clean up, and be standby;
2) lyophilisation:
A. precooling: make Flos Rosae Rugosae in 1-30 minute, reduce to-25 ℃～-30 ℃ from room temperature; Make the material quick-freezing to the material eutectic point;
B. vacuum drying: making the moisture in the raw material is gaseous state from solid-state direct distillation; The dry vacuum that adopts is 15～19Pa, Flos Rosae Rugosae is warming up to 30 ℃～35 ℃ from initial temperature-40 ℃～-50 ℃ with 8 ℃～12 ℃ the speed of per hour raising, material temperature is stabilized in 30 ℃～35 ℃ and continues drying, and vacuum drying total time is 5～15 hours;
3) coarse powder processing: dried Flos Rosae Rugosae is crushed to the granule that particle diameter is 0.5～2.0mm with general pulverizer;
4) superfine grinding: adopt fluidized bed airflow crushing technology processing super fine powder of rose, its machined parameters scope: air consumption 3～20m
3/ min, air pressure 0.5～1.0mPa, air velocity 350～500m/s, grading wheel rotating speed 4000～18000r/min; The super fine powder of rose granularity is 1000～3000 orders.
Be specially:
1. select for use the new fresh-rose of place of production region conforms pollution-free food home environment quality technology standard to make raw material;
2. remove impurity is cleaned: remove the rotten Flos Rosae Rugosae in the new fresh-rose, new fresh-rose is cleaned up in clear water;
3. precooling stage: make the material quick-freezing to the material eutectic point, be specially: above-mentioned material tiles into dish, opening compressor freezes in advance to hothouse, behind Wen Da-13 ℃～-17 ℃ of about 10～15 minutes hothouse shelf plates, the glove charging tray is in frozen vacuum dryer, cryogenic temperature-40 ℃～-30 ℃ is set again, and cooling time reaches-25 ℃～-30 ℃ with temperature of charge and is as the criterion, general 1-30 minute;
4. vacuum drying: making the moisture in the material is gaseous state from solid-state direct distillation, specifically: material freezing fully after, open vacuum pump earlier to the water vessel evacuation, again to the hothouse evacuation, energising heating shelf replenishes the required heat of water sublimed in the material then, and the plate temperature is linear to be promoted, per hour improve 8 ℃～12 ℃ approximately, the limiting temperature that the shelf heating is set is 40 ℃; Keep dry the vacuum of chamber at 15～19Pa, and water vessel vacuum is at 10～12Pa; Keep the water vessel temperature between-40 ℃～-50 ℃; After 5～15 hours, distillation is finished; Treat to stop when temperature of charge is stabilized in 30 ℃～35 ℃ desorption process; At this moment, material water ratio is 2～5%;
5. the sealing of Flos Rosae Rugosae dry product is preserved, and prevents moisture absorption;
6. coarse powder processing: earlier the Flos Rosae Rugosae dry product is crushed to 0.5～2.0mm size particles with general pulverizer;
7. superfine grinding: Flos Rosae Rugosae coarse powder impouring fluidized bed counter jet mill pulverizing chamber, with the high velocity air is power, material is by intergranular bump itself, and air-flow makes material pulverizing, breakage of particles refinement, machined parameters: air consumption 3～20m to effects such as the impact of material, shearing, frictions
3/ min, air pressure 0.5～1.0mPa, air velocity 350～500m/s; Material drops into grader through feeder, under the effect of classification vortex power, the thickness powder separates, the classified wheel of fine powder of satisfying granularity requirements enters the fine powder trapping system, coarse powder and reunion shape fine powder are reduced to the secondary air place, by the centrifugal ascending air of spiral material is washed strongly, the thickness powder is separated once more, grading wheel rotating speed 4000～18000r/min; The granularity of super fine powder of rose finished product is 1000～3000 orders, and the finished product moisture content is 6～8%.
8. the collection manufactured goods must granularity be 1000～3000 purpose Flos Rosae Rugosae micropowders.
