CN104609453A - 一种立方状沉淀碳酸钙的制备方法 - Google Patents
一种立方状沉淀碳酸钙的制备方法 Download PDFInfo
- Publication number
- CN104609453A CN104609453A CN201410685357.8A CN201410685357A CN104609453A CN 104609453 A CN104609453 A CN 104609453A CN 201410685357 A CN201410685357 A CN 201410685357A CN 104609453 A CN104609453 A CN 104609453A
- Authority
- CN
- China
- Prior art keywords
- calcium carbonate
- carbonation reaction
- preparation
- gained
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 173
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 229940088417 precipitated calcium carbonate Drugs 0.000 title abstract 3
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 79
- 238000006243 chemical reaction Methods 0.000 claims abstract description 34
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 238000001035 drying Methods 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 230000005587 bubbling Effects 0.000 claims abstract description 9
- 238000010298 pulverizing process Methods 0.000 claims abstract description 9
- 239000011541 reaction mixture Substances 0.000 claims abstract description 9
- 230000032683 aging Effects 0.000 claims description 19
- 239000012756 surface treatment agent Substances 0.000 claims description 16
- 239000011159 matrix material Substances 0.000 claims description 15
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 14
- 239000004202 carbamide Substances 0.000 claims description 14
- 108010046334 Urease Proteins 0.000 claims description 13
- 239000000920 calcium hydroxide Substances 0.000 claims description 11
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 11
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 10
- 235000011089 carbon dioxide Nutrition 0.000 claims description 10
- 235000019738 Limestone Nutrition 0.000 claims description 8
- 230000018044 dehydration Effects 0.000 claims description 8
- 238000006297 dehydration reaction Methods 0.000 claims description 8
- 239000006028 limestone Substances 0.000 claims description 8
- 238000000746 purification Methods 0.000 claims description 8
- 238000007670 refining Methods 0.000 claims description 8
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 claims description 8
- 238000004381 surface treatment Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 abstract description 15
- 239000002245 particle Substances 0.000 abstract description 6
- 239000002002 slurry Substances 0.000 abstract description 6
- 238000001723 curing Methods 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 abstract 1
- 235000011941 Tilia x europaea Nutrition 0.000 abstract 1
- 239000006071 cream Substances 0.000 abstract 1
- 239000004571 lime Substances 0.000 abstract 1
- 238000011085 pressure filtration Methods 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 239000013078 crystal Substances 0.000 description 6
- 229920001971 elastomer Polymers 0.000 description 5
- 238000009825 accumulation Methods 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000004033 plastic Substances 0.000 description 4
- 229920003023 plastic Polymers 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 3
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 3
- 229910001424 calcium ion Inorganic materials 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
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CN201410685357.8A CN104609453B (zh) | 2014-11-25 | 2014-11-25 | 一种立方状沉淀碳酸钙的制备方法 |
Applications Claiming Priority (1)
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CN201410685357.8A CN104609453B (zh) | 2014-11-25 | 2014-11-25 | 一种立方状沉淀碳酸钙的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104609453A true CN104609453A (zh) | 2015-05-13 |
CN104609453B CN104609453B (zh) | 2016-08-24 |
Family
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Family Applications (1)
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CN201410685357.8A Active CN104609453B (zh) | 2014-11-25 | 2014-11-25 | 一种立方状沉淀碳酸钙的制备方法 |
Country Status (1)
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107827137A (zh) * | 2017-12-04 | 2018-03-23 | 青州宇信钙业股份有限公司 | 一种大粒径立方状沉淀碳酸钙的制备方法 |
CN109437273A (zh) * | 2018-12-19 | 2019-03-08 | 广西合山市华纳新材料科技有限公司 | 一种单分散立方形沉淀碳酸钙的制备方法 |
CN114291836A (zh) * | 2021-12-31 | 2022-04-08 | 连州市凯恩斯纳米材料有限公司 | 碳酸钙晶型控制剂、其应用、及立方形碳酸钙的制备方法 |
CN114380315A (zh) * | 2021-09-22 | 2022-04-22 | 湖南新绿方药业有限公司 | 一种药用碳酸钙的纯化方法及其生产设备 |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1631789A (zh) * | 2003-12-24 | 2005-06-29 | 上海华明高技术(集团)有限公司 | 纳米级碳酸钙颗粒的制备方法 |
CN1631791A (zh) * | 2004-11-30 | 2005-06-29 | 上海耀华纳米科技有限公司 | 一种超细活性碳酸钙及其制备工艺和应用 |
CN1778934A (zh) * | 2005-10-10 | 2006-05-31 | 东南大学 | 利用微生物沉积制备碳酸钙的方法 |
CN1807252A (zh) * | 2006-01-18 | 2006-07-26 | 内蒙古蒙西纳米材料有限责任公司 | 密封材料专用纳米级活性碳酸钙的制备方法 |
CN101570342A (zh) * | 2009-06-11 | 2009-11-04 | 福建省万旗非金属材料有限公司 | 一种利用低品位石灰石湿法制备硅酮密封胶专用高白度纳米碳酸钙的方法 |
JP2011157700A (ja) * | 2010-01-29 | 2011-08-18 | Ehime Univ | 地盤改良方法 |
CN102295306A (zh) * | 2011-06-14 | 2011-12-28 | 连州市凯恩斯纳米材料有限公司 | 一种连续合成碳酸钙的碳化器及碳酸钙的生产方法 |
CN103663527A (zh) * | 2012-09-25 | 2014-03-26 | 上海华明高技术(集团)有限公司 | 立方形超细碳酸钙颗粒的制备方法 |
US20140239535A1 (en) * | 2010-04-27 | 2014-08-28 | Biomason, Inc. | Methods for Making Construction Materials Using Enzyme Producing Bacteria |
-
2014
- 2014-11-25 CN CN201410685357.8A patent/CN104609453B/zh active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1631789A (zh) * | 2003-12-24 | 2005-06-29 | 上海华明高技术(集团)有限公司 | 纳米级碳酸钙颗粒的制备方法 |
CN1631791A (zh) * | 2004-11-30 | 2005-06-29 | 上海耀华纳米科技有限公司 | 一种超细活性碳酸钙及其制备工艺和应用 |
CN1778934A (zh) * | 2005-10-10 | 2006-05-31 | 东南大学 | 利用微生物沉积制备碳酸钙的方法 |
CN1807252A (zh) * | 2006-01-18 | 2006-07-26 | 内蒙古蒙西纳米材料有限责任公司 | 密封材料专用纳米级活性碳酸钙的制备方法 |
CN101570342A (zh) * | 2009-06-11 | 2009-11-04 | 福建省万旗非金属材料有限公司 | 一种利用低品位石灰石湿法制备硅酮密封胶专用高白度纳米碳酸钙的方法 |
JP2011157700A (ja) * | 2010-01-29 | 2011-08-18 | Ehime Univ | 地盤改良方法 |
US20140239535A1 (en) * | 2010-04-27 | 2014-08-28 | Biomason, Inc. | Methods for Making Construction Materials Using Enzyme Producing Bacteria |
CN102295306A (zh) * | 2011-06-14 | 2011-12-28 | 连州市凯恩斯纳米材料有限公司 | 一种连续合成碳酸钙的碳化器及碳酸钙的生产方法 |
CN103663527A (zh) * | 2012-09-25 | 2014-03-26 | 上海华明高技术(集团)有限公司 | 立方形超细碳酸钙颗粒的制备方法 |
Non-Patent Citations (3)
Title |
---|
IVAN SONDI, ET AL.: ""Homogeneous precipitation of calcium carbonates by enzyme catalyzed reaction"", 《JOURNAL OF COLLOID AND INTERFACE SCIENCE》 * |
张晓艳: ""纳米碳酸钙粒子改性环氧树脂胶粘剂性能研究"", 《复合材料加工》 * |
张生生等: ""碳化法制备超细碳酸钙反应中凝胶现象的研究"", 《中国粉体技术》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107827137A (zh) * | 2017-12-04 | 2018-03-23 | 青州宇信钙业股份有限公司 | 一种大粒径立方状沉淀碳酸钙的制备方法 |
CN109437273A (zh) * | 2018-12-19 | 2019-03-08 | 广西合山市华纳新材料科技有限公司 | 一种单分散立方形沉淀碳酸钙的制备方法 |
CN109437273B (zh) * | 2018-12-19 | 2020-09-08 | 广西合山市华纳新材料科技有限公司 | 一种单分散立方形沉淀碳酸钙的制备方法 |
CN114380315A (zh) * | 2021-09-22 | 2022-04-22 | 湖南新绿方药业有限公司 | 一种药用碳酸钙的纯化方法及其生产设备 |
CN114380315B (zh) * | 2021-09-22 | 2024-01-26 | 湖南新绿方药业有限公司 | 一种药用碳酸钙的纯化方法及其生产设备 |
CN114291836A (zh) * | 2021-12-31 | 2022-04-08 | 连州市凯恩斯纳米材料有限公司 | 碳酸钙晶型控制剂、其应用、及立方形碳酸钙的制备方法 |
CN114291836B (zh) * | 2021-12-31 | 2023-09-19 | 连州市凯恩斯纳米材料有限公司 | 碳酸钙晶型控制剂、其应用、及立方形碳酸钙的制备方法 |
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Publication number | Publication date |
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CN104609453B (zh) | 2016-08-24 |
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GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method for cubic precipitated calcium carbonate Effective date of registration: 20190515 Granted publication date: 20160824 Pledgee: Bank of Communications Ltd. the Guangxi Zhuang Autonomous Region branch Pledgor: GUANGXI HUANA NEW MATERIALS TECHNOLOGY Co.,Ltd. Registration number: 2019450000021 |
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CP03 | Change of name, title or address |
Address after: 530103 No.29, Ganwei street, Ganwei Town, Wuming District, Nanning City, Guangxi Zhuang Autonomous Region Patentee after: Guangxi Warner New Material Co.,Ltd. Address before: 530103 No.29, Ganwei street, Ganwei Town, Wuming County, Nanning City, Guangxi Zhuang Autonomous Region Patentee before: GUANGXI HUANA NEW MATERIALS TECHNOLOGY Co.,Ltd. |
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CP03 | Change of name, title or address | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20160824 Pledgee: Bank of Communications Ltd. the Guangxi Zhuang Autonomous Region branch Pledgor: GUANGXI HUANA NEW MATERIALS TECHNOLOGY Co.,Ltd. Registration number: 2019450000021 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |