CN106592282A - 一种腈纶阻染剂及其制备方法 - Google Patents

一种腈纶阻染剂及其制备方法 Download PDF

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CN106592282A
CN106592282A CN201611100927.8A CN201611100927A CN106592282A CN 106592282 A CN106592282 A CN 106592282A CN 201611100927 A CN201611100927 A CN 201611100927A CN 106592282 A CN106592282 A CN 106592282A
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曾凡跃
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Qinnan District Productivity Promotion Center Qinzhou
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/70—Material containing nitrile groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
    • D06P1/613—Polyethers without nitrogen
    • D06P1/6131—Addition products of hydroxyl groups-containing compounds with oxiranes
    • D06P1/6133—Addition products of hydroxyl groups-containing compounds with oxiranes from araliphatic or aliphatic alcohols
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491—(Thio)urea or (cyclic) derivatives
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67316—Acids
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

本发明公开了一种腈纶阻染剂及其制备方法，由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚6‑10份、硫酸3‑5份、硝酸2‑4份、脂肪伯胺5‑7份、磷酸3‑5份、盐酸4‑6份、仲胺8‑12份、叔胺1‑5份、尿素6‑8份，本发明产品环保、对人体无毒副作用，成本低廉，阻染效果极佳，适合推广应用。

Description

一种腈纶阻染剂及其制备方法
技术领域
本发明涉及衣物阻染领域，具体而言涉及一种腈纶阻染剂及其制备方法。
背景技术
腈纶具有柔软、膨松、易染、色泽鲜艳、耐光、抗菌、不怕虫蛀等优点，保暖性比羊毛高15％左右。腈纶纯纺织物采用100％的腈纶纤维制成，100％毛型腈纶纤维加工的精纺腈纶女式呢，具有松结构特征，其色泽艳丽，手感柔软有弹性，质地不松不烂，适合制作中低档女用服装。而采用100％的腈纶膨体纱为原料，可制得平纹或斜纹组织的腈纶膨体大衣呢，具有手感丰满，保暖轻松的毛型织物特征，适合制作春秋冬季大衣、便服等。因此腈纶面料已成为服装面料的重要组成部分。
腈纶阻染剂是在腈纶织物染色前对其进行阻染处理，以减少染色时活性染料沾染腈纶。传统的腈纶阻染剂，环保性能差，无法达到欧盟国家的标准；制备工艺繁杂；且很难达到阻染效果。
发明内容
本发明提供了一种腈纶阻染剂及其制备方法，本发明产品环保、对人体无毒副作用，成本低廉，阻染效果极佳，适合推广应用。
为实现上述目的，本发明提供如下技术方案：
一种腈纶阻染剂及其制备方法，由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚6-10份、硫酸3-5份、硝酸2-4份、脂肪伯胺5-7份、磷酸3-5份、盐酸4-6份、仲胺8-12份、叔胺1-5份、尿素6-8份。
进一步：由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚6份、硫酸3份、硝酸2份、脂肪伯胺5份、磷酸3份、盐酸4份、仲胺8份、叔胺1份、尿素6份。
进一步：由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚8份、硫酸4份、硝酸3份、脂肪伯胺6份、磷酸4份、盐酸5份、仲胺10份、叔胺3份、尿素7份。
进一步：由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚10份、硫酸5份、硝酸4份、脂肪伯胺7份、磷酸5份、盐酸6份、仲胺12份、叔胺5份、尿素8份。
进一步：本发明制备方法具有如下步骤：
步骤一、将配方中的乳化剂类、脂肪胺类依次加入反应釜，开搅拌转速300rpm，加入配方中总水量的50％，再加入无机酸类，尿素搅拌；
步骤二、系统缓慢升温到70-80℃后，保温反应3小时，然后降温到50℃，称取配方中余量水加入反应釜中搅拌20分钟；
步骤三、完成后静置，过滤出料既得成品。
本发明的有益效果是：
1、本发明产品环保、对人体无毒副作用；
2、成本低廉，阻染效果极佳，适合推广应用。
具体实施方式
下面将结合本发明实施例，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
实施例一：
一种腈纶阻染剂由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚6-10份、硫酸3-5份、硝酸2-4份、脂肪伯胺5-7份、磷酸3-5份、盐酸4-6份、仲胺8-12份、叔胺1-5份、尿素6-8份。
实施例二：
一种腈纶阻染剂由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚6份、硫酸3份、硝酸2份、脂肪伯胺5份、磷酸3份、盐酸4份、仲胺8份、叔胺1份、尿素6份。
实施例三：
一种腈纶阻染剂由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚8份、硫酸4份、硝酸3份、脂肪伯胺6份、磷酸4份、盐酸5份、仲胺10份、叔胺3份、尿素7份。
实施例四：
一种腈纶阻染剂由以下质量份数配方成分组成：脂肪醇聚氧乙烯醚10份、硫酸5份、硝酸4份、脂肪伯胺7份、磷酸5份、盐酸6份、仲胺12份、叔胺5份、尿素8份。
实施例五：
一种腈纶阻染剂的制备方法制备方法包括如下步骤：
步骤一、将上述材料按比例配置，并且将浓缩磷脂、淀粉糖酯、吐温、食盐、蛋白溶液混合均匀；
步骤一、将配方中的乳化剂类、脂肪胺类依次加入反应釜，开搅拌转速300rpm，加入配方中总水量的50％，再加入无机酸类，尿素搅拌；
步骤二、系统缓慢升温到70-80℃后，保温反应3小时，然后降温到50℃，称取配方中余量水加入反应釜中搅拌20分钟；
步骤三、完成后静置，过滤出料既得成品。
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。

Claims (5)

1.一种腈纶阻染剂，其特征在于：由以下质量份数配方成分组成：
脂肪醇聚氧乙烯醚6-10份、硫酸3-5份、硝酸2-4份、脂肪伯胺5-7份、磷酸3-5份、盐酸4-6份、仲胺8-12份、叔胺1-5份、尿素6-8份。
2.根据权利要求1所述的一种腈纶阻染剂，其特征在于：由以下质量份数配方成分组成：
脂肪醇聚氧乙烯醚6份、硫酸3份、硝酸2份、脂肪伯胺5份、磷酸3份、盐酸4份、仲胺8份、叔胺1份、尿素6份。
3.根据权利要求1所述的一种腈纶阻染剂，其特征在于：由以下质量份数配方成分组成：
脂肪醇聚氧乙烯醚8份、硫酸4份、硝酸3份、脂肪伯胺6份、磷酸4份、盐酸5份、仲胺10份、叔胺3份、尿素7份。
4.根据权利要求1所述的一种腈纶阻染剂，其特征在于：由以下质量份数配方成分组成：
脂肪醇聚氧乙烯醚10份、硫酸5份、硝酸4份、脂肪伯胺7份、磷酸5份、盐酸6份、仲胺12份、叔胺5份、尿素8份。
5.一种根据权利要求1所述的一种腈纶阻染剂的制备方法，其特征在于：包括如下步骤：
步骤一、将配方中的乳化剂类、脂肪胺类依次加入反应釜，开搅拌转速300rpm，加入配方中总水量的50％，再加入无机酸类，尿素搅拌；
步骤二、系统缓慢升温到70-80℃后，保温反应3小时，然后降温到50℃，称取配方中余量水加入反应釜中搅拌20分钟；
步骤三、完成后静置，过滤出料既得成品。
CN201611100927.8A 2016-12-05 2016-12-05 一种腈纶阻染剂及其制备方法 Pending CN106592282A (zh)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105887519A (zh) * 2016-04-25 2016-08-24 广州市番禺区协运来化工用品有限公司 一种腈纶阻染剂及其制备方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105887519A (zh) * 2016-04-25 2016-08-24 广州市番禺区协运来化工用品有限公司 一种腈纶阻染剂及其制备方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
《最新染料使用大全》编写组: "《最新染料使用大全》", 31 August 1996 *

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