CN105408253A - 制备具有mww骨架结构的含钛沸石材料的方法 - Google Patents

制备具有mww骨架结构的含钛沸石材料的方法 Download PDF

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Publication number
CN105408253A
CN105408253A CN201480020219.6A CN201480020219A CN105408253A CN 105408253 A CN105408253 A CN 105408253A CN 201480020219 A CN201480020219 A CN 201480020219A CN 105408253 A CN105408253 A CN 105408253A
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CN
China
Prior art keywords
titanium
mww
weight
skeleton structure
zeolitic material
Prior art date
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Pending
Application number
CN201480020219.6A
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English (en)
Chinese (zh)
Inventor
A-N·帕乌莱斯库
U·穆勒
H-J·卢茨伊勒
G·尤尔
R·拜耳
R·福格尔桑
J·H·泰勒斯
D·里德尔
D·乌尔班奇克
U·韦格利
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BASF SE
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BASF SE
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Priority to CN201910169392.7A priority Critical patent/CN110002463B/zh
Publication of CN105408253A publication Critical patent/CN105408253A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C01B39/085—Group IVB- metallosilicates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Epoxy Compounds (AREA)
CN201480020219.6A 2013-02-05 2014-02-05 制备具有mww骨架结构的含钛沸石材料的方法 Pending CN105408253A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910169392.7A CN110002463B (zh) 2013-02-05 2014-02-05 制备具有mww骨架结构的含钛沸石材料的方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13154021.3 2013-02-05
EP13154021 2013-02-05
PCT/EP2014/052205 WO2014122152A1 (en) 2013-02-05 2014-02-05 Process for preparing a titanium-containing zeolitic material having an mww framework structure

Related Child Applications (1)

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CN201910169392.7A Division CN110002463B (zh) 2013-02-05 2014-02-05 制备具有mww骨架结构的含钛沸石材料的方法

Publications (1)

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CN105408253A true CN105408253A (zh) 2016-03-16

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CN201480020219.6A Pending CN105408253A (zh) 2013-02-05 2014-02-05 制备具有mww骨架结构的含钛沸石材料的方法
CN201910169392.7A Active CN110002463B (zh) 2013-02-05 2014-02-05 制备具有mww骨架结构的含钛沸石材料的方法

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Country Status (15)

Country Link
US (1) US10029244B2 (enExample)
EP (1) EP2953895B1 (enExample)
JP (2) JP6491604B2 (enExample)
KR (1) KR102210984B1 (enExample)
CN (2) CN105408253A (enExample)
BR (1) BR112015018003B1 (enExample)
ES (1) ES2731815T3 (enExample)
HU (1) HUE043845T2 (enExample)
MX (1) MX377403B (enExample)
MY (1) MY182905A (enExample)
PL (1) PL2953895T3 (enExample)
RU (1) RU2650973C2 (enExample)
SG (2) SG11201506135WA (enExample)
WO (1) WO2014122152A1 (enExample)
ZA (1) ZA201506447B (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110062654A (zh) * 2016-12-13 2019-07-26 巴斯夫欧洲公司 制备含钛沸石的方法
CN110078094A (zh) * 2019-04-15 2019-08-02 华东师范大学 一种层间扩层的mww结构分子筛的制备方法
CN110420134A (zh) * 2019-08-28 2019-11-08 广州骏朗生物科技有限公司 一种片状硅石/纳米TiO2复合材料及其制备方法
CN110944942A (zh) * 2017-09-07 2020-03-31 雪佛龙美国公司 Afx骨架类型分子筛的合成

