CN104825356B - A kind of anti-bacterial hand lotion and preparation method thereof - Google Patents

A kind of anti-bacterial hand lotion and preparation method thereof Download PDF

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CN104825356B
CN104825356B CN201510216598.2A CN201510216598A CN104825356B CN 104825356 B CN104825356 B CN 104825356B CN 201510216598 A CN201510216598 A CN 201510216598A CN 104825356 B CN104825356 B CN 104825356B
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extract
hand lotion
mixed
bacterial hand
wetting agent
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CN201510216598.2A
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CN104825356A (en
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郭伊妮
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威莱(广州)日用品有限公司
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Abstract

The invention belongs to detergent applications, be specifically related to a kind of anti-bacterial hand lotion and preparation method thereof.The anti-bacterial hand lotion of the present invention is mainly made up of polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine, alkyl polyglucoside, polyquaternary ammonium salt, fatty glyceride, wetting agent, mixed plant extract, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, Jojoba oil, 1,2 pentanediols and essence.Its preparation method is first with water dissolution polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and the fatty glyceride of total amount 70 80%;Then Jojoba oil, polyquaternary ammonium salt, wetting agent are mixed with alkyl polyglucoside, above two mixed liquor is mixed, adds remaining component and stir.The anti-bacterial hand lotion of the present invention has skin protection skin moistening, antibacterial bacteriostatic, and antiallergic is releived, antiinflammatory, improves the microcirculatory effect of hand, is that a kind of disinfecting and decontaminating ability is strong, the significant multifunctional liquid soap of skin protection soothing effect.

Description

A kind of anti-bacterial hand lotion and preparation method thereof

Technical field

The invention belongs to detergent applications, be specifically related to a kind of anti-bacterial hand lotion and preparation method thereof.

Background technology

Along with people's living standard and the raising of quality of life, hand-washing article is had higher requirement by people, the past, Owing to fancy soap has good dirt-removing power, people use always fancy soap as hand-washing article, but, due to fancy soap in use Easily landing, chance water and high temperature can soften and naturally consume, and fancy soap is alkalescence, wash rear skin easily dry, matt, especially Easily it is infected with dirt on hand and antibacterial, becomes secondary pollution source, cause people to start in public places not in use by fancy soap.Due to It is gentle that handwashing liquid has performance, easy to use, sanitation and hygiene and easily stored advantage, gradually replaces fancy soap to be widely used in house Front yard and public place.

The basic components of handwashing liquid typically add surfactant, compose fat agent, skin moistening wetting agent, pH adjusting agent, thickening agent, Hard water resistance dose, subtract lubrication prescription, preservative and outward appearance regulator etc., make handwashing liquid have disinfecting, antimicrobial effect notable, flesh is moistened in protection Skin and the pleasant advantage of outward appearance.At present, in order to improve irritating effect that cleaning is antibacterial and reduction is to skin, more and more Handwashing liquid adds plant extract to reach above effect.

Chinese patent application 201310561303.6 discloses a kind of purple perilla hand sanitizer, and this handwashing liquid is extracted by Folium Perillae Thing, fatty alcohol-polyoxyethylene ether phosphate monoester, dodecyltriethanolamine sulfate, glyceryl monostearate, glycerol and biology are anti- Microbial inoculum forms, and wherein biological antibiosis agent is patchouli alcohol and aloe-emodin, has fungistatic effect obvious, the effect of safety and Health Really.Chinese patent application 201310453878.6 discloses a kind of Pure natural antibacterial hand sanitizer, this handwashing liquid by aloe extraction liquid, Radix et Caulis Opuntiae Dillenii extract, lanoline, tea seed cake extract cocos nucifera oil, amido propyl betaine, glycerol, cocos nucifera oil, sodium carboxymethyl cellulose, dry Ligustrum lucidum Ait fruit, fresh Folium Cinnamomi porrecti, tetraoxygen lauryl alcohol ether, polyvinyl alcohol form, and this handwashing liquid has strong detergency, fragrance is held For a long time, avirulence, non-stimulated to skin, with rear feel smooth comfortable, have the function of sterilization concurrently.

But, the handwashing liquid of above interpolation plant extract mainly stresses antibacterial effect, be short of to the nursing washing rear both hands, Lacking antiallergic to releive, improve the effects such as hand microcirculation, after causing washing one's hands, being dried easily occur in both hands, the phenomenon of decortication.Therefore, grind Study carefully when exploitation is a kind of washes one's hands and can produce sliding and oiliness sense of touch, protective layer can be formed at skin surface after washing, protect skin, have Effect plays the effects such as antiinflammatory, antibacterial, antiallergic is releived, and has and improve the microcirculatory function of hand, and preservative free adds, non-stimulated The handwashing liquid of property is current research direction.

Summary of the invention

Easily occur doing to both hands after washing the nursing of rear hand, causing washing one's hands to solve the handwashing liquid shortcoming of prior art Dry, the defect of the phenomenon of decortication, it is an object of the invention to provide a kind of anti-bacterial hand lotion and preparation method thereof, more than solving Defect.

The present invention provides a kind of anti-bacterial hand lotion, and this handwashing liquid includes following components and percentage by weight thereof: poly alkyl alcohol Oxygen vinyl Ether sodium sulfate 6.0-8.0%, cocamido propyl betaine 6.0-8.0%, alkyl polyglucoside 1.0-3.0%, polyquaternary ammonium salt 0.05-0.3%, fatty glyceride 0.08-3.0%, wetting agent 2.0-4.0%, mixed plant extract 0.05-2.0%, ethylenediamine Tetraacethyl four sodium 0.05-2.0%, sodium chloride 0.01-2.0%, citric acid 0.05-0.3%, Jojoba oil 0.01-0.1%, 1,2-penta Glycol 0.1-2.0%, essence 0.1-1.0%, water 65.0-84.5%.

The preferred formula of anti-bacterial hand lotion of the present invention includes following components and percentage by weight thereof: aliphatic alcohol polyethenoxy Ether sodium sulfate 7.0%, cocamido propyl betaine 7.0%, alkyl polyglucoside 2.0%, polyquaternary ammonium salt 0.1%, fatty glyceride 1%, Wetting agent 3.0%, mixed plant extract 1.0%, tetrasodium ethylenediamine tetraacetate 1.0%, sodium chloride 0.5%, citric acid 0.1%, flash Bar oil 0.05%, 1,2-pentanediol 0.5%, essence 0.2%, water 76.55%.

Further, described fatty glyceride is glycerol monostearate, stearic acid double glyceride, decanoyl/octanoyl glycerides With the one in tripalmitin, preferably decanoyl/octanoyl glycerides.

In the anti-bacterial hand lotion of the present invention, alkyl polyglucoside is Dodecyl Glucoside, Dodecyl Glucoside be surface tension low, Without cloud point, wetting power is strong, detergency is notable, non-stimulated to skin, biodegradation is thorough rapidly, can be with any type surface activity Agent compounds, and cooperative effect is obvious, the significant advantage of thickening effect, is a kind of comprehensive green surfactant of performance.

Preferably, in the anti-bacterial hand lotion of the present invention, polyquaternary ammonium salt is polyquaternary ammonium salt-7.

Wherein, described wetting agent is mixed by sodium lactate, PEG-7 olive oil acid esters and glycerol 1-3:1-2:1-3 by volume It is combined into, the volume ratio more preferably 1:1:1 of sodium lactate, PEG-7 olive oil acid esters and glycerol, sodium lactate, PEG-7 olive The wetting agent of olive oleate and glycerol 1:1:1 by volume mixing composition has skin moistening skin protection, after being possible to prevent to use handwashing liquid Xerosis cutis, the effect of the phenomenon of decortication.Wherein, PEG-7 olive oil acid esters, English name is PEG-7 OLIVATE, is purchased from Biochemical corp of Hugezeal Bio-chemical Australia Inc(Australia).

In the anti-bacterial hand lotion of the present invention, mixed plant extract is extracted by Radix Astragali extract, camomile extract, Rhizoma Zingiberis Recens Thing, Herba Plantaginis extract and Flos Nelumbinis extract 0.5-2:1-3:1-3:0.5-2:0.5-2 in mass ratio mixes composition, and mass ratio enters One step is preferably 1:1:2:1:1.Wherein Radix Astragali extract (Astragalus membranaceous), Herba Plantaginis extract (Pkabtagi kabceikata) and Flos Nelumbinis extract (Pkabtagi kabceikata) be purchased from receive Tu Ruikesi commerce and trade (on Sea) company limited, camomile extract (Extrapone Camomile Special) is purchased from fragrant (Shanghai) Co., Ltd. of moral, Rhizoma Zingiberis Recens extract (Extrapone Camomile Special) is purchased from Lang De company of Korea S hundred.This mixed plant extract has Antibiotic and sterilizing, antiallergic is releived, and improves hand microcirculation, the effect of antiinflammatory.

It addition, present invention also offers a kind of method preparing anti-bacterial hand lotion, comprise the following steps:

(1) it is initially charged the water dissolution polyoxyethylenated alcohol sodium sulfate of each component total amount 70-80%, cocamidopropyl propyl amide Glycine betaine and fatty glyceride, stirring is to being completely dissolved;

(2) add mix in container by Jojoba oil, polyquaternary ammonium salt, wetting agent and alkyl polyglucoside and stir, will mix Uniform mixed liquor adds the mixed liquor mixing of step (1), and rinses mixing container with the water of surplus, and flushing water adds step in the lump Suddenly in the mixed liquor of (1);

(3) mixed liquor obtained toward step (2) add mixed plant extract, tetrasodium ethylenediamine tetraacetate, citric acid, 1, 2-pentanediol and essence, stir;

(4) being added by sodium chloride in the mixed liquor of step (3), adjustment liquid viscosity is 2000-3000mPa.s, to obtain final product.

The anti-bacterial hand lotion of the present invention is with polyoxyethylenated alcohol sodium sulfate as primary surfactant, with coconut oleoyl amine third Base glycine betaine, alkyl polyglucoside and fatty glyceride are as cosurfactant, primary surfactant and cosurfactant Agent compatibility is reasonable, is formed and removes grease and go dirt ability strong, foaming abundancy and stablize, flexibility is good, little to skin irritation, life The solution that thing degradability is good.It addition, the handwashing liquid of the present invention with the addition of the natural of sodium lactate, PEG-7 olive oil acid esters and glycerol Moisturizing ingredient and polyquaternary ammonium salt-7, have the effect of skin protection skin moistening to skin after washing one's hands, is possible to prevent to use both hands after handwashing liquid What skin became is dried, the phenomenon even peeled.

The anti-bacterial hand lotion of the present invention also added mixed plant extract, makes handwashing liquid have antibacterial bacteriostatic, and antiallergic relaxes Slow, antiinflammatory, improves hand microcirculation, and effectively keeps the both hands resistivity to antibacterial, and this mixed plant extracts Thing and 1,2-pentanediol has mixed anti-corrosive antibacterial effect, is possible to prevent and suppresses the growth of handwashing liquid antibacterial, extends depositing of product Put the time limit, and this preservative is non-stimulated to skin, nontoxic, it is a kind of environmental protection, the preservative of safety.

Each component compatibility of anti-bacterial hand lotion of the present invention is reasonable, forms antibacterial effect obvious, skin protection skin moistening effect notable and Handwashing liquid to the safety and environmental protection of no skin irritation.

Compared with prior art, the anti-bacterial hand lotion of the present invention has the advantage that

(1) anti-bacterial hand lotion surfactant compatibility of the present invention is reasonable, and dirt-removing power is strong, and biological degradability is good, Er Qietian Add natural moisture preserving agent, skin is had significant skin protection soothing effect;

(2) anti-bacterial hand lotion of the present invention is also added with mixed plant extract, makes handwashing liquid have antibacterial bacteriostatic, and antiallergic relaxes Slow, antiinflammatory, improves the microcirculatory effect of hand, and effectively keeps the both hands resistivity to antibacterial, and this mixed plant carries Taking thing and 1,2-pentanediol has mixed anti-corrosive antibacterial effect, is possible to prevent and suppresses the growth of handwashing liquid antibacterial, extends product Deposit the time limit.

Detailed description of the invention:

Below by way of the description of detailed description of the invention, the invention will be further described, but this is not the limit to the present invention System, those skilled in the art are according to the basic thought of the present invention, and various modifications may be made or improves, but without departing from this The basic thought of invention, the most within the scope of the present invention.

Embodiment 1, the anti-bacterial hand lotion of the present invention

Handwashing liquid includes following components and percentage by weight thereof:

Polyoxyethylenated alcohol sodium sulfate 6.0%, cocamido propyl betaine 6.0%, alkyl polyglucoside 1.0%, polyquaternary amine Salt 0.01%, fatty glyceride 0.1%, wetting agent 2.0%, mixed plant extract 0.1%, tetrasodium ethylenediamine tetraacetate 0.05%, Sodium chloride 0.01%, citric acid 0.05%, Jojoba oil 0.01%, 1,2-pentanediol 0.1%, essence 0.1%, water 84.47%, described Wetting agent is mixed by sodium lactate, PEG-7 olive oil acid esters and glycerol 2:1:2 by volume and forms, and described mixed plant extracts Thing is by Radix Astragali extract, camomile extract, Rhizoma Zingiberis Recens extract, Herba Plantaginis extract and Flos Nelumbinis extract 0.5:1 by volume: 1:0.5:0.5 mixes composition.

Preparation method:

(1) water dissolution polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and the fat of 700g it are initially charged Acid glyceride, stirring is to being completely dissolved;

(2) add to mix in container by 0.1g Jojoba oil, 0.1g polyquaternary ammonium salt, 20g wetting agent and 10g alkyl polyglucoside and stir Mix uniformly, the mixed liquor of mix homogeneously is added the mixed liquor mixing of step (1), and rinses mixing container, punching with the water of surplus Wash water adds in the mixed liquor of step (1) in the lump;

(3) mixed liquor obtained toward step (2) add 1g mixed plant extract, 0.5g tetrasodium ethylenediamine tetraacetate, 0.5g citric acid, 1g1,2-pentanediol and 1g essence, stir;

(4) it is 2000mPa.s that 0.1g sodium chloride adds adjustment liquid viscosity in the mixed liquor of step (3), to obtain final product.

Embodiment 2, the anti-bacterial hand lotion of the present invention

Handwashing liquid includes following components and percentage by weight thereof:

Polyoxyethylenated alcohol sodium sulfate 7.0%, cocamido propyl betaine 7.0%, alkyl polyglucoside 2.0%, polyquaternary amine Salt 0.1%, fatty glyceride 1%, wetting agent 3.0%, mixed plant extract 1.0%, tetrasodium ethylenediamine tetraacetate 1.0%, chlorination Sodium 0.5%, citric acid 0.1%, Jojoba oil 0.05%, 1,2-pentanediol 0.5%, essence 0.2%, water 76.55%, described wetting agent Being mixed by sodium lactate, PEG-7 olive oil acid esters and glycerol 1:1:1 by volume and form, described mixed plant extract is by Huang Stilbene extract, camomile extract, Rhizoma Zingiberis Recens extract, Herba Plantaginis extract and Flos Nelumbinis extract 1:1:2:1:1 by volume mixes It is combined into.

Preparation method such as embodiment 1.

Embodiment 3, the anti-bacterial hand lotion of the present invention

Handwashing liquid includes following components and percentage by weight thereof:

Polyoxyethylenated alcohol sodium sulfate 8.0%, cocamido propyl betaine 8.0%, alkyl polyglucoside 2.0%, polyquaternary amine Salt 0.3%, fatty glyceride 2.0%, wetting agent 4.0%, mixed plant extract 2.0%, tetrasodium ethylenediamine tetraacetate 2.0%, chlorine Change sodium 1.0%, citric acid 0.3%, Jojoba oil 0.1%, 1,2-pentanediol 2.0%, essence 1.0%, water 67.3%, described wetting agent Being mixed by sodium lactate, PEG-7 olive oil acid esters and glycerol 3:2:3 by volume and form, described mixed plant extract is by Huang Stilbene extract, camomile extract, Rhizoma Zingiberis Recens extract, Herba Plantaginis extract and Flos Nelumbinis extract 2:3:3:2:2 by volume mixes It is combined into.

Preparation method such as embodiment 1.

Comparative example one, a kind of anti-bacterial hand lotion

Handwashing liquid composition:

The content of polyoxyethylenated alcohol sodium sulfate is 14.0%, and the content of cocamido propyl betaine is 0, remaining Composition and preparation method such as embodiment 2.

Comparative example two, a kind of anti-bacterial hand lotion

Handwashing liquid composition:

The content of polyoxyethylenated alcohol sodium sulfate is 8.5%, and the content of cocamido propyl betaine is 8.5%, its Remaining composition and preparation method such as embodiment 2.

Comparative example three, a kind of anti-bacterial hand lotion

Handwashing liquid composition:

The content of 1,2-pentanediol is 0, and the content of mixed plant extract is 1.5%, and remaining composition and preparation method are strictly according to the facts Execute example 2.

Test example 1, the pH value of anti-bacterial hand lotion of the present invention and biological degradability determination test

1, subjects: prepared by the embodiment of the present invention 1, embodiment 2, embodiment 3, comparative example one and comparative example two antibacterial Handwashing liquid.

2, test method:

2.1, the embodiment of the present invention 1, embodiment 2, embodiment 3, comparative example one and are tested by the method for testing of GB/T6368 The pH value of the anti-bacterial hand lotion of comparative example two preparation, test temperature is 25 DEG C, implements with the distilled water configuration newly boiled and cool down Example 1-3 and the anti-bacterial hand lotion of comparative example one-two preparation, mass concentration is 1:10, and mixing can measure the pH of anti-bacterial hand lotion Value.

2.2, embodiment 1, embodiment 2, embodiment 3, comparative example one and comparative example two are measured according to the method for GB/T15818 The surfactant biodegradation of the anti-bacterial hand lotion of preparation.

3, result of the test: result of the test is as shown in table 1.

The pH value test result of table 1 anti-bacterial hand lotion of the present invention

Index Embodiment 1 Embodiment 2 Embodiment 3 Comparative example one Comparative example two PH value 6.3 6.5 6.8 6.5 7.0 Biological degradability % 94 97 95 90 91

The pH value of anti-bacterial hand lotion prepared by the present invention is all in the range of 4.0-10.0, basic to skin after absorption of human body Nonirritant, the biological degradability of the surfactant used by the anti-bacterial hand lotion of the present invention is all higher than 90%, is a kind of decontamination energy Power is strong, the handwashing liquid that biological degradability is good.

Test example 2, the bactericidal assay of anti-bacterial hand lotion of the present invention

1, subjects: the embodiment of the present invention 1, embodiment 2, embodiment 3 and the anti-bacterial hand lotion of comparative example three preparation.

2, test method: measured the embodiment of the present invention 1 by GB/15979-2002 appendix C in the method for testing of regulation, implement Example 2, embodiment 3 and the anti-bacterial hand lotion of comparative example three preparation.

3, result of the test: result of the test is as shown in table 2.

The bactericidal assay result of table 2 anti-bacterial hand lotion of the present invention

The sterilizing rate of the anti-bacterial hand lotion of the present invention is all higher than 90%, is added with mixed plant extract and 1,2-pentanediol Handwashing liquid anti-corrosive antibacterial effect notable, be possible to prevent and suppress the growth of handwashing liquid antibacterial, extend product deposits the time limit.

Claims (5)

1. an anti-bacterial hand lotion, it is characterised in that be made up of following components and percentage by weight thereof:
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%, cocamido propyl betaine 6.0-8.0%, alkyl polyglucoside 1.0- 3.0%, polyquaternary ammonium salt 0.05-0.3%, fatty glyceride 0.08-3.0%, wetting agent 2.0-4.0%, mixed plant extract Thing 0.05-2.0%, tetrasodium ethylenediamine tetraacetate 0.05-2.0%, sodium chloride 0.01-2.0%, citric acid 0.05-0.3%, suddenly Bar oil 0.01-0.1%, 1,2-pentanediol 0.1-2.0%, essence 0.1-1.0%, water 65.0-84.5% suddenly;Described wetting agent by Sodium lactate, PEG-7 olive oil acid esters and glycerol 1-3:1-2:1-3 by volume mixing composition, described mixed plant extract by Radix Astragali extract, camomile extract, Rhizoma Zingiberis Recens extract, Herba Plantaginis extract and Flos Nelumbinis extract 0.5-2:1-3 in mass ratio: 1-3:0.5-2:0.5-2 mixes composition;Described fatty glyceride is glycerol monostearate, stearic acid double glyceride, the pungent last of the ten Heavenly stems One in acid glyceride and tripalmitin;Described alkyl polyglucoside is Dodecyl Glucoside;Described polyquaternary ammonium salt is poly-season Ammonium salt-7.
2. anti-bacterial hand lotion as claimed in claim 1, it is characterised in that be made up of following components and percentage by weight thereof:
Polyoxyethylenated alcohol sodium sulfate 7.0%, cocamido propyl betaine 7.0%, alkyl polyglucoside 2.0%, polyquaternary amine Salt 0.1%, fatty glyceride 1.0%, wetting agent 3.0%, mixed plant extract 1.0%, tetrasodium ethylenediamine tetraacetate 1.0%, sodium chloride 0.5%, citric acid 0.1%, Jojoba oil 0.05%, 1,2-pentanediol 0.5%, essence 0.2%, water 76.55%.
3. anti-bacterial hand lotion as claimed in claim 1, it is characterised in that described wetting agent is by sodium lactate, PEG-7 Fructus Canarii albi oleic acid Ester and glycerol 1:1:1 by volume mixes composition.
4. anti-bacterial hand lotion as claimed in claim 1, it is characterised in that described mixed plant extract by Radix Astragali extract, Camomile extract, Rhizoma Zingiberis Recens extract, Herba Plantaginis extract and Flos Nelumbinis extract 1:1:2:1:1 in mass ratio mixes composition.
5. the preparation method of an anti-bacterial hand lotion as claimed in claim 1, it is characterised in that comprise the following steps: (1) is first Add water dissolution polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and the fat of each component total amount 70-80% Acid glyceride, stirring is to being completely dissolved;
(2) add to mix in container by Jojoba oil, polyquaternary ammonium salt, wetting agent and alkyl polyglucoside and stir, by mix homogeneously Mixed liquor add in the mixed liquor of step (1) and mix, and rinse with the water of surplus and mix container, flushing water adds step in the lump (1) in mixed liquor;
(3) mixed liquor obtained toward step (2) adds mixed plant extract, tetrasodium ethylenediamine tetraacetate, citric acid, 1,2-penta Glycol and essence, stir;
(4) being added by sodium chloride in the mixed liquor of step (3), adjustment liquid viscosity is 2000-3000mPa.s, to obtain final product.
CN201510216598.2A 2015-04-30 2015-04-30 A kind of anti-bacterial hand lotion and preparation method thereof CN104825356B (en)

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CN104434698B (en) * 2014-12-16 2018-02-09 皖南医学院 A kind of antistatic, radiation proof hair cream and preparation method thereof

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CN106983675A (en) * 2017-03-19 2017-07-28 长沙协浩吉生物工程有限公司 A kind of compound method of ferment hand cleanser

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