CN106278542A - A kind of Passifolra edulis Biological pesticidal organic fertilizer material - Google Patents
A kind of Passifolra edulis Biological pesticidal organic fertilizer material Download PDFInfo
- Publication number
- CN106278542A CN106278542A CN201610596225.7A CN201610596225A CN106278542A CN 106278542 A CN106278542 A CN 106278542A CN 201610596225 A CN201610596225 A CN 201610596225A CN 106278542 A CN106278542 A CN 106278542A
- Authority
- CN
- China
- Prior art keywords
- passifolra edulis
- parts
- organic fertilizer
- biological
- fertilizer material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
Abstract
The invention discloses a kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: sheep stool 75 100 parts, chicken manure 75 100 parts, 75 100 parts of duck excrement, 20 30 parts of waste residue, 10 20 parts of Pomacea canaliculata powder, biological bacteria 48 parts, trace element 26 parts, water-retaining agent 26 parts, dispersant 26 parts, conditioner 26 parts.The Passifolra edulis Biological pesticidal organic fertilizer material of the present invention can not only preventing disease and pest effectively, and can be balanced nutritious, improve soil environment, promote that Passifolra edulis is quickly grown up healthy and sound, shorten growth cycle, improve Passifolra edulis yield, reduce production cost.
Description
[technical field]
The invention belongs to fertilizer preparing technical field, be specifically related to a kind of Passifolra edulis Biological pesticidal organic fertilizer material.
[background technology]
China is a large agricultural country, and pesticide and chemical fertilizer play highly important effect in agricultural production, along with people
Living standard and the raising of health perception, people pay much attention to the safety of agricultural product, to nuisanceless, the need of pollution-free food
Ask and increase year by year.
Cultural control pest and disease damage and Passifolra edulis institute to fertilize, mainly stir with chemicals and toxic pesticides are blended at present
Mix, in being manured into soil or on Passifolra edulis, life-time service year in year out, substantial amounts of pesticide and chemical fertilizer, cause insect to produce drug resistance
Property, soil compaction, water source soil is polluted, Passifolra edulis Quality Down, pesticide residues exceed standard and have a strong impact on the body and mind of people
Health and the Passifolra edulis competitiveness in market.Therefore the Passifolra edulis fertilizer developing a kind of Biocidal type is development trend.
[summary of the invention]
The present invention provides a kind of Passifolra edulis Biological pesticidal organic fertilizer material, to solve substantial amounts of pesticide and fertilizer application, causes
Insect produces drug resistance, soil compaction, water source soil pollution, Passifolra edulis Quality Down, and pesticide residues exceed standard serious and cause food
Product security problems.The Passifolra edulis Biological pesticidal organic fertilizer material of the present invention can not only preventing disease and pest effectively, and battalion can be equalized
Support, improve soil environment, promote that Passifolra edulis is quickly grown up healthy and sound, shorten growth cycle, improve Passifolra edulis yield, reduce and produce into
This.
For solve above technical problem, the present invention by the following technical solutions:
A kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: include following raw material:
Sheep stool 75-100 part, chicken manure 75-100 part, duck excrement 75-100 part, waste residue 20-30 part, Pomacea canaliculata powder 10-20 part, biological bacteria 4-8
Part, trace element 2-6 part, water-retaining agent 2-6 part, dispersant 2-6 part, conditioner 2-6 part；
Described waste residue include marc, bagasse, edible fungi residues, sugar slag, acid-sludge, fecula, manioc waste, citric acid waste,
One or more in soy sauce residues, residue of monosodium glutamate, Glycine max (L.) Merr.；
Described biological bacteria includes that nitrogen-fixing bacteria, brood cell liver bacterium, enzymatic microorganism, yeast, actinomycetes, root nodule bacteria, phosphobacteria, potassium are thin
One or more in bacterium, phosphate solubilizing bacteria；
Described trace element includes one or more in ferrum, boron, manganese, copper, zinc, molybdenum；
Described water-retaining agent include polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch-grafted third
One or more in olefin(e) acid sodium；
Described dispersant include the one in polyethylene glycol oxide, polyurethane, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium, PTPP (potassium tripolyphosphate) or
Multiple；
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 70-80 DEG C and carries out
Evaporation and concentration, being concentrated into pH value is 2.5-3.5, stops heating, left at room temperature activation 13-15h, is subsequently adding ammonium carbonate regulation
PH value is to 6.2-7.6, it is thus achieved that humic acid solution, is dried humic acid solution to water content≤6%, mistake after pulverizing at 85-105 DEG C
100-300 mesh sieve, prepares humic acids；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., the Qin
Skin, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera co-grinding,
Extract medicinal liquid in ultrasonic assistant ethanol extraction FAXIA, gained medical filtration, be concentrated into after water content≤20% to obtain mixture A,
Gained mixture A is dried to water content≤6% at 90-100 DEG C, crosses 100-300 mesh sieve, prepare Insecticidal combinations after pulverizing
Thing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, mildew-resistant
Agent and distilled water, mix homogeneously obtains mixture B, carries out making 1.5-2.5mm granule and at 90-100 DEG C by described mixture B
It is dried to water content≤6%, prepares conditioner.
Further, Cacumen Platycladi described in step S2, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L,
Dioscorea zingiberensis, Aloe, Azadirachta Indica A., Cortex Fraxini, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L.,
Leaf of Pterocarya Stenoptera, with weight portion for unit 35:35:35:35:35:35:25:25:25:20:20:20:16:16:16:12:12:12:
9:9 ratio forms.
Further, the condition of the extraction of ultrasonic assistant ethanol extraction method described in step S2 medicinal liquid is: solid-liquid ratio is 1:
12-16, ultrasonic power is 160-180W, and concentration of alcohol is 60%-80%, and Extracting temperature is 60-70 DEG C, and extraction time is
40-60min。
Further, described solid-liquid ratio is 1:15, and ultrasonic power is 170W, and concentration of alcohol is 75%, and Extracting temperature is
70 DEG C, extraction time is 40min.
Further, soil conditioner described in step S3 includes following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata
Powder.
Further, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder press 10-30:10-20 in units of weight portion:
10-15:4-6 ratio forms.
Further, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder press 30:20:12:5 ratio in units of weight portion
Example forms.
Further, one or both during antifungus agent described in step S3 includes quinoxyfen, triazolone.
Further, step S1 described in step S3 prepare humic acids, step S2 prepare Pesticidal combination, soil adjust
Manage agent, antifungus agent and distilled water in units of weight portion in 30-45:0.04-0.05:35-50:0.06-0.1:8-10 ratio group
Become.
Further, Pesticidal combination that described step S1 prepares humic acids, step S2 prepare, soil conditioner, anti-
Mould dose is formed in 35:0.04:40:0.06:9 ratio in units of weight portion with distilled water.
Containing numerous nutritional labelings in waste residue, it is possible to provide plant growing to need as Passifolra edulis Biological pesticidal organic fertilizer material
The nutrition asked, promotes plant growing.
Pomacea canaliculata is individual greatly, feeding habits are wide, strong adaptability, growth and breeding are fast, yield is high, low price, and Pomacea canaliculata powder contains
Rich in protein, carotene, multivitamin and mineral, the aminoacid that its breaks down proteins becomes can promote root growth,
Strong sprout, healthy tree, the photosynthetic function of enhancing blade and crop degeneration-resistant.
The Passifolra edulis Biological pesticidal organic fertilizer material that biological bacteria is made has the function of volume increase, improving quality, also has and significantly subtracts
Nitrate in few plant, nitrite and content of beary metal, improve the effect such as chemical fertilizer utilization ratio and fertilizing soil.
Boron compares in plant and concentrates in stem apex, the tip of a root, blade and floral organ, and the content in dicotyledon is usually
Higher than monocotyledon.Boron can improve the nitrogenase activity of legume root nodule bacteria, increases amount of nitrogen fixation, and during boron deficiency, root stays not to be sent out
Reach, affect amount of nitrogen fixation.Boron can also strengthen crop anti-adversity.
Ferrum is that chlorophyll formation is indispensable, is difficult to transfer in plant body, lacks so blade " chlorosis " is plant
The performance of ferrum, and first this chlorosis show on young leaflet tablet.
Copper participates in the photosynthesis of plant, Repiration, nitrogen metabolism, the resistance of enhancing plant.When lacking copper, plant strain growth is thin
Weak, young leaves turns to be yellow, wilting withered, and blade tip curling is turned white, and has necrotic spot.
Zinc can promote that crop carries out photosynthesis, and it is the constituent of multiple enzyme, and during zinc deficiency, crop growth occurs
Stagnate.
Containing manganese in plant chloroplast, manganese can promote germination and seedling growth in period, affects the light of crop during manganese deficiency
Cooperation use, Repiration, nitrate nitrogen accumulation in vivo.Show as chlorosis yellow between blade arteries and veins, have brown speckle.
Molybdenum is nitrogen-fixing microorganism, particularly fixes during air nitrogen necessary with the root nodule bacteria of legume symbiosis.With
Time can promote again leaf photosynthesis intensity.When lacking molybdenum, plant is short and small, and chlorosis between blade arteries and veins, leaf margin is dried-up, inward curl, and one-tenth withers
Listless state.
Water-retaining agent can strengthen soil water-retaining performance, improvement Soil structure, reduce the deep percolation of water and loss of soil nutrient,
Improve efficiency of water application.
Polyethylene glycol oxide is water-wet side, can be combined with Passifolra edulis Biological pesticidal organic fertilizer material particle, soluble polyurethane tree
Fat has good resistance to water, and its strand well can stretch in water, is arranged in interface uniformly, increases space bit
Resistance, makes Passifolra edulis Biological pesticidal organic fertilizer material particle be quickly dispersed in water；Water soluble polyurethane resin has wettability simultaneously
Can, it is possible to make hydrone quickly immerse Passifolra edulis Biological pesticidal organic fertilizer material particle, promote Passifolra edulis Biological pesticidal organic fertilizer material
Dissolving.Di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium, PTPP (potassium tripolyphosphate) is water solublity, and has dispersibility, and PTPP (potassium tripolyphosphate) is water solublity
Inorganic dispersant, its dispersive property is excellent, can reduce the viscous of Passifolra edulis Biological pesticidal organic fertilizer material particle and high molecular polymer
Degree, can make Passifolra edulis Biological pesticidal organic fertilizer material particle be quickly dispersed in water, high molecular polymer also can be made to play it simultaneously
Dispersibility.
The humic acids utilizing vinegar factory waste liquid to make contains the strong of substantial amounts of organic matter and beneficial element, beneficially crops
Kang Chengchang, shortens growth cycle.
Antifungus agent, refers to prevent microorganism from causing mouldy medicament, has the strongest suppression to antibacterial, fungus, kills
Effect.
Containing volatile oil, flavone, tannic acid and tannin class phenolic constituent in Cacumen Platycladi, have antiinflammatory, antioxidation, hemostasis,
Antibacterial parasite killing etc. act on.
Herba Menthae has the effects such as parasite killing, antibacterial, sterilization, antiinflammatory, has stronger to dysentery bacterium, Bacillus typhi and escherichia coli
Inhibitory action.
Caulis et Folium Lactucae sativae profit the five internal organs, qualcomm meridian, diuresis, improving eyesight sharps teeth, promoting lactation, hard muscles and bones, has the effect of antibacterial parasite killing.
Herba Anabasis aphyllae belongs to chenopod, for dicotyledon, has heat-clearing and toxic substances removing, anti-inflammation, pain relieving parasite killing etc. and makees
With, can be used for rural area preparation pesticide of eliminating the four pests--rats, bedbugs, flies and mosquitoes, disinfestation and deratization is used.
Folium paulowniae extract has antibacterial and antivirus action, and propanol extraction thing all has antibacterial activity, In vitro Bactericidal Experiments
Proving, Folium paulowniae extract is relatively strong to staphylococcus aureus, bacillus subtilis effect, and extract panlownin and sesamin, these are two years old
Pyrethrin and allyl cinerin are killed insecticide (fly, mosquito etc.) effect by composition potentiation.
The total alkaloid of sophora alopecuroide extracted in Herba Sophorae alopecuroidis have antiinflammatory, anticancer, antiallergic action, anti-arrhythmia, antiulcer,
Leukocyte increasing, relieving asthma, antipyretic, parasite killing, calmness, analgesia, the effect such as antiviral；Herba Sophorae alopecuroidis powder external is to staphylococcus, big
Enterobacteria, streptococcus, fungus, bacterium protein of Gardnerella vaginalis and infusorian have suppression or killing action；The killing ability of Herba Sophorae alopecuroidis plant between
Between anabasine (Anadasine) and lupinine (Lupinine), eulexine is Biocidal agriculture the effective elements of the medicine.
Artemisia absinihium L bitter in the mouth, cold in nature, poisonous, there is heat clearing and damp drying, drive the effects such as ascarid, stomach invigorating, antibacterial parasite killing, to multiple coccus,
Bacillus, fungus and virus etc. all have suppression and killing action.
Dioscorea zingiberensis extract multiple grain storage pest, desert locusts and mythimna separata etc. are shown certain repellent, fumigate, tag,
Stomach toxicity, growth inhibited or oviposition deterrence isoreactivity；Meanwhile, some agricultural pathogenic bacterias had the strongest bactericidal action.
Aloe contains lignin, aloietic acid, Saponin, anthraquinone, aloin, vitamin, oxidase, lipase, amylase, relies ammonia
The multiple nutritional components such as acid, leucine, threonine, isoleucine, phenylalanine, valine.Extract component Aloe in Aloe
Tincture is the material that antibiotic property is the strongest, can kill the pathogenic bacterias such as fungus, mycete, antibacterial, virus, and the growth of suppression and eliminating pathogen is numerous
Growing, the pathogenic bacteria class of aloe antibiotic sterilization has: diphtheria bacterium, tetanolysin, pulmonitis strain, lactic acid bacteria, dysentery bacillus, coliform, Bubonic plague
The diseases such as bacterium, cholera bacteria and initiation otitis media, cystitis, pyesis, measles, rabies, poliomyelitis, epidemic encephalitis
Pathogenic bacteria.
Azadirachta Indica A. belongs to Meliaceae, comes from Southeast Asia, containing Azadirachta Indica A., solannin etc., has good disinsection efficiency, insect
Once contacting, growth will be suppressed.
