CN106146574A - 一种微波‑超声复合提取甜叶菊叶中甜菊糖苷的方法 - Google Patents
一种微波‑超声复合提取甜叶菊叶中甜菊糖苷的方法 Download PDFInfo
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- CN106146574A CN106146574A CN201610446966.7A CN201610446966A CN106146574A CN 106146574 A CN106146574 A CN 106146574A CN 201610446966 A CN201610446966 A CN 201610446966A CN 106146574 A CN106146574 A CN 106146574A
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- leaf
- stevioside
- stevlae rebaudianae
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- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims abstract description 11
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- 108010059892 Cellulase Proteins 0.000 claims description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 5
- 229940106157 cellulase Drugs 0.000 claims description 5
- -1 stevioside Glycosides Chemical class 0.000 claims description 5
- 235000011149 sulphuric acid Nutrition 0.000 claims description 5
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- 244000228451 Stevia rebaudiana Species 0.000 description 1
- 235000006092 Stevia rebaudiana Nutrition 0.000 description 1
- 239000004383 Steviol glycoside Substances 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
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- NJYVDFDTLLZVMG-UHFFFAOYSA-N echinacoside Natural products CC1OC(OC2C(O)C(OCCc3ccc(O)c(O)c3)OC(COC4OC(CO)C(O)C(O)C4O)C2OC(=O)C=Cc5cc(O)cc(O)c5)C(O)C(O)C1O NJYVDFDTLLZVMG-UHFFFAOYSA-N 0.000 description 1
- 230000003311 flocculating effect Effects 0.000 description 1
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- 235000019411 steviol glycoside Nutrition 0.000 description 1
- 150000008144 steviol glycosides Chemical class 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/24—Condensed ring systems having three or more rings
- C07H15/256—Polyterpene radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
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Abstract
Description
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CN201610446966.7A CN106146574B (zh) | 2016-06-17 | 2016-06-17 | 一种微波-超声复合提取甜叶菊叶中甜菊糖苷的方法 |
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CN201610446966.7A CN106146574B (zh) | 2016-06-17 | 2016-06-17 | 一种微波-超声复合提取甜叶菊叶中甜菊糖苷的方法 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107371672A (zh) * | 2017-06-14 | 2017-11-24 | 湖南祥民制药有限公司 | 一种提高甜叶菊reb‑d得率的方法 |
CN108033986A (zh) * | 2018-02-07 | 2018-05-15 | 内蒙古昶辉生物科技股份有限公司 | 甜菊素的制备方法 |
CN108047286A (zh) * | 2017-12-12 | 2018-05-18 | 蚌埠市华东生物科技有限公司 | 一种从甜叶菊中提取甜菊糖苷的方法 |
CN108101947A (zh) * | 2018-01-09 | 2018-06-01 | 内蒙古昶辉生物科技股份有限公司 | 一种甜菊糖苷的提取方法 |
CN108918731A (zh) * | 2018-06-28 | 2018-11-30 | 安徽蚌埠惠农甜叶菊高科技发展有限公司 | 一种大量获得甜叶菊叶片产物甜菊糖苷rm的方法 |
CN111345460A (zh) * | 2018-12-20 | 2020-06-30 | 重庆积玉生物工程有限公司 | 一种多穗石柯天然甜味剂的制作方法 |
CN114105339A (zh) * | 2021-12-09 | 2022-03-01 | 宝钢湛江钢铁有限公司 | 一种去除雨水中cod、氨氮和悬浮物的方法 |
CN114249777A (zh) * | 2021-11-19 | 2022-03-29 | 安徽金源药业有限公司 | 一种提取淫羊藿苷的方法 |
CN114456216A (zh) * | 2020-11-09 | 2022-05-10 | 江苏施宇甜生物科技有限公司 | 提取高纯度甜菊糖苷的方法 |
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CN101062077A (zh) * | 2007-06-18 | 2007-10-31 | 石任兵 | 一种同时制备甜叶菊总甜菊苷和甜叶菊总黄酮的方法 |
CN101798329A (zh) * | 2010-03-19 | 2010-08-11 | 赣州菊隆高科技实业有限公司 | 一种超声波提取甜菊糖甙的方法 |
CN102127128A (zh) * | 2010-12-02 | 2011-07-20 | 田景振 | 一种利用酶耦合膜分离技术提取甜菊苷的新工艺 |
CN102199177A (zh) * | 2011-03-23 | 2011-09-28 | 武汉普赛特膜技术循环利用有限公司 | 一种纯天然高纯度甜菊糖的生产方法 |
CN102977163A (zh) * | 2012-12-17 | 2013-03-20 | 晨光生物科技集团股份有限公司 | 甜菊糖的工业化制备方法 |
CN105418703A (zh) * | 2015-12-12 | 2016-03-23 | 常州大学 | 一种从甜叶菊中提取纯化甜菊糖甙的方法 |
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2016
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CN101062077A (zh) * | 2007-06-18 | 2007-10-31 | 石任兵 | 一种同时制备甜叶菊总甜菊苷和甜叶菊总黄酮的方法 |
CN101798329A (zh) * | 2010-03-19 | 2010-08-11 | 赣州菊隆高科技实业有限公司 | 一种超声波提取甜菊糖甙的方法 |
CN102127128A (zh) * | 2010-12-02 | 2011-07-20 | 田景振 | 一种利用酶耦合膜分离技术提取甜菊苷的新工艺 |
CN102199177A (zh) * | 2011-03-23 | 2011-09-28 | 武汉普赛特膜技术循环利用有限公司 | 一种纯天然高纯度甜菊糖的生产方法 |
CN102977163A (zh) * | 2012-12-17 | 2013-03-20 | 晨光生物科技集团股份有限公司 | 甜菊糖的工业化制备方法 |
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丰雪 等: "甜菊糖苷提取新方法", 《南昌大学学报(理科版)》 * |
付娟娟 等: "超声波辅助纤维素酶提取甜菊糖苷", 《中国食品添加剂》 * |
刘东强 等: "甜菊糖苷的超声波提取及纯化工艺研究", 《中国调味品》 * |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107371672A (zh) * | 2017-06-14 | 2017-11-24 | 湖南祥民制药有限公司 | 一种提高甜叶菊reb‑d得率的方法 |
CN108047286A (zh) * | 2017-12-12 | 2018-05-18 | 蚌埠市华东生物科技有限公司 | 一种从甜叶菊中提取甜菊糖苷的方法 |
CN108101947A (zh) * | 2018-01-09 | 2018-06-01 | 内蒙古昶辉生物科技股份有限公司 | 一种甜菊糖苷的提取方法 |
CN108033986A (zh) * | 2018-02-07 | 2018-05-15 | 内蒙古昶辉生物科技股份有限公司 | 甜菊素的制备方法 |
CN108918731A (zh) * | 2018-06-28 | 2018-11-30 | 安徽蚌埠惠农甜叶菊高科技发展有限公司 | 一种大量获得甜叶菊叶片产物甜菊糖苷rm的方法 |
CN111345460A (zh) * | 2018-12-20 | 2020-06-30 | 重庆积玉生物工程有限公司 | 一种多穗石柯天然甜味剂的制作方法 |
CN114456216A (zh) * | 2020-11-09 | 2022-05-10 | 江苏施宇甜生物科技有限公司 | 提取高纯度甜菊糖苷的方法 |
CN114249777A (zh) * | 2021-11-19 | 2022-03-29 | 安徽金源药业有限公司 | 一种提取淫羊藿苷的方法 |
CN114105339A (zh) * | 2021-12-09 | 2022-03-01 | 宝钢湛江钢铁有限公司 | 一种去除雨水中cod、氨氮和悬浮物的方法 |
CN114105339B (zh) * | 2021-12-09 | 2023-10-13 | 宝钢湛江钢铁有限公司 | 一种去除雨水中cod、氨氮和悬浮物的方法 |
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Denomination of invention: A Method of Microwave Ultrasonic Composite Extraction of Steviol Glycosides from Stevia Leaves Granted publication date: 20181012 Pledgee: Agricultural Bank of China Limited Wuhe County Branch Pledgor: BENGBU HUADONG BIOLOGICAL TECHNOLOGY Co.,Ltd. Registration number: Y2024980005085 |
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