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL3206756T3 (pl) 2014-10-14 2019-06-28 Basf Se Zastosowanie heksadeka-8,15-dienalu jako aromatycznej substancji chemicznej
US10704794B2 (en) 2015-04-07 2020-07-07 Brown University Apparatus and method for passively cooling an interior
US20180224137A1 (en) * 2015-04-07 2018-08-09 Brown University Apparatus and method for passively cooling an interior
JP2018522009A (ja) 2015-07-15 2018-08-09 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アリールプロペンの調製方法
BR112018000519A2 (pt) 2015-07-15 2018-09-11 Basf Se processo para preparar um composto, e, uso de um catalisador poroso sólido
KR102470492B1 (ko) * 2016-09-06 2022-11-23 바스프 에스이 Mww 골격 구조를 갖는 붕소 함유 제올라이트의 고체열 합성
WO2018115118A1 (en) * 2016-12-20 2018-06-28 Basf Se Use of an acid treatment to decrease the plasticity of a composition comprising a titanium-containing zeolitic material having framework type mww
KR102503496B1 (ko) * 2016-12-20 2023-02-23 바스프 에스이 골격 타입 mww를 갖는 티타늄 함유 제올라이트 물질을 포함하는 압출성 조성물의 제조 방법
RU2762171C2 (ru) * 2017-01-18 2021-12-16 Басф Се Способ получения формованного изделия, содержащего цинк и титансодержащий цеолит
DE102018205122A1 (de) 2018-04-05 2018-10-25 Basf Se Verfahren zur Herstellung von Acrylsäurederivaten mittels oxidativer Kondensation aus Essigsäurederivaten
MX2021002336A (es) 2018-08-31 2021-07-15 Techstyle Mat Inc Sistema multifuncional para gestion pasiva de calor y agua.
KR102244509B1 (ko) * 2018-12-27 2021-04-23 고려대학교 산학협력단 폐수처리용 촉매, 이의 제조방법 및 이를 이용한 폐수처리 방법
US12195755B2 (en) 2019-05-20 2025-01-14 Brown University Placental lipid bilayer for cell-free molecular interaction studies
US12509559B2 (en) 2019-10-28 2025-12-30 Brown University Bacterial beta-lactamase responsive hydrogels
KR102408100B1 (ko) * 2021-05-31 2022-06-15 충북대학교 산학협력단 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매의 제조방법 및 이에 따라 제조된 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매
EP4634142A1 (en) 2022-12-13 2025-10-22 Basf Se Process for the production of an alkylstyrene and of an alkylphenyl propionic acid

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1639064A (zh) * 2002-03-07 2005-07-13 昭和电工株式会社 钛硅酸盐及其制备方法和在制备氧化化合物中的用途
CN102740968A (zh) * 2009-11-27 2012-10-17 巴斯夫欧洲公司 制备钛沸石催化剂的方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1485321A (en) 1919-05-26 1924-02-26 Elgin Nat Watch Co Device for lapping gauges
JPH0228774A (ja) 1988-07-18 1990-01-30 Anritsu Corp 多点測定パタンの入力方法
JPH11502804A (ja) * 1995-03-17 1999-03-09 シェブロン ユー．エス．エー．インコーポレイテッド 有機テンプレート及びアミンを用いたゼオライトの製造
JP2002102709A (ja) 2000-09-29 2002-04-09 Showa Denko Kk 酸化化合物製造用結晶性ｍｗｗ型チタノシリケート触媒、該触媒の製造方法、及び該触媒を用いた酸化化合物の製造方法
US7011802B2 (en) 2000-12-22 2006-03-14 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
US7323154B2 (en) 2002-03-07 2008-01-29 Showa Denko K.K. Titanosilicate, process for its production, and its use in producing oxidized compound
JP4241068B2 (ja) 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
DE10232406A1 (de) 2002-07-17 2004-01-29 Basf Ag Verfahren zur Herstellung eines zeolithhaltigen Feststoffes
US20040054199A1 (en) * 2002-09-17 2004-03-18 Basf Aktiengesellschaft Process for epoxidation and catalyst to be used therein
RU2299854C2 (ru) * 2003-02-03 2007-05-27 Сова Денко К.К. Модифицированный слоистый металлосиликатный материал и способ его получения
DE10320635A1 (de) * 2003-05-08 2004-11-18 Basf Ag Verfahren zur Herstellung von Propylenoxid
BRPI0413709A (pt) 2003-08-21 2006-10-17 Pfizer Prod Inc compostos para o tratamento de distúrbios neurodegenerativos
US7273826B2 (en) * 2005-07-26 2007-09-25 Lyondell Chemical Technology, L.P. Epoxidation catalyst
JP2008200553A (ja) * 2007-02-16 2008-09-04 Sumitomo Chemical Co Ltd チタノシリケート触媒
US8124555B2 (en) 2010-02-01 2012-02-28 Lyondell Chemical Technology L.P. Process for making titanium-MWW zeolite
EP2582625B1 (en) 2010-06-18 2017-03-22 Basf Se Organotemplate-free synthetic process for the production of a zeolitic material of the lev-type structure, zeolitic material thus obtained and use thereof
KR20140057473A (ko) 2010-11-23 2014-05-13 릴라이언스 인더스트리즈 리미티드 Ｍｗｗ형 제올라이트 제조 방법
JP2012236177A (ja) * 2011-05-13 2012-12-06 Sumitomo Chemical Co Ltd チタノシリケート含有触媒の製造方法
WO2013117536A2 (en) * 2012-02-07 2013-08-15 Basf Se Micropowder and molding containing a zeolitic material containing ti and zn

