CN105273488A - Antibacterial printing ink and preparation method thereof - Google Patents
Antibacterial printing ink and preparation method thereof Download PDFInfo
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- CN105273488A CN105273488A CN201410350766.2A CN201410350766A CN105273488A CN 105273488 A CN105273488 A CN 105273488A CN 201410350766 A CN201410350766 A CN 201410350766A CN 105273488 A CN105273488 A CN 105273488A
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Abstract
The invention discloses an antibacterial printing ink comprising the components in parts by weight: 10-18 parts of methylated amino resin, 10-15 parts of ketoaldehyde resin, 6-10 parts of glycerin, 2-6 parts of oleic acid, 15-25 parts of medium oil alkyd resin, 10-12 parts of tripropylene glycol diacrylate, 8-10 parts of dipentaerythritol hexaacrylate, 5-10 parts of zinc borate, 1-5 parts of nano silver, 4-8 parts of an organic pigment, and 5-10 parts of an auxiliary agent. The antibacterial printing ink has the beneficial effects that the printing ink is uniform in texture and high in adhesion firmness; after zinc borate is added, the fire-proof flame-retardant performance of the printing ink is improved; and with addition of nano silver, on one hand, the appearance texture of the printing ink is improved, on the other hand, due to the microscopic properties of nano silver, the printing ink has the sterilization and antibacterial effects, and has less harm to human bodies.
Description
Technical field
The invention belongs to printing-ink paint field, particularly relate to a kind of antimicrobial form printing-ink and preparation method thereof.
Background technology
The color (form and aspect) of printing-ink, body bone (rheological property such as rare thick, degree of mobilization) and drying property be three of printing-ink
Important performance.Their kind is a lot, and physical properties is also different, and what have is very thick, very sticky; And have quite rare.What have makes low-melting ink vehicle with vegetables oil; Some resins and solvent or water etc. make low-melting ink vehicle.These are all decide according to the object of printing and stock, printing process, the type of printing plate and drying means etc.The rate of drying of printing-ink, thixotropy, skeleton property have tremendous influence to production efficiency, quality product, and the composition of printing-ink has impact to human body, how to study to harm as far as possible little, production efficiency is high, fire-retardant, eco-friendly printing-ink has profound significance to printing-ink paint development.
Summary of the invention
The object of the present invention is to provide a kind of antimicrobial form printing-ink and preparation method thereof, to improve the fire retardant performance of conventional printing inks, also make printing-ink possess the antibacterial effect of sterilization, use value is high simultaneously.
For achieving the above object, the invention provides following technical scheme:
A kind of germ resistance printing-ink, its component is by weight:
Methyl-etherified aminoresin 10-18 part, ketone resin 10-15 part, glycerine 6-10 part, oleic acid 2-6 part, medium oil alkyd resin 15-25 part, tri (propylene glycol) diacrylate 10-12 part, double pentaerythritol methacrylate 8-10 part, zinc borate 5-10 part, nanometer silver 1-5 part, pigment dyestuff 4-8 part, auxiliary agent 5-10 part.
Described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 3-5 part, tri (propylene glycol) diacrylate 2-3 part, morpholine 3-4 part, methacrylic acid 1-2 part, tea-polyphenol 1-2 part, ricinolic acid 2-3 part, oxidation inhibitor 10351-2 part, linking agent TAC1-2 part, ethanol 15-30 part; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 65 DEG C-75 DEG C, stirs after 15-30 minute and leave standstill 5-10 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minute, to obtain final product.
A kind of preparation method of germ resistance printing-ink, comprise the following steps: by methyl-etherified aminoresin, ketone resin, glycerine, oleic acid, medium oil alkyd resin mixing, under stirring at 1000 revs/min, 75 DEG C are heated to the speed of 5 DEG C/minute, add double pentaerythritol methacrylate, tri (propylene glycol) diacrylate, stirring reaction 15 minutes, leave standstill and add zinc borate and nanometer silver after 2-3 minute, continue stirring reaction 10 minutes, add other remaining components, continue stirring reaction 2 hours, grinding distribution becomes the slurry of 30 μm, to obtain final product.
The invention has the beneficial effects as follows: printing-ink is homogeneous, adhere firmly degree is high, after adding zinc borate, improve the fire retardant performance of printing-ink, add the outer tube texture that nanometer silver improves printing-ink on the one hand, on the other hand due to the microscopic characteristics of nanometer silver, the printing-ink made is provided with sterilization, antibacterial effect is little to harm.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
A kind of germ resistance printing-ink, its component is by weight:
15 parts, methyl-etherified aminoresin, ketone resin 10 parts, glycerine 6 parts, oleic acid 4 parts, medium oil alkyd resin 20 parts, tri (propylene glycol) diacrylate 10 parts, double pentaerythritol methacrylate 10 parts, zinc borate 10 parts, nanometer silver 3 parts, pigment dyestuff 6 parts, auxiliary agent 8 parts.
Described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 4 parts, tri (propylene glycol) diacrylate 2 parts, morpholine 3 parts, methacrylic acid 1 part, tea-polyphenol 2 parts, ricinolic acid 3 parts, 10352 parts, oxidation inhibitor, linking agent TAC1-2 part, ethanol 15-30 part; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 65 DEG C-75 DEG C, stirs after 15-30 minute and leave standstill 5-10 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minute, to obtain final product.