Advantage of the present invention is:
1. guaranteed that the biochemical activity of nutrient substance is not damaged in the Flos Rosae Rugosae.Because the present invention has adopted this new and high technology of vacuum lyophilization, realized keeping in processing procedure product structure constant, nutritive value is constant, and especially the biological activity of temperature-sensitive sensitivity and readily oxidizable substance is not damaged, the processing technique favorable reproducibility, viable economically.
2. Flos Rosae Rugosae nutrition dissolving eduction rate obviously increases.
3. meet sanitary standard, have the environmental protection characteristics, each link does not have any chemical treating process.
4. product has good cost performance.The present invention through product fineness that lyophilisation makes between 1000～3000 orders, take the back and better bioavailability is arranged than Flos Rosae Rugosae or coarse powder product, thereby provide condition for reducing consumption, provide possibility for reducing use cost, injected new vitality for simultaneously the application and development of related medical health product.
5. the present invention adopts high velocity air mill comminuting method, and is easy and simple to handle, operation is few, process time is short, do not have other side reaction, Flos Rosae Rugosas pollen purity height, pollution-free, can produce in batches.
The specific embodiment
Below in conjunction with specific embodiment in detail the present invention is described in detail.
Embodiment 1
1. select for use the new fresh-rose of place of production region conforms pollution-free food home environment quality technology standard to make raw material;
2. remove impurity is cleaned: remove the rotten Flos Rosae Rugosae in the new fresh-rose, new fresh-rose is cleaned up in clear water;
3. precooling stage: make the material quick-freezing to the material eutectic point, be specially: above-mentioned material tiles into dish, opening compressor freezes in advance to hothouse, behind Wen Da-15 ℃ of about 15 minutes hothouse shelf plate, the glove charging tray is in frozen vacuum dryer, cryogenic temperature-40 ℃ is set again, and cooling time reaches-25 ℃ with temperature of charge and is as the criterion, and present embodiment is 20 minutes;
4. vacuum drying: concrete operations be treat material freezing fully after, open vacuum pump earlier to the water vessel evacuation, again to the hothouse evacuation, shelf is heated in energising then, the plate temperature is linear to be promoted, and per hour improves 10 ℃ approximately, and the limiting temperature that the shelf heating is set is 40 ℃; Keep dry the vacuum of chamber at 15Pa, and water vessel vacuum is at 12Pa; Keep the water vessel temperature at-45 ℃; After 6 hours, distillation is finished; Treat to stop when temperature of charge is stabilized in 30 ℃ desorption process; At this moment, material water ratio is 5%;
5. the sealing of Flos Rosae Rugosae dry product is preserved, and prevents moisture absorption;
6. coarse powder processing: earlier the Flos Rosae Rugosae dry product is crushed to the 2.0mm size particles with general pulverizer;
7. superfine grinding: Flos Rosae Rugosae coarse powder impouring fluidized bed counter jet mill pulverizing chamber, with the high velocity air is power, material is by intergranular bump itself, and air-flow makes material pulverizing, breakage of particles refinement, machined parameters: air consumption 20m to effects such as the impact of material, shearing, frictions
3/ min, air pressure 1.0mPa, air velocity 500m/s; Material drops into grader through feeder, under the effect of classification vortex power, the thickness powder separates, the classified wheel of fine powder of satisfying granularity requirements enters the fine powder trapping system, coarse powder and reunion shape fine powder are reduced to the secondary air place, by the centrifugal ascending air of spiral material is washed strongly, the thickness powder is separated once more, grading wheel rotating speed 14000r/min.
8. the collection manufactured goods must granularity be 2000～3000 purpose Flos Rosae Rugosae micropowders, and the finished product moisture content is 7%.
Embodiment 2
Difference from Example 1 is:
Open compressor in the step 4) to hothouse shelf refrigeration, 10 minutes after plate Wen Da-13 ℃, the glove charging tray was provided with cryogenic temperature-30 ℃ again in frozen vacuum dryer, and cooling time reaches-28 ℃ with temperature of charge and is as the criterion, and present embodiment is 30 minutes;
Step 5) keeps dry the vacuum of chamber at 17Pa, and water vessel vacuum is at 12Pa; Keep the water vessel temperature at-50 ℃; Shelf plate temperature is linear in the process of vacuum drying promotes by per hour improving 8 ℃ of settings, and the limiting temperature of shelf heating is 40 ℃; After 10 hours, distillation is finished; Treat to stop when temperature of charge is stabilized in 35 ℃ desorption process; At this moment, material water ratio is 3%;
Machined parameters in the step 8) superfine grinding: air consumption 15m
3/ min, air pressure 0.5mPa, air velocity 350m/s, the grading wheel rotating speed 6500r/min of grader.
Step 9) is collected manufactured goods, and the manufactured goods granularity is that 1000～2000 orders, moisture content are 6%.
Embodiment 3
Difference from Example 1 is:
Open compressor in the step 4) to hothouse shelf refrigeration, 14 minutes after plate Wen Da-16 ℃, the glove charging tray was provided with cryogenic temperature-40 ℃ again in frozen vacuum dryer, and cooling time reaches-28 ℃ with temperature of charge and is as the criterion, and present embodiment is 15 minutes;
Shelf plate temperature is linear in the step 5) process of vacuum drying promotes by per hour improving 12 ℃ of settings; Finish process of vacuum drying after 15 hours; At this moment, material water ratio is 2%;
Machined parameters in the step 8) superfine grinding: air consumption 15m
3/ min, air pressure 0.8mPa, air velocity 450m/s, the grading wheel rotating speed 10000r/min of grader.
Step 9) is collected manufactured goods, and the manufactured goods granularity is that 1500～2500 orders, moisture content are 6%.
The product that adopts the inventive method to produce has epigranular, good dispersion, no processing pollution, characteristics such as retains biological activity composition and temperature-sensitive composition to greatest extent, its health-care effect is rapid-action with making, assimilate fully, and can also reduce consumption, improved the utilization rate of Flos Rosae Rugosae nutritional labeling greatly.
Claims (3)
1. the preparation method of a super fine powder of rose is characterized in that:
1) be raw material with fresh Flos Rosae Rugosae, remove impurity, water clean up, and be standby;
2) lyophilisation:
A. precooling: make Flos Rosae Rugosae in 1-30 minute, reduce to-25 ℃～-30 ℃ from room temperature;
B. vacuum drying: the dry vacuum that adopts is 15～19Pa, Flos Rosae Rugosae is warming up to 30 ℃～35 ℃ from initial temperature-40 ℃～-50 ℃ with 8 ℃～12 ℃ the speed of per hour raising, material temperature is stabilized in 30 ℃～35 ℃ and continues drying, and vacuum drying total time is 5～15 hours;
3) coarse powder processing: dried Flos Rosae Rugosae is crushed to the granule that particle diameter is 0.5～2.0mm with general pulverizer;
4) superfine grinding: adopt fluidized bed airflow crushing technology processing super fine powder of rose, its machined parameters scope: air consumption 3～20m
3/ min, air pressure 0.5～1.0mPa, air velocity 350～500m/s, grading wheel rotating speed 4000～18000r/min; The super fine powder of rose granularity is 1000～3000 orders.
2. preparation method according to claim 1 is characterized in that: drug of choice is made raw material with, edible rose flower, carries out lyophilisation through remove impurity, after cleaning;
Described lyophilisation is two stages with different parameters, the one, in the precooling stage, concrete parameter: the temperature that controls environment is earlier put into material to-13 ℃～-17 ℃, cryogenic temperature-40 ℃～-30 ℃ is set again, in 1-30 minute, makes temperature of charge reach-25 ℃～-30 ℃;
The 2nd, the vacuum drying stage, concrete parameter: hothouse vacuum is 15～19Pa, water vessel vacuum is 10～12Pa and freezes to-40 ℃～-50 ℃, the aqueous vapor distillation time is 5～15 hours, the heat-conduction medium linear temperature increase, per hour raise 8 ℃～12 ℃, establishing limiting temperature is 40 ℃, ends when temperature of charge is stabilized in 30 ℃～35 ℃.
