CN106404932A - 一种动物源性食品中β‑受体激动剂残留量的检测方法 - Google Patents
一种动物源性食品中β‑受体激动剂残留量的检测方法 Download PDFInfo
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- CN106404932A CN106404932A CN201610723501.1A CN201610723501A CN106404932A CN 106404932 A CN106404932 A CN 106404932A CN 201610723501 A CN201610723501 A CN 201610723501A CN 106404932 A CN106404932 A CN 106404932A
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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Abstract
Description
时间/min | A/% | B/% |
0 | 96 | 4 |
2 | 96 | 4 |
8 | 20 | 80 |
21 | 77 | 23 |
22 | 5 | 95 |
25 | 5 | 95 |
25.5 | 96 | 4 |
物质名称 | 斜率 | 截距 | 线性拟合相关系数 |
盐酸克仑特罗 | 1.523593 | 0.042159 | 0.9991 |
莱克多巴胺 | 1.364837 | 0.11713 | 0.9984 |
沙丁胺醇 | 0.878222 | 0.003971 | 0.9989 |
项目名称 | 盐酸克仑特罗 | 莱克多巴胺 | 沙丁胺醇 |
浓度(ng/mL) | 0.25 | 0.25 | 0.25 |
1 | 43777.6804 | 3443.2284 | 2200.1838 |
2 | 42910.4044 | 3858.9456 | 2326.1125 |
3 | 41838.2995 | 3597.1483 | 2105.1140 |
4 | 42121.4705 | 3530.6675 | 2183.8607 |
5 | 41091.2370 | 3464.8996 | 1976.6298 |
6 | 41582.7626 | 3613.3266 | 2220.4414 |
7 | 41349.3925 | 3513.5578 | 2210.0368 |
Avg | 42095.8924 | 3574.5391 | 2174.6256 |
RSD(%) | 2.3 | 3.9 | 5.0 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107179358A (zh) * | 2017-03-23 | 2017-09-19 | 苏州农业职业技术学院 | 动物毛发中瘦肉精残留的检测方法 |
CN108982712A (zh) * | 2018-10-08 | 2018-12-11 | 山东越品检验检测有限公司 | 一种测定猪肉中的沙美特罗、茚达特罗、奥达特罗的方法 |
CN109061019A (zh) * | 2018-10-19 | 2018-12-21 | 山东省新世纪检测认证中心有限公司 | 一种预防高胶原蛋白含量基质成冻的前处理方法 |
CN109061018A (zh) * | 2018-10-19 | 2018-12-21 | 山东省新世纪检测认证中心有限公司 | 一种预防高蛋白质含量基质成冻的前处理方法 |
CN109115920A (zh) * | 2018-11-02 | 2019-01-01 | 中国水产科学研究院东海水产研究所 | 利用液相色谱-串联质谱法同时检测水产品中18种β-受体激动剂的方法 |
CN111443147A (zh) * | 2020-04-09 | 2020-07-24 | 中维安全检测认证集团有限公司 | 一种检测食品中沙丁胺醇的方法 |
CN114563507A (zh) * | 2021-10-13 | 2022-05-31 | 中国农业科学院农业质量标准与检测技术研究所 | 一种动物组织内的β-受体激动剂残留的处理方法、检测方法及应用 |
CN115128189A (zh) * | 2022-07-14 | 2022-09-30 | 北京市农产品质量安全中心 | 一种动物毛发样品中β-受体激动剂药物残留检测的处理、确认方法及应用 |
Citations (2)
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CN101949898A (zh) * | 2010-08-10 | 2011-01-19 | 上海安谱科学仪器有限公司 | 一种动物源性食品中多种碱性药物残留量的检测方法 |
CN104897842A (zh) * | 2015-06-23 | 2015-09-09 | 山东出入境检验检疫局检验检疫技术中心 | 检测动物源食品中残留药物的方法及液质数据库 |
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2016
- 2016-08-25 CN CN201610723501.1A patent/CN106404932B/zh active Active
Patent Citations (2)
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CN101949898A (zh) * | 2010-08-10 | 2011-01-19 | 上海安谱科学仪器有限公司 | 一种动物源性食品中多种碱性药物残留量的检测方法 |
CN104897842A (zh) * | 2015-06-23 | 2015-09-09 | 山东出入境检验检疫局检验检疫技术中心 | 检测动物源食品中残留药物的方法及液质数据库 |
Non-Patent Citations (4)
Title |
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FAN SAI等: "Simultaneous Detection of Residues of 25 β2-Agonists and 23 β-Blockers in Animal Foods by High-Performance Liquid Chromatography Coupled with Linear Ion Trap Mass Spectrometry", 《JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY》 * |
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刘先军等: "超高压液相色谱-串联质谱法检测动物组织中26种β -受体激动剂", 《中国食品卫生杂志》 * |
徐成钢等: "高效液相色谱-串联质谱法测定猪肉中3种α-受体兴奋剂残留", 《分析测试学报》 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107179358A (zh) * | 2017-03-23 | 2017-09-19 | 苏州农业职业技术学院 | 动物毛发中瘦肉精残留的检测方法 |
CN108982712A (zh) * | 2018-10-08 | 2018-12-11 | 山东越品检验检测有限公司 | 一种测定猪肉中的沙美特罗、茚达特罗、奥达特罗的方法 |
CN109061019A (zh) * | 2018-10-19 | 2018-12-21 | 山东省新世纪检测认证中心有限公司 | 一种预防高胶原蛋白含量基质成冻的前处理方法 |
CN109061018A (zh) * | 2018-10-19 | 2018-12-21 | 山东省新世纪检测认证中心有限公司 | 一种预防高蛋白质含量基质成冻的前处理方法 |
CN109115920A (zh) * | 2018-11-02 | 2019-01-01 | 中国水产科学研究院东海水产研究所 | 利用液相色谱-串联质谱法同时检测水产品中18种β-受体激动剂的方法 |
CN111443147A (zh) * | 2020-04-09 | 2020-07-24 | 中维安全检测认证集团有限公司 | 一种检测食品中沙丁胺醇的方法 |
CN111443147B (zh) * | 2020-04-09 | 2022-05-06 | 中维安全检测认证集团有限公司 | 一种检测食品中沙丁胺醇的方法 |
CN114563507A (zh) * | 2021-10-13 | 2022-05-31 | 中国农业科学院农业质量标准与检测技术研究所 | 一种动物组织内的β-受体激动剂残留的处理方法、检测方法及应用 |
CN114563507B (zh) * | 2021-10-13 | 2023-11-10 | 中国农业科学院农业质量标准与检测技术研究所 | 一种动物组织内的β-受体激动剂残留的处理方法、检测方法及应用 |
CN115128189A (zh) * | 2022-07-14 | 2022-09-30 | 北京市农产品质量安全中心 | 一种动物毛发样品中β-受体激动剂药物残留检测的处理、确认方法及应用 |
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