CN1060684C - 通过缩聚制备液体有机硅氧烷聚合物的方法 - Google Patents
通过缩聚制备液体有机硅氧烷聚合物的方法 Download PDFInfo
- Publication number
- CN1060684C CN1060684C CN94112919A CN94112919A CN1060684C CN 1060684 C CN1060684 C CN 1060684C CN 94112919 A CN94112919 A CN 94112919A CN 94112919 A CN94112919 A CN 94112919A CN 1060684 C CN1060684 C CN 1060684C
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- further characterized
- catalyst
- reative cell
- reagent
- reaction
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 8
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- 125000000094 2-phenylethyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])C([H])([H])* 0.000 description 1
- DXIJHCSGLOHNES-UHFFFAOYSA-N 3,3-dimethylbut-1-enylbenzene Chemical compound CC(C)(C)C=CC1=CC=CC=C1 DXIJHCSGLOHNES-UHFFFAOYSA-N 0.000 description 1
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 1
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- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 1
- 125000006038 hexenyl group Chemical group 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
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- 229910052757 nitrogen Inorganic materials 0.000 description 1
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Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
- C08G77/08—Preparatory processes characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/122—Pulverisation by spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Silicon Polymers (AREA)
- Glass Compositions (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9325342.5 | 1993-12-10 | ||
| GB939325342A GB9325342D0 (en) | 1993-12-10 | 1993-12-10 | Process for polymerisation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1106832A CN1106832A (zh) | 1995-08-16 |
| CN1060684C true CN1060684C (zh) | 2001-01-17 |
Family
ID=10746433
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN94112919A Expired - Lifetime CN1060684C (zh) | 1993-12-10 | 1994-12-08 | 通过缩聚制备液体有机硅氧烷聚合物的方法 |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US5492992A (https=) |
| EP (1) | EP0657209B1 (https=) |
| JP (1) | JP3668996B2 (https=) |
| KR (1) | KR100342326B1 (https=) |
| CN (1) | CN1060684C (https=) |
| AT (1) | ATE166798T1 (https=) |
| AU (1) | AU679583B2 (https=) |
| BR (1) | BR9404922A (https=) |
| CA (1) | CA2137645C (https=) |
| DE (1) | DE69410755T2 (https=) |
| ES (1) | ES2119092T3 (https=) |
| GB (1) | GB9325342D0 (https=) |
| IN (1) | IN183322B (https=) |
| PL (1) | PL177736B1 (https=) |
| RU (1) | RU2135528C1 (https=) |
| TW (1) | TW323291B (https=) |
| ZA (1) | ZA948933B (https=) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0837842A4 (en) * | 1995-06-07 | 1999-03-31 | Twenty First Century Res Corp | METHODS AND DEVICES FOR OBTAINING INTERMEDIATE OXIDATION PRODUCTS BY CONTROLLING CONVERSIONS AND TEMPERATURES IN AN ATOMIZED LIQUID |
| JPH0995534A (ja) * | 1995-09-28 | 1997-04-08 | Toshiba Silicone Co Ltd | ポリオルガノシロキサン粒子の連続製造方法 |
| US6365670B1 (en) * | 2000-03-10 | 2002-04-02 | Wacker Silicones Corporation | Organopolysiloxane gels for use in cosmetics |
| GB0018162D0 (en) | 2000-07-26 | 2000-09-13 | Dow Corning Sa | Polymerisation reactor and process |
| SE527528C2 (sv) | 2004-06-22 | 2006-04-04 | Bone Support Ab | Anordning för framställning av härdbar massa samt användning av anordningen |
| EP3218540A4 (en) * | 2014-11-12 | 2018-07-11 | The University Of Houston System | Soil-resistant, stain-resistant fluorine-free coatings and methods of applying on materials |
| US11345821B2 (en) | 2014-11-12 | 2022-05-31 | University Of Houston System | Weather-resistant, fungal-resistant, and stain-resistant coatings and methods of applying on wood, masonry, or other porous materials |
| US10704191B2 (en) | 2014-11-12 | 2020-07-07 | University Of Houston System | Soil-resistant, stain-resistant coatings and methods of applying on textile or other flexible materials |
| CN108137811A (zh) * | 2015-11-04 | 2018-06-08 | 美国陶氏有机硅公司 | 制备有机聚硅氧烷的方法 |
| CN108854930A (zh) * | 2018-08-22 | 2018-11-23 | 江苏先导干燥科技有限公司 | 一种新型智能喷雾反应装置及其反应方法 |
