CN106490047A - A kind of tea tree specific complex agricultural chemicals and preparation method thereof - Google Patents
A kind of tea tree specific complex agricultural chemicals and preparation method thereof Download PDFInfo
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- CN106490047A CN106490047A CN201610926307.3A CN201610926307A CN106490047A CN 106490047 A CN106490047 A CN 106490047A CN 201610926307 A CN201610926307 A CN 201610926307A CN 106490047 A CN106490047 A CN 106490047A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/30—Microbial fungi; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Health & Medical Sciences (AREA)
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- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
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- Biotechnology (AREA)
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- Natural Medicines & Medicinal Plants (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides a kind of tea tree specific complex agricultural chemicals, belongs to technical field of pesticide.A kind of tea tree specific complex agricultural chemicals, it is made up of pine needle meal, agricultural crop straw, fowl and animal excrement, bone slag, rapeseed dregs, trace element, compound amino acid, sodium selenite, humic acid, Tea Saponin and Chinese medicine composition, the Chinese medicine composition is prepared from by the raw material of following weight portion：Not 10 ~ 30 parts of 10 ~ 30 parts of Chinese honey locust, 10 ~ 30 parts of rhizoma arisaematis, flea, 10 ~ 30 parts of lilac, 5 ~ 20 parts of Chinese cassia tree, 5 ~ 20 parts of carnation, 5 ~ 20 parts of the bark of official magnolia, 5 ~ 15 parts of holy basil, 3 ~ 12 parts of cacumen biotae, 3 ~ 12 parts of the tuber of pinellia, 3 ~ 12 parts of common banana rhizome, 1 ~ 10 part of Radix Glycyrrhizae.Combination of pesticide and fertilizer of the present invention, raw material Synergistic, gained composite pesticide fertility are strong, improve crop yield, and antibacterial insecticidal effect is notable.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of tea tree specific complex agricultural chemicals and preparation method thereof.
Background technology
China region is broad, and north and south, across the torrid zone, subtropical zone, warm temperate zone, is the original producton location of tea tree in the world.Tea tree suitable
Answering property is stronger, and either high mountain or Plain can grow, but Tea Pest species is various, and fauna is complicated, has had a strong impact on tea
The production of leaf.Diseases and pests of tea tree species is a lot, according to statistics.The common disease of the tea tree recorded has kind more than 30, insect to have more than 40
Kind.The pathogen major part for causing disease for tea plant is fungi, in addition with bacterium, MLO, nematode, algae and parasitics kind
Sub- plant etc., it is insect that Pests of Tea-Plants is most of, also has mite class.Tea tree has pest and disease damage from leaf, stem, root to flowers fruit,
Wherein many with bud-leaf pest species, harm is maximum.The lighter affects tea growth. and cause tree vigo(u)r to fail.Severe one causes tealeaves to subtract
Produce, tea quality declines, diseases and pests of tea tree typically makes the tealeaves underproduction 10 ~ 20%, when occurring serious, or even can adopt without tea.And into
Tea quality decline, directly affects the tealeaves output value.The main bud-leaf disease of tealeaves has gall of tea, tea white star, tea shoot rot etc., main stem
Disease has red rust algae disease, tea branch diplostomiasis, Phomopsis theae etc., and in old tea place, common stem disease has lichens, liver moss, felt fungus etc..
Tea tree root disease mainly has root rot and tea shoot root knot nematode disease etc..Tea tree main pests species have leafhopper class (smaller green leaf hopper), mite
Class (tea orange tassel mite), inner thorn aleyrodid, cluster caterpillar, poison moth class (mainly having the black poison moth of Euproctis pseudoconspersa, tea), looper class (have paulownia looper, tea chi
Earwig), leaf rollerses (including tea olethreutid and Homona cqffearia), weevil class (based on the beautiful line weevil of tea), slug moth class, aphid decline
Moth class etc..
Biological control is the indispensable part of plant protection, for tea tree planting, refer to using biological and
Method that its product controls insect, including traditional natural enemy using and sterile insect technique, insect hormone and pheromones utilize.Raw
The shortcomings of thing preventing and treating can overcome chemical prevention to cause pest resistance to insecticide, kill natural enemy and pollute environment, is organic tea pests control
In important component part.With the development and the raising of living standards of the people of social economy, it is in integrated pest management
Status and effect more and more important, it has also become developing country's control of insect and developed country's organic foodstuff production area research
Focus.21 century, people are required to pollution-free food, the requirement more and more higher of pollution-free food, especially quality and safety of tea
Even more almost " harshness ", and during Tea Production, the threat of pest and disease damage affects the good quality and high output of tealeaves always, applies related
It is a kind of effective measures that chemical pesticide carries out preventing and treating, but a large amount of administration can cause the residual exceeded, pest resistance to insecticide of environmental pollution, agriculture again
A series of problems for affecting tealeaves sustainable developments such as enhancing, agricultural cost increase.Therefore, it is biological that diseases and pests of tea tree is actively developed
Preventing and treating, or mutually coordinate to carry out prevention and elimination of disease and pests with other prophylactico-therapeutic measures, advantageously reduce pollution of the agricultural chemicals to environment, it is ensured that tealeaves matter
Amount safety.
The patent of Application No. 201010258102 discloses a kind of special organic-inorganic compound pesticide fertilizer containing bacterium of tea tree, its
Zymotechnique is that 1. the CMS of extraction 35%, 15% offal, 20% tea grounds, 30% edible fungi leftovers uniformly mix；2. upper
State the saccharomycete dry powder of penetrating 0.1% and the 3% jelly bacillus that makes as suppression bactericide with compound bio alkali in mixture, put
Line bacterium mixed liquor, composting 168 hours；3. spray in the above-mentioned fermentation materials per 625kg 1% alum, 0.5% borax, 0.1%
Copper sulphate and the lysate of 0.3% Cosan, and urea 230kg, MAP 120kg, potassium sulfate 100kg is added, stir
Even, bank up 72 hours；4. should meet in detecting step medicine fertilizer 3. after composting：Organic matter, moisture content, nitrogen, phosphorus, potassium, effective viable bacteria
The content of the materials such as number；5. the qualified semi-finished product disc granulation by step 4., packed products after low temperature drying, screening, detection.
There is the medicine fertilizer activating soil, improvement tea root environment, suppression to kill the effect such as tea strongylid, sickle-like bacteria, to organic tea garden, without public affairs
The construction in evil tea place has important function.The patent of Application No. 201510311015 discloses a kind of tea tree fertilizer special for organic,
Component including following masses percentage：Paulownia bran 5-10%, pine bark 5-10%, Cortex Cunninghamiae Lanceolatae 5-8%, tea stalk slag 10-15%, peanut press pulp
10-15%, cake of camellia oleifera seeds 5-10%, Chinese medicine slag 10-20%, sheep excrement surplus.The invention adds Chinese medicine on the basis of pure fertilizer
Slag, the characteristics of with combination of pesticide and fertilizer, makes this fertile comprehensive nutrition, equilibrium, rationally, fully meets the nutrient demand of growth of tea plant,
While fertilising can improved soil, environmental protection, improve tealeaves yield and quality.It is biological anti-that above-mentioned technology gives us
Control the new method of diseases and pests of tea tree, medicine, fertilizer unification, these fertilizers both can be used as the supply sources of manure of tea tree nutrition, again can be with
Agricultural chemicals as antibacterial desinsection.And the realization of combination of pesticide and fertilizer effect depends on the synergy of medicine and fertilizer, although tea tree exists
The nutritional need in each stage can be grasped by us according to long-term practice operation, complexity yet with raw material and various
Property, medicine and fertilizer is carried out science group it is equipped with to realize the effect above but not a duck soup.And the medicine fertilizer conjunction despite the use of of above-mentioned technology
One theory, but it is partial to mostly the supply of nutrition, booster action is but only played to the preventing and treating of pest and disease damage, effect does not show
Write, this for valuable natural resources of Chinese medicinal materials for be undoubtedly a kind of waste.
Content of the invention
In view of this, the technical problem to be solved is to provide a kind of composite pesticide, can either be growth of tea plant
Nutrient is provided, can effectively prevent and treat tea tree common disease and pest again, preventive effect is notable, safety non-pollution.
For solving above-mentioned technical problem, the technical solution adopted in the present invention is：
A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：10 ~ 20 parts of pine needle meal, agricultural crop straw
10 ~ 20 parts, 20 ~ 30 parts of fowl and animal excrement, 5 ~ 15 parts of bone slag, 5 ~ 15 parts of rapeseed dregs, micro- 1 ~ 10 part, compound amino acid 1 ~ 10
1 ~ 10 part of part, 0.5 ~ 3 part of sodium selenite, 1 ~ 5 part of humic acid, 1 ~ 10 part of Tea Saponin and Chinese medicine composition, the Chinese medicine composition
It is prepared from by the raw material of following weight portion：10 ~ 30 parts of Chinese honey locust, 10 ~ 30 parts of rhizoma arisaematis, flea stop 10 ~ 30 parts, lilac 10 ~ 30
Part, 5 ~ 20 parts of Chinese cassia tree, 5 ~ 20 parts of carnation, 5 ~ 20 parts of the bark of official magnolia, 5 ~ 15 parts of holy basil, 3 ~ 12 parts of cacumen biotae, 3 ~ 12 parts of the tuber of pinellia, sweet
3 ~ 12 parts of any of several broadleaf plants root, 1 ~ 10 part of Radix Glycyrrhizae.
Preferably, the Chinese medicine composition is prepared from by the raw material of following weight portion：20 ~ 25 parts of Chinese honey locust, rhizoma arisaematis 20 ~
25 parts, flea stop 20 ~ 25 parts, 20 ~ 25 parts of lilac, 10 ~ 15 parts of Chinese cassia tree, 10 ~ 15 parts of carnation, 10 ~ 15 parts of the bark of official magnolia, holy basil 8 ~
12 parts, 6 ~ 8 parts of cacumen biotae, 7 ~ 10 parts of the tuber of pinellia, 7 ~ 10 parts of common banana rhizome, 7 ~ 10 parts of Radix Glycyrrhizae.
Preferably, the Chinese medicine composition is prepared from by the raw material of following weight portion：22 parts of Chinese honey locust, 25 parts of rhizoma arisaematis,
Not 25 parts of flea, 22 parts of lilac, 12 parts of Chinese cassia tree, 12 parts of carnation, 12 parts of the bark of official magnolia, 10 parts of holy basil, 7 parts of cacumen biotae, the tuber of pinellia 8
Part, 9 parts of common banana rhizome, 8 parts of Radix Glycyrrhizae.
Preferably, the tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：15 ~ 18 parts of pine needle meal,
12 ~ 15 parts of agricultural crop straw, 22 ~ 28 parts of fowl and animal excrement, 8 ~ 12 parts of bone slag, 8 ~ 12 parts of rapeseed dregs, 4 ~ 7 parts of trace element, compound
4 ~ 6 parts of 5 ~ 8 parts of amino acid, 1 ~ 2 part of sodium selenite, 2 ~ 4 parts of humic acid, 5 ~ 7 parts of Tea Saponin and Chinese medicine composition.
Preferably, the Chinese medicine composition is prepared by following methods, specifically includes following steps：
1）Weigh 10 ~ 30 parts of Chinese honey locust, 10 ~ 30 parts of the rhizoma arisaematis of weight portion respectively, mix, crush, obtain comminuting matter I；Respectively
Weigh weight portion flea stop 10 ~ 30 parts, 10 ~ 30 parts of lilac, 5 ~ 20 parts of carnation, 5 ~ 20 parts of the bark of official magnolia, 3 ~ 12 parts of the tuber of pinellia, banana
1 ~ 10 part of 3 ~ 12 parts of root and Radix Glycyrrhizae, mixing are crushed, and obtain comminuting matter II；Chinese cassia tree 5 ~ 20 part, zero mound of weight portion are weighed respectively
Fragrant 5 ~ 15 parts and 3 ~ 12 parts of cacumen biotae, mixing are crushed, and obtain comminuting matter III；
2）The comminuting matter I is added to supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row refrigerated centrifuge, removes impurity, and vacuum drying obtains extract I；
3）The water of 4 ~ 6 times of its weight is added in the comminuting matter II, is soaked 15 ~ 20 minutes, start supersonic generator, plus
Heat is kept for 45 ~ 60 minutes, filters while hot, obtain filtrate I and the dregs of a decoction to 60 ~ 70 DEG C；After I natural cooling of filtrate, by the filter
When liquid I is concentrated into 75 DEG C, relative density is 1.12 ~ 1.15 medicinal extract, adds the second that volume fraction is 75 ~ 80% in the medicinal extract
Alcoholic solution, 25 ~ 30 DEG C of temperature are kept for 18 ~ 24 hours, then filter, obtain filtrate II and sediment, the filtrate II is reduced pressure
When being concentrated into 55 DEG C, relative density is 1.20 ~ 1.25 lotion；
4）The water of 3 ~ 5 times of its weight is added in the comminuting matter III, is added in distilling flask, is distilled, control distillation
Speed oozes the drop of solution 2 ~ 3 for backflow per second, and distillation time is 40 ~ 60 minutes, and distillation is extracted 2 ~ 3 times, extract is merged and is used
Organic solvent is extracted, sub-cloud solution, and vacuum revolving instrument steams organic solvent, obtains final product product of distillation product of distillation；
5）The extract I, lotion and product of distillation are separately dried, are crushed, merged, obtain final product.
Preferably, step 2）Described in extract pressure be 35 ~ 50MPa, extraction temperature be 30 ~ 45 DEG C, CO2Fluid flow
For 30 ~ 50L/h, extraction time is 2 ~ 4h.
Preferably, step 2）Described in ethanol volume fraction be 90 ~ 95%, addition be 200 ~ 400ml.
Preferably, step 3）Described in medicinal extract and the ethanol solution w/v 1g：10~20ml.
A kind of preparation method of tea tree specific complex agricultural chemicals, comprises the following steps：
1）The pine needle meal 10 ~ 20 part of dry weight portion, agricultural crop straw 10 ~ 20 part, bone slag 5 ~ 15 part, rapeseed dregs are weighed respectively
5 ~ 15 parts and 1 ~ 10 part of Chinese medicine composition, crush, mixing；It is subsequently adding 20 ~ 30 parts of fowl and animal excrement, the humic acid 1 ~ 5 of weight portion
Part, mixing, add water wetting, adopts citric acid or lime stone to adjust pH for 6 ~ 8, and it is 35 ~ 40% to control humidity, and temperature is 55 ~ 65
DEG C, covered using plastic foil, bank up 7 ~ 10 days, obtain windrow；
2）Trace element 1 ~ 10 part, compound amino acid 1 ~ 10 part, sodium selenite 0.5 ~ 3 part and the Tea Saponin of weight portion are weighed respectively
1 ~ 10 part, with the abundant mix of the windrow, obtain final product composite pesticide.
Compared with prior art, its advantage is as follows for the present invention：
1）Present invention applicant has deeply research to tea tree planting, and based on growth of tea plant environment and rule, there is provided a kind of tea tree
Specific complex agricultural chemicals, the source of manure and botanical pesticide are assembled and making carry out furtheing investigate, mixture and research.The compound agriculture of the present invention
Medicine can promote tea tree growth of seedling as base manure, meet demand of the seedling to nutrition such as nitrogen phosphorus；As topdressing or foliage fertilizer makes
With, tea growth can be accelerated, tea quality is improved, while strengthen the resistance against diseases of tea tree and its tealeaves, reduction disease hidden danger.This
Invention composite pesticide by science compounding obtain, in practice it has proved which is not only nutritious, comprehensive, be suitable for tea tree Seedling Stage,
Growth period and its nutritional need of picking time, alternative in either phase or whole use, promote the sprouting of And Development of Tea Shoot with
Growth, improves effective component content in fresh tea leaf, improves tea leaf quality, improves tea tree anti-adversity ability, and effective disease-resisting, insecticidal shows
Writing reduces pest and disease damage occurrence probability.
2）Chinese medicine composition of the present invention is raw materials used to be natural plants source material, wide material sources, and safety and environmental protection, from root
The upper pollution problem for solving residues of pesticides in environment, plant and its soil etc..Wherein, Chinese honey locust, another name Chinese honey locust (fruit), Chinese honey locust, big soap
Pod, outstanding knife, chicken dwell son, are the ripening fruits of legume Chinese honey locust, and warm in nature, taste is pungent, salty, slightly poisonous, return lung warp, large intestine channel contain
Multiple saponin(es, saponin(e increase can respiratory tract secretion and produce phlegm-dispelling functions；Stimulating gastrointestinal mucous membrane produces diarrhoea, and corrosion stomach lining is produced
Raw absorption is poisoned；There is inhibitory action to some Gram-negative enteral pathogenic bacteria and some dermatophytes.Rhizoma arisaematis, is plant day
The dry tuber of Southern Star section rhizoma arisaematis, bitter, pungent, temperature；Poisonous, return lung, liver, the spleen channel, eliminating dampness and eliminating phlegm, expelling wind and relieving convulsion, mass dissipating and swelling eliminating.
Flea stops, and is the rhizome of liliaceous plantization Paris polyphylla, bitter, trembles with fear, and mild toxicity is clearing heat and detoxicating；Swelling and pain relieving；Cool liver is calmed the frightened.Lilac, be
The bark of Oleaceae plants lilac, bitter, cold in nature, enter stomach, liver, three warp of courage, heat-clearing, removing toxic substances, dampness removing, removing jaundice.Chinese cassia tree, is Lauraceae
The dry bark of plant Chinese cassia tree, taste is pungent, sweet, extremely hot in nature, returns kidney, spleen, the heart, Liver Channel, has mends fire supporing yang, guiding fire to origin, cold dispelling to stop
Bitterly, effect of warming meridian.Carnation, is Caryophyllaceae, Carnation perennial herb, is used as medicine with leaf.The bark of official magnolia, is Magnoliacea plant
The bark of Magnolia bilola, toil, temperature；Enter spleen, stomach, large intestine channel, middle benefit gas, lower gas, eliminating dampness, dissolving phlegm.Holy basil, is that Primulaceae is planted
The whole herb with root of thing Lysimachia foenum-graecum, gas fragrance are strong, mildly bitter flavor, with the tender thin, celadon of cauline leaf, drying, fragrance dense, without silt person be
Good.Cacumen biotae, is that cupressaceae plant arbor-vitae dries branch and leaf, cooling blood and hemostasis, preventing phlegm from forming and stopping coughing, growing and blacking hair.The tuber of pinellia, is day south
The dry tuber of the star section plant tuber of pinellia, taste is pungent are warm in nature, returns spleen, stomach, lung channel, with eliminating dampness and eliminating phlegm, stopping nausea and vomiting by lowering the adverse flow of QI, dissolving lump and resolving mass
Effect.Common banana rhizome, is the rhizome of Musaceae plant banana, sweet puckery, trembles with fear, heat-clearing, cool blood, removing toxic substances.Radix Glycyrrhizae, is that legume is sweet
The effect of dry root of grass and rhizome, with invigorating the spleen and benefiting qi, clearing heat and detoxicating, expelling phlegm and arresting coughing, relieving spasm to stop pain, coordinating the drug actions of a prescription.Above-mentioned
After raw material is compounded by science, mutual help has significantly preventing and treating effect to the pest and disease damage that the whole growth cycle of tea tree occurs
Really, good absorbing effect, does not have any harm to non-target object.
Specific embodiment
For a better understanding of the present invention, present disclosure, but this are further fairly set out with reference to embodiment
Bright protection content is not limited solely to the following examples.In the following description, give a large amount of concrete details so as to
More thorough understanding of the invention is provided.It will be apparent, however, to one skilled in the art that the present invention can be with
It is carried out without the need for one or more of these details.
Embodiment 1：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：16 parts of pine needle meal, agriculture
14 parts of crop material, 25 parts of fowl and animal excrement, 10 parts of bone slag, 10 parts of rapeseed dregs, 6 parts of trace element, 7 parts of compound amino acid, sub- selenium
5 parts of 2 parts of sour sodium, 3 parts of humic acid, 6 parts of Tea Saponin and Chinese medicine composition, original of the Chinese medicine composition by following weight portion
Material is prepared from：Not 25 parts of 22 parts of Chinese honey locust, 25 parts of rhizoma arisaematis, flea, 22 parts of lilac, 12 parts of Chinese cassia tree, 12 parts of carnation, the bark of official magnolia 12
Part, 10 parts of holy basil, 7 parts of cacumen biotae, 8 parts of the tuber of pinellia, 9 parts of common banana rhizome, 8 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper is than 0.5 ~ 1.2：0.1~0.8：0.3~1.The compound amino acid is paddy ammonia
Acid, alanine, glycine, proline and aspartic acid are with weight than 0.5 ~ 1：0.2~0.8：2~3：0.5~1.2：0.05 ~ 1.2 group
Into mixture.
In the present embodiment, the trace element is zinc, iron and copper, and the weight of the zinc, iron and copper compares 0.8：0.5：
0.6.The compound amino acid compares 0.6 for glutamic acid, alanine, glycine, proline and aspartic acid with weight：0.5：2.5：
0.7：The mixture of 0.3 composition.
In the present invention, pine needle meal is the tender or withered branch of pine tree children and needle, obtained mixing after drying, crushing
Thing.Agricultural crop straw refer to broad bean stalk, peanut straw and mung bean stalk drying, crush after mixture.Fowl and animal excrement refers to chicken
Excrement and cow dung compare 1 with weight：The mixture of 2 collocation.Bone slag, refers to these poultry bone residues of chicken bone, duck bone and frontal bone
The mixture that collects.Rapeseed dregs, is the accessory substance of rapeseed product, and contained nutrient enriches.Humic acid, is by death
Biomass are chronically formed through microorganism decomposition and inversion, although the raw materials used such as pine needle meal of the present invention, agricultural crop straw etc. are through corruption
After ripe, it is also possible to be converted to part humic acid, but content is extremely limited.Tea Saponin, is the class candy extracted by tea seed
Glucoside compound, can be obviously improved its physicochemical property for agricultural chemicals, improve effective accumulated amount of the medicament on target, be allowed to contribute to
Pesticide efficacy gives full play to.
The present embodiment Chinese medicine composition is obtained by following preparation methods, specifically includes following steps：
1）Weigh Chinese honey locust, the rhizoma arisaematis of above-mentioned weight portion respectively, mix, crush, obtain comminuting matter I；Weigh respectively above-mentioned heavy
The flea of amount part stops, lilac, carnation, the bark of official magnolia, the tuber of pinellia, common banana rhizome and Radix Glycyrrhizae, mixing crushes, and obtains comminuting matter II；Respectively
Chinese cassia tree, holy basil and the cacumen biotae of weight portion is weighed, is mixed, crushed, obtain comminuting matter III；
2）The comminuting matter I is added to supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row refrigerated centrifuge, removes impurity, and vacuum drying obtains extract I；
3）The water of 5 times of its weight is added in the comminuting matter II, is soaked 18 minutes, start supersonic generator, be heated to
65 DEG C, kept for 55 minutes, filter while hot, obtain filtrate I and the dregs of a decoction；After I natural cooling of filtrate, the filtrate I is concentrated into
When 75 DEG C, relative density is 1.13 medicinal extract, in the medicinal extract add volume fraction be 80% ethanol solution, 28 DEG C of temperature,
Kept for 20 hours, then filter, obtain filtrate II and sediment, relative density is when the filtrate II is evaporated to 55 DEG C
1.23 lotion；
4）The water of 4 times of its weight is added in the comminuting matter III, is added in distilling flask, is distilled, control distillation speed
Spending and the drop of solution 2 ~ 3 being oozed for backflow per second, distillation time is 50 minutes, and distillation is extracted 2 times, by extract merging organic solvent
Extracted, sub-cloud solution, vacuum revolving instrument steams organic solvent, obtains final product product of distillation product of distillation；
5）The extract I, lotion and product of distillation are separately dried, are crushed, merged, obtain final product.
In the present embodiment, step 2）Described in extract pressure be 40MPa, extraction temperature be 35 DEG C, CO2Fluid flow is
40L/h, extraction time are 2.5h.
In the present embodiment, step 2）Described in ethanol volume fraction be 95%, addition is 300ml.
In the present embodiment, step 3）Described in medicinal extract and the ethanol solution w/v 1g：15ml.
In the present invention, step 4）The organic solvent can be selected using dichloromethane or chloroform, similarly hereinafter.
A kind of preparation method of tea tree specific complex agricultural chemicals, comprises the following steps：
1）Weigh respectively 16 parts of the pine needle meal of dry weight portion, 14 parts of agricultural crop straw, 10 parts of bone slag, 10 parts of rapeseed dregs and in
5 parts of drug composition, crushes, mixing；25 parts of fowl and animal excrement, 3 parts of the humic acid of weight portion is subsequently adding, is mixed, add water wetting, adopts
It is 6 ~ 8 that pH is adjusted with citric acid or lime stone, and it is 35 ~ 40% to control humidity, and temperature is 55 ~ 65 DEG C, is covered using plastic foil, heap
Put 7 ~ 10 days, obtain windrow；
2）Trace element 6 part, compound amino acid 7 part, sodium selenite 2 part and the Tea Saponin 6 part of weight portion are weighed respectively, and described
The abundant mix of windrow, obtains final product composite pesticide.
The using method of tea tree specific complex agricultural chemicals of the present invention is：The root soil of tea tree is directly applied to, as tea tree
Fertilizer in Seedling Stage, growth period and/or picking time.
Embodiment 2：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：15 parts of pine needle meal, agriculture
12 parts of crop material, 22 parts of fowl and animal excrement, 8 parts of bone slag, 8 parts of rapeseed dregs, 4 parts of trace element, 5 parts of compound amino acid, selenous acid
4 parts of 1 part of sodium, 2 parts of humic acid, 5 parts of Tea Saponin and Chinese medicine composition, raw material of the Chinese medicine composition by following weight portion
It is prepared from：Not 15 parts of 15 parts of Chinese honey locust, 15 parts of rhizoma arisaematis, flea, 15 parts of lilac, 10 parts of Chinese cassia tree, 10 parts of carnation, the bark of official magnolia 10
Part, 10 parts of holy basil, 7 parts of cacumen biotae, 7 parts of the tuber of pinellia, 7 parts of common banana rhizome, 5 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 0.5：0.1：0.3.The compound amino acid is glutamic acid, alanine, sweet
Propylhomoserin, proline and aspartic acid compare 0.5 with weight：0.2：2：0.5：The mixture of 0.05 composition.
The present embodiment Chinese medicine composition is obtained by following preparation methods, specifically includes following steps：
1）Weigh Chinese honey locust, the rhizoma arisaematis of above-mentioned weight portion respectively, mix, crush, obtain comminuting matter I；Weigh respectively above-mentioned heavy
The flea of amount part stops, lilac, carnation, the bark of official magnolia, the tuber of pinellia, common banana rhizome and Radix Glycyrrhizae, mixing crushes, and obtains comminuting matter II；Respectively
Chinese cassia tree, holy basil and the cacumen biotae of weight portion is weighed, is mixed, crushed, obtain comminuting matter III；
2）The comminuting matter I is added to supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row refrigerated centrifuge, removes impurity, and vacuum drying obtains extract I；
3）The water of 4 times of its weight is added in the comminuting matter II, is soaked 15 minutes, start supersonic generator, be heated to
60 DEG C, kept for 45 minutes, filter while hot, obtain filtrate I and the dregs of a decoction；After I natural cooling of filtrate, the filtrate I is concentrated into
When 75 DEG C, relative density is 1.12 medicinal extract, in the medicinal extract add volume fraction be 75% ethanol solution, 25 DEG C of temperature,
Kept for 18 hours, then filter, obtain filtrate II and sediment, relative density is when the filtrate II is evaporated to 55 DEG C
1.20 lotion；
4）The water of 3 times of its weight is added in the comminuting matter III, is added in distilling flask, is distilled, control distillation speed
Spending and the drop of solution 2 ~ 3 being oozed for backflow per second, distillation time is 40 minutes, and distillation is extracted 3 times, by extract merging organic solvent
Extracted, sub-cloud solution, vacuum revolving instrument steams organic solvent, obtains final product product of distillation product of distillation；
5）The extract I, lotion and product of distillation are separately dried, are crushed, merged, obtain final product.
In the present embodiment, step 2）Described in extract pressure be 35MPa, extraction temperature be 45 DEG C, CO2Fluid flow is
30L/h, extraction time are 4h.
In the present embodiment, step 2）Described in ethanol volume fraction be 90%, addition is 400ml.
In the present embodiment, step 3）Described in medicinal extract and the ethanol solution w/v 1g：10ml.
A kind of preparation method of tea tree specific complex agricultural chemicals, comprises the following steps：
1）Pine needle meal 15 part, agricultural crop straw 12 part, bone slag 8 part, rapeseed dregs 8 part and the Chinese medicine of dry weight portion are weighed respectively
4 parts of composition, crushes, mixing；22 parts of fowl and animal excrement, 2 parts of the humic acid of weight portion is subsequently adding, is mixed, add water wetting, adopted
It is 6 ~ 8 that citric acid or lime stone adjust pH, and it is 35 ~ 40% to control humidity, and temperature is 55 ~ 65 DEG C, is covered using plastic foil, is banked up
7 ~ 10 days, obtain windrow；
2）Trace element 4 part, compound amino acid 5 part, sodium selenite 1 part and the Tea Saponin 5 part of weight portion are weighed respectively, and described
The abundant mix of windrow, obtains final product composite pesticide.
The using method of the tea tree specific complex agricultural chemicals is repeated no more with embodiment 1.
Embodiment 3：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：18 parts of pine needle meal, agriculture
15 parts of crop material, 28 parts of fowl and animal excrement, 12 parts of bone slag, 12 parts of rapeseed dregs, 7 parts of trace element, 8 parts of compound amino acid, sub- selenium
6 parts of 1.8 parts of sour sodium, 4 parts of humic acid, 7 parts of Tea Saponin and Chinese medicine composition, the Chinese medicine composition is by following weight portion
Raw material is prepared from：Not 13 parts of 13 parts of Chinese honey locust, 13 parts of rhizoma arisaematis, flea, 13 parts of lilac, 8 parts of Chinese cassia tree, 8 parts of carnation, the bark of official magnolia 8
Part, 8 parts of holy basil, 6 parts of cacumen biotae, 6 parts of the tuber of pinellia, 6 parts of common banana rhizome, 4 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 1.2：0.8：1.The compound amino acid is glutamic acid, alanine, sweet ammonia
Acid, proline and aspartic acid compare 1 with weight：0.8：3：1.2：The mixture of 1.2 compositions.
The present embodiment Chinese medicine composition is obtained by following preparation methods, specifically includes following steps：
1）Weigh Chinese honey locust, the rhizoma arisaematis of above-mentioned weight portion respectively, mix, crush, obtain comminuting matter I；Weigh respectively above-mentioned heavy
The flea of amount part stops, lilac, carnation, the bark of official magnolia, the tuber of pinellia, common banana rhizome and Radix Glycyrrhizae, mixing crushes, and obtains comminuting matter II；Respectively
Chinese cassia tree, holy basil and the cacumen biotae of weight portion is weighed, is mixed, crushed, obtain comminuting matter III；
2）The comminuting matter I is added to supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row refrigerated centrifuge, removes impurity, and vacuum drying obtains extract I；
3）The water of 6 times of its weight is added in the comminuting matter II, is soaked 20 minutes, start supersonic generator, be heated to
70 DEG C, kept for 60 minutes, filter while hot, obtain filtrate I and the dregs of a decoction；After I natural cooling of filtrate, the filtrate I is concentrated into
When 75 DEG C, relative density is 1.15 medicinal extract, in the medicinal extract add volume fraction be 75% ethanol solution, 30 DEG C of temperature,
Kept for 24 hours, then filter, obtain filtrate II and sediment, relative density is when the filtrate II is evaporated to 55 DEG C
1.25 lotion；
4）The water of 5 times of its weight is added in the comminuting matter III, is added in distilling flask, is distilled, control distillation speed
Spending and the drop of solution 2 ~ 3 being oozed for backflow per second, distillation time is 60 minutes, and distillation is extracted 2 times, by extract merging organic solvent
Extracted, sub-cloud solution, vacuum revolving instrument steams organic solvent, obtains final product product of distillation product of distillation；
5）The extract I, lotion and product of distillation are separately dried, are crushed, merged, obtain final product.
In the present embodiment, step 2）Described in extract pressure be 50MPa, extraction temperature be 30 DEG C, CO2Fluid flow is
50L/h, extraction time are 2h.
In the present embodiment, step 2）Described in ethanol volume fraction be 95%, addition is 200ml.
In the present embodiment, step 3）Described in medicinal extract and the ethanol solution w/v 1g：20ml.
A kind of preparation method of tea tree specific complex agricultural chemicals, comprises the following steps：
1）Weigh respectively 18 parts of the pine needle meal of dry weight portion, 15 parts of agricultural crop straw, 12 parts of bone slag, 12 parts of rapeseed dregs and in
6 parts of drug composition, crushes, mixing；20 ~ 30 parts of fowl and animal excrement, 1 ~ 5 part of the humic acid of weight portion is subsequently adding, is mixed, add water profit
Wet, adopt citric acid or lime stone to adjust pH for 6 ~ 8, it is 35 ~ 40% to control humidity, and temperature is 55 ~ 65 DEG C, is covered using plastic foil
Lid, banks up 7 ~ 10 days, obtains windrow；
2）Trace element 7 part, compound amino acid 8 part, sodium selenite 1.8 part and the Tea Saponin 7 part of weight portion are weighed respectively, with institute
The abundant mix of windrow is stated, composite pesticide is obtained final product.
The using method of the tea tree specific complex agricultural chemicals is repeated no more with embodiment 1.
Embodiment 4：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：10 parts of pine needle meal, agriculture
10 parts of crop material, 20 parts of fowl and animal excrement, 5 parts of bone slag, 5 parts of rapeseed dregs, 1 part of trace element, 1 part of compound amino acid, selenous acid
1 part of 0.5 part of sodium, 1 part of humic acid, 1 part of Tea Saponin and Chinese medicine composition, raw material system of the Chinese medicine composition by following weight portion
Standby form：18 parts of Chinese honey locust, 18 parts of rhizoma arisaematis, flea stop 18 parts, 18 parts of lilac, 12 parts of Chinese cassia tree, 12 parts of carnation, 12 parts of the bark of official magnolia,
12 parts of holy basil, 8 parts of cacumen biotae, 8 parts of the tuber of pinellia, 8 parts of common banana rhizome, 6 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 1：0.6：0.7.The compound amino acid is glutamic acid, alanine, sweet ammonia
Acid, proline and aspartic acid compare 0.6 with weight：0.4：2.3：0.6：The mixture of 0.3 composition.