3. preparation method according to claim 1 is characterized in that: described remove impurity, cleaning are meant the rotten Flos Rosae Rugosae of removing in the new fresh-rose, and new fresh-rose is cleaned up in clear water.
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| CNA2007101591066A CN101461852A (en) | 2007-12-21 | 2007-12-21 | Method for preparing super fine powder of rose |
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| CN101664218B (en) * | 2009-09-28 | 2012-12-05 | 艾志毅 | Instant medlar juice solid beverage and processing method thereof |
| CN103229883A (en) * | 2013-05-21 | 2013-08-07 | 广东嘉豪食品股份有限公司 | Method for manufacturing rose honey-containing collagen polypeptide tea |
| CN103504300A (en) * | 2013-09-24 | 2014-01-15 | 甘肃省检验检疫科学技术研究院 | Preparation method for rose starch through vacuum freeze-drying |
| CN103689796A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Lemon grass porous particle and application thereof in cigarettes |
| CN104621659A (en) * | 2015-01-22 | 2015-05-20 | 河北科技师范学院 | Preparation method of rose ultrafine powder |
| CN105441195A (en) * | 2015-12-03 | 2016-03-30 | 李嘉 | Purifying method for rose essential oil |
| CN106135587A (en) * | 2016-08-12 | 2016-11-23 | 四川省盛祥玫瑰生态农业开发有限公司 | A kind of processing method of rose tea |
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| CN108185432A (en) * | 2017-12-31 | 2018-06-22 | 西双版纳天恩生物科技开发有限公司 | The preparation method of Flos Rosae Rugosas pollen is lyophilized |
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| CN101664218B (en) * | 2009-09-28 | 2012-12-05 | 艾志毅 | Instant medlar juice solid beverage and processing method thereof |
| CN103229883A (en) * | 2013-05-21 | 2013-08-07 | 广东嘉豪食品股份有限公司 | Method for manufacturing rose honey-containing collagen polypeptide tea |
| CN103504300A (en) * | 2013-09-24 | 2014-01-15 | 甘肃省检验检疫科学技术研究院 | Preparation method for rose starch through vacuum freeze-drying |
| CN103689796A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Lemon grass porous particle and application thereof in cigarettes |
| CN104621659A (en) * | 2015-01-22 | 2015-05-20 | 河北科技师范学院 | Preparation method of rose ultrafine powder |
| CN105441195A (en) * | 2015-12-03 | 2016-03-30 | 李嘉 | Purifying method for rose essential oil |
| CN106190739A (en) * | 2016-07-22 | 2016-12-07 | 许备占 | Wild Hibisci Mutabilis dinner party with singsong girls in attendance |
| CN106135587A (en) * | 2016-08-12 | 2016-11-23 | 四川省盛祥玫瑰生态农业开发有限公司 | A kind of processing method of rose tea |
| CN108185432A (en) * | 2017-12-31 | 2018-06-22 | 西双版纳天恩生物科技开发有限公司 | The preparation method of Flos Rosae Rugosas pollen is lyophilized |
| CN108295999A (en) * | 2018-01-22 | 2018-07-20 | 张藜泷 | A kind of Khotan jade superfine powder and preparation method thereof |
| CN108295999B (en) * | 2018-01-22 | 2019-11-19 | 张藜泷 | A kind of Khotan jade superfine powder and preparation method thereof |
| CN113750001A (en) * | 2021-03-24 | 2021-12-07 | 北京东方淼森生物科技有限公司 | Mirabilis jalapa seed powder and preparation method and application thereof |
| CN113750001B (en) * | 2021-03-24 | 2022-07-01 | 北京东方淼森生物科技有限公司 | Mirabilis jalapa seed powder and preparation method and application thereof |
| CN116264903A (en) * | 2021-12-16 | 2023-06-20 | 沈阳农业大学 | Rose coated peanut and preparation method thereof |
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