Cortex Fraxini has antibacterial insecticidal action, to staphylococcus aureus, bacillus subtilis, escherichia coli, beer yeast,
Bacterium wine yeast etc. has obvious inhibitory action, is usually used in controlling bacillary dysentery clinically, enteritis, leucorrhea, chronic gas
Guan Yan, conjunctival congestion and swelling pain etc..
Radix Sophorae Flavescentis belongs to herbaceos perennial；It is taken as Radix Aconiti and the succedaneum of Radix Aconiti Kusnezoffii to use at the Northwest's Radix Sophorae Flavescentis, with
The traditional medicine of the ethnic groups such as Shi Yeshi Kazak, the Hui ethnic group, is mainly used in pain relieving, dehumidifying, cold-dispelling.
Roots of Euphorbia soongarica is herbaceos perennial, main product in Gansu, the ground such as Xinjiang and Russia, in new thick area conduct
The succedaneum of the Radix Euphorbiae Pekinensis uses, and has effect of removing fluid-retention by purgation, dispersing swelling and dissipating binds.
The extract of leaf of tea tree has potent bactericidal action, and Camellia sinensis can effectively tackle for various fungal infections, can
Kill staphylococcus aureus, diphtheria corynebacterium.
Flos Daturae is botanical pesticide, has extremely strong sterilization, insecticidal action.
Pyrethrum contains 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, deinsectization
Chrysanthemum has toxic action to various insects such as mosquito, fly, Cimex bedbug and Blatta seu periplaneta etc..
Fructus Capsici can alleviate chest and abdomen cold type of pain, prevents dysentery, kills and press down stomach abdomen entozoa, controls heart disease and coronary artery is hard
Change, there is sterilization, anticorrosion, seasoning, nutrition, the function such as dispel cold.
Sabadilla is Melanthiaceae perennial plant, and extract has insecticidal properties, may be used for jumping disturb, meadow night
Moth, louse, thrips, fleahopper and Blatta seu periplaneta etc..
Nicotiana tabacum L. have promoting the circulation of QI to relieve pain, dampness, subside a swelling, effects such as parasite killing of detoxifying.
Leaf of Pterocarya Stenoptera has the effects such as antibacterial, parasite killing, removing toxic substances, and leaf is poisonous, can used as pesticides insecticide.
The method have the advantages that
(1) present invention utilizes vinegar factory waste liquid to prepare humic acids, the beneficially resource of garbage, reduces the one-tenth of the present invention
This；
(2) the conditioner composition major part degradable of the present invention, will not bring environmental pollution；
(3) the Passifolra edulis Biological pesticidal organic fertilizer material of the present invention can not only preventing disease and pest effectively, and can be balanced nutritious,
Improve soil environment, promote that Passifolra edulis is quickly grown up healthy and sound, shorten growth cycle, improve Passifolra edulis yield；
(4) the Passifolra edulis Biological pesticidal organic fertilizer material of the present invention is effective, beneficially popularization and application.
[detailed description of the invention]
It is specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: sheep stool 75 parts, chicken manure
75 parts, 75 parts of duck excrement, bagasse 20 parts, 10 parts of Pomacea canaliculata powder, 4 parts of nitrogen-fixing bacteria, ferrum element 2 parts, polyacrylamide 2 parts, conditioning
Agent 2 parts, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium 2 parts.
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 70 DEG C and is evaporated
Concentrate, being concentrated into pH value is 2.5, stop heating, left at room temperature activation 13h, be subsequently adding ammonium carbonate regulation pH value to 6.2,
Obtaining humic acid solution, being dried at 85 DEG C by humic acid solution to water content is 6%, crosses 100 mesh sieve after pulverizing, and prepared corruption is planted
Acid；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., the Qin
Skin, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera, with weight portion
For unit in 35:35:35:35:35:35:25:25:25:20:20:20:16:16:16:12:12:12:9: 9 ratio mixed powders
Broken, extract medicinal liquid in ultrasonic assistant ethanol extraction FAXIA, condition is: solid-liquid ratio is 1:12, and ultrasonic power is 160W, ethanol
Concentration is 60%, and Extracting temperature is 60 DEG C, and extraction time is 60min, and gained medical filtration, to be concentrated into water content be after 20%
It is 6% that mixture A, gained mixture A are dried to water content at 90 DEG C, crosses 100 mesh sieve, prepare Insecticidal combinations after pulverizing
Thing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, mildew-resistant
Agent and distilled water, mix homogeneously obtains mixture B, carries out described mixture B making 1.5-2.5mm granule and being dried at 90 DEG C
Be 6% to water content, prepare conditioner, described step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil adjust
Reason agent, antifungus agent and distilled water are formed in 30:0.04:35:0.06:8 ratio in units of weight portion, described soil conditioner bag
Include following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder are with weight
Part is formed in 10:10:10:4 ratio for unit, and described antifungus agent is quinoxyfen.
Embodiment 2
A kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: sheep stool 100 parts, chicken manure
100 parts, 100 parts of duck excrement, edible fungi residues 10 parts, sugar slag 10 parts, acid-sludge 10 parts, 20 parts of Pomacea canaliculata powder, brood cell liver bacterium 3 parts, ferment
Bacterium 3 parts, 2 parts of yeast, boron element 2 parts, manganese element 2 parts, copper 2 parts, sodium polyacrylate 2 parts, polyacrylic acid potassium 2 parts, poly-
Ammonium acrylate 2 parts, conditioner 6 parts, ethylene oxide 2 parts, polyurethane 2 parts, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium 2 parts.
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 80 DEG C and is evaporated
Concentrate, being concentrated into pH value is 3.5, stop heating, left at room temperature activation 15h, be subsequently adding ammonium carbonate regulation pH value to 7.6,
Obtaining humic acid solution, being dried at 105 DEG C by humic acid solution to water content is 4%, crosses 300 mesh sieve after pulverizing, and prepared corruption is planted
Acid；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., the Qin
Skin, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera, with weight portion
For unit 35:35:35:35:35:35:25:25:25:20:20:20:16:16:16:12:12:12:9: 9 ratio co-grindings,
Extracting medicinal liquid in ultrasonic assistant ethanol extraction FAXIA, condition is: solid-liquid ratio is 1:16, and ultrasonic power is 180W, and ethanol is dense
Degree is 80%, and Extracting temperature is 80 DEG C, and extraction time is 40min, and gained medical filtration, to be concentrated into water content be must to mix after 16%
It is 4% that compound A, gained mixture A are dried to water content at 100 DEG C, crosses 300 mesh sieve, prepare Pesticidal combination after pulverizing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, mildew-resistant
Agent and distilled water, mix homogeneously obtains mixture B, carries out described mixture B making 1.5-2.5mm granule and doing at 100 DEG C
Dry to water content be 4%, prepare conditioner, described step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil
Conditioner, antifungus agent and distilled water are formed in 45:0.05:50:0.1:10 ratio in units of weight portion, described soil conditioner
Including following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder are with weight
Amount part is that unit is formed in 30:20:15:6 ratio, and described antifungus agent is triazolone.
Embodiment 3
A kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: sheep stool 90 parts, chicken manure
90 parts, 90 parts of duck excrement, fecula 5 parts, manioc waste 5 parts, citric acid waste 5 parts, soy sauce residues 5 parts, residue of monosodium glutamate 5 parts, Pomacea canaliculata powder 16
Part, 1 part of actinomycetes, root nodule bacteria 1 part, phosphobacteria 1 part, B. mucilaginocus 1 part, phosphate solubilizing bacteria 1 part, copper 1 part, zinc element 1 part, molybdenum unit
Element 1 part, ferrum element 1 part, polyacrylic acid potassium 1 part, ammonium polyacrylate 1 part, 1 part of starch graft acrylic acid sodium, conditioner 3 parts, poly-
Urethane 1 part, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium 1 part, PTPP (potassium tripolyphosphate) 1 part.
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 75 DEG C and is evaporated
Concentrate, being concentrated into pH value is 3, stop heating, left at room temperature activation 14h, be subsequently adding ammonium carbonate regulation pH value to 6.9, obtain
Obtaining humic acid solution, being dried at 95 DEG C by humic acid solution to water content is 5%, crosses 200 mesh sieve, prepare humic acids after pulverizing；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., the Qin
Skin, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera, with weight portion
For unit 35:35:35:35:35:35:25:25:25:20:20:20:16:16:16:12:12:12:9: 9 ratio co-grindings,
Extracting medicinal liquid in ultrasonic assistant ethanol extraction FAXIA, condition is: solid-liquid ratio is 1:14, and ultrasonic power is 170W, and ethanol is dense
Degree is 70%, and Extracting temperature is 65 DEG C, and extraction time is 50min, and gained medical filtration, to be concentrated into water content be must to mix after 18%
It is 5% that compound A, gained mixture A are dried to water content at 95 DEG C, crosses 200 mesh sieve, prepare Pesticidal combination after pulverizing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, mildew-resistant
Agent and distilled water, mix homogeneously obtains mixture B, carries out described mixture B making 1.5-2.5mm granule and being dried at 95 DEG C
Be 5% to water content, prepare conditioner, described step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil adjust
Reason agent, antifungus agent and distilled water are formed in 38:0.04:42:0.08:9 ratio in units of weight portion, described soil conditioner bag
Include following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder are with weight
Part is formed in 20:15:12:5 ratio for unit, and described antifungus agent is quinoxyfen, triazolone.