Embodiment 5：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：20 parts of pine needle meal, agriculture
20 parts of crop material, 30 parts of fowl and animal excrement, 15 parts of bone slag, 15 parts of rapeseed dregs, 10 parts of trace element, 10 parts of compound amino acid, Asia
10 parts of 3 parts of sodium selenate, 5 parts of humic acid, 10 parts of Tea Saponin and Chinese medicine composition, original of the Chinese medicine composition by following weight portion
Material is prepared from：Not 20 parts of 20 parts of Chinese honey locust, 20 parts of rhizoma arisaematis, flea, 20 parts of lilac, 10 parts of Chinese cassia tree, 10 parts of carnation, the bark of official magnolia 10
Part, 8 parts of holy basil, 6 parts of cacumen biotae, 7 parts of the tuber of pinellia, 7 parts of common banana rhizome, 7 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 0.8：0.7：0.2.The compound amino acid is glutamic acid, alanine, sweet
Propylhomoserin, proline and aspartic acid compare 0.8 with weight：0.6：2.6：1.0：The mixture of 0.7 composition.
Embodiment 6：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：12 parts of pine needle meal, agriculture
12 parts of crop material, 23 parts of fowl and animal excrement, 6 parts of bone slag, 7 parts of rapeseed dregs, 3 parts of trace element, 2 parts of compound amino acid, selenous acid
2 parts of 0.8 part of sodium, 2 parts of humic acid, 3 parts of Tea Saponin and Chinese medicine composition, raw material system of the Chinese medicine composition by following weight portion
Standby form：25 parts of Chinese honey locust, 22 parts of rhizoma arisaematis, flea stop 22 parts, 25 parts of lilac, 15 parts of Chinese cassia tree, 15 parts of carnation, 15 parts of the bark of official magnolia,
12 parts of holy basil, 8 parts of cacumen biotae, 0 part of the tuber of pinellia, 10 parts of common banana rhizome, 10 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 0.7：0.3：0.6.The compound amino acid is glutamic acid, alanine, sweet
Propylhomoserin, proline and aspartic acid compare 0.7 with weight：0.4：2.7：1.0：The mixture of 0.8 composition.
Embodiment 7：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：18 parts of pine needle meal, agriculture
15 parts of crop material, 26 parts of fowl and animal excrement, 13 parts of bone slag, 12 parts of rapeseed dregs, 7 parts of trace element, 6 parts of compound amino acid, sub- selenium
6.5 parts of 2.5 parts of sour sodium, 4 parts of humic acid, 7 parts of Tea Saponin and Chinese medicine composition, original of the Chinese medicine composition by following weight portion
Material is prepared from：10 parts of Chinese honey locust, 10 parts of rhizoma arisaematis, flea stop 10 parts, 10 parts of lilac, 5 parts of Chinese cassia tree, 5 parts of carnation, 5 parts of the bark of official magnolia,
5 parts of holy basil, 3 parts of cacumen biotae, 3 parts of the tuber of pinellia, 3 parts of common banana rhizome, 1 part of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 1：0.3：0.6.The compound amino acid is glutamic acid, alanine, sweet ammonia
Acid, proline and aspartic acid compare 0.6 with weight：0.4：2.5：1：The mixture of 0.08 composition.
Embodiment 8：A kind of tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：15 parts of pine needle meal, agriculture
18 parts of crop material, 25 parts of fowl and animal excrement, 12 parts of bone slag, 14 parts of rapeseed dregs, 9 parts of trace element, 8 parts of compound amino acid, sub- selenium
8 parts of 2 parts of sour sodium, 4 parts of humic acid, 9 parts of Tea Saponin and Chinese medicine composition, raw material system of the Chinese medicine composition by following weight portion
Standby form：30 parts of Chinese honey locust, 30 parts of rhizoma arisaematis, flea stop 30 parts, 30 parts of lilac, 20 parts of Chinese cassia tree, 20 parts of carnation, 20 parts of the bark of official magnolia,
15 parts of holy basil, 12 parts of cacumen biotae, 12 parts of the tuber of pinellia, 12 parts of common banana rhizome, 10 parts of Radix Glycyrrhizae.
In the present invention, trace element and compound amino acid can be voluntarily prepared according to formula as below：The trace element is
Zinc, iron and copper, and the weight of the zinc, iron and copper compares 0.8：0.5：0.6.The compound amino acid is glutamic acid, alanine, sweet
Propylhomoserin, proline and aspartic acid compare 0.7 with weight：0.3：2.5：0.8：The mixture of 0.9 composition.
Embodiment 9：Tea tree specific complex agricultural chemicals described by the present embodiment, as different from Example 1：Also include：Micro-
3 weight portion of bacteria agent, the microbial bacterial agent are made up of 40% Trichoderma harzianum of mass percent and 60% beauveria bassiana.
Trichoderma harzianum, Trichoderma harzianum, pulvis, living bacteria count >=200,000,000 cfu/g；Beauveria bassiana,
Streptomyces microflavus, pulvis, living bacteria count >=20,000,000,000 cfu/g.Above-mentioned microbial inoculum can be obtained by market purchase
Obtain or voluntarily culture is obtained.
Embodiment 10：Tea tree specific complex agricultural chemicals described by the present embodiment, with embodiment 1 except that：Also include：
4 weight portion of microbial bacterial agent, the microbial bacterial agent are made up of 50% Trichoderma harzianum of mass percent and 50% beauveria bassiana.
Comparative example 1：Tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：16 parts of pine needle meal, crops
14 parts of stalk, 25 parts of fowl and animal excrement, 10 parts of bone slag, 10 parts of rapeseed dregs, 6 parts of trace element, 7 parts of compound amino acid, sodium selenite 2
Part, 3 parts of humic acid, 6 parts of Tea Saponin.Preparation method refers to embodiment 1.
Comparative example 2：Tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：22 parts of Chinese honey locust, rhizoma arisaematis 25
Part, not 25 parts of flea, 22 parts of lilac, 12 parts of Chinese cassia tree, 12 parts of carnation, 12 parts of the bark of official magnolia, 10 parts of holy basil, 7 parts of cacumen biotae, the tuber of pinellia
8 parts, 9 parts of common banana rhizome, 8 parts of Radix Glycyrrhizae.Preparation method refers to embodiment 1.
Comparative example 3：Tea tree specific complex agricultural chemicals, is prepared from by the raw material of following weight portion：16 parts of pine needle meal, crops
14 parts of stalk, 25 parts of fowl and animal excrement, 10 parts of bone slag, 10 parts of rapeseed dregs, 6 parts of trace element, 7 parts of compound amino acid, sodium selenite 2
Part, 3 parts of humic acid, 6 parts of Tea Saponin, 22 parts of Chinese honey locust.Preparation method refers to embodiment 1.
Field test effect
Reagent agent：
Experimental group：A1~A6：It is followed successively by the agricultural chemicals of the preparation of embodiment 1 ~ 4,9 ~ 10；
Control group：B1~B35：It is followed successively by the agricultural chemicals of the preparation of comparative example 1 ~ 3；
B0：Non- dispenser.
The tea place age of tree is 10 years, 10 process of experimental design, often processes and is repeated 3 times, altogether 30 cells, and each cell is
30, random alignment.
Fertilising is carried out in 10 days 2 months, April 15, July 10 and September respectively on the 15th, is applied fertilizer 4 times altogether, and each cell is applied
Reagent agent 60kg.
1st, resultant effect
Cured leaf yield to experimental group A1 ~ A6, control group B1 ~ planted tea trees of B3 and B0（Kg/ mus）, main diseases and insect pests species,
Pest and disease damage probability of happening（%）Counted, objects of statistics is the tea tree in 30 cells 36 of same period plantation, and statistics is such as
Shown in table 1.
1 composite pesticide of table is counted to the effect of apple cultivation
Can be seen by table 1, apply the product that experimental group A1 ~ A6 of the present invention and control group B1 ~ B3 agricultural chemicals can improve per mu yield tealeaves
Amount, while compared with control group B0, experimental group A1 ~ A6 can improve cured leaf yield 42.2 ~ 60.9%, control group B1 can improve cured leaf
Yield 23.0%, control group B2 can improve cured leaf yield 18.0%, and control group B3 can improve cured leaf yield 31.3%.For experimental group
Effect of increasing production for, A5 ＞ A6 ＞ A1 ＞ A2 ＞ A3 ＞ A4；For the effect of increasing production of control group, B3 ＞ B1 ＞ B2.On
Data display is stated, agricultural chemicals of the present invention obtains good synergy, and significantly, volume increase is projected fertilizer efficiency.
The agricultural chemicals for applying experimental group A1 ~ A6 and control group B2 of the present invention can obviously reduce the probability of happening of main diseases and insect pests,
It is without substantially ill.Compared with control group B0, it is 92.3 ~ 97.0% that experimental group A1 ~ A6 can reduce pest and disease damage incidence, control
It is 21.7% that group B1 can reduce pest and disease damage incidence, and it is 79.3% that control group B2 can reduce pest and disease damage incidence, and control group B3 can drop
Low pest and disease damage incidence is 48.9%.For the pest and disease damage incidence of experimental group, A5 ＜ A6 ＜ A1 ＜ A2 ＜ A3 ＜ A4；Right
For the pest and disease damage incidence of control group, B1 ＞ B3 ＞ B2.There is data phase with disease in the yield of experimental group and control group
Compare and can draw, tea yield, explanation can be significantly improved using agricultural chemicals of the present invention while disease probability of happening is reduced
The occupation mode of combination of pesticide and fertilizer of the present invention can significantly increase the diseases and insect pests resistance of tealeaves, can dramatically increase yield again, overall
Effect is significant.
2nd, the effect of anti-leaf roller
Each point insect population is investigated before dispenser, every 3 days after 10 days 2 months, April 15, the dispenser on the 15th of July 10 and September, respectively
The population number of investigation each point, every time investigation in the morning 5：30——8：30 are carried out.The not dry front investigation of dew in the morning, per cell
50 bud tips (1 bud, 3,4 leaf) of investigation, record its insect population number.Count each cell population number, calculate each process Revision insect recluced rate and
Prevention effect, to correct Revision insect recluced rate as prevention effect, the results are shown in Table 2, and carries out significance of difference test, and formula is such as
Under：
Revision insect recluced rate (%)=[(population number after the process of before processing insect population one)/before processing insect population] × 100%；
Prevention effect (%)=[(one check plot Revision insect recluced rate for the treatment of region Revision insect recluced rate)/(1- check plots Revision insect recluced rate)] ×
100%.
The field control effect of 2 leaf roller of table
Can be seen by table 2, compared with control group B0, experimental group A1 ~ A6 is excellent to the prevention effect of leaf roller, in whole tea tree
Growth cycle in apply 4 times, the quantity of leaf roller has different degrees of decline every time.In experimental group, the preventive effect of A5 is best,
When applying first time, preventive effect reaches 93.5%, and increasing with application times, and preventive effect gradually increases, until it reaches 100%
Preventive effect.Compared with A5, the preventive effect of experimental group A1 slightly shows weak, illustrates the addition of microbial bacterial agent to improving agricultural chemicals of the present invention to leaf roll
The preventive effect of moth is beneficial, can be preferably.Control group B1 ~ B3 also has different degrees of preventive effect, but substantially low, especially
B1 increases with application times, and preventive effect but there occurs decline, illustrates B1 to leaf roller substantially without prevention effect.By Chinese honey locust and B1
After being used in mixed way, preventive effect is improved, but still the effect less than control group B2.The above results show that agricultural chemicals of the present invention can
To be particularly the preventing and treating agricultural chemicals of leaf roller as tea-plant pests
3rd, disease resistance effect
Every 6 days respectively in 50 young leaves of each cell random searching before dispenser, after September reagent on the 15th, by grade scale range estimation point
Level, record investigation result, and relative prevention effect is calculated according to disease index, the results are shown in Table 3；
With respect to prevention effect/%=（Control disease index-process disease index）/ control disease index × 100.
3 disease-controlling effect of table
As can be seen from Table 3, agricultural chemicals of the present invention has obvious prevention effect to tea zonate spot, the red leaf disease of tea and dark brown pinta,
Especially the prevention effect of dark brown pinta is more preferable.And control group B1 is very low to the prevention effect of above-mentioned disease, B2 is to above-mentioned disease
Preventive effect substantially good compared with B1, but still significantly lower than experimental group preventive effect.B3 increases compared with B1 to the resistance of above-mentioned disease,
But still it is less than 25%, hence it is evident that on the weak side.The medicine of above-mentioned as shown by data agricultural chemicals of the present invention, fertile Synergistic, improve jointly tea tree from
Resistivity of the body to disease so that preventive effect is significantly increased.
Although the foregoing describing the specific embodiment of the present invention, those familiar with the art should manage
Solution, the specific embodiment described by us are merely exemplary, rather than for the restriction to the scope of the present invention, are familiar with this
Equivalent modification and change that the technical staff in field is made in the spirit according to the present invention, should all cover the present invention's
In scope of the claimed protection.
Claims (9)
1. a kind of tea tree specific complex agricultural chemicals, it is characterised in that：It is prepared from by the raw material of following weight portion：Pine needle meal 10 ~ 20
Part, 10 ~ 20 parts of agricultural crop straw, 20 ~ 30 parts of fowl and animal excrement, 5 ~ 15 parts of bone slag, 5 ~ 15 parts of rapeseed dregs, trace element 1 ~ 10 part,
1 ~ 10 part of 1 ~ 10 part of compound amino acid, 0.5 ~ 3 part of sodium selenite, 1 ~ 5 part of humic acid, 1 ~ 10 part of Tea Saponin and Chinese medicine composition,
The Chinese medicine composition is prepared from by the raw material of following weight portion：10 ~ 30 parts of Chinese honey locust, 10 ~ 30 parts of rhizoma arisaematis, flea stop 10 ~ 30
Part, 10 ~ 30 parts of lilac, 5 ~ 20 parts of Chinese cassia tree, 5 ~ 20 parts of carnation, 5 ~ 20 parts of the bark of official magnolia, 5 ~ 15 parts of holy basil, cacumen biotae 3 ~ 12
Part, 3 ~ 12 parts of the tuber of pinellia, 3 ~ 12 parts of common banana rhizome, 1 ~ 10 part of Radix Glycyrrhizae.
2. tea tree specific complex agricultural chemicals as claimed in claim 1, it is characterised in that：The Chinese medicine composition is by following weight portion
Raw material be prepared from：Not 20 ~ 25 parts of 20 ~ 25 parts of Chinese honey locust, 20 ~ 25 parts of rhizoma arisaematis, flea, 20 ~ 25 parts of lilac, Chinese cassia tree 10 ~ 15
Part, 10 ~ 15 parts of carnation, 10 ~ 15 parts of the bark of official magnolia, 8 ~ 12 parts of holy basil, 6 ~ 8 parts of cacumen biotae, 7 ~ 10 parts of the tuber of pinellia, common banana rhizome 7 ~ 10
Part, 7 ~ 10 parts of Radix Glycyrrhizae.
3. tea tree specific complex agricultural chemicals as claimed in claim 2, it is characterised in that：The Chinese medicine composition is by following weight portion
Raw material be prepared from：Not 25 parts of 22 parts of Chinese honey locust, 25 parts of rhizoma arisaematis, flea, 22 parts of lilac, 12 parts of Chinese cassia tree, 12 parts of carnation, thickness
12 parts of Piao, 10 parts of holy basil, 7 parts of cacumen biotae, 8 parts of the tuber of pinellia, 9 parts of common banana rhizome, 8 parts of Radix Glycyrrhizae.
4. the tea tree specific complex agricultural chemicals as described in any one of claim 1 ~ 3, it is characterised in that：Raw material by following weight portion
It is prepared from：15 ~ 18 parts of pine needle meal, 12 ~ 15 parts of agricultural crop straw, 22 ~ 28 parts of fowl and animal excrement, 8 ~ 12 parts of bone slag, rapeseed dregs 8 ~
12 parts, 4 ~ 7 parts of trace element, 5 ~ 8 parts of compound amino acid, 1 ~ 2 part of sodium selenite, 2 ~ 4 parts of humic acid, 5 ~ 7 parts of Tea Saponin and in
4 ~ 6 parts of drug composition.
5. tea tree specific complex agricultural chemicals as claimed in claim 4, it is characterised in that：The Chinese medicine composition is by following methods
Prepare, specifically include following steps：
1）Weigh 10 ~ 30 parts of Chinese honey locust, 10 ~ 30 parts of the rhizoma arisaematis of weight portion respectively, mix, crush, obtain comminuting matter I；Respectively
Weigh weight portion flea stop 10 ~ 30 parts, 10 ~ 30 parts of lilac, 5 ~ 20 parts of carnation, 5 ~ 20 parts of the bark of official magnolia, 3 ~ 12 parts of the tuber of pinellia, banana
1 ~ 10 part of 3 ~ 12 parts of root and Radix Glycyrrhizae, mixing are crushed, and obtain comminuting matter II；Chinese cassia tree 5 ~ 20 part, zero mound of weight portion are weighed respectively
Fragrant 5 ~ 15 parts and 3 ~ 12 parts of cacumen biotae, mixing are crushed, and obtain comminuting matter III；
2）The comminuting matter I is added to supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is carried out
Refrigerated centrifuge, removes impurity, and vacuum drying obtains extract I；
3）The water of 4 ~ 6 times of its weight is added in the comminuting matter II, is soaked 15 ~ 20 minutes, start supersonic generator, plus
Heat is kept for 45 ~ 60 minutes, filters while hot, obtain filtrate I and the dregs of a decoction to 60 ~ 70 DEG C；After I natural cooling of filtrate, by the filter
When liquid I is concentrated into 75 DEG C, relative density is 1.12 ~ 1.15 medicinal extract, adds the second that volume fraction is 75 ~ 80% in the medicinal extract
Alcoholic solution, 25 ~ 30 DEG C of temperature are kept for 18 ~ 24 hours, then filter, obtain filtrate II and sediment, the filtrate II is reduced pressure
When being concentrated into 55 DEG C, relative density is 1.20 ~ 1.25 lotion；
4）The water of 3 ~ 5 times of its weight is added in the comminuting matter III, is added in distilling flask, is distilled, control distillation
Speed oozes the drop of solution 2 ~ 3 for backflow per second, and distillation time is 40 ~ 60 minutes, and distillation is extracted 2 ~ 3 times, extract is merged and is used
Organic solvent is extracted, sub-cloud solution, and vacuum revolving instrument steams organic solvent, obtains final product product of distillation product of distillation；
5）The extract I, lotion and product of distillation are separately dried, are crushed, merged, obtain final product.
6. tea tree specific complex agricultural chemicals as claimed in claim 5, it is characterised in that：Step 2）Described in extract pressure be 35
~ 50MPa, extraction temperature are 30 ~ 45 DEG C, CO2Fluid flow is 30 ~ 50L/h, and extraction time is 2 ~ 4h.
7. tea tree specific complex agricultural chemicals as claimed in claim 6, it is characterised in that：Step 2）Described in ethanol volume fraction
For 90 ~ 95%, addition is 200 ~ 400ml.
8. tea tree specific complex agricultural chemicals as claimed in claim 5, it is characterised in that：Step 3）Described in medicinal extract and the ethanol
The w/v 1g of solution：10~20ml.
9. a kind of preparation method of tea tree specific complex agricultural chemicals, comprises the following steps：
1）The pine needle meal 10 ~ 20 part of dry weight portion, agricultural crop straw 10 ~ 20 part, bone slag 5 ~ 15 part, rapeseed dregs are weighed respectively
5 ~ 15 parts and 1 ~ 10 part of Chinese medicine composition, crush, mixing；It is subsequently adding 20 ~ 30 parts of fowl and animal excrement, the humic acid 1 ~ 5 of weight portion
Part, mixing, add water wetting, adopts citric acid or lime stone to adjust pH for 6 ~ 8, and it is 35 ~ 40% to control humidity, and temperature is 55 ~ 65
DEG C, covered using plastic foil, bank up 7 ~ 10 days, obtain windrow；
2）Trace element 1 ~ 10 part, compound amino acid 1 ~ 10 part, sodium selenite 0.5 ~ 3 part and the Tea Saponin of weight portion are weighed respectively
1 ~ 10 part, with the abundant mix of the windrow, obtain final product composite pesticide.
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| CN110432267A (en) * | 2019-08-22 | 2019-11-12 | 西南大学 | A kind of auxiliary agent for preventing and treating tetranychid |
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