A kind of preparation method of germ resistance printing-ink, comprise the following steps: by methyl-etherified aminoresin, ketone resin, glycerine, oleic acid, medium oil alkyd resin mixing, under stirring at 1000 revs/min, 75 DEG C are heated to the speed of 5 DEG C/minute, add double pentaerythritol methacrylate, tri (propylene glycol) diacrylate, stirring reaction 15 minutes, leave standstill and add zinc borate and nanometer silver after 2-3 minute, continue stirring reaction 10 minutes, add other remaining components, continue stirring reaction 2 hours, grinding distribution becomes the slurry of 30 μm, to obtain final product.
Embodiment 2:
A kind of germ resistance printing-ink, its component is by weight:
10 parts, methyl-etherified aminoresin, ketone resin 15 parts, glycerine 5 parts, oleic acid 4 parts, medium oil alkyd resin 25 parts, tri (propylene glycol) diacrylate 10 parts, double pentaerythritol methacrylate 8 parts, zinc borate 10 parts, nanometer silver 1 part, pigment dyestuff 6 parts, auxiliary agent 10 parts.
Described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 4 parts, tri (propylene glycol) diacrylate 2 parts, morpholine 3 parts, methacrylic acid 1 part, tea-polyphenol 2 parts, ricinolic acid 3 parts, 10352 parts, oxidation inhibitor, linking agent TAC1-2 part, ethanol 15-30 part; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 65 DEG C-75 DEG C, stirs after 15-30 minute and leave standstill 5-10 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minute, to obtain final product.
A kind of preparation method of germ resistance printing-ink, comprise the following steps: by methyl-etherified aminoresin, ketone resin, glycerine, oleic acid, medium oil alkyd resin mixing, under stirring at 1000 revs/min, 75 DEG C are heated to the speed of 5 DEG C/minute, add double pentaerythritol methacrylate, tri (propylene glycol) diacrylate, stirring reaction 15 minutes, leave standstill and add zinc borate and nanometer silver after 2-3 minute, continue stirring reaction 10 minutes, add other remaining components, continue stirring reaction 2 hours, grinding distribution becomes the slurry of 30 μm, to obtain final product.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (3)
1. a germ resistance printing-ink, is characterized in that, its component is by weight:
15 parts, methyl-etherified aminoresin, ketone resin 10 parts, glycerine 6 parts, oleic acid 4 parts, medium oil alkyd resin 20 parts, tri (propylene glycol) diacrylate 10 parts, double pentaerythritol methacrylate 10 parts, zinc borate 10 parts, nanometer silver 3 parts, pigment dyestuff 6 parts, auxiliary agent 8 parts.
2. a kind of germ resistance printing-ink according to claim 1, it is characterized in that, described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 4 parts, tri (propylene glycol) diacrylate 2 parts, morpholine 3 parts, methacrylic acid 1 part, tea-polyphenol 2 parts, ricinolic acid 3 parts, 10352 parts, oxidation inhibitor, linking agent TAC1-2 part, ethanol 15-30 part; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 65 DEG C-75 DEG C, stirs after 15-30 minute and leave standstill 5-10 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minute, to obtain final product.
3. the preparation method of a kind of germ resistance printing-ink as claimed in claim 1, it is characterized in that, by methyl-etherified aminoresin, ketone resin, glycerine, oleic acid, medium oil alkyd resin mixing, under stirring at 1000 revs/min, 75 DEG C are heated to the speed of 5 DEG C/minute, add double pentaerythritol methacrylate, tri (propylene glycol) diacrylate, stirring reaction 15 minutes, leave standstill and add zinc borate and nanometer silver after 2-3 minute, continue stirring reaction 10 minutes, add other remaining components, continue stirring reaction 2 hours, grinding distribution becomes the slurry of 30 μm, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350766.2A CN105273488A (en) | 2014-07-23 | 2014-07-23 | Antibacterial printing ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350766.2A CN105273488A (en) | 2014-07-23 | 2014-07-23 | Antibacterial printing ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105273488A true CN105273488A (en) | 2016-01-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410350766.2A Pending CN105273488A (en) | 2014-07-23 | 2014-07-23 | Antibacterial printing ink and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107778986A (en) * | 2017-10-31 | 2018-03-09 | 扬州市祥华新材料科技有限公司 | A kind of printing-ink and its manufacture method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103804988A (en) * | 2013-10-30 | 2014-05-21 | 合肥市华美光电科技有限公司 | Heat-resistant and oxidation-resistant printing ink and preparation method thereof |
-
2014
- 2014-07-23 CN CN201410350766.2A patent/CN105273488A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103804988A (en) * | 2013-10-30 | 2014-05-21 | 合肥市华美光电科技有限公司 | Heat-resistant and oxidation-resistant printing ink and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107778986A (en) * | 2017-10-31 | 2018-03-09 | 扬州市祥华新材料科技有限公司 | A kind of printing-ink and its manufacture method |
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Application publication date: 20160127 |