CN105246958B - 2,5‑呋喃‑二羧酸的酯化 - Google Patents
2,5‑呋喃‑二羧酸的酯化 Download PDFInfo
- Publication number
- CN105246958B CN105246958B CN201380064025.1A CN201380064025A CN105246958B CN 105246958 B CN105246958 B CN 105246958B CN 201380064025 A CN201380064025 A CN 201380064025A CN 105246958 B CN105246958 B CN 105246958B
- Authority
- CN
- China
- Prior art keywords
- alcohol
- reaction
- ester
- fdca
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P17/00—Preparation of heterocyclic carbon compounds with only O, N, S, Se or Te as ring hetero atoms
- C12P17/02—Oxygen as only ring hetero atoms
- C12P17/04—Oxygen as only ring hetero atoms containing a five-membered hetero ring, e.g. griseofulvin, vitamin C
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Microbiology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261739761P | 2012-12-20 | 2012-12-20 | |
| US61/739,761 | 2012-12-20 | ||
| PCT/US2013/073821 WO2014099438A2 (en) | 2012-12-20 | 2013-12-09 | Esterification of 2,5-furan-dicarboxylic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105246958A CN105246958A (zh) | 2016-01-13 |
| CN105246958B true CN105246958B (zh) | 2018-02-02 |
Family
ID=50979377
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380064025.1A Active CN105246958B (zh) | 2012-12-20 | 2013-12-09 | 2,5‑呋喃‑二羧酸的酯化 |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US9765045B2 (https=) |
| EP (1) | EP2935229B1 (https=) |
| JP (1) | JP6370307B2 (https=) |
| KR (1) | KR101963478B1 (https=) |
| CN (1) | CN105246958B (https=) |
| AU (1) | AU2013363501B2 (https=) |
| BR (1) | BR112015014183B1 (https=) |
| CA (1) | CA2895186C (https=) |
| ES (1) | ES2642005T3 (https=) |
| MX (1) | MX362292B (https=) |
| SG (1) | SG11201503646TA (https=) |
| WO (1) | WO2014099438A2 (https=) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2013338397B2 (en) * | 2012-10-29 | 2017-11-16 | Archer Daniels Midland Company | Alcohol-mediated esterification of carboxylic acids with carbonates |
| CA2921489C (en) * | 2013-08-30 | 2021-06-29 | Furanix Technologies B.V. | Process for purifying an acid composition comprising 2-formyl-furan-5-carboxylic acid and 2,5-furandicarboxylic acid |
| US9944615B2 (en) | 2014-05-08 | 2018-04-17 | Eastman Chemical Company | Purifying crude furan 2,5-dicarboxylic acid by hydrogenation and a purge zone |
| US9604202B2 (en) | 2014-05-08 | 2017-03-28 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
| US10010812B2 (en) | 2014-05-08 | 2018-07-03 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
| JP6452428B2 (ja) * | 2014-12-18 | 2019-01-16 | 花王株式会社 | ハロゲン系樹脂用可塑剤 |
| US10160740B2 (en) | 2015-03-20 | 2018-12-25 | The Board Of Trustees Of The Leland Stanford Junior University | Carbonate-promoted carboxylation reactions for the synthesis of valuable organic compounds |
| PL3283470T3 (pl) | 2015-04-14 | 2024-05-06 | E I Du Pont De Nemours | Sposoby wytwarzania kwasu 2,5-furanodikarboksylowego i jego pochodnych |
| US20190084952A1 (en) * | 2015-07-24 | 2019-03-21 | E I Du Pont De Nemours And Company | Process for producing 2,5-furandicarboxylic acid dialkyl ester |
| EP3434672B1 (en) * | 2015-07-24 | 2020-02-19 | DuPont Industrial Biosciences USA, LLC | Processes for preparing 2,5-furandicarboxylic acid |
| WO2017091437A1 (en) * | 2015-11-24 | 2017-06-01 | Archer Daniels Midland Company | Organotin catalysts in esterification processes of furan-2,5-dicarboxylic acid (fdca) |
| EP3402787A4 (en) | 2016-01-13 | 2019-11-27 | Stora Enso Oyj | PROCESS FOR THE PREPARATION OF 2,5-FURANDIC ACETIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF |
| WO2018187031A1 (en) * | 2017-04-05 | 2018-10-11 | Archer Daniels Midland Company | Novel esterification catalyst and uses thereof |
| EP4071142B1 (en) * | 2017-06-22 | 2023-10-04 | Archer Daniels Midland Company | Process for making esters of 2,5-furandicarboxylic acid |
| EP3652161A1 (en) | 2017-07-12 | 2020-05-20 | Stora Enso Oyj | Purified 2,5-furandicarboxylic acid pathway products |
| US20190023837A1 (en) | 2017-07-20 | 2019-01-24 | Eastman Chemical Company | Production of polyethylene furanoate in a retrofitted polyester plant |
| WO2019214576A1 (zh) * | 2018-05-10 | 2019-11-14 | 中国科学院长春应用化学研究所 | 2,5-呋喃二甲酸的制备方法 |
| US11236199B2 (en) * | 2018-06-25 | 2022-02-01 | Eastman Chemical Company | Oxidation process to produce 5-(alkoxycarbonyl)furan-2-carboxylic acids (ACFC) |
| US20190389820A1 (en) * | 2018-06-25 | 2019-12-26 | Eastman Chemical Company | Process for producing 5-(alkoxycarbonyl)furan-2-carboxylic acids and compositions containing same |
| US11440895B2 (en) | 2018-06-25 | 2022-09-13 | Eastman Chemical Company | Oxidation process to produce 5-(alkoxycarbonyl)furan-2-carboxylic acids (ACFC) |
| JP7163659B2 (ja) * | 2018-08-06 | 2022-11-01 | 三菱ケミカル株式会社 | グルカル酸生産能を有する高耐酸性微生物、及びそれを用いたグルカル酸の製造方法 |
| CN112585123A (zh) * | 2018-08-31 | 2021-03-30 | 伊士曼化工公司 | 在改造的dmt设备中生产纯化呋喃-2,5-二甲酸二烷基酯(dafd) |
| US10526301B1 (en) * | 2018-10-18 | 2020-01-07 | Eastman Chemical Company | Production of purified dialkyl-furan-2,5-dicarboxylate (DAFD) in a retrofitted DMT plant |
| US11787774B2 (en) | 2019-09-05 | 2023-10-17 | Eastman Chemical Company | Efficient process for producing 5-(alkoxycarbonyl)-furan-2-carboxylic acids |
| CA3187611A1 (en) * | 2020-08-12 | 2022-02-17 | Iman TABER | Purification of 2,5-furandicarboxylic acid, dimethyl ester and other esterified products |
| WO2022049384A1 (en) | 2020-09-03 | 2022-03-10 | Imperial College Innovations Limited | Surfactants |
| KR102640902B1 (ko) * | 2021-11-08 | 2024-02-27 | 한국생산기술연구원 | 테트라히드로퓨란-2,5-디카르복실산을 이용한 테트라히드로퓨란-2,5-디에스터의 제조 및 분리 정제 방법 |
| CN115286598B (zh) * | 2022-07-01 | 2024-04-26 | 中国石油化工股份有限公司 | 一种2,5-呋喃二甲酸二酯类化合物的合成方法 |
| CN117362252B (zh) * | 2023-10-08 | 2024-09-10 | 华东师范大学 | 一种从呋喃制备2,5-呋喃二甲酸二甲酯的方法 |
| CN117624093A (zh) * | 2023-12-06 | 2024-03-01 | 中科国生(杭州)科技有限公司 | 一种5-十二烷氧羰基呋喃-2-羧酸钠的制备方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2657666A1 (en) * | 2008-03-13 | 2009-09-13 | Bioamber S.A.S. | Process for the direct production of esters of carboxylic acids from fermentation broths |
| US7772414B1 (en) * | 2006-11-14 | 2010-08-10 | Aerophase, Inc. | Process for producing biodiesel fuel products |
| WO2012101015A1 (en) * | 2011-01-28 | 2012-08-02 | Süd-Chemie AG | Process for manufacturing esters of 2,5-furandicarboxylic acid |
| CN102648191A (zh) * | 2009-10-07 | 2012-08-22 | 福兰尼克斯科技公司 | 制备2,5-呋喃二甲酸及其酯的方法 |
| CN102666521A (zh) * | 2009-10-07 | 2012-09-12 | 福兰尼克斯科技公司 | 2,5-呋喃二甲酸和2,5-呋喃二甲酸的二烷基酯的制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5071754A (en) * | 1990-01-23 | 1991-12-10 | Battelle Memorial Institute | Production of esters of lactic acid, esters of acrylic acid, lactic acid, and acrylic acid |
| CN100594220C (zh) * | 2003-03-05 | 2010-03-17 | 伊士曼化工公司 | 聚合物共混物 |
| CN1938257A (zh) * | 2004-01-29 | 2007-03-28 | 齐凯姆公司 | 有机酸的回收 |
| DE102004008042A1 (de) * | 2004-02-19 | 2005-09-01 | Goldschmidt Gmbh | Verfahren zur Herstellung von Aminosäureestern und deren Säure-Additions-Salzen |
| DE102004047869A1 (de) * | 2004-10-01 | 2006-04-06 | Goldschmidt Gmbh | Verfahren zur enzymatischen Synthese von Pyroglutaminsäureestern |
| WO2007038496A2 (en) * | 2005-09-27 | 2007-04-05 | Chemic Laboratories, Inc. | Synthesis of fatty alcohol esters of hydroxy carboxylic acids, the use of the same as percutaneous permeation enhancers |
| US8105809B2 (en) * | 2008-07-03 | 2012-01-31 | Accera, Inc. | Enzymatic synthesis of acetoacetate esters and derivatives |
| US8188305B2 (en) * | 2009-02-03 | 2012-05-29 | David Miller | Method of producing biodiesel with supercritical alcohol and apparatus for same |
| DE102009028975A1 (de) * | 2009-08-28 | 2011-03-03 | Evonik Oxeno Gmbh | Esterderivate der 2,5-Furandicarbonsäure und ihre Verwendung als Weichmacher |
| US8859788B2 (en) * | 2012-06-22 | 2014-10-14 | Eastman Chemical Company | Esterification of furan-2,5-dicarboxylic acid to a dialkyl-furan-2,5-dicarboxylate vapor with rectification |
| US8658810B2 (en) * | 2012-06-22 | 2014-02-25 | Eastman Chemical Company | Method for producing purified dialkyl-furan-2,5-dicarboxylate vapor |
-
2013
- 2013-12-09 MX MX2015007903A patent/MX362292B/es active IP Right Grant
- 2013-12-09 ES ES13866244.0T patent/ES2642005T3/es active Active
- 2013-12-09 WO PCT/US2013/073821 patent/WO2014099438A2/en not_active Ceased
- 2013-12-09 AU AU2013363501A patent/AU2013363501B2/en active Active
- 2013-12-09 BR BR112015014183-8A patent/BR112015014183B1/pt active IP Right Grant
- 2013-12-09 CN CN201380064025.1A patent/CN105246958B/zh active Active
- 2013-12-09 EP EP13866244.0A patent/EP2935229B1/en active Active
- 2013-12-09 CA CA2895186A patent/CA2895186C/en active Active
- 2013-12-09 SG SG11201503646TA patent/SG11201503646TA/en unknown
- 2013-12-09 US US14/650,586 patent/US9765045B2/en active Active
- 2013-12-09 KR KR1020157019516A patent/KR101963478B1/ko active Active
- 2013-12-09 JP JP2015549448A patent/JP6370307B2/ja active Active
-
2017
- 2017-08-11 US US15/674,726 patent/US10155736B2/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7772414B1 (en) * | 2006-11-14 | 2010-08-10 | Aerophase, Inc. | Process for producing biodiesel fuel products |
| CA2657666A1 (en) * | 2008-03-13 | 2009-09-13 | Bioamber S.A.S. | Process for the direct production of esters of carboxylic acids from fermentation broths |
| CN102648191A (zh) * | 2009-10-07 | 2012-08-22 | 福兰尼克斯科技公司 | 制备2,5-呋喃二甲酸及其酯的方法 |
| CN102666521A (zh) * | 2009-10-07 | 2012-09-12 | 福兰尼克斯科技公司 | 2,5-呋喃二甲酸和2,5-呋喃二甲酸的二烷基酯的制备方法 |
| WO2012101015A1 (en) * | 2011-01-28 | 2012-08-02 | Süd-Chemie AG | Process for manufacturing esters of 2,5-furandicarboxylic acid |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2895186C (en) | 2019-10-22 |
| JP6370307B2 (ja) | 2018-08-08 |
| EP2935229B1 (en) | 2017-06-28 |
| AU2013363501A1 (en) | 2015-05-28 |
| BR112015014183A2 (pt) | 2017-07-11 |
| US9765045B2 (en) | 2017-09-19 |
| CA2895186A1 (en) | 2014-06-26 |
| EP2935229A4 (en) | 2016-01-27 |
| WO2014099438A2 (en) | 2014-06-26 |
| SG11201503646TA (en) | 2015-07-30 |
| US10155736B2 (en) | 2018-12-18 |
| MX2015007903A (es) | 2015-10-05 |
| KR20150095931A (ko) | 2015-08-21 |
| AU2013363501B2 (en) | 2016-12-01 |
| CN105246958A (zh) | 2016-01-13 |
| BR112015014183B1 (pt) | 2021-03-16 |
| ES2642005T3 (es) | 2017-11-14 |
| EP2935229A2 (en) | 2015-10-28 |
| MX362292B (es) | 2019-01-10 |
| US20170369463A1 (en) | 2017-12-28 |
| WO2014099438A3 (en) | 2015-07-16 |
| JP2016506407A (ja) | 2016-03-03 |
| US20150315166A1 (en) | 2015-11-05 |
| KR101963478B1 (ko) | 2019-03-28 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |