FR3012140B1 - Unite et procede pour la purification de methacrylate de methyle brut - Google Patents

Unite et procede pour la purification de methacrylate de methyle brut

Info

Publication number
FR3012140B1
FR3012140B1 FR1360186A FR1360186A FR3012140B1 FR 3012140 B1 FR3012140 B1 FR 3012140B1 FR 1360186 A FR1360186 A FR 1360186A FR 1360186 A FR1360186 A FR 1360186A FR 3012140 B1 FR3012140 B1 FR 3012140B1
Authority
FR
France
Prior art keywords
purification
unit
methyl methacrylate
raw methyl
raw
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1360186A
Other languages
English (en)
Other versions
FR3012140A1 (fr
Inventor
Yves Bernardin
Xavier Marcarian
Romain Billon
Florent Vallet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Trinseo Europe GmbH
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1360186A priority Critical patent/FR3012140B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to CN201480057191.3A priority patent/CN105636929B/zh
Priority to PCT/EP2014/072367 priority patent/WO2015055843A1/fr
Priority to US15/029,300 priority patent/US10793505B2/en
Priority to EP14786193.4A priority patent/EP3057933B1/fr
Priority to BR112016008639-2A priority patent/BR112016008639B1/pt
Priority to MX2016004484A priority patent/MX2016004484A/es
Publication of FR3012140A1 publication Critical patent/FR3012140A1/fr
Application granted granted Critical
Publication of FR3012140B1 publication Critical patent/FR3012140B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0446—Juxtaposition of mixers-settlers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
FR1360186A 2013-10-18 2013-10-18 Unite et procede pour la purification de methacrylate de methyle brut Expired - Fee Related FR3012140B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1360186A FR3012140B1 (fr) 2013-10-18 2013-10-18 Unite et procede pour la purification de methacrylate de methyle brut
PCT/EP2014/072367 WO2015055843A1 (fr) 2013-10-18 2014-10-17 Unité et procédé de purification de méthacrylate de méthyle brut
US15/029,300 US10793505B2 (en) 2013-10-18 2014-10-17 Unit and process for purification of crude methyl methacrylate
EP14786193.4A EP3057933B1 (fr) 2013-10-18 2014-10-17 Unité et procédé de purification de méthacrylate de méthyle brut
CN201480057191.3A CN105636929B (zh) 2013-10-18 2014-10-17 用于纯化粗甲基丙烯酸甲酯的单元和方法
BR112016008639-2A BR112016008639B1 (pt) 2013-10-18 2014-10-17 Unidade e processo para purificação de metil metacrilato bruto
MX2016004484A MX2016004484A (es) 2013-10-18 2014-10-17 Unidad y proceso para la purificacion de metacrilato de metilo sin refinar.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1360186A FR3012140B1 (fr) 2013-10-18 2013-10-18 Unite et procede pour la purification de methacrylate de methyle brut

Publications (2)

Publication Number Publication Date
FR3012140A1 FR3012140A1 (fr) 2015-04-24
FR3012140B1 true FR3012140B1 (fr) 2016-08-26

Family

ID=50023735

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1360186A Expired - Fee Related FR3012140B1 (fr) 2013-10-18 2013-10-18 Unite et procede pour la purification de methacrylate de methyle brut

Country Status (7)

Country Link
US (1) US10793505B2 (fr)
EP (1) EP3057933B1 (fr)
CN (1) CN105636929B (fr)
BR (1) BR112016008639B1 (fr)
FR (1) FR3012140B1 (fr)
MX (1) MX2016004484A (fr)
WO (1) WO2015055843A1 (fr)

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CN105111081B (zh) * 2015-08-11 2017-04-19 中国石油集团东北炼化工程有限公司吉林设计院 一种降低甲基丙烯酸甲酯中的甲基丙烯酸含量的方法
MA52119A (fr) 2015-10-19 2018-08-29 Ncyte Corp Composés hétérocycliques utilisés comme immunomodulateurs
SG11201804152RA (en) 2015-11-19 2018-06-28 Incyte Corp Heterocyclic compounds as immunomodulators
WO2017112730A1 (fr) 2015-12-22 2017-06-29 Incyte Corporation Composés hétérocycliques utilisés comme immunomodulateurs
ES2906460T3 (es) 2016-05-06 2022-04-18 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
ES2905980T3 (es) 2016-05-26 2022-04-12 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
CN105964007B (zh) * 2016-05-31 2018-01-09 青岛理工大学 一种分离正丁醇‑异丁醇混合物的设备和工艺
PL3472167T3 (pl) 2016-06-20 2022-12-19 Incyte Corporation Związki heterocykliczne jako immunomodulatory
ES2930092T3 (es) 2016-07-14 2022-12-07 Incyte Corp Compuestos heterocíclicos como inmunomoduladores
EP3507349A1 (fr) * 2016-08-31 2019-07-10 Ecolab Usa Inc. Méthode d'inhibition de la polymérisation dans une eau de procédé
KR102078396B1 (ko) * 2016-09-13 2020-02-17 주식회사 엘지화학 선택 증류 장치 및 증류 방법.
WO2018118461A1 (fr) * 2016-12-20 2018-06-28 Dow Global Technologies Llc Procédés d'utilisation d'un inhibiteur de polymérisation n-oxyle dans un décanteur de lavage pour la préparation de méthacrylate de méthyle
US20180179201A1 (en) 2016-12-22 2018-06-28 Incyte Corporation Heterocyclic compounds as immunomodulators
BR112019012993A2 (pt) 2016-12-22 2019-12-03 Incyte Corp derivados de benzo-oxazol como imunomoduladores
EP3558973B1 (fr) 2016-12-22 2021-09-15 Incyte Corporation Dérivés pyridine utilisés en tant qu'immunomodulateurs
AU2019245288C1 (en) 2018-03-30 2024-01-18 Incyte Corporation Heterocyclic compounds as immunomodulators
CA3099994A1 (fr) 2018-05-11 2019-11-04 Incyte Corporation Derives de tetrahydro-imidazo[4,5-c]pyridine en tant qu'immunomodulateurs de pd-l1
WO2020261720A1 (fr) * 2019-06-28 2020-12-30 旭化成株式会社 Procédé de production de méthacrylate de méthyle
AR119624A1 (es) 2019-08-09 2021-12-29 Incyte Corp Sales de un inhibidor de pd-1 / pd-l1
MX2022005651A (es) 2019-11-11 2022-07-27 Incyte Corp Sales y formas cristalinas de un inhibidor de la proteina de muerte celular programada 1 (pd-1)/ligando de muerte celular programada 1 (pd-l1).
CN113461525A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 甲基丙烯酸甲酯的精制方法
CN113461845B (zh) * 2020-03-30 2023-03-31 中石油吉林化工工程有限公司 一种pmma生产装置
CN113457186B (zh) * 2020-03-30 2022-10-04 中石油吉林化工工程有限公司 提高粗mma分离塔分离效果的方法
CN113461526A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 甲基丙烯酸甲酯的萃取方法和系统
CN113457193B (zh) * 2021-06-25 2023-01-17 济南大学 一种分离甲醇-甲缩醛-甲酸甲酯混合物的装置及方法
CN113599856B (zh) * 2021-08-11 2022-03-25 安徽晟捷新能源科技股份有限公司 一种nmp精馏塔底焦油再利用的设备
CN114292186A (zh) * 2022-01-14 2022-04-08 万华化学集团股份有限公司 一种高纯度mma的制备方法
WO2023210564A1 (fr) * 2022-04-27 2023-11-02 住友化学株式会社 Composition
CN115888181B (zh) * 2023-02-23 2023-05-23 山东宏旭化学股份有限公司 一种甲基丙烯酸甲酯生产用萃取塔及其萃取方法

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Also Published As

Publication number Publication date
BR112016008639B1 (pt) 2022-04-12
US10793505B2 (en) 2020-10-06
US20160251297A1 (en) 2016-09-01
BR112016008639A2 (fr) 2017-08-01
CN105636929A (zh) 2016-06-01
FR3012140A1 (fr) 2015-04-24
WO2015055843A1 (fr) 2015-04-23
EP3057933B1 (fr) 2021-05-12
CN105636929B (zh) 2019-10-01
EP3057933A1 (fr) 2016-08-24
MX2016004484A (es) 2016-06-21

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TP Transmission of property

Owner name: TRINSEO EUROPE GMBH, CH

Effective date: 20210921

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Effective date: 20230606