Embodiment 4
A kind of Passifolra edulis Biological pesticidal organic fertilizer material, in units of weight portion, including following raw material: sheep stool 80 parts, chicken manure
80 parts, 80 parts of duck excrement, soy sauce residues 5 parts, residue of monosodium glutamate 5 parts, Glycine max (L.) Merr. 4 parts, marc 4 parts, bagasse 4 parts, 12 parts of Pomacea canaliculata powder,
1 part of nitrogen-fixing bacteria, brood cell liver bacterium 1 part, enzymatic microorganism 1 part, 1 part of yeast, 1 part of actinomycetes, molybdenum element 1 part, ferrum element 1 part, copper coin
Element 1 part, sodium polyacrylate 1 part, polyacrylic acid potassium 1 part, ammonium polyacrylate 1 part, conditioner 4 parts, polyethylene glycol oxide 1 part, poly-ammonia
Ester 1 part, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium 1 part.
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 75 DEG C and is evaporated
Concentrate, being concentrated into pH value is 3.2, stop heating, left at room temperature activation 13h, be subsequently adding ammonium carbonate regulation pH value to 7.2,
Obtaining humic acid solution, being dried at 100 DEG C by humic acid solution to water content is 6%, crosses 300 mesh sieve after pulverizing, and prepared corruption is planted
Acid；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., the Qin
Skin, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera, with weight portion
For unit 35:35:35:35:35:35:25:25:25:20:20:20:16:16:16:12:12:12:9: 9 ratio co-grindings,
Extracting medicinal liquid in ultrasonic assistant ethanol extraction FAXIA, condition is: solid-liquid ratio is 1:15, and ultrasonic power is 170W, and ethanol is dense
Degree is 75%, and Extracting temperature is 70 DEG C, and extraction time is 40min, and gained medical filtration, to be concentrated into water content be must to mix after 20%
It is 6% that compound A, gained mixture A are dried to water content at 100 DEG C, crosses 300 mesh sieve, prepare Pesticidal combination after pulverizing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, mildew-resistant
Agent and distilled water, mix homogeneously obtains mixture B, carries out described mixture B making 1.5-2.5mm granule and doing at 100 DEG C
Dry to water content be 6%, prepare conditioner, described step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil
Conditioner, antifungus agent and distilled water are formed in 35:0.04:40:0.06:9 ratio in units of weight portion, described soil conditioner
Including following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder, described turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder are with weight
Amount part is that unit is formed in 30:20:12:5 ratio, and described antifungus agent is quinoxyfen, triazolone.
For verifying the effect of Passifolra edulis Biological pesticidal organic fertilizer material of the present invention, by following experimental verification.
Choose the Passifolra edulis ground that six block specifications are basically identical, be set to Passifolra edulis ground a, Passifolra edulis ground b, Passifolra edulis ground c, hundred perfume
Fruit ground d, Passifolra edulis ground e, Passifolra edulis ground f, Passifolra edulis ground g, Passifolra edulis ground h, plant Passifolra edulis tree, wherein Passifolra edulis ground on eight pieces of ground
The common Passifolra edulis Biocidal that a, Passifolra edulis ground b, Passifolra edulis ground c, Passifolra edulis ground d use same not have Biocidal has
Machine fertilizer, Passifolra edulis ground e, Passifolra edulis ground f, Passifolra edulis ground g, Passifolra edulis ground h use the Passifolra edulis life of embodiment 1,2,3,4 respectively
Thing insecticidal organic fertilizer material, with 150 kilograms of calculating of every mu of fertilising, observes the Passifolra edulis tree growing state on eight pieces of Passifolra edulis ground.Result
Display: Passifolra edulis tree gloss difference, plant that Passifolra edulis ground a, Passifolra edulis ground b, Passifolra edulis ground c, Passifolra edulis ground d kind are planted are unhealthy,
The speed of growth is slow, and plant is little, yields poorly, and hundred that Passifolra edulis ground e, Passifolra edulis ground f, Passifolra edulis ground g, Passifolra edulis ground h kind are planted are fragrant
Fruit tree good luster, plant is healthy, leaf dark green plump, fast growth, and plant is big, and yield is high, and does not uses product of the present invention
Passifolra edulis compare, every mu increase production 435.2-468.4 kilogram, and use product of the present invention Passifolra edulis ground in pest and disease damage base
Originally do not have, it is seen that the Passifolra edulis Biological pesticidal organic fertilizer material of the present invention can not only preventing disease and pest effectively, and can be balanced in nutrition,
Improve soil environment, promote that Passifolra edulis is quickly grown up healthy and sound, shorten growth cycle, improve Passifolra edulis yield.
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations, for the technical field of the invention
Those of ordinary skill for, without departing under present inventive concept premise, it is also possible to make some simple deduction or replace, all answer
When being considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (10)
1. a Passifolra edulis Biological pesticidal organic fertilizer material, it is characterised in that in units of weight portion, including following raw material: sheep stool
75-100 part, chicken manure 75-100 part, duck excrement 75-100 part, waste residue 20-30 part, Pomacea canaliculata powder 10-20 part, biological bacteria 4-8 part, micro-
Secondary element 2-6 part, water-retaining agent 2-6 part, dispersant 2-6 part, conditioner 2-6 part；
Described waste residue includes marc, bagasse, edible fungi residues, sugar slag, acid-sludge, fecula, manioc waste, citric acid waste, soy sauce
One or more in slag, residue of monosodium glutamate, Glycine max (L.) Merr.；
Described biological bacteria include nitrogen-fixing bacteria, brood cell liver bacterium, enzymatic microorganism, yeast, actinomycetes, root nodule bacteria, phosphobacteria, B. mucilaginocus,
One or more in phosphate solubilizing bacteria；
Described trace element includes one or more in ferrum, boron, manganese, copper, zinc, molybdenum；
Described water-retaining agent includes polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch graft acrylic acid
One or more in sodium；
Described dispersant includes the one or many in polyethylene glycol oxide, polyurethane, di-2-ethylhexylphosphine oxide naphthalene sulfonic acid potassium, PTPP (potassium tripolyphosphate)
Kind；
The preparation method of described conditioner comprises the following steps:
S1: vinegar factory waste liquid is stood clarification, it is thus achieved that supernatant, then described supernatant is heated to 70-80 DEG C and is evaporated
Concentrating, being concentrated into pH value is 2.5-3.5, stops heating, left at room temperature activation 13-15h, is subsequently adding ammonium carbonate regulation pH value
To 6.2-7.6, it is thus achieved that humic acid solution, humic acid solution is dried to water content≤6% at 85-105 DEG C, after pulverizing, crosses 100-
300 mesh sieve, prepare humic acids；
S2: by Cacumen Platycladi, Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., Cortex Fraxini,
Radix Sophorae Flavescentis, Roots of Euphorbia soongarica, leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera co-grinding, super
Extract medicinal liquid under sound wave Assisted Ethanol extraction method, gained medical filtration, be concentrated into after water content≤20% to obtain mixture A, gained
Mixture A is dried to water content≤6% at 90-100 DEG C, crosses 100-300 mesh sieve, prepare Pesticidal combination after pulverizing；
S3: weigh respectively step S1 prepare humic acids, step S2 prepare Pesticidal combination, soil conditioner, antifungus agent and
Distilled water, mix homogeneously obtains mixture B, carries out described mixture B making 1.5-2.5mm granule and being dried at 90-100 DEG C
To water content≤6%, prepare conditioner.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 1, it is characterised in that Cacumen Platycladi described in step S2,
Herba Menthae, Caulis et Folium Lactucae sativae, Herba Anabasis aphyllae, Folium paulowniae, Herba Sophorae alopecuroidis, Artemisia absinihium L, Dioscorea zingiberensis, Aloe, Azadirachta Indica A., Cortex Fraxini, Radix Sophorae Flavescentis, Roots of Euphorbia soongarica,
Leaf of tea tree, Flos Daturae, Pyrethrum, Fructus Capsici, sabadilla, Nicotiana tabacum L., leaf of Pterocarya Stenoptera, with weight portion for unit 35:35:35:35:
35:35:25:25:25:20:20:20:16:16:16:12:12:12:9:9 ratio forms.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 1, it is characterised in that described in step S2, ultrasound wave is auxiliary
The condition helping ethanol extraction method to extract medicinal liquid is: solid-liquid ratio is 1:12-16, and ultrasonic power is 160-180W, and concentration of alcohol is
60%-80%, Extracting temperature is 60-70 DEG C, and extraction time is 40-60min.
The most according to claim 3, Passifolra edulis Biological pesticidal organic fertilizer material, it is characterised in that described solid-liquid ratio is 1:15 super
Acoustic power is 170W, and concentration of alcohol is 75%, and Extracting temperature is 70 DEG C, and extraction time is 40min.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 1, it is characterised in that soil conditioning described in step S3
Agent includes following raw material: turfy soil, cattle manure, sugarcane bagasse, Pomacea canaliculata powder.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 5, it is characterised in that described turfy soil, cattle manure, sucrose
Slag, Pomacea canaliculata powder are formed in 10-30:10-20:10-15:4-6 ratio in units of weight portion.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 6, it is characterised in that described turfy soil, cattle manure, sucrose
Slag, Pomacea canaliculata powder are formed in 30:20:12:5 ratio in units of weight portion.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 1, it is characterised in that antifungus agent bag described in step S3
Include in quinoxyfen, triazolone one or both.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 1, it is characterised in that step S1 system described in step S3
Humic acids, step S2 prepare Pesticidal combination, soil conditioner, antifungus agent and distilled water press in units of weight portion
30-45:0.04-0.05:35-50:0.06-0.1:8-10 ratio forms.
Passifolra edulis Biological pesticidal organic fertilizer material the most according to claim 9, it is characterised in that the corruption that described step S1 prepares
35:0.04 pressed in units of weight portion by Pesticidal combination, soil conditioner, antifungus agent and distilled water that phytic acid, step S2 prepare:
40:0.06:9 ratio forms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610596225.7A CN106278542A (en) | 2016-07-26 | 2016-07-26 | A kind of Passifolra edulis Biological pesticidal organic fertilizer material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610596225.7A CN106278542A (en) | 2016-07-26 | 2016-07-26 | A kind of Passifolra edulis Biological pesticidal organic fertilizer material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106278542A true CN106278542A (en) | 2017-01-04 |
Family
ID=57652353
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610596225.7A Pending CN106278542A (en) | 2016-07-26 | 2016-07-26 | A kind of Passifolra edulis Biological pesticidal organic fertilizer material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106278542A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106982636A (en) * | 2017-04-27 | 2017-07-28 | 广西乐业华东投资有限公司 | A kind of diseases prevention method for culturing seedlings of passion fruit |
| CN109942342A (en) * | 2017-12-21 | 2019-06-28 | 兴业县众旺种植专业合作社 | A kind of passion fruit foliar fertilizer |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105198664A (en) * | 2015-09-29 | 2015-12-30 | 广西百润源农业有限公司 | Organic fertilizer with insecticides and method for preparing organic fertilizer |
| CN105394111A (en) * | 2015-12-16 | 2016-03-16 | 广西南宁智翠科技咨询有限公司 | Organic conditioner utilizing starch industrial production wastewater and preparation method thereof |
| CN105542783A (en) * | 2015-12-16 | 2016-05-04 | 罗永城 | Humic acid type inorganic water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof |
-
2016
- 2016-07-26 CN CN201610596225.7A patent/CN106278542A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105198664A (en) * | 2015-09-29 | 2015-12-30 | 广西百润源农业有限公司 | Organic fertilizer with insecticides and method for preparing organic fertilizer |
| CN105394111A (en) * | 2015-12-16 | 2016-03-16 | 广西南宁智翠科技咨询有限公司 | Organic conditioner utilizing starch industrial production wastewater and preparation method thereof |
| CN105542783A (en) * | 2015-12-16 | 2016-05-04 | 罗永城 | Humic acid type inorganic water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106982636A (en) * | 2017-04-27 | 2017-07-28 | 广西乐业华东投资有限公司 | A kind of diseases prevention method for culturing seedlings of passion fruit |
| CN109942342A (en) * | 2017-12-21 | 2019-06-28 | 兴业县众旺种植专业合作社 | A kind of passion fruit foliar fertilizer |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105175170A (en) | Ecological organic fertilizer and preparation method thereof | |
| CN105061062A (en) | Special-effect biological organic fertilizer and preparation method thereof | |
| CN105272741A (en) | Biological organic pesticide-containing fertilizer and preparation method thereof | |
| CN105198602A (en) | Fertilizer with natural insecticidal effect and preparation method thereof | |
| CN105394111A (en) | Organic conditioner utilizing starch industrial production wastewater and preparation method thereof | |
| CN105061063A (en) | Organic fertilizer and preparation method thereof | |
| CN105254445A (en) | Biological insecticidal organic fertilizer and preparation method thereof | |
| CN105542777A (en) | Humic acid type water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof | |
| CN106490047A (en) | A kind of tea tree specific complex agricultural chemicals and preparation method thereof | |
| CN105399567A (en) | Henry steudnera tuber controlled-release fertilizer, and preparation method thereof | |
| CN105272527A (en) | Sweet potato controlled release fertilizer and preparation method thereof | |
| CN105272539A (en) | Organic plant medicinal fertilizer with desinsection and sterilization efficacy, and preparation method thereof | |
| CN105254425A (en) | Ecological organic fertilizer and preparing method thereof | |
| CN105237138A (en) | Release-controlled fertilizer for Chinese yam and preparation method thereof | |
| CN105254426A (en) | Organic fertilizer and preparation method thereof | |
| CN105272605A (en) | Fertilizer and preparation method thereof | |
| CN105198661A (en) | Biological disinsection organic fertilizer and preparation method thereof | |
| CN106478275A (en) | A kind of composite pesticide of preventing and treating tobacco diseases and preparation method thereof | |
| CN105419813A (en) | Novel conditioning agent utilizing starch industry production wastewater and preparation method of novel conditioning agent | |
| CN105198591A (en) | Leaf mustard controlled-release fertilizer and preparation method thereof | |
| CN105198604A (en) | Fragrant taro controlled-release fertilizer and preparation method thereof | |
| Gajjela et al. | Prospect of liquid organic manure on organic bitter gourd cultivation | |
| CN105542778A (en) | Humic acid type organic water-retaining agent and preparation method thereof | |
| CN105272606A (en) | Controlled release fertilizer for tomatoes and preparation method of controlled release fertilizer | |
| CN105503385A (en) | Conditioner using production wastewater in starch industry and preparation method of conditioner |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |