CN106433933A - 一种铌合金冷镦工艺润滑剂组合物 - Google Patents

一种铌合金冷镦工艺润滑剂组合物 Download PDF

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CN106433933A
CN106433933A CN201610841074.7A CN201610841074A CN106433933A CN 106433933 A CN106433933 A CN 106433933A CN 201610841074 A CN201610841074 A CN 201610841074A CN 106433933 A CN106433933 A CN 106433933A
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niobium alloy
alloy cold
agent
cold heading
lubricant compositions
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黄福川
黄军
陈帆
陈一帆
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Guangxi University
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Abstract

本发明公开了一种铌合金冷镦工艺润滑剂组合物，采用VHVI 10基础油作为基础油，配合多种复合添加剂。它们包括：抗氧剂、金属减活剂、防锈剂、油性剂、摩擦改进剂、极压剂、抗磨剂、抗泡剂、分散剂、粘附剂、抗氧抗腐剂等。本发明的组合物具有良好的承载抗磨性、挤压性、低温流动扩散性、润滑性、冷却性，油膜强度大、油膜厚度保持稳定，无异味、不刺激皮肤，能提高光洁度，保护被加工零件表面不锈蚀和氧化，减少动力能耗，低温流动性好，良好的抗泡性、抗乳化性、热氧化定性好，减少沉淀物和漆膜的产生，成型件易清洗。

Description

一种铌合金冷镦工艺润滑剂组合物
技术领域
本发明一种铌合金冷镦工艺润滑剂组合物属于铬合金冷镦工艺领域。
背景技术
铌是灰白色金属，熔点2468℃，沸点4742℃，密度8.57克/立方厘米。室温下铌在空气中稳定，在氧气中红热时也不被完全氧化，高温下与硫、氮、碳直接化合，能与钛、锆、铪、钨形成合金。不与无机酸或碱作用，也不溶于王水，但可溶于氢氟酸。纯铌在电子管中用于除去残留气体，钢中掺铌能提高钢在高温时的抗氧化性，改善钢的焊接性能。铌还用于制造高温金属陶瓷。
冷镦加工是利用模具在常温下对金属棒料镦粗(常为局部镦粗)成形的锻造方法。冷镦是另一种形式的镦锻工艺。更具金属型变理论，在常温下对金属坯料施加一定的压力，使之在模腔产生变形。按规定的形状和尺寸成形。冷镦工艺广泛应用于中小零件以及各种类型的标准件。
冷镦工艺的主要特征是无切削加工，材料利用率高，利用率达80～90％，且金属材料流线不会被切断，因此成品强度比切削加工或铸造成型零件强度更高，在一定的批量生产条件下，冷镦加工成本要比其它加工成本低得多，适用于通常需要切削件以及紧固件等形状对称的产品加工。产品的尺寸精度、重量精度及力学性能等都能达到较高的要求。
润滑剂应具有的特点：良好的承载抗磨性、挤压性(不拉毛、拉伤、有效延长冲模的使用寿命)、低温流动扩散性、润滑性、冷却性，油膜强度大、油膜厚度保持稳定，无异味、不刺激皮肤等。提高光洁度，保护被加工零件表面不锈蚀和氧化，减少动力能耗，低温流动性好，良好的抗泡性、抗乳化性、热氧化定性好，减少沉淀物和漆膜的产生，成型件易清洗。
发明内容
本发明要解决的技术问题是提供一种具有良好的承载抗磨性、挤压性、低温流动扩散性、润滑性、冷却性，油膜强度大、油膜厚度保持稳定，无异味、不刺激皮肤，能提高光洁度，保护被加工零件表面不锈蚀和氧化，减少动力能耗，低温流动性好，良好的抗泡性、抗乳化性、热氧化定性好，减少沉淀物和漆膜的产生，成型件易清洗的铌合金冷镦工艺润滑剂组合物。
本发明采用以下技术方案解决上述技术问题：
一种铌合金冷镦工艺润滑剂组合物，采用VHVI 10基础油作为基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量
基础油 余量
抗氧剂 0.05％～0.5％
金属减活剂 0.03％～0.6％
防锈剂 0.03％～0.3％
油性剂 4％～8％
摩擦改进剂 4％～8％
极压剂 3％～5％
抗磨剂 3％～6％
抗泡剂 10～50ppm
分散剂 2～3％
粘附剂 3～6％
抗氧抗腐剂 0.3～0.8％
以上各组分质量百分比总和为100％。
抗氧剂是质量比50％的酚酯型抗氧剂T508和50％的含铜抗氧剂T542的复合；金属减活剂是质量比50％的杂环化合物T571和50％的噻三唑衍生物T551的复合。
防锈剂是质量比50％的烯基丁二酸半酯T747和50％的苯骈三氮唑T706的复合物。
油性剂是硫化烯烃棉籽油T405；摩擦改进剂是油酸乙基酯。
极压剂是硫代磷酸胺盐T307。
抗磨剂是氯化石蜡T302；抗泡剂是甲基硅油T901。
分散剂是硼化聚异丁烯丁二酰亚胺T154B。
吸附剂是乙丙共聚物T613A。
抗氧抗腐剂是硫磷丁辛基锌盐T202。
本发明的有益效果在于：本发明铌合金冷镦工艺润滑剂具有良好的承载抗磨性、挤压性(不拉毛、拉伤、有效延长冲模的使用寿命)、低温流动扩散性、润滑性、冷却性，油膜强度大、油膜厚度保持稳定，无异味、不刺激皮肤等。提高光洁度，保护被加工零件表面不锈蚀和氧化，减少动力能耗，低温流动性好，良好的抗泡性、抗乳化性、热氧化定性好，减少沉淀物和漆膜的产生，成型件易清洗。
具体实施方式
实施例1：
将以下各组分按质量百分比调和而成：
组分 质量百分比含量
VHVI10基础油 余量
质量比50％的酚酯型抗氧剂(T508)和50％的含铜抗氧剂(T542)复合 0.1％
质量比50％的杂环化合物(T571)和50％的噻三唑衍生物(T551)复合 0.3％
质量比50％的烯基丁二酸半酯(T747)和50％的苯骈三氮唑(T706)复合 0.3％
硫化烯烃棉籽油(T405) 4％
油酸乙基酯 5％
硫代磷酸胺盐(T307) 5％
氯化石蜡(T302) 3％
甲基硅油(T901) 40ppm
硼化聚异丁烯丁二酰亚胺(T154B) 2％
乙丙共聚物(T613A) 6％
硫磷丁辛基锌盐(T202) 0.8％
以上各组分质量百分比总和为100％。
实施例2：
将以下各组分按质量百分比调和而成：
组分 质量百分比含量
VHVI10基础油 余量
质量比50％的酚酯型抗氧剂(T508)和50％的含铜抗氧剂(T542)复合 0.06％
质量比50％的杂环化合物(T571)和50％的噻三唑衍生物(T551)复合 0.5％
质量比50％的烯基丁二酸半酯(T747)和50％的苯骈三氮唑(T706)复合 0.3％
硫化烯烃棉籽油(T405) 5％
油酸乙基酯 4％
硫代磷酸胺盐(T307) 3％
氯化石蜡(T302) 4％
甲基硅油(T901) 30ppm
硼化聚异丁烯丁二酰亚胺(T154B) 2.5％
乙丙共聚物(T613A) 4％
硫磷丁辛基锌盐(T202) 0.3％
以上各组分质量百分比总和为100％。
实施例3：
将以下各组分按质量百分比调和而成：
组分 质量百分比含量
VHVI10基础油 余量
质量比50％的酚酯型抗氧剂(T508)和50％的含铜抗氧剂(T542)复合 0.3％
质量比50％的杂环化合物(T571)和50％的噻三唑衍生物(T551)复合 0.5％
质量比50％的烯基丁二酸半酯(T747)和50％的苯骈三氮唑(T706)复合 0.03％
硫化烯烃棉籽油(T405) 4.5％
油酸乙基酯 5.5％
硫代磷酸胺盐(T307) 3.5％
氯化石蜡(T302) 4％
甲基硅油(T901) 20ppm
硼化聚异丁烯丁二酰亚胺(T154B) 2.5％
乙丙共聚物(T613A) 5.5％
硫磷丁辛基锌盐(T202) 0.7％
以上各组分质量百分比总和为100％。
实施例3产品典型技术指标：
项目 指标
100℃运动粘度mm2/s 10.8
闪点(开口)/℃ 235
倾点/℃ -15
粘度指数 128
摩擦系数 0.07
腐蚀实验(铜片，100℃，3h)/级 1
氧化安定性(旋转氧弹性，150℃)min 410
抗乳化度82℃(40-37-3)/min 11
(极压性实验)四球机试验Pb/N 980
(极压性实验)四球机试验PD/N 8080
梯姆肯/N 350
起泡性试验24℃ 150/0
96℃ 100/0
后24℃ 100/0
FZG，级 14
机械杂质，％ 无
水分，％ 痕迹
水溶性酸或碱 无
蒸发损失(诺亚克法，250℃,1h)(m),％ 10
安定性试验(-10℃) 合格

Claims (9)

1.一种铌合金冷镦工艺润滑剂组合物，其特征在于：采用VHVI 10基础油作为基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量 基础油 余量 抗氧剂 0.05％～0.5％ 金属减活剂 0.03％～0.6％ 防锈剂 0.03％～0.3％ 油性剂 4％～8％ 摩擦改进剂 4％～8％ 极压剂 3％～5％ 抗磨剂 3％～6％ 抗泡剂 10～50ppm 分散剂 2～3％ 粘附剂 3～6％ 抗氧抗腐剂 0.3～0.8％
以上各组分质量百分比总和为100％。
2.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于抗氧剂是质量比50％的酚酯型抗氧剂T508和50％的含铜抗氧剂T542的复合；金属减活剂是质量比50％的杂环化合物T571和50％的噻三唑衍生物T551的复合。
3.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于防锈剂是质量比50％的烯基丁二酸半酯T747和50％的苯骈三氮唑T706的复合物。
4.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于油性剂是硫化烯烃棉籽油T405；摩擦改进剂是油酸乙基酯。
5.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于极压剂是硫代磷酸胺盐T307。
6.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于抗磨剂是氯化石蜡T302；抗泡剂是甲基硅油T901。
7.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于分散剂是硼化聚异丁烯丁二酰亚胺T154B。
8.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于吸附剂是乙丙共聚物T613A。
9.如权利要求1所述的一种铌合金冷镦工艺润滑剂组合物，其特征在于抗氧抗腐剂是硫磷丁辛基锌盐T202。
CN201610841074.7A 2016-09-21 2016-09-21 一种铌合金冷镦工艺润滑剂组合物 Pending CN106433933A (zh)

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* Cited by examiner, † Cited by third party
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CN113698350A (zh) * 2021-07-01 2021-11-26 新乡市瑞丰新材料股份有限公司 一种高效咪唑啉型防锈剂的制备方法及其组合应用

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Application publication date: 20170222