CN104800123A - Antibacterial soap-based shower gel and preparation method thereof - Google Patents
Antibacterial soap-based shower gel and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an antibacterial soap-based shower gel and a preparation method thereof. The shower gel comprises the following ingredients: thymol, salicylic acid, plants extracts, ethyl alcohol, propylene glycol, erythritol, lauric acid, myristic acid, palmitic acid, potassium hydroxide, glycol distearate, dihexyl sodium sulfosuccinate, cocamidopropyl betaine, sodium cocoyl glycinate, polyquaternium-7, polyglyceryl fatty acid ester composition, ethylene diamine tetraacetic acid tetrasodium, sodium chloride, citric acid, essence, a preservative and water. The antibacterial soap-based shower gel is soft and friendly to skin, can effectively resist bacteria and moisturize skin and is particularly applicable to people with thicker cuticle, high grease secretion, skin pruritus and tinea corporis.
Description
Technical field
The invention belongs to daily use chemicals articles for washing technical field, be specifically related to a kind of antibacterial soap base bath gel and preparation method thereof.
Background technology
Bath gel, a kind of liquid ceanser used when being and having a bath.Bath gel is divided into two classes, i.e. soap base type and non-soap fundamental mode surfactant type according to the kind of its formula primary surfactant used by the national standard of bath gel.Soap base type bath gel forms based on the principle modification of soapmaking, its foaming abundancy, be easy to cleaning, but the defat of soap base bath gel is stronger.
Along with growth in the living standard, bath gel replaces fancy soap to become the first-selection of people's bath product gradually.But people are no longer simply clean skin to the functional requirement of bath gel, the institute that more focuses on taking a shower brings the effect of refrigerant pleasant, moist soft and smooth impression and antibacterial bacteriostatic, to the efficacy requirements also more and more refinement of product.The dust in air such as human sweat, scurf is combined and forms accumulating foulants on skin, dirt is assembled a large amount of microorganisms, it is likely wherein sex pheromone, certain threat is brought to the health of people, particularly horny layer is thicker, fat secretion is vigorous, have the crowd of skin itching and tinea, the crowd that horny layer is thicker, fat secretion is vigorous due to cutin thickness, fat secretion vigorous, the pathogenic microorganism on skin is easily grown, and then encroaches on skin; Skin itching is the infection owing to being subject to antibacterial or fungus mostly, if if having skin itching and have the crowd of tinea to be subject to the stimulation of extraneous antibacterial, fungus again, its symptom can be increased the weight of, if there is a kind of bath gel to clean dirt, certain pathogenic microorganism can also be removed simultaneously, alleviate skin itching and tinea etc. symptom, so this bath gel will have broad application prospects.
Patent documentation CN 100571675 C discloses a kind of ice cool shower cream, it comprises cocamido propyl betaine, sodium laureth sulfate, lauryl alcohol ether sulfosuccinates disodium, 2-methyl isophthalic acid, ammediol, EDETATE SODIUM, polyquaternary ammonium salt-26, Polyethylene Glycol methyl glucose dioleate, trichloro hydroxyl diphenyl ether, Kazon, lauryl sulfate diethanolamine, methyl glucoside ether-20, hydroxypropyl cellulose, glycerol, propylene glycol, essence, Herba Menthae, citric acid and water, this bath gel has degermation, but its antibacterial effect need to strengthen.
Patent documentation CN 104306295 A discloses a kind of antipruritic moisture-keeping shower cream, comprises cocoanut oil diethan olamide, hydroxyethyl urea, milk, PEG400, Radix Angelicae Sinensis extract, Flos Lonicerae extract, dodecylbenzene sodium sulfonate, isethionic acid ester, ethanedioic acid two stearic acid, rose essence, citric acid, sodium chloride, Dodecydimethylammonium bronides and deionized water.This bath gel has moisturizing itching-relieving action, but its effect need to improve.
Therefore, be necessary a kind of effectively anti-bacteria wet keeping of research, and be particularly suitable for the bath gel that horny layer is thicker, fat secretion is vigorous, have the crowd of skin itching and tinea to use.
Summary of the invention
The object of the present invention is to provide a kind of antibacterial soap base bath gel, it can effective anti-bacteria wet keeping, is particularly suitable for that horny layer is thicker, fat secretion is vigorous, have the crowd of skin itching and tinea to use.
The present invention is by the following technical programs to realize above-mentioned purpose, a kind of antibacterial soap base bath gel, be made up of the raw material of following weight percent meter: thymol 0.1 ~ 0.5%, salicylic acid 0.1 ~ 0.5%, plant extract 0.2 ~ 2.0%, ethanol 0.2 ~ 1%, propylene glycol 0.5 ~ 3.5%, erithritol 0.3 ~ 0.8%, lauric acid 2 ~ 8%, myristic acid 4 ~ 9%, Palmic acid 2 ~ 8%, potassium hydroxide 1.5 ~ 6%, glycol distearate 1 ~ 2%, 2-Sulfosuccinic acid ethylhexyl sodium 1 ~ 5%, cocamido propyl betaine 3 ~ 7%, sodium cocoyl glycinate 1 ~ 5%, polyquaternary ammonium salt-7 0.1 ~ 1.5%, polyglyceryl fatty acid ester compositions 0.3 ~ 3%, tetrasodium ethylenediamine tetraacetate 0.1 ~ 1%, sodium chloride 0.2 ~ 1.5%, citric acid 0.1 ~ 1%, essence 0.2 ~ 1%, antiseptic 0.1 ~ 0.3%, surplus is water.
As the preferred embodiment of the present invention, described antibacterial soap base bath gel is made up of the raw material of following weight percent meter: thymol 0.25%, salicylic acid 0.25%, plant extract 1.5%, ethanol 0.5%, propylene glycol 2.0%, erithritol 0.5%, lauric acid 3%, myristic acid 7%, Palmic acid 5%, potassium hydroxide 4%, glycol distearate 1.5%, 2-Sulfosuccinic acid ethylhexyl sodium 3%, cocamido propyl betaine 5%, sodium cocoyl glycinate 2%, polyquaternary ammonium salt-7 0.6%, polyglyceryl fatty acid ester compositions 1%, tetrasodium ethylenediamine tetraacetate 0.2%, sodium chloride 0.5%, citric acid 0.1%, essence 0.5%, antiseptic 0.1%, water 61.5%.
Further, described antiseptic is the mixture of phenoxyethanol and Methylisothiazolinone, and the weight ratio of phenoxyethanol and Methylisothiazolinone is 9:1.
Further, described polyglyceryl fatty acid ester compositions comprises one in polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters or its combination.
Further, described polyglyceryl fatty acid ester compositions is the compound of polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters.
Further, the weight ratio of described polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters is 5:3:2.
Present invention also offers the preparation method of described antibacterial soap base bath gel, comprise the following steps:
(1) thymol, salicylic acid are added in ethanol be dissolved to transparent, then add plant extract, propylene glycol is stirred to completely transparent, is prepared into bactericidal composition, for subsequent use;
(2) in the water of component weight 45 ~ 55%, add potassium hydroxide dissolve and stir, then add lauric acid, myristic acid, Palmic acid, Keep agitation is heated to 75 ~ 85 DEG C, insulation neutralization reaction 50 ~ 60min;
(3), after having reacted, add ethylene glycol bisthioglycolate stearic acid, 2-Sulfosuccinic acid ethylhexyl sodium, cocamido propyl betaine, polyglyceryl fatty acid ester compositions, and stir;
(4) system is cooled to 55 ~ 65 DEG C, adds sodium cocoyl glycinate, polyquaternary ammonium salt-7, and stirs;
(5) system is cooled to 35 ~ 45 DEG C, then in system, adds erithritol, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, essence, is stirred to and dissolves completely;
(6) add the bactericidal composition of step (1), stir, finally add antiseptic and water, stir.
Plant extract of the present invention is purchased from Kang Bo company of the U.S., product type is Campo Plantservative WM, this plant extract contains Flos Lonicerae extract, the Flos Lonicerae extract of 25% and the Jojoba oil of 10% of 65%, has good antibacterial and bacteriostasis.Described plant extract and thymol and salicylic acid composite, to gram positive bacteria, negative bacterium, mycete, yeast, fungus (especially to the large brood cell Trichophyton of causing a disease and Candida albicans), there is very strong antibacterial activity after testing.Salicylic acid activity when pH2 ~ 5 is the strongest, but salicylic acid is absorbed by the skin in acid condition very soon, and there is not metabolism, its secretion excretion is very slow, may produce and gather, be applied in soap base bath gel alkaline system of the present invention, pH is higher, salicylic acid forms potassium salicylate, and the foam exquisiteness of soap base bath gel own is enriched and was easy to water, is therefore not easy generation and gathers.
Potassium hydroxide and lauric acid in raw material of the present invention, myristic acid and Palmic acid generation neutralization reaction generate soap base, because the defat of soap base bath gel is stronger, add that thymol and salicylic acid have stronger stimulation to mucocutaneous, in order to solve zest problem, the present invention includes polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and the composite polyglyceryl fatty acid ester compositions of polyglycereol-3 cocos nucifera oil acid esters, said composition component is worked in coordination with, not only there is remarkable skinfeel and moisture-keeping efficacy, can also obviously reduce formula zest, coordinate erithritol again, the recovery of skin barrier function can be promoted, thus reduce system to the zest of skin.
Therefore, compared with prior art, advantage of the present invention is:
(1) the present invention's antibacterial soap base bath gel antibacterial effect is strong, reaches 99.9%, reach the requirement of antibiotic rate >=90% in " extraordinary bath shampoo " standard to the killing rate of colon bacillus, staphylococcus aureus, Candida albicans;
(2) the present invention's antibacterial soap base bath gel moisture-keeping efficacy is remarkable, washs moisture content of skin increase percentage rate after 2 hours and is greater than 15%, effectively alleviate the tight sense of skin because soap base bath gel defat strong band comes;
(3) the present invention's antibacterial soap base bath gel anti-bacteria wet keeping is effective, the gentle nonirritant of the antibacterial soap base bath gel of the present invention simultaneously, be particularly suitable for that horny layer is thicker, fat secretion is vigorous, have the crowd of skin itching and tinea to use, contribute to its relief of symptoms, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, antibacterial soap base bath gel of the present invention and preparation method thereof is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
embodiment 1, the antibacterial soap base bath gel of the present invention and preparation thereof
Formula: thymol 2.5g, salicylic acid 2.5g, plant extract 15g, ethanol 5g, propylene glycol 20g, erithritol 5g, lauric acid 30g, myristic acid 70g, Palmic acid 50g, potassium hydroxide 40g, glycol distearate 15g, 2-Sulfosuccinic acid ethylhexyl sodium 30g, cocamido propyl betaine 50g, sodium cocoyl glycinate 20g, polyquaternary ammonium salt-7 6g, polyglyceryl fatty acid ester compositions 10g(is polyglycereol-6 caprylate 5g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 3g, polyglycereol-3 cocos nucifera oil acid esters 2g), tetrasodium ethylenediamine tetraacetate 2g, sodium chloride 5g, citric acid 1g, essence 5g, antiseptic 1g(is phenoxyethanol 0.9g wherein, Methylisothiazolinone 0.1g), water 615g.
Preparation: (1) thymol, salicylic acid are added in ethanol be dissolved to transparent, then add plant extract, propylene glycol is stirred to completely transparent, is prepared into bactericidal composition, for subsequent use;
(2) in the water of component weight 50%, add potassium hydroxide dissolve and stir, then add lauric acid, myristic acid, Palmic acid, Keep agitation is heated to 80 DEG C, insulation neutralization reaction 55min;
(3), after having reacted, add ethylene glycol bisthioglycolate stearic acid, 2-Sulfosuccinic acid ethylhexyl sodium, cocamido propyl betaine, polyglyceryl fatty acid ester compositions, and stir;
(4) system is cooled to 60 DEG C, adds sodium cocoyl glycinate, polyquaternary ammonium salt-7, and stirs;
(5) system is cooled to 40 DEG C, then in system, adds erithritol, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, essence, is stirred to and dissolves completely;
(6) add the bactericidal composition of step (1), stir, finally add antiseptic and water, stir.
embodiment 2, the antibacterial soap base bath gel of the present invention and preparation thereof
Formula: thymol 1g, salicylic acid 5g, plant extract 10g, ethanol 2g, propylene glycol 35g, erithritol 3g, lauric acid 20g, myristic acid 90g, Palmic acid 20g, potassium hydroxide 15g, glycol distearate 10g, 2-Sulfosuccinic acid ethylhexyl sodium 10g, cocamido propyl betaine 70g, sodium cocoyl glycinate 10g, polyquaternary ammonium salt-7 1g, polyglyceryl fatty acid ester compositions 12g(is polyglycereol-6 caprylate 6g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 3.6g, polyglycereol-3 cocos nucifera oil acid esters 2.4g), tetrasodium ethylenediamine tetraacetate 10g, sodium chloride 2g, citric acid 8g, essence 2g, antiseptic 2g(is phenoxyethanol 1.8g wherein, Methylisothiazolinone 0.2g), water 662g.
Preparation: (1) thymol, salicylic acid are added in ethanol be dissolved to transparent, then add plant extract, propylene glycol is stirred to completely transparent, is prepared into bactericidal composition, for subsequent use;
(2) in the water of component weight 45%, add potassium hydroxide dissolve and stir, then add lauric acid, myristic acid, Palmic acid, Keep agitation is heated to 75 DEG C, insulation neutralization reaction 60min;
(3), after having reacted, add ethylene glycol bisthioglycolate stearic acid, 2-Sulfosuccinic acid ethylhexyl sodium, cocamido propyl betaine, polyglyceryl fatty acid ester compositions, and stir;
(4) system is cooled to 55 DEG C, adds sodium cocoyl glycinate, polyquaternary ammonium salt-7, and stirs;
(5) system is cooled to 35 DEG C, then in system, adds erithritol, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, essence, is stirred to and dissolves completely;
(6) add the bactericidal composition of step (1), stir, finally add antiseptic and water, stir.
embodiment 3, the antibacterial soap base bath gel of the present invention and preparation thereof
Formula: thymol 5g, salicylic acid 1g, plant extract 20g, ethanol 10g, propylene glycol 5g, erithritol 8g, lauric acid 80g, myristic acid 40g, Palmic acid 80g, potassium hydroxide 60g, glycol distearate 20g, 2-Sulfosuccinic acid ethylhexyl sodium 50g, cocamido propyl betaine 30g, sodium cocoyl glycinate 50g, polyquaternary ammonium salt-7 15g, polyglyceryl fatty acid ester compositions 30g(is polyglycereol-6 caprylate 15g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 9g, polyglycereol-3 cocos nucifera oil acid esters 6g), tetrasodium ethylenediamine tetraacetate 1g, sodium chloride 15g, citric acid 9g, essence 10g, antiseptic 10g(is phenoxyethanol 9g wherein, Methylisothiazolinone 1g), water 451g.
Preparation: (1) thymol, salicylic acid are added in ethanol be dissolved to transparent, then add plant extract, propylene glycol is stirred to completely transparent, is prepared into bactericidal composition, for subsequent use;
(2) in the water of component weight 55%, add potassium hydroxide dissolve and stir, then add lauric acid, myristic acid, Palmic acid, Keep agitation is heated to 85 DEG C, insulation neutralization reaction 50min;
(3), after having reacted, add ethylene glycol bisthioglycolate stearic acid, 2-Sulfosuccinic acid ethylhexyl sodium, cocamido propyl betaine, polyglyceryl fatty acid ester compositions, and stir;
(4) system is cooled to 65 DEG C, adds sodium cocoyl glycinate, polyquaternary ammonium salt-7, and stirs;
(5) system is cooled to 45 DEG C, then in system, adds erithritol, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, essence, is stirred to and dissolves completely;
(6) add the bactericidal composition of step (1), stir, finally add antiseptic and water, stir.
comparative example 1,
Formula: thymol 10g, salicylic acid 10g, ethanol 5g, propylene glycol 20g, erithritol 5g, lauric acid 30g, myristic acid 70g, Palmic acid 50g, potassium hydroxide 40g, glycol distearate 15g, 2-Sulfosuccinic acid ethylhexyl sodium 30g, cocamido propyl betaine 50g, sodium cocoyl glycinate 20g, polyquaternary ammonium salt-7 6g, polyglyceryl fatty acid ester compositions 10g(is polyglycereol-6 caprylate 5g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 3g, polyglycereol-3 cocos nucifera oil acid esters 2g), tetrasodium ethylenediamine tetraacetate 2g, sodium chloride 5g, citric acid 1g, essence 5g, antiseptic 1g(is phenoxyethanol 0.9g wherein, Methylisothiazolinone 0.1g), water 615g.
Preparation method is with embodiment 1.
comparative example 2,
Formula: plant extract 20g, ethanol 5g, propylene glycol 20g, erithritol 5g, lauric acid 30g, myristic acid 70g, Palmic acid 50g, potassium hydroxide 40g, glycol distearate 15g, 2-Sulfosuccinic acid ethylhexyl sodium 30g, cocamido propyl betaine 50g, sodium cocoyl glycinate 20g, polyquaternary ammonium salt-7 6g, polyglyceryl fatty acid ester compositions 10g(is polyglycereol-6 caprylate 5g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 3g, polyglycereol-3 cocos nucifera oil acid esters 2g), tetrasodium ethylenediamine tetraacetate 2g, sodium chloride 5g, citric acid 1g, essence 5g, antiseptic 1g(is phenoxyethanol 0.9g wherein, Methylisothiazolinone 0.1g), water 615g.
Preparation method is with embodiment 1.
comparative example 3,
Formula: thymol 2.5g, salicylic acid 2.5g, plant extract 15g, ethanol 5g, propylene glycol 20g, erithritol 15g, lauric acid 30g, myristic acid 70g, Palmic acid 50g, potassium hydroxide 40g, glycol distearate 15g, 2-Sulfosuccinic acid ethylhexyl sodium 30g, cocamido propyl betaine 50g, sodium cocoyl glycinate 20g, polyquaternary ammonium salt-7 6g, tetrasodium ethylenediamine tetraacetate 2g, sodium chloride 5g, citric acid 1g, essence 5g, antiseptic 1g(is phenoxyethanol 0.9g wherein, Methylisothiazolinone 0.1g), water 615g.
Preparation method is with embodiment 1.
comparative example 4,
Formula: thymol 2.5g, salicylic acid 2.5g, plant extract 15g, ethanol 5g, propylene glycol 20g, lauric acid 30g, myristic acid 70g, Palmic acid 50g, potassium hydroxide 40g, glycol distearate 15g, 2-Sulfosuccinic acid ethylhexyl sodium 30g, cocamido propyl betaine 50g, sodium cocoyl glycinate 20g, polyquaternary ammonium salt-7 6g, polyglyceryl fatty acid ester compositions 15g(is polyglycereol-6 caprylate 5g wherein, polyglycereol-4 certain herbaceous plants with big flowers acid esters 3g, polyglycereol-3 cocos nucifera oil acid esters 2g), tetrasodium ethylenediamine tetraacetate 2g, sodium chloride 5g, citric acid 1g, essence 5g, antiseptic 1g(is phenoxyethanol 0.9g wherein, Methylisothiazolinone 0.1g), water 615g.
Preparation method is with embodiment 1.
the anti-microbial property test of test example one, the antibacterial soap base bath gel of the present invention
Measure the antibacterial effect of the bath gel of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 2 preparation according to GB19877.2-2005 " extraordinary bath shampoo ", its result is as following table 1:
The antibacterial effect of the antibacterial soap base bath gel of table 1 the present invention
Can be obtained by upper table 1, the good anti-bacterial effect of the embodiment of the present invention 1 ~ 3 bath gel, 99.9% is reached to the killing rate of colon bacillus, staphylococcus aureus, Candida albicans, reach the requirement of antibiotic rate >=90% in " extraordinary bath shampoo " standard, therefore the antibacterial soap base bath gel of the present invention reaches the rank of antibacterial bath cream, wherein the sterilizing rate of embodiment 1 is the highest, illustrate each component of embodiment 1 and proportioning synergism the strongest.Not containing plant extract in comparative example 1 bath gel, comparative example 2 bath gel is only containing plant extract, all low compared to embodiment 1 ~ 3 of its sterilizing rate, illustrate that plant extract of the present invention and thymol and salicylic acid exist very strong synergism, three is composite plays very strong antibacterial action.
the zest test of test example two, the antibacterial soap base bath gel of the present invention
Carry out dermoreaction scoring according to the bath gel of " cosmetics health specification " (version in 2007) skin irritation/corrosion test to embodiment 1 and comparative example 3 ~ 4, concrete operations are as follows:
1, laboratory animal: healthy white rabbit 12, female, 1.8 ~ 2.2kg, skin zero damage, is divided into 3 groups, often organizes 4.
2, experimental procedure:
Before 2.1 tests, experiment white rabbit back spinal column diamond wool is cut by 24h, and not lesional epidermis is respectively 3cm × 3cm about unhairing scope.
2.2 get tested material (i.e. embodiment 1 and comparative example 3 ~ 4 bath gel) 0.5g is directly coated on skin, then uses two layers of gauze (2.5cm × 2.5cm) and one deck cellophane to cover, then is fixed with nonirritant adhesive plaster and binder.Opposite side skin in contrast.Adopt blocking test, application 2h.Residual tested material is removed with warm water after off-test.
2.3 observe smear position dermoreaction in removing 1,24,48 and 72h after tested material, dermoreaction scoring is carried out by table 2, carry out overall merit with the meansigma methods of animal subject integration, respectively observe time point top average according to 24h, 48h and 72h, judge skin irritation intensity by table 3.
Table 2 skin wound repair is marked
Table 3 skin irritation strength grading
3, experimental result: see the following form 4 according to table 2 and table 3 statistical result
The irritation test result of the antibacterial soap base bath gel of table 4 the present invention
Can be obtained by upper table 4, the antibacterial soap base bath gel of the present invention is to no skin irritation, but when lacking the composite polyglyceryl fatty acid ester compositions of polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters in system (comparative example 3), the zest of bath gel strengthens, slight stimulation is produced to skin, causes skin erythema and edema; And when lacking erithritol in system (comparative example 4), the zest of bath gel also has slight enhancing, illustrate that the composite polyglyceryl fatty acid ester compositions of polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters is indispensable in technical solution of the present invention, three's composition is worked in coordination with, can obviously reduce formula zest, coordinate erithritol again, further reduce system to the zest of skin.
the moistening effect test of test example three, the antibacterial soap base bath gel of the present invention
1, trial target: bath gel prepared by the embodiment of the present invention 1 ~ 3 and comparative example 3.
2, tested crowd
Number: 32 people
Age: between 24 ~ 30 years old
Sex: female 20 people, male 12 people
Grouping: be divided into 4 groups, often organizes female 5 people, male 3 people.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
3, method of testing: in the position of volunteer's right hand inner forearm 5 square centimeters, draw test zone, tests water content and the moisture content of skin of washing after 2 hours of the front skin of washing respectively, calculates the percentage rate that water content increases with moisture tester.
4, test result: see the following form 5.
The moistening effect test result of the antibacterial soap base bath gel of table 5 the present invention
Can be obtained by upper table 5, the moistening effect of the antibacterial soap base bath gel of the present invention is good, and wash moisture content of skin increase percentage rate after 2 hours and be greater than 15%, especially best with the moistening effect of embodiment 1, reach 16%, each component synergism is the strongest; Embodiment 1 ~ 3 is compared with comparative example 3 simultaneously, water content increases percentage rate and improves about 7%, illustrate that the composite polyglyceryl fatty acid ester compositions of polyglycereol-6 caprylate of the present invention, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters can not only reduce the zest of system, effectively can also improve the performance of keeping humidity of system, alleviate the tight sense of skin after taking a shower.
Below be only the preferred embodiment of the present invention, it should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For those skilled in the art, without departing from the spirit and scope of the present invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (7)
1. an antibacterial soap base bath gel, it is characterized in that, be made up of the raw material of following weight percent meter: thymol 0.1 ~ 0.5%, salicylic acid 0.1 ~ 0.5%, plant extract 0.2 ~ 2.0%, ethanol 0.2 ~ 1%, propylene glycol 0.5 ~ 3.5%, erithritol 0.3 ~ 0.8%, lauric acid 2 ~ 8%, myristic acid 4 ~ 9%, Palmic acid 2 ~ 8%, potassium hydroxide 1.5 ~ 6%, glycol distearate 1 ~ 2%, 2-Sulfosuccinic acid ethylhexyl sodium 1 ~ 5%, cocamido propyl betaine 3 ~ 7%, sodium cocoyl glycinate 1 ~ 5%, polyquaternary ammonium salt-7 0.1 ~ 1.5%, polyglyceryl fatty acid ester compositions 0.3 ~ 3%, tetrasodium ethylenediamine tetraacetate 0.1 ~ 1%, sodium chloride 0.2 ~ 1.5%, citric acid 0.1 ~ 1%, essence 0.2 ~ 1%, antiseptic 0.1 ~ 0.3%, surplus is water.
2. antibacterial soap base bath gel as claimed in claim 1, it is characterized in that, described antibacterial soap base bath gel is made up of the raw material of following weight percent meter: thymol 0.25%, salicylic acid 0.25%, plant extract 1.5%, ethanol 0.5%, propylene glycol 2.0%, erithritol 0.5%, lauric acid 3%, myristic acid 7%, Palmic acid 5%, potassium hydroxide 4%, glycol distearate 1.5%, 2-Sulfosuccinic acid ethylhexyl sodium 3%, cocamido propyl betaine 5%, sodium cocoyl glycinate 2%, polyquaternary ammonium salt-7 0.6%, polyglyceryl fatty acid ester compositions 1%, tetrasodium ethylenediamine tetraacetate 0.2%, sodium chloride 0.5%, citric acid 0.1%, essence 0.5%, antiseptic 0.1%, water 61.5%.
3. antibacterial soap base bath gel as claimed in claim 1 or 2, is characterized in that, described antiseptic is the mixture of phenoxyethanol and Methylisothiazolinone, and the weight ratio of phenoxyethanol and Methylisothiazolinone is 9:1.
4. antibacterial soap base bath gel as claimed in claim 1 or 2, is characterized in that, described polyglyceryl fatty acid ester compositions comprises one in polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters or its combination.
5. antibacterial soap base bath gel as claimed in claim 4, is characterized in that, described polyglyceryl fatty acid ester compositions is the compound of polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters.
6. antibacterial soap base bath gel as claimed in claim 5, is characterized in that, the weight ratio of described polyglycereol-6 caprylate, polyglycereol-4 certain herbaceous plants with big flowers acid esters and polyglycereol-3 cocos nucifera oil acid esters is 5:3:2.
7. prepare as arbitrary in claim 1 ~ 6 as described in the method for antibacterial soap base bath gel, it is characterized in that, comprise the following steps:
(1) thymol, salicylic acid are added in ethanol be dissolved to transparent, then add plant extract, propylene glycol is stirred to completely transparent, is prepared into bactericidal composition, for subsequent use;
(2) in the water of component weight 45 ~ 55%, add potassium hydroxide dissolve and stir, then add lauric acid, myristic acid, Palmic acid, Keep agitation is heated to 75 ~ 85 DEG C, insulation neutralization reaction 50 ~ 60min;
(3), after having reacted, add ethylene glycol bisthioglycolate stearic acid, 2-Sulfosuccinic acid ethylhexyl sodium, cocamido propyl betaine, polyglyceryl fatty acid ester compositions, and stir;
(4) system is cooled to 55 ~ 65 DEG C, adds sodium cocoyl glycinate, polyquaternary ammonium salt-7, and stirs;
(5) system is cooled to 35 ~ 45 DEG C, then in system, adds erithritol, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, essence, is stirred to and dissolves completely;
(6) add the bactericidal composition of step (1), stir, finally add antiseptic and water, stir.
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| CN105232432A (en) * | 2015-11-18 | 2016-01-13 | 李爱冰 | Traditional Chinese medicine bath cream and preparation method thereof |
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