CN105016726A - 纳米氧化锆复合陶瓷材料、仿牙色纳米氧化锆复合陶瓷牙及其制备方法 - Google Patents
纳米氧化锆复合陶瓷材料、仿牙色纳米氧化锆复合陶瓷牙及其制备方法 Download PDFInfo
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- CN105016726A CN105016726A CN201510385200.8A CN201510385200A CN105016726A CN 105016726 A CN105016726 A CN 105016726A CN 201510385200 A CN201510385200 A CN 201510385200A CN 105016726 A CN105016726 A CN 105016726A
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- 239000002131 composite material Substances 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 44
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 title abstract 8
- 229910001928 zirconium oxide Inorganic materials 0.000 title abstract 8
- 229910010293 ceramic material Inorganic materials 0.000 title abstract 4
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- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims abstract description 11
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims abstract description 11
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005642 Oleic acid Substances 0.000 claims abstract description 11
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 11
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims abstract description 11
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 11
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 11
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims abstract description 11
- 239000008117 stearic acid Substances 0.000 claims abstract description 11
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 120
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 110
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 80
- 238000002156 mixing Methods 0.000 claims description 65
- 239000000243 solution Substances 0.000 claims description 60
- 238000010792 warming Methods 0.000 claims description 59
- 239000000758 substrate Substances 0.000 claims description 52
- 238000009413 insulation Methods 0.000 claims description 49
- 238000003756 stirring Methods 0.000 claims description 45
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 40
- 235000006408 oxalic acid Nutrition 0.000 claims description 40
- 229920000058 polyacrylate Polymers 0.000 claims description 40
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- 238000003786 synthesis reaction Methods 0.000 claims description 27
- ZXGIFJXRQHZCGJ-UHFFFAOYSA-N erbium(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Er+3].[Er+3] ZXGIFJXRQHZCGJ-UHFFFAOYSA-N 0.000 claims description 25
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 claims description 25
- PLDDOISOJJCEMH-UHFFFAOYSA-N neodymium(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Nd+3].[Nd+3] PLDDOISOJJCEMH-UHFFFAOYSA-N 0.000 claims description 25
- MMKQUGHLEMYQSG-UHFFFAOYSA-N oxygen(2-);praseodymium(3+) Chemical compound [O-2].[O-2].[O-2].[Pr+3].[Pr+3] MMKQUGHLEMYQSG-UHFFFAOYSA-N 0.000 claims description 25
- 238000005245 sintering Methods 0.000 claims description 25
- 238000002844 melting Methods 0.000 claims description 20
- 230000008018 melting Effects 0.000 claims description 20
- 238000001816 cooling Methods 0.000 claims description 10
- 238000002347 injection Methods 0.000 claims description 10
- 239000007924 injection Substances 0.000 claims description 10
- 239000003350 kerosene Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 8
- 238000001746 injection moulding Methods 0.000 claims description 5
- 229910000311 lanthanide oxide Inorganic materials 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 2
- 238000005452 bending Methods 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 3
- 230000035699 permeability Effects 0.000 abstract description 2
- 238000010586 diagram Methods 0.000 description 4
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- 241000237502 Ostreidae Species 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
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- 239000012620 biological material Substances 0.000 description 1
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- 239000005548 dental material Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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- 210000000214 mouth Anatomy 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
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- 229960001957 stomatological preparations Drugs 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 229910052845 zircon Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
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- Dental Prosthetics (AREA)
- Dental Preparations (AREA)
Abstract
Description
抗弯强度,MPa | 断裂韧性,MN/m3/2 | 色度差 | |
实施例1 | 1200 | 9.1 | ±1 |
实施例2 | 1198 | 8.9 | ±0.5 |
实施例3 | 1202 | 9 | ±1 |
Claims (7)
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CN201510385200.8A CN105016726B (zh) | 2015-07-04 | 2015-07-04 | 纳米氧化锆复合陶瓷材料、仿牙色纳米氧化锆复合陶瓷牙及其制备方法 |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106866140A (zh) * | 2017-03-10 | 2017-06-20 | 南通通州湾新材料科技有限公司 | 一种彩色陶瓷手机外壳的制造方法 |
CN107573061A (zh) * | 2017-08-25 | 2018-01-12 | 南通通州湾新材料科技有限公司 | 蜂窝状盲孔增韧氧化锆陶瓷外壳的制造方法及其应用 |
CN108066158A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种断裂韧性高的陶瓷牙材料及其制备方法和应用 |
CN108069707A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种色差小的陶瓷复合材料及其制备方法和应用 |
CN108069714A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种氧化锆基生物陶瓷及其制备方法和应用 |
CN108309475A (zh) * | 2018-02-05 | 2018-07-24 | 上海御齿台医疗科技有限公司 | 安全种植牙方法 |
CN109987969A (zh) * | 2019-04-29 | 2019-07-09 | 成都贝施美生物科技有限公司 | 一种快速浸泡氧化锆义齿染色液 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1519406A (zh) * | 2003-01-24 | 2004-08-11 | 中国科学院上海硅酸盐研究所 | 注射成型氧化锆制品的制作方法 |
JP2007022889A (ja) * | 2005-07-21 | 2007-02-01 | Matsushita Electric Works Ltd | 歯科補綴物用セラミック焼結体、歯科補綴物及びそれらの製造方法 |
CN102010199A (zh) * | 2010-11-19 | 2011-04-13 | 湖南正阳精密陶瓷有限公司 | 一种氧化锆陶瓷套管的生产方法 |
CN103113102A (zh) * | 2013-03-15 | 2013-05-22 | 湖南正阳精密陶瓷有限公司 | 一种氧化锆陶瓷插芯及其制备方法 |
CN103121840A (zh) * | 2012-03-23 | 2013-05-29 | 中新棠国业(北京)科技有限责任公司 | 多层色半透明氧化锆全瓷牙科修复材料的制备 |
-
2015
- 2015-07-04 CN CN201510385200.8A patent/CN105016726B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1519406A (zh) * | 2003-01-24 | 2004-08-11 | 中国科学院上海硅酸盐研究所 | 注射成型氧化锆制品的制作方法 |
JP2007022889A (ja) * | 2005-07-21 | 2007-02-01 | Matsushita Electric Works Ltd | 歯科補綴物用セラミック焼結体、歯科補綴物及びそれらの製造方法 |
CN102010199A (zh) * | 2010-11-19 | 2011-04-13 | 湖南正阳精密陶瓷有限公司 | 一种氧化锆陶瓷套管的生产方法 |
CN103121840A (zh) * | 2012-03-23 | 2013-05-29 | 中新棠国业(北京)科技有限责任公司 | 多层色半透明氧化锆全瓷牙科修复材料的制备 |
CN103113102A (zh) * | 2013-03-15 | 2013-05-22 | 湖南正阳精密陶瓷有限公司 | 一种氧化锆陶瓷插芯及其制备方法 |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106866140A (zh) * | 2017-03-10 | 2017-06-20 | 南通通州湾新材料科技有限公司 | 一种彩色陶瓷手机外壳的制造方法 |
CN107573061A (zh) * | 2017-08-25 | 2018-01-12 | 南通通州湾新材料科技有限公司 | 蜂窝状盲孔增韧氧化锆陶瓷外壳的制造方法及其应用 |
CN108066158A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种断裂韧性高的陶瓷牙材料及其制备方法和应用 |
CN108069707A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种色差小的陶瓷复合材料及其制备方法和应用 |
CN108069714A (zh) * | 2017-12-08 | 2018-05-25 | 郑州搜趣信息技术有限公司 | 一种氧化锆基生物陶瓷及其制备方法和应用 |
CN108309475A (zh) * | 2018-02-05 | 2018-07-24 | 上海御齿台医疗科技有限公司 | 安全种植牙方法 |
CN109987969A (zh) * | 2019-04-29 | 2019-07-09 | 成都贝施美生物科技有限公司 | 一种快速浸泡氧化锆义齿染色液 |
CN109987969B (zh) * | 2019-04-29 | 2021-07-06 | 成都贝施美生物科技有限公司 | 一种快速浸泡氧化锆义齿染色液 |
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Application publication date: 20151104 Assignee: Zhongguancun Technology Leasing Co.,Ltd. Assignor: Shenzhen yurucheng oral material Co.,Ltd. Contract record no.: X2023980034654 Denomination of invention: Nano zirconia composite ceramic material, imitation tooth color nano zirconia composite ceramic teeth and their preparation method Granted publication date: 20170329 License type: Exclusive License Record date: 20230412 |
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Denomination of invention: Nano zirconia composite ceramic material, imitation tooth color nano zirconia composite ceramic teeth and their preparation method Effective date of registration: 20230414 Granted publication date: 20170329 Pledgee: Zhongguancun Technology Leasing Co.,Ltd. Pledgor: Shenzhen yurucheng oral material Co.,Ltd. Registration number: Y2023980038096 |