CN113750001A - Mirabilis jalapa seed powder and preparation method and application thereof - Google Patents

Mirabilis jalapa seed powder and preparation method and application thereof Download PDF

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Publication number
CN113750001A
CN113750001A CN202110312206.8A CN202110312206A CN113750001A CN 113750001 A CN113750001 A CN 113750001A CN 202110312206 A CN202110312206 A CN 202110312206A CN 113750001 A CN113750001 A CN 113750001A
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mirabilis jalapa
seed powder
particle size
jalapa seed
mirabilis
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CN113750001B (en
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刘有停
张卫红
吕永博
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Nutri Woods Bio Tech Beijing Co ltd
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Nutri Woods Bio Tech Beijing Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/008—Preparations for oily skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Abstract

The invention relates to mirabilis jalapa seed powder and a preparation method and application thereof. The Mirabilis jalapa seed powder provided by the invention has the particle size distribution that the Dv (50) is less than or equal to 5 mu m, and the specific surface area is more than or equal to 800m2In terms of/kg. Compared with the conventional superfine powder, the mirabilis jalapa seed powder disclosed by the invention is smaller in particle size, good in skin affinity, oil-controlling, easy to apply, and more exquisite and smooth in skin and more uniform to apply after being applied.

Description

Mirabilis jalapa seed powder and preparation method and application thereof
Technical Field
The invention relates to the field of daily cosmetics, and in particular relates to mirabilis jalapa seed powder and a preparation method and application thereof.
Background
With the improvement of living standard, the requirements of people on the efficacy and safety of skin care products are higher and higher, and facial stains, facial roughness, aging and even skin diseases such as acne and comedo and the like caused by heredity, environmental pollution, ultraviolet irradiation, bad living habits or other reasons also become problems which puzzle people of all ages.
Early whitening active ingredients used in whitening spot-lightening skin care products include mercury compounds, parahormones, hydroquinone and the like, and although the whitening active ingredients act rapidly, the skin protection barrier is damaged, the water-oil balance is broken, and the self-renewal capacity of the skin is weakened after long-term use. And the whitening agents such as kojic acid, vitamin C and derivatives thereof also have the defects of potential safety hazard, poor stability or unobvious efficacy and the like.
Mirabilis jalapa seeds, which have been described as a fragrant plantain lily foundation cosmetic effect in dream of Red mansions. Mirabilis jalapa seeds are cleaned and peeled off, and contain white powder. At present, Mirabilis jalapa seed powder used in the market is applied to a skin care raw material after being subjected to conventional shelling and grinding, and the problems of skin irritation, poor skin-friendly effect, poor skin feeling and the like easily occur in practical application due to large particle size of the powder. However, if the particle size of the powder is too fine to reach the nanometer level, the powder is easy to block pores and enter the body after percutaneous absorption, and the exogenous substance influencing the normal physiological function of the skin can break the skin balance state, improve the permeability, reduce the selectivity and destroy the barrier function of the skin (Wuyan Yi, Tian Shuo, Bai Ming, etc. the medicine based on the functional characteristics of the skin can be absorbed through the skin in a new thinking [ J ] world traditional Chinese medicine, 2020,015(003) (361, 363,368 ]), so as to bring a series of potential safety risks. Based on the method, the mirabilis jalapa seed powder which is suitable in particle size range, mild, small in irritation and good in experience and skin-friendly property is developed, and has a wide application prospect.
Disclosure of Invention
Aiming at the defects of the prior art, the first purpose of the invention is to provide the mirabilis jalapa seed powder with smaller granularity than the conventional superfine powder, the particle size range and the specific surface area of the mirabilis jalapa seed powder are suitable, and the mirabilis jalapa seed powder has the advantages of being mild, small in irritation, good in experience feeling and good in skin-friendly property when being used in a skin care product.
The second purpose of the invention is to provide a preparation method of the mirabilis jalapa seed powder.
The third purpose of the invention is to provide the application of the mirabilis jalapa seed powder in skin care products
In a first aspect, the invention provides mirabilis jalapa seed powder, and the particle size distribution of the mirabilis jalapa seed powder meets the requirement that Dv (50) is less than or equal to 5 mu m, and the ratioThe surface area is more than or equal to 800m2/kg。
According to some embodiments of the invention, the Mirabilis jalapa seed meal has a particle size distribution such that 1 μm Dv (50) 4 μm.
According to a preferred embodiment of the invention, the particle size distribution of the mirabilis jalapa seed powder satisfies 2 μm Dv (50) 3 μm.
According to some specific embodiments of the present invention, the Mirabilis jalapa seed powder may have a particle size distribution Dv (50) of 1.5 μm, 2.0 μm, 2.5 μm, 3.0 μm, 3.5 μm, 4.0 μm, 4.5 μm.
According to some embodiments of the invention, the Mirabilis jalapa seed meal has a particle size distribution satisfying Dv (90) ≦ 50 μm.
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a particle size distribution such that 10 μm Dv (90) 40 μm.
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a particle size distribution such that Dv (90) is 20 μm or less and 40 μm or less.
According to some specific embodiments of the present invention, the particle size distribution Dv (90) of the mirabilis jalapa seed meal may be 5.0 μm, 6.0 μm, 8.0 μm, 9.0 μm, 10.0 μm, 15.0 μm, 20.0 μm, 30.0 μm, 40.0 μm, and points between the above values.
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a particle size distribution satisfying Dv (10) ≦ 1 μm.
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a particle size distribution such that Dv (10) is 0.5 μm or less and 1 μm or less.
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a particle size distribution such that Dv (10) is 0.7 μm or less and 0.95 μm or less.
According to some specific embodiments of the present invention, the particle size distribution Dv (10) of the mirabilis jalapa seed meal may be 0.55 μm, 0.6 μm, 0.65 μm, 0.7 μm, 0.75 μm, 0.8 μm, 0.9 μm, 0.95 μm, 1.0 μm.
In the invention, Dv (10) represents that 10% of particles of the mirabilis jalapa seed powder have a particle size smaller than the value in the volume-based particle size distribution; dv (50) represents a particle size distribution of the mirabilis jalapa seed powder on a volume basis, at which 50% of the particles have a particle size smaller than the value; dv (90) represents a particle size distribution of the Mirabilis jalapa seed powder on a volume basis, at which 90% of the particles have a particle size smaller than the value.
According to the invention, the full-range value of the particle size of the mirabilis jalapa seed powder is 5-30 μm.
According to some specific embodiments of the present invention, the particle size of Mirabilis jalapa seed powder may have a range of 8 μm, 10 μm, 12 μm, 15 μm, 18 μm, 20 μm, 22 μm, 25 μm, 28 μm, 30 μm.
According to a preferred embodiment of the invention, the particle size of the mirabilis jalapa seed powder has a full-range value of 5-25 μm.
According to a non-preferred embodiment of the present invention, the particle size of Mirabilis jalapa seed powder has a range of 10-25 μm.
In the invention, the full-range distribution of the particle sizes of the mirabilis jalapa seed powder is narrow, which shows that the particle size distribution of the mirabilis jalapa seed powder is relatively concentrated. In the invention, the full-range value of the particle size of the mirabilis jalapa seed powder is calculated by the following formula:
the overall distance value is (DV (90) -DV (10)),
the smaller the value, the smaller the degree of dispersion, and conversely, the greater the degree of dispersion.
According to some embodiments of the present invention, the Mirabilis jalapa seed powder has a specific surface area of 800-2/kg。
According to the preferred embodiment of the invention, the specific surface area of the mirabilis jalapa seed powder is 800-2000m2/kg。
According to some embodiments of the invention, the Mirabilis jalapa seed powder has a specific surface area of 1000-1500m2/kg。
According to some specific embodiments of the present invention, the Mirabilis jalapa seed powder may have a specific surface area of 900m2/kg、1000m2/kg、1100m2/kg、1200m2/kg、1300m2/kg、1400m2/kg、1500m2/kg、1600m2/kg、1700m2/kg、1800m2/kg、1900m2Kg, and points between the above values.
In the present invention, the specific surface area is an average value of the weight specific surface areas.
According to some embodiments of the present invention, the mirabilis jalapa seed powder is obtained by pulverizing mirabilis jalapa seed particles with an air flow pulverizer, preferably a QLM03 type air flow pulverizer.
The inventor of the invention finds that the particle size distribution Dv (50) and the specific surface area of the mirabilis jalapa seed powder are very important for the effect of the mirabilis jalapa seed powder in skin care products in the research process. The particle size distribution Dv (50) and the specific surface area of the mirabilis jalapa seed powder are limited in the above range, so that the mirabilis jalapa seed powder has unexpected technical effects in the application of skin care products, particularly in the aspects of oil control and skin feeling experience.
In a second aspect, the invention provides a preparation method of mirabilis jalapa seed powder, which comprises the following steps:
s1: providing mirabilis jalapa seed particles;
s2: carrying out shelling treatment and coating removal treatment on the mirabilis jalapa seed particles;
s3: carrying out grading and screening treatment on the mirabilis jalapa seed particles subjected to shelling treatment and coating removal treatment obtained in the step S2;
s4: crushing the mirabilis jalapa seed particles obtained in the step 3 after the grading and screening treatment by using an airflow crusher;
s5: and (4) screening the crushed mirabilis jalapa seed particles obtained in the step (S4) to obtain the mirabilis jalapa seed powder.
According to the present invention, the step S1 further includes pre-treating the mirabilis jalapa seed particles.
According to some embodiments of the invention, the pre-treatment comprises a water wash and drying treatment.
According to some embodiments of the invention, in step S1, the average particle size of Mirabilis jalapa seed particles is greater than or equal to 5 mm.
According to a preferred embodiment of the present invention, in step S1, the average particle size of the mirabilis jalapa seed particles is 5-10mm, and may be, for example, 5mm, 6mm, 7mm, 8mm, 9mm, or 10 mm.
According to some embodiments of the invention, in step S1, the mirabilis jalapa seed particles have a moisture content of < 5%. In the invention, the moisture content refers to the moisture content of the mirabilis jalapa seed particle raw material used for preparing the mirabilis jalapa seed powder in the method.
According to some embodiments of the invention, in step S3, the mesh number of the mirabilis jalapa seed particles after the grading and screening treatment is less than or equal to 100 meshes.
According to some embodiments of the present invention, in step S3, the mesh size of the mirabilis jalapa seed particles after the classification and screening process is 100-300 meshes.
According to some embodiments of the present invention, in step S3, the mesh number of the mirabilis jalapa seed particles after the classification and screening process may be 100 mesh, 130 mesh, 150 mesh, 180 mesh, 200 mesh, 220 mesh, 250 mesh, 300 mesh, and the values therebetween.
According to still other embodiments of the present invention, in step S3, the mesh size of the mirabilis jalapa seed particles after the classification and screening process is 100-200 meshes.
According to some embodiments of the invention, in step S4, the jet mill is a model QLM03 jet mill.
According to some embodiments of the invention, in step S4, the pulverization process is a low-temperature pulverization process.
According to some embodiments of the present invention, in step S4, the low-temperature pulverization treatment temperature is 0 to 4 ℃, and may be, for example, 1 ℃,2 ℃,3 ℃.
According to some embodiments of the invention, in step S5, the screening process is controlled using a cyclone collector of a jet mill.
According to some embodiments of the invention, in step S5, the screening process controls the particle size of the prepared mirabilis jalapa seed powder to be 1200-2000 mesh.
According to a preferred embodiment of the invention, in step S5, the screening process controls the particle size of the prepared mirabilis jalapa seed powder to be 1200-1600 meshes.
According to some specific embodiments of the present invention, in step S5, the screening process controls the particle size of the prepared mirabilis jalapa seed powder to be 1200 mesh, 1250 mesh, 1300 mesh, 1350 mesh, 1400 mesh, 1450 mesh, 1500 mesh, 1550 mesh, 1600 mesh.
The preparation method can be used for obtaining the mirabilis jalapa seed powder with proper particle size distribution and specific surface area, and the mirabilis jalapa seed powder has unexpected technical effects when being applied to skin care products, particularly in the aspects of oil control and skin feeling experience.
In a third aspect, the invention provides application of the mirabilis jalapa seed powder according to the first aspect or the mirabilis jalapa seed powder prepared by the method according to the second aspect in preparing a skin care product.
According to some embodiments of the invention, the skin care product is a whitening product, a make-up product, or an oil control product.
According to some embodiments of the invention, the cosmetic product is BB cream, honey powder, loose powder or powder film, and the like.
The preparation process of the mirabilis jalapa seed powder mainly comprises the following steps:
water washing of mirabilis jalapa seeds → airing → screening → mechanical shelling → de-coating → crushing → screening.
Compared with the prior art, the Mirabilis jalapa seed powder has the beneficial effects that:
(1) the mirabilis jalapa seed powder prepared by the superfine powder technology has smaller granularity than the conventional superfine powder, good skin-friendly property, oil control and easy application, and the skin after the application is more delicate and smooth and is more uniform.
(2) The mirabilis jalapa seed powder disclosed by the invention is applied to various cosmetics such as BB cream, honey powder, loose powder and powder film, can be used for immediately homogenizing skin color, efficiently covering blemishes, improving skin darkness and the like, and has the characteristics of large specific surface, good skin affinity and the like.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to example 1 of the present invention.
FIG. 2 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to example 3 of the present invention.
FIG. 3 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to comparative example 1 of the present invention.
FIG. 4 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to comparative example 2 of the present invention.
FIG. 5 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to comparative example 3 of the present invention.
FIG. 6 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to comparative example 4 of the present invention.
FIG. 7 shows a particle size distribution diagram of Mirabilis jalapa seed powder prepared according to comparative example 5 of the present invention.
Fig. 8 shows the results of the evaluation of skin-friendly effect using mirabilis jalapa seed powder prepared according to example 1 of the present invention, in which fig. 8A shows the state before application and fig. 8B shows the state after application.
Fig. 9 shows the results of the evaluation of skin-friendly effect using mirabilis jalapa seed powder prepared according to comparative example 1 of the present invention, in which fig. 9A shows the state before application and fig. 9B shows the state after application.
Fig. 10 shows a radar chart for skin feel evaluation performed in application example 3 according to the present invention.
The specific implementation mode is as follows:
the present invention will be described in detail below with reference to the drawings and examples, but the present invention is not limited to the examples.
In the following examples and comparative examples, the sources of the main apparatus used are shown in Table 1, and other apparatuses or apparatuses used in the present invention are conventional apparatuses or apparatuses unless otherwise specified.
TABLE 1 Instrument Equipment and sources thereof
Figure BDA0002990266030000061
Figure BDA0002990266030000071
In the following examples and comparative examples, the production base of Mirabilis jalapa seeds used was Gansu spring.
In the following examples and comparative examples, the particle size distribution was measured by laser diffraction method (reference standard: GB/T19077-2016 particle size analysis laser diffraction method).
Pretreatment of raw materials: washing Mirabilis jalapa seeds with water, and air drying until water content is less than 5%.
Example 1
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (controlling the water content to be less than 5%), controlling the particle size of the Mirabilis jalapa seeds to be more than 5mm by using a machine for screening, shelling by using a mechanical quick shelling machine, removing coatings by using a conventional shelling machine, then carrying out classification screening to ensure that the particle size of the Mirabilis jalapa seeds passes through a 100-mesh sieve (taking undersize materials for standby), crushing at 1 +/-1 ℃ by using a QLM03 type jet mill, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1250 meshes, enabling the Mirabilis jalapa seeds to enter a collector through a turbine along with air flow, and sterilizing by using cobalt 60 irradiation dose of 4kGy to obtain a sample of example 1.
Example 2
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (controlling the water content to be less than 5%), controlling the particle size of the Mirabilis jalapa seeds to be more than 5mm by using a machine for screening, shelling by using a mechanical quick shelling machine, removing coatings by using a conventional shelling machine, then carrying out classification screening to ensure that the particle size of the Mirabilis jalapa seeds passes through a 150-mesh sieve (taking undersize materials for standby), crushing at 1 +/-1 ℃ by using a QLM03 type jet mill, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1500 meshes, enabling the Mirabilis jalapa seeds to enter a collector through a turbine along with air flow, and sterilizing by using cobalt 60 irradiation dose of 4kGy to obtain a sample of example 2.
Example 3
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (controlling the water content to be less than 5%), controlling the particle size of the Mirabilis jalapa seeds to be more than 5mm by using a machine for screening, shelling by using a mechanical quick shelling machine, removing coatings by using a conventional shelling machine, then carrying out classified screening to ensure that the particle size of the Mirabilis jalapa seeds passes through a 200-mesh sieve (taking undersize materials for standby), crushing at 1 +/-1 ℃ by using a QLM03 type jet mill, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1600 meshes, enabling the Mirabilis jalapa seeds to enter a collector through a turbine along with air flow, and sterilizing by using cobalt 60 irradiation dose of 4kGy to obtain a sample in example 3.
Comparative example 1
The mirabilis jalapa seeds are washed and dried in advance (the water content is controlled to be less than 5%), the mirabilis jalapa seeds are screened by a machine to control the particle size of the mirabilis jalapa seeds to be more than 5mm, a mechanical quick huller is used for hulling, a conventional huller is used for hulling, then grading screening is adopted, CJ-20 traditional Chinese medicine superfine pulverizer is used for crushing for 10min at normal temperature, and cobalt 60 irradiation dose of 4kGy is used for sterilization, so that the sample of comparative example 1 is obtained.
Comparative example 2
The method comprises the steps of elutriating and airing Mirabilis jalapa seeds in advance (controlling the water content to be less than 5%), controlling the particle size of the Mirabilis jalapa seeds to be more than 5mm by machine screening, removing shells by using a mechanical quick huller, removing coatings by using a conventional huller, then crushing for 10min by using a BJ800A multifunctional crusher at normal temperature, grading layer by layer (80 meshes-100 meshes-120 meshes-150 meshes-200 meshes) and screening to obtain undersize materials, and sterilizing by adopting cobalt 60 irradiation dose of 4kGy to obtain a sample of a comparative example 2.
Comparative example 3
The method comprises the steps of elutriating and airing Mirabilis jalapa seeds in advance (controlling the water content to be less than 5%), controlling Mirabilis jalapa seed powder to be more than 5mm by using a machine for screening, shelling by using a mechanical quick huller, coating by using a conventional huller, carrying out no grading screening treatment, then crushing by using a QLM03 type jet mill at 1 +/-1 ℃, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1500 meshes, enabling the Mirabilis jalapa seed powder to enter a collector through a turbine along with air flow, and sterilizing by using cobalt 60 irradiation dose of 4kGy to obtain a sample of a comparative example 3.
Comparative example 4
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (the water content is controlled to be less than 5%), controlling the Mirabilis jalapa seed powder to be below 5mm by using a machine for screening, shelling by using a mechanical quick shelling machine, coating by using a conventional shelling machine, then carrying out grading screening to ensure that the particle size of the Mirabilis jalapa seed powder passes through a 100-mesh sieve (undersize materials are taken for standby), crushing at 1 +/-1 ℃ by using a QLM03 type jet mill, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1250 meshes, enabling the Mirabilis jalapa seed powder to enter a collector through a turbine along with air flow, and sterilizing by using cobalt 60 irradiation dose of 4kGy to obtain a sample of a comparative example 4.
Comparative example 5
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (controlling the water content to be less than 5%), controlling the Mirabilis jalapa seed powder to be more than 5mm by machine screening, shelling by using a mechanical quick shelling machine, coating by using a conventional shelling machine, then carrying out grading screening to ensure that the particle size of the Mirabilis jalapa seed powder passes through a 100-mesh sieve (taking undersize materials for standby), crushing by using a QLM03 type jet mill at 25 +/-1 ℃, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1250 meshes, enabling the Mirabilis jalapa seed powder to enter a collector through a turbine along with air flow, and sterilizing by adopting cobalt 60 irradiation dose of 4kGy to obtain a sample of a comparative example 5.
Comparative example 6
The method comprises the following steps of washing and airing Mirabilis jalapa seeds with water in advance (controlling the water content to be less than 5%), controlling the Mirabilis jalapa seed powder to be more than 5mm by machine screening, shelling by using a mechanical quick shelling machine, coating by using a conventional shelling machine, then carrying out grading screening to ensure that the particle size of the Mirabilis jalapa seed powder passes through a 120-mesh sieve (taking undersize materials for standby), crushing by using a QLM03 type jet mill at 12 +/-1 ℃, adjusting a cyclone recoverer controller to enable the powder mesh number to be 1250 meshes, enabling the Mirabilis jalapa seed powder to enter a collector through a turbine along with air flow, and sterilizing by adopting cobalt 60 irradiation dose of 4kGy to obtain a sample of comparative example 6.
COMPARATIVE EXAMPLE 7 (competitive rice starch)
Rice starch, commercial flour, manufacturer: nurture Care co, Ltd; the commodity number is: CRP-100.
The specific surface area and the particle size distribution of the mirabilis jalapa seed powder obtained in the above examples and comparative examples were evaluated by a laser particle size scatterometer, and the results are shown in table 2. The particle size distribution diagrams of the mirabilis jalapa seed powder prepared in example 1 and example 3 are respectively shown in fig. 1 and fig. 2, and the particle size distribution diagrams of the mirabilis jalapa seed powder prepared in comparative examples 1-6 are respectively shown in fig. 3-7.
TABLE 2 particle size distribution under the respective preparation processes
Figure BDA0002990266030000091
Figure BDA0002990266030000101
Note:
the specific surface area in the table is the specific surface area under unit weight;
② full distance ═ DV(90)-DV(10) Smaller value, smaller degree of dispersion, and conversely, larger degree of dispersion.
Examples of application skin care applications
Application example 1 skin-friendly Effect test
Mirabilis jalapa seed powder prepared in example 1 and comparative example 1 was applied to the skin as a cosmetic makeup powder, and the efficacy was evaluated by the skin-friendly effect, and the results are shown in fig. 8 and 9. Fig. 8 shows the result of evaluating the skin-friendly effect of mirabilis jalapa seed powder prepared according to example 1 of the present invention, where fig. 8A shows that the mirabilis jalapa seed powder before application is fine, and fig. 8B shows that the mirabilis jalapa seed powder after application is easy to apply, disperse and skin-friendly. Fig. 9 shows the results of the evaluation of the skin-friendly effect using the mirabilis jalapa seed powder prepared according to comparative example 1 of the present invention, in which fig. 9A shows that the mirabilis jalapa seed powder before application is fine, and fig. 9B shows that the mirabilis jalapa seed powder after application has floating powder and has poor skin-friendly effect.
Application example 2 oil absorption Effect test
The Mirabilis jalapa seed powders prepared in the above examples 1-3 and comparative examples 1-6 are respectively adopted, and the oil absorption amount test is performed to compare the difference effect of the Mirabilis jalapa seed powder prepared in the invention and the Mirabilis jalapa seed powder prepared in the comparative example in the aspect of oil absorption effect.
The oil absorption was measured with reference to GB/T5211.15-1988, measurement of oil absorption of pigments, and the results are shown in Table 3.
Table 3 oil absorption test results
Figure BDA0002990266030000102
Figure BDA0002990266030000111
As can be seen from Table 3, compared with the Mirabilis jalapa seed powder prepared in comparative examples 1-6, the Mirabilis jalapa seed powder prepared in the invention has a better oil absorption effect, and can exert a more effective oil control effect when applied to cosmetics. The particle size distribution D of Mirabilis jalapa seed powderV(50) And the specific surface area and the like are limited within the above range, so that the composition has unexpected technical effects in the application of skin care products, particularly in the aspects of oil control and skin feeling experience.
Application example 3 evaluation of skin feel after application
The mirabilis jalapa seed powder prepared in example 1, example 3, comparative example 1, comparative example 2 and comparative example 5 and comparative example 7 (a commercially available competitive product) were applied to the flexed side of the forearm, respectively. The number of volunteers was: 10 persons. Skin feel was evaluated subjectively. The evaluation process is as follows:
a) before testing, the bent side of the forearm is cleaned by clear water, and after the forearm is naturally dried, 6 circle marks with the diameter of 4-6cm are respectively made on the inner side of the forearm of a volunteer;
b) randomly smearing the mirabilis jalapa seed powder samples prepared in the above examples 1 and 3 and the comparative examples 1, 2 and 5 and the commercial competitive products of the comparative example 7 in circles respectively;
c) simultaneously comparing skin feeling characteristic differences of 6 samples, and sequencing according to the property intensity of each index, wherein the evaluation indexes are as follows:
indexes in smearing are as follows: spreadability, thickness, moistness;
indexes after smearing are as follows: oily gloss, soft feel, smooth feel;
d) results of ranking the 6 samples were analyzed for significant differences in sensory properties using the Friedman rank sum test. When the volunteer population was 10 at a significance level of 5%, the chi-square test cut-off was 11.07 and statistical data was performed by IBM SPSS statics 25 analysis software to analyze significance between groups of samples.
The skin feel evaluation results are shown in Table 4.
Table 4 evaluation of rank sum and significance analysis for skin feel
Figure BDA0002990266030000121
Note:
1) the F test value is more than 11.07, or the p value is less than or equal to 0.05, which indicates that the significant difference exists; on the contrary, F value is less than 11.07, or p value is more than 0.05, which indicates no significant difference;
2) the larger the data in the table, the stronger the evaluation index alone in the item.
From the results of skin feel evaluation, in combination with Friedman test analysis, it can be seen that the mirabilis jalapa seed powder prepared in the example has significant differences between the other 4 sample groups in spreading, wherein the effects of the example 3 and the example 1 are equivalent and are obviously better than those of the comparative example 1, the comparative example 7 (market competitive product), the comparative example 5 and the comparative example 2.
After the skin care product is applied, the skin care product has significant differences in oil brightness, softness and smooth feeling, and the skin care product is equivalent to the skin care product in examples 1, 3 and 7 and superior to the skin care product in comparative examples 1, 2 and 5; the effects of example 3 and example 1 are equivalent to each other in terms of conditioning the skin, namely, soft feeling and smooth feeling, and are superior to those of other comparative examples in the invention, and the difference between the groups is significant (p is less than 0.05).
The skin feel evaluation radar chart of application example 3 is shown in fig. 9. It can be seen that the particle size distribution Dv (50) and the specific surface area of the mirabilis jalapa seed powder in a specific range can enable the spreading performance of the mirabilis jalapa seed powder in smearing and the skin feeling experience in deoiling luminosity, softness and smooth feeling after smearing to be better.
The above examples are given for the purpose of illustrating the invention clearly and not for the purpose of limiting the same, and it will be apparent to those skilled in the art that, in light of the foregoing description, numerous modifications and variations can be made in the form and details of the embodiments of the invention described herein, and it is not intended to be exhaustive or to limit the invention to the precise forms disclosed.

Claims (10)

1. Mirabilis jalapa seed powder with particle size distribution satisfying Dv (50) less than or equal to 5 μm and specific surface area greater than or equal to 800m2/kg。
2. The mirabilis jalapa seed powder of claim 1, wherein the particle size distribution of the mirabilis jalapa seed powder satisfies 1 μm ≤ Dv (50) ≤ 4 μm; and/or the specific surface area of the mirabilis jalapa seed powder is 800-2500m2/kg。
3. The mirabilis jalapa seed powder of claim 1, wherein the particle size population of the mirabilis jalapa seed powder is 5-30 μm.
4. The mirabilis jalapa seed powder of claim 1 or 2, wherein the particle size distribution of the mirabilis jalapa seed powder satisfies Dv (90) of 50 μm or less.
5. A preparation method of Mirabilis jalapa seed powder comprises the following steps:
s1: providing mirabilis jalapa seeds;
s2: carrying out shelling treatment and coating removal treatment on the mirabilis jalapa seeds;
s3: carrying out grading and screening treatment on the mirabilis jalapa seed particles subjected to shelling treatment and coating removal treatment obtained in the step S2;
s4: crushing the mirabilis jalapa seed particles obtained in the step 3 after the grading and screening treatment by using an airflow crusher;
s5: and (4) screening the crushed mirabilis jalapa seed particles obtained in the step (S4) to obtain the mirabilis jalapa seed powder.
6. The method of claim 5, wherein the step S1 further comprises pre-treating the Mirabilis jalapa seeds;
the pretreatment comprises water washing and drying treatment.
7. The method according to claim 5 or 6, wherein in step S1, the average particle size of Mirabilis jalapa seeds is greater than or equal to 5 mm; and/or the Mirabilis jalapa seeds have a moisture content of < 5%.
8. The method according to claim 5, wherein in step S3, the particle size of the Mirabilis jalapa seed particles after the classifying and screening treatment is less than or equal to 100 meshes; and/or
In step S4, the jet mill is a QLM03 type jet mill; and/or the crushing treatment is low-temperature crushing treatment; the low-temperature crushing treatment temperature is 0-4 ℃.
9. The method according to claim 5, wherein in step S5, the screening process is controlled using a cyclone collector of a jet mill;
the particle mesh number of the prepared mirabilis jalapa seed powder is controlled to be 1200-2000 meshes.
10. Use of Mirabilis jalapa seed powder according to any of claims 1-4 or Mirabilis jalapa seed powder prepared according to any of claims 5-9 in the preparation of a skin care product, preferably a whitening product, a make-up product or an oil control product, such as BB cream, honey powder, loose powder or powder film.
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Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101167833A (en) * 2007-10-22 2008-04-30 南昌大学 Method for preparing raspberry superfine powder by gas phase method and solid phase method superfine crushing technology
CN101322730A (en) * 2008-07-11 2008-12-17 新疆医科大学第一附属医院 Method for processing blackcurrant seed
CN101327016A (en) * 2008-07-09 2008-12-24 清华大学 Ultramicro ginger powder and method for producing the same
CN101461852A (en) * 2007-12-21 2009-06-24 中国科学院沈阳应用生态研究所 Method for preparing super fine powder of rose
CN103816085A (en) * 2014-03-03 2014-05-28 西北大学 Mirabilis jalapa seed endosperm extract and application thereof in cosmetics
CN104490738A (en) * 2014-12-30 2015-04-08 青岛海芬海洋生物科技有限公司 Mirabilis jalapa whitening concealer
CN105380868A (en) * 2015-12-23 2016-03-09 广州聚注专利研发有限公司 Acne removal foundation make-up and preparation method thereof
CN105726367A (en) * 2016-04-12 2016-07-06 广州智媛生物科技有限公司 Foundation make-up containing natural mineral color clay and preparing method thereof
CN109200191A (en) * 2018-11-29 2019-01-15 陕西国际商贸学院 Restrain myogenic, Chinese materia medica preparation of light speckles, beautification and white and preparation method thereof
CN111011772A (en) * 2019-12-23 2020-04-17 中国热带农业科学院农产品加工研究所 Method for preparing longan superfine powder by superfine grinding

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101167833A (en) * 2007-10-22 2008-04-30 南昌大学 Method for preparing raspberry superfine powder by gas phase method and solid phase method superfine crushing technology
CN101461852A (en) * 2007-12-21 2009-06-24 中国科学院沈阳应用生态研究所 Method for preparing super fine powder of rose
CN101327016A (en) * 2008-07-09 2008-12-24 清华大学 Ultramicro ginger powder and method for producing the same
CN101322730A (en) * 2008-07-11 2008-12-17 新疆医科大学第一附属医院 Method for processing blackcurrant seed
CN103816085A (en) * 2014-03-03 2014-05-28 西北大学 Mirabilis jalapa seed endosperm extract and application thereof in cosmetics
CN104490738A (en) * 2014-12-30 2015-04-08 青岛海芬海洋生物科技有限公司 Mirabilis jalapa whitening concealer
CN105380868A (en) * 2015-12-23 2016-03-09 广州聚注专利研发有限公司 Acne removal foundation make-up and preparation method thereof
CN105726367A (en) * 2016-04-12 2016-07-06 广州智媛生物科技有限公司 Foundation make-up containing natural mineral color clay and preparing method thereof
CN109200191A (en) * 2018-11-29 2019-01-15 陕西国际商贸学院 Restrain myogenic, Chinese materia medica preparation of light speckles, beautification and white and preparation method thereof
CN111011772A (en) * 2019-12-23 2020-04-17 中国热带农业科学院农产品加工研究所 Method for preparing longan superfine powder by superfine grinding

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