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1639064A (zh) * 2002-03-07 2005-07-13 昭和电工株式会社 钛硅酸盐及其制备方法和在制备氧化化合物中的用途
CN102740968A (zh) * 2009-11-27 2012-10-17 巴斯夫欧洲公司 制备钛沸石催化剂的方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
PENG WU ET AL.: "Preparation of B-free Ti-MWW through reversible structural conversion", 《CHEM.COMMUN.》 *
中国材料研究学会: "《2004年材料科学与工程新进展》", 30 June 2005, 北京：冶金工业出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110062654A (zh) * 2016-12-13 2019-07-26 巴斯夫欧洲公司 制备含钛沸石的方法
CN110062654B (zh) * 2016-12-13 2023-04-28 巴斯夫欧洲公司 制备含钛沸石的方法
CN110944942A (zh) * 2017-09-07 2020-03-31 雪佛龙美国公司 Afx骨架类型分子筛的合成
CN110944942B (zh) * 2017-09-07 2023-01-24 雪佛龙美国公司 Afx骨架类型分子筛的合成
CN110078094A (zh) * 2019-04-15 2019-08-02 华东师范大学 一种层间扩层的mww结构分子筛的制备方法
CN110420134A (zh) * 2019-08-28 2019-11-08 广州骏朗生物科技有限公司 一种片状硅石/纳米TiO2复合材料及其制备方法
CN110420134B (zh) * 2019-08-28 2022-04-15 广州骏朗生物科技有限公司 一种片状硅石/纳米TiO2复合材料及其制备方法

Also Published As

Publication number Publication date
HUE043845T2 (hu) 2019-09-30
JP6491604B2 (ja) 2019-03-27
BR112015018003B1 (pt) 2021-12-28
MX377403B (es) 2025-03-07
KR102210984B1 (ko) 2021-02-02
WO2014122152A1 (en) 2014-08-14
ZA201506447B (en) 2020-01-29
JP6955815B2 (ja) 2021-10-27
CN110002463A (zh) 2019-07-12
US20150368115A1 (en) 2015-12-24
RU2650973C2 (ru) 2018-04-18
ES2731815T3 (es) 2019-11-19
EP2953895B1 (en) 2019-03-20
KR20150115909A (ko) 2015-10-14
RU2015137732A (ru) 2017-03-14
SG11201506135WA (en) 2015-11-27
JP2016506904A (ja) 2016-03-07
MX2015010047A (es) 2016-03-04
BR112015018003A2 (pt) 2017-07-11
SG10201705892RA (en) 2017-08-30
JP2019112301A (ja) 2019-07-11
EP2953895A1 (en) 2015-12-16
MY182905A (en) 2021-02-05
CN110002463B (zh) 2022-10-11
US10029244B2 (en) 2018-07-24
PL2953895T3 (pl) 2019-09-30

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