| JP7389061B2 (ja) | 2018-08-24 | 2023-11-29 | ダウ シリコーンズ コーポレーション | ヒドロキシル末端ポリジオルガノシロキサンの縮合重合のため方法 |
| CN112469769B (zh) | 2018-08-24 | 2022-07-08 | 美国陶氏有机硅公司 | 用于羟基封端的聚二有机硅氧烷的缩合聚合的方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1192894A (fr) * | 1957-03-13 | 1959-10-29 | Tno | Procédé et appareil pour la préparation d'un produit pulvérulent |
| FR1367524A (fr) * | 1963-05-11 | 1964-07-24 | Appareil de réaction pour synthèses organiques | |
| EP0080147A2 (en) * | 1981-11-19 | 1983-06-01 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | A process for producing a coagulated latex and apparatus therefor |
| EP0522776A1 (en) * | 1991-07-12 | 1993-01-13 | Dow Corning S.A. | Polymerisation reactor and polymerisation process |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5662803A (en) * | 1979-10-29 | 1981-05-29 | Mitsubishi Electric Corp | Fine particles of crosslinked polymer and their production |
| JPS5662804A (en) * | 1979-10-29 | 1981-05-29 | Mitsubishi Electric Corp | Particles of polymer containing a flame retarder and their production |
| DE3106711C2 (de) * | 1981-02-24 | 1986-07-03 | Dr. Melchior Entwicklungsgesellschaft mbH & Co KG, 5630 Remscheid | Verfahren zur kontinuierlichen Herstellung von kleinen Kunststoffteilchen |
-
1993
- 1993-12-10 GB GB939325342A patent/GB9325342D0/en active Pending
-
1994
- 1994-11-10 ZA ZA948933A patent/ZA948933B/xx unknown
- 1994-11-16 IN IN957CA1994 patent/IN183322B/en unknown
- 1994-11-25 TW TW083110985A patent/TW323291B/zh not_active IP Right Cessation
- 1994-12-05 US US08/349,658 patent/US5492992A/en not_active Expired - Lifetime
- 1994-12-05 AT AT94309041T patent/ATE166798T1/de active
- 1994-12-05 EP EP94309041A patent/EP0657209B1/en not_active Expired - Lifetime
- 1994-12-05 DE DE69410755T patent/DE69410755T2/de not_active Expired - Lifetime
- 1994-12-05 ES ES94309041T patent/ES2119092T3/es not_active Expired - Lifetime
- 1994-12-08 CN CN94112919A patent/CN1060684C/zh not_active Expired - Lifetime
- 1994-12-08 AU AU80328/94A patent/AU679583B2/en not_active Ceased
- 1994-12-08 CA CA002137645A patent/CA2137645C/en not_active Expired - Fee Related
- 1994-12-09 PL PL94306201A patent/PL177736B1/pl not_active IP Right Cessation
- 1994-12-09 BR BR9404922A patent/BR9404922A/pt not_active IP Right Cessation
- 1994-12-09 KR KR1019940033401A patent/KR100342326B1/ko not_active Expired - Lifetime
- 1994-12-09 RU RU94043802A patent/RU2135528C1/ru not_active IP Right Cessation
- 1994-12-12 JP JP30787694A patent/JP3668996B2/ja not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1192894A (fr) * | 1957-03-13 | 1959-10-29 | Tno | Procédé et appareil pour la préparation d'un produit pulvérulent |
| FR1367524A (fr) * | 1963-05-11 | 1964-07-24 | Appareil de réaction pour synthèses organiques | |
| EP0080147A2 (en) * | 1981-11-19 | 1983-06-01 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | A process for producing a coagulated latex and apparatus therefor |
| EP0522776A1 (en) * | 1991-07-12 | 1993-01-13 | Dow Corning S.A. | Polymerisation reactor and polymerisation process |
Also Published As
| Publication number | Publication date |
|---|---|
| KR100342326B1 (ko) | 2002-12-06 |
| PL177736B1 (pl) | 2000-01-31 |
| DE69410755T2 (de) | 1998-11-05 |
| IN183322B (https=) | 1999-11-20 |
| GB9325342D0 (en) | 1994-02-16 |
| CN1106832A (zh) | 1995-08-16 |
| US5492992A (en) | 1996-02-20 |
| KR950018173A (ko) | 1995-07-22 |
| AU8032894A (en) | 1995-06-15 |
| JPH07207035A (ja) | 1995-08-08 |
| JP3668996B2 (ja) | 2005-07-06 |
| ATE166798T1 (de) | 1998-06-15 |
| BR9404922A (pt) | 1995-08-08 |
| CA2137645A1 (en) | 1995-06-11 |
| AU679583B2 (en) | 1997-07-03 |
| ES2119092T3 (es) | 1998-10-01 |
| RU94043802A (ru) | 1996-11-20 |
| EP0657209B1 (en) | 1998-06-03 |
| TW323291B (https=) | 1997-12-21 |
| ZA948933B (en) | 1995-07-18 |
| CA2137645C (en) | 2006-04-25 |
| DE69410755D1 (de) | 1998-07-09 |
| RU2135528C1 (ru) | 1999-08-27 |
| EP0657209A1 (en) | 1995-06-14 |
| PL306201A1 (en) | 1995-06-12 |
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