CN105636929B - 用于纯化粗甲基丙烯酸甲酯的单元和方法 - Google Patents

用于纯化粗甲基丙烯酸甲酯的单元和方法 Download PDF

Info

Publication number
CN105636929B
CN105636929B CN201480057191.3A CN201480057191A CN105636929B CN 105636929 B CN105636929 B CN 105636929B CN 201480057191 A CN201480057191 A CN 201480057191A CN 105636929 B CN105636929 B CN 105636929B
Authority
CN
China
Prior art keywords
tower
mma
tetramethyl
unit according
destilling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201480057191.3A
Other languages
English (en)
Chinese (zh)
Other versions
CN105636929A (zh
Inventor
Y.贝尔纳丹
R.比永
X.马卡里安
F.瓦莱
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Trinseo Europe GmbH
Original Assignee
Arkema SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema SA filed Critical Arkema SA
Publication of CN105636929A publication Critical patent/CN105636929A/zh
Application granted granted Critical
Publication of CN105636929B publication Critical patent/CN105636929B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0446—Juxtaposition of mixers-settlers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201480057191.3A 2013-10-18 2014-10-17 用于纯化粗甲基丙烯酸甲酯的单元和方法 Active CN105636929B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR13.60186 2013-10-18
FR1360186A FR3012140B1 (fr) 2013-10-18 2013-10-18 Unite et procede pour la purification de methacrylate de methyle brut
PCT/EP2014/072367 WO2015055843A1 (en) 2013-10-18 2014-10-17 Unit and process for purification of crude methyl methacrylate

Publications (2)

Publication Number Publication Date
CN105636929A CN105636929A (zh) 2016-06-01
CN105636929B true CN105636929B (zh) 2019-10-01

Family

ID=50023735

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201480057191.3A Active CN105636929B (zh) 2013-10-18 2014-10-17 用于纯化粗甲基丙烯酸甲酯的单元和方法

Country Status (7)

Country Link
US (1) US10793505B2 (cg-RX-API-DMAC10.html)
EP (1) EP3057933B1 (cg-RX-API-DMAC10.html)
CN (1) CN105636929B (cg-RX-API-DMAC10.html)
BR (1) BR112016008639B1 (cg-RX-API-DMAC10.html)
FR (1) FR3012140B1 (cg-RX-API-DMAC10.html)
MX (1) MX2016004484A (cg-RX-API-DMAC10.html)
WO (1) WO2015055843A1 (cg-RX-API-DMAC10.html)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105111081B (zh) * 2015-08-11 2017-04-19 中国石油集团东北炼化工程有限公司吉林设计院 一种降低甲基丙烯酸甲酯中的甲基丙烯酸含量的方法
TW201718581A (zh) 2015-10-19 2017-06-01 英塞特公司 作為免疫調節劑之雜環化合物
SG10202004618TA (en) 2015-11-19 2020-06-29 Incyte Corp Heterocyclic compounds as immunomodulators
US20170174671A1 (en) 2015-12-17 2017-06-22 Incyte Corporation Heterocyclic compounds as immunomodulators
SI3394033T1 (sl) 2015-12-22 2021-03-31 Incyte Corporation Heterociklične spojine kot imunomodulatorji
AR108396A1 (es) 2016-05-06 2018-08-15 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
MA45116A (fr) 2016-05-26 2021-06-02 Incyte Corp Composés hétérocycliques comme immunomodulateurs
CN105964007B (zh) * 2016-05-31 2018-01-09 青岛理工大学 一种分离正丁醇‑异丁醇混合物的设备和工艺
ES2927984T3 (es) 2016-06-20 2022-11-14 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
ES2930092T3 (es) 2016-07-14 2022-12-07 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
WO2018044644A1 (en) * 2016-08-31 2018-03-08 Ecolab USA, Inc. Method to inhibit polymerization in a process water
KR102078396B1 (ko) * 2016-09-13 2020-02-17 주식회사 엘지화학 선택 증류 장치 및 증류 방법.
WO2018118461A1 (en) * 2016-12-20 2018-06-28 Dow Global Technologies Llc Methods of using n-oxyl polymerization inhibitor in a wash settler for preparing methyl methacrylate
WO2018119236A1 (en) 2016-12-22 2018-06-28 Incyte Corporation Triazolo[1,5-a]pyridine derivatives as immunomodulators
WO2018119221A1 (en) 2016-12-22 2018-06-28 Incyte Corporation Pyridine derivatives as immunomodulators
MX391981B (es) 2016-12-22 2025-03-21 Incyte Corp Derivados de benzooxazol como inmunomoduladores.
SMT202300065T1 (it) 2018-03-30 2023-05-12 Incyte Corp Composti eterociclici come immunomodulatori
PL3790877T3 (pl) 2018-05-11 2023-06-12 Incyte Corporation Pochodne tetrahydroimidazo[4,5-c]pirydyny jako immunomodulatory pd-l1
FR3096368B1 (fr) * 2019-05-23 2021-04-23 Arkema France Procede perfectionne de fabrication d’acrylates d’alkyle de purete elevee
KR20220027726A (ko) 2019-06-28 2022-03-08 아사히 가세이 가부시키가이샤 메타크릴산메틸의 제조 방법
WO2021030162A1 (en) 2019-08-09 2021-02-18 Incyte Corporation Salts of a pd-1/pd-l1 inhibitor
CN114829366A (zh) 2019-11-11 2022-07-29 因赛特公司 Pd-1/pd-l1抑制剂的盐及结晶形式
CN113461845B (zh) * 2020-03-30 2023-03-31 中石油吉林化工工程有限公司 一种pmma生产装置
CN113461525A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 甲基丙烯酸甲酯的精制方法
CN113457186B (zh) * 2020-03-30 2022-10-04 中石油吉林化工工程有限公司 提高粗mma分离塔分离效果的方法
CN113461526A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 甲基丙烯酸甲酯的萃取方法和系统
US20240342628A1 (en) * 2020-10-13 2024-10-17 Will Cody Whipple Continuous vacuum distillation system and method
CN113457193B (zh) * 2021-06-25 2023-01-17 济南大学 一种分离甲醇-甲缩醛-甲酸甲酯混合物的装置及方法
CN113599856B (zh) * 2021-08-11 2022-03-25 安徽晟捷新能源科技股份有限公司 一种nmp精馏塔底焦油再利用的设备
CN114292186A (zh) * 2022-01-14 2022-04-08 万华化学集团股份有限公司 一种高纯度mma的制备方法
JPWO2023210564A1 (cg-RX-API-DMAC10.html) * 2022-04-27 2023-11-02
CN115888181B (zh) * 2023-02-23 2023-05-23 山东宏旭化学股份有限公司 一种甲基丙烯酸甲酯生产用萃取塔及其萃取方法
CN120079126B (zh) * 2025-05-06 2025-07-25 福建贝莱特生物科技有限公司 用于3,5-二氯-2-戊酮生产的蒸馏装置及其控制方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5207874A (en) * 1989-12-22 1993-05-04 Atochem Process for the purification of glycidyl (meth)acrylate
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
CN1622930A (zh) * 2002-09-03 2005-06-01 三菱化学株式会社 (甲基)丙烯酸类的制造方法
CN101180259A (zh) * 2005-05-20 2008-05-14 赢创罗姆有限责任公司 制备（甲基）丙烯酸烷基酯的方法
WO2013146609A1 (ja) * 2012-03-26 2013-10-03 旭化成ケミカルズ株式会社 アセトニトリルの精製方法

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR813164A (fr) * 1937-07-06 1937-05-27 Bataafsche Petroleum Procédé de distillation
US3085153A (en) * 1959-04-13 1963-04-09 Phillips Petroleum Co Control system for separation processes
US3449215A (en) * 1966-09-08 1969-06-10 Phillips Petroleum Co Distillation column control with biasing signal as feedback correction for computed product flow rate
JPS51146418A (en) * 1975-06-10 1976-12-16 Nippon Zeon Co Ltd Purification of methacrylic esters
US5092983A (en) * 1986-09-12 1992-03-03 The Standard Oil Company Process for separating extractable organic material from compositions comprising said extractable organic material intermixed with solids and water using a solvent mixture
CA2012935A1 (en) * 1989-03-31 1990-09-30 Hirozo Segawa Purification and preparation processes for methyl methacrylate
US5435892A (en) * 1993-08-30 1995-07-25 Mitsubishi Rayon Co., Ltd. Process for separating methanol and methyl acrylate or methyl methacrylate
US5980695A (en) * 1996-11-14 1999-11-09 Transglobal Industrial Services, Inc. Apparatus for vacuum distillation of solvents
JP4593725B2 (ja) * 2000-04-14 2010-12-08 株式会社日本触媒 易重合性物質の製造方法および精製塔
US6939444B2 (en) * 2001-06-14 2005-09-06 Rohm And Haas Company Sulfur-bearing residue treatment system
CN1307145C (zh) * 2001-08-22 2007-03-28 三菱化学株式会社 容易聚合化合物用蒸馏装置
TWI254648B (en) * 2002-05-01 2006-05-11 Rohm & Haas Process for manufacturing high purity methacrylic acid
JP4032033B2 (ja) * 2003-06-30 2008-01-16 ローム アンド ハース カンパニー 高純度メタクリル酸の製造法
BRPI0416460B1 (pt) * 2003-11-17 2015-12-01 Mitsubishi Chem Corp equipamento tipo coluna para um composto facilmente polimerizável.
US20050189296A1 (en) * 2004-03-01 2005-09-01 Mitsubishi Chemical Corporation Method for handling (meth) acrylic ester-containing solution
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
US8157969B2 (en) * 2006-06-01 2012-04-17 Rohm And Haas Company Method and apparatus for minimizing accumulation of polymer on process equipment, especially safety devices
DE102006059513A1 (de) * 2006-12-14 2008-06-19 Evonik Röhm Gmbh Verfahren zur Herstellung von Methacrylsäure alkylestern mittels azeotroper Destillation
JP2009062289A (ja) * 2007-09-04 2009-03-26 Nippon Shokubai Co Ltd アクリル酸及び（メタ）アクリル酸エステルの製造方法
FR2931822B1 (fr) * 2008-05-30 2012-11-02 Arkema France Methacrylate de methyle derive de la biomasse, procede de fabrication, utilisations et polymeres correspondants.

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5207874A (en) * 1989-12-22 1993-05-04 Atochem Process for the purification of glycidyl (meth)acrylate
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
CN1622930A (zh) * 2002-09-03 2005-06-01 三菱化学株式会社 (甲基)丙烯酸类的制造方法
CN101180259A (zh) * 2005-05-20 2008-05-14 赢创罗姆有限责任公司 制备（甲基）丙烯酸烷基酯的方法
WO2013146609A1 (ja) * 2012-03-26 2013-10-03 旭化成ケミカルズ株式会社 アセトニトリルの精製方法

Also Published As

Publication number Publication date
CN105636929A (zh) 2016-06-01
BR112016008639B1 (pt) 2022-04-12
US10793505B2 (en) 2020-10-06
BR112016008639A2 (cg-RX-API-DMAC10.html) 2017-08-01
WO2015055843A1 (en) 2015-04-23
MX2016004484A (es) 2016-06-21
FR3012140A1 (cg-RX-API-DMAC10.html) 2015-04-24
EP3057933B1 (en) 2021-05-12
US20160251297A1 (en) 2016-09-01
FR3012140B1 (fr) 2016-08-26
EP3057933A1 (en) 2016-08-24

Similar Documents

Publication Publication Date Title
CN105636929B (zh) 用于纯化粗甲基丙烯酸甲酯的单元和方法
JP3937462B2 (ja) アクリル酸精製法
JP4350937B2 (ja) アクロレイン又はプロピオンアルデヒドを希薄な水性流から回収するプロセス
US11084774B2 (en) Esterification unit for producing crude methyl methacrylate, esterification process using said unit and plant comprising said unit
SA07270507B1 (ar) عملية لإنتاج حمض (ميث) أكريليك
JP2008101013A (ja) 高純度メタクリル酸の製造法
US10941103B2 (en) Process for continuously preparing n-butyl acrylate or isobutyl acrylate
CN102892743A (zh) 经侧出口蒸馏分离丙烯酸
KR101891680B1 (ko) 아크릴레이트 제조 방법
EP3406587A1 (en) Recovery method for (meth)acrylic acid
CN112262119B (zh) 纯化轻质丙烯酸酯的方法
JP2005239564A (ja) （メタ）アクリル酸エステルの製造方法
US7622607B2 (en) Method for purifying (meth)acrylic acid obtained by oxidizing a gaseous substrate
CN100447122C (zh) 防止(甲基)丙烯酸或其酯的处理装置堵塞的方法
CN110099891A (zh) 通过蒸馏将纯丙烯酸2-乙基己酯或纯丙烯酸2-丙基庚酯从相应的粗丙烯酸烷基酯中分离的方法
US7253313B2 (en) Method for purifying (meth)acrylic acid by oxidising a gaseous substrate
US20050107629A1 (en) Method for producing ethyl acrylate
CN1697676A (zh) 易聚合化合物的容器
JP2004300139A (ja) アクリル酸類の精製装置および方法
JP7034163B2 (ja) 蒸留により粗製ｔｅｒｔ－ブチル（メタ）アクリレートから純粋なｔｅｒｔ－ブチル（メタ）アクリレートを取得する方法
WO2017111277A1 (ko) (메트)아크릴산의 연속 회수 방법
JP2007063214A (ja) メタクリル酸メチルの品質改良法
JP2005036015A (ja) アクリル酸精製法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20210909

Address after: Horgen Switzerland

Patentee after: Trinseo Europe Ltd.

Address before: Cologne, France

Patentee before: ARKEMA FRANCE