CN104169249B - 乙酸的制备方法 - Google Patents

乙酸的制备方法 Download PDF

Info

Publication number
CN104169249B
CN104169249B CN201380013825.0A CN201380013825A CN104169249B CN 104169249 B CN104169249 B CN 104169249B CN 201380013825 A CN201380013825 A CN 201380013825A CN 104169249 B CN104169249 B CN 104169249B
Authority
CN
China
Prior art keywords
weight
concentration
acetic acid
water
methyl acetate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
CN201380013825.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN104169249A (zh
Inventor
清水雅彦
三浦裕幸
上野贵史
中岛英彦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daicel Corp
Original Assignee
Daicel Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=49161142&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN104169249(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd
Publication of CN104169249A publication Critical patent/CN104169249A/zh
Application granted granted Critical
Publication of CN104169249B publication Critical patent/CN104169249B/zh
Ceased legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201380013825.0A 2012-03-14 2013-03-12 乙酸的制备方法 Ceased CN104169249B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2012057570 2012-03-14
JP2012-057570 2012-03-14
PCT/JP2013/056766 WO2013137236A1 (ja) 2012-03-14 2013-03-12 酢酸の製造方法

Publications (2)

Publication Number Publication Date
CN104169249A CN104169249A (zh) 2014-11-26
CN104169249B true CN104169249B (zh) 2016-03-30

Family

ID=49161142

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380013825.0A Ceased CN104169249B (zh) 2012-03-14 2013-03-12 乙酸的制备方法

Country Status (13)

Country Link
US (2) US9006483B2 (cg-RX-API-DMAC7.html)
EP (1) EP2826767B2 (cg-RX-API-DMAC7.html)
JP (1) JP6158788B2 (cg-RX-API-DMAC7.html)
KR (1) KR102040693B1 (cg-RX-API-DMAC7.html)
CN (1) CN104169249B (cg-RX-API-DMAC7.html)
BR (1) BR112014022682B1 (cg-RX-API-DMAC7.html)
ES (1) ES2640292T5 (cg-RX-API-DMAC7.html)
IN (1) IN2014DN06541A (cg-RX-API-DMAC7.html)
MX (1) MX343501B (cg-RX-API-DMAC7.html)
MY (2) MY166788A (cg-RX-API-DMAC7.html)
SG (1) SG11201404601QA (cg-RX-API-DMAC7.html)
TW (1) TWI547477B (cg-RX-API-DMAC7.html)
WO (1) WO2013137236A1 (cg-RX-API-DMAC7.html)

Families Citing this family (55)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7820855B2 (en) 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
BR112013014804B1 (pt) 2010-12-15 2019-08-13 Daicel Corp processo para produzir ácido acético, método para inibir a produção de iodeto de hidrogênio, ou aumento da concentração de iodeto de hidrogênio em um vaporizador, em um processo de produção de ácido acético, e processo ou método
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
MX2017004287A (es) * 2014-10-02 2017-07-19 Celanese Int Corp Proceso para la produccion de acido acetico.
ES2807618T3 (es) 2014-11-14 2021-02-23 Celanese Int Corp Procesos para producir ácido acético a partir de un medio de reacción que tiene bajo contenido de yoduro de etilo
EP3218105B1 (en) 2014-11-14 2020-10-14 Celanese International Corporation Processes for improving acetic acid yield by removing iron
CN107108432A (zh) * 2014-11-14 2017-08-29 国际人造丝公司 闪蒸包含乙酸锂的反应介质的方法
US9233907B1 (en) 2014-11-14 2016-01-12 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
US9540304B2 (en) 2014-11-14 2017-01-10 Celanese International Corporation Processes for producing an acetic acid product having low butyl acetate content
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
CN107108430B (zh) 2014-11-14 2019-05-10 国际人造丝公司 具有倾析器控制的生产乙酸的方法
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
CN107108431B (zh) 2014-11-14 2023-02-03 国际人造丝公司 通过引入锂化合物生产乙酸的方法
US9340481B1 (en) 2014-11-14 2016-05-17 Celanese International Corporation Process for flashing a reaction medium comprising lithium acetate
US9458077B2 (en) 2014-11-14 2016-10-04 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
KR102493740B1 (ko) 2015-01-30 2023-01-30 셀라니즈 인터내셔날 코포레이션 아세트산의 제조 방법
RS59401B1 (sr) 2015-01-30 2019-11-29 Celanese Int Corp Postupci proizvodnje sirćetne kiseline
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
CA2976310A1 (en) * 2015-02-25 2016-09-01 Sabic Global Technologies B.V. Process for removing impurities from acetic acid
JP5866051B1 (ja) * 2015-07-01 2016-02-17 セラニーズ・インターナショナル・コーポレーション 酢酸の製造方法
US9382186B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for producing acetic acid
US9382183B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for flashing a reaction medium
US9302974B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
JP5952951B1 (ja) * 2015-07-01 2016-07-13 セラニーズ・インターナショナル・コーポレーション 酢酸の製造方法
KR102702563B1 (ko) 2015-09-29 2024-09-05 주식회사 다이셀 아세트산 제조 방법
SG11201800858SA (en) 2015-09-30 2018-04-27 Daicel Corp Method and apparatus for producing acetic acid
US9416088B1 (en) * 2015-10-02 2016-08-16 Celanese International Corporation Process to produce acetic acid with recycle of water
ES2928708T3 (es) * 2015-10-02 2022-11-22 Celanese Int Corp Proceso para producir ácido acético con reciclaje de agua
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
US9957216B2 (en) 2015-11-13 2018-05-01 Celanese International Corporation Processes for producing acetic acid
SG11201802571YA (en) * 2016-03-01 2018-04-27 Daicel Corp Method for producing acetic acid
WO2018008172A1 (en) * 2016-07-07 2018-01-11 Daicel Corporation Process for producing acetic acid
US10265639B2 (en) 2016-07-07 2019-04-23 Daicel Corporation Process for producing acetic acid
US10428004B2 (en) 2017-01-18 2019-10-01 Daicel Corporation Method for producing acetic acid
MX2019008473A (es) * 2017-01-18 2019-09-18 Daicel Corp Metodo para producir acido acetico.
CN110248920B (zh) 2017-01-18 2022-12-09 株式会社大赛璐 乙酸的制备方法
CN110248921B (zh) * 2017-03-08 2022-12-09 株式会社大赛璐 乙酸的制备方法
US10550058B2 (en) * 2017-03-08 2020-02-04 Daicel Corporation Method for producing acetic acid
KR102328843B1 (ko) * 2017-03-28 2021-11-19 주식회사 다이셀 아세트산의 제조 방법
US10308581B2 (en) 2017-03-28 2019-06-04 Daicel Corporation Method for producing acetic acid
CN107141213A (zh) * 2017-05-24 2017-09-08 北京三聚环保新材料股份有限公司 一种甲醇羰基化合成醋酸的方法
ES2867879T3 (es) 2018-05-15 2021-10-21 Daicel Corp Método de producción de ácido acético
CN110325503B (zh) * 2018-05-29 2023-05-02 株式会社大赛璐 乙酸的制备方法
CN110785397B (zh) * 2018-05-29 2022-12-02 株式会社大赛璐 乙酸的制备方法
WO2019229857A1 (ja) * 2018-05-29 2019-12-05 株式会社ダイセル 酢酸の製造方法
EP3599231B1 (en) 2018-05-29 2021-07-14 Daicel Corporation Acetic acid production method
JP6588656B1 (ja) * 2018-05-29 2019-10-09 株式会社ダイセル 酢酸の製造方法
US10807935B2 (en) 2018-11-02 2020-10-20 Celanese International Corporation Process for continuous acetic acid production
KR102357192B1 (ko) * 2019-08-28 2022-02-07 한국과학기술원 복합 열교환형 다성분 공비 혼합물의 분별증류장치 및 이를 이용한 분별증류방법
KR102673700B1 (ko) * 2021-05-31 2024-06-07 주식회사 엘지화학 이소프로필 알코올 제조방법
US12227693B2 (en) * 2022-09-09 2025-02-18 Saudi Arabian Oil Company Aqueous fluid compositions and barite scale removal therewith

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3791935A (en) * 1971-11-10 1974-02-12 Monsanto Co Purification of carboxylic acids
CN1067372C (zh) * 1995-04-27 2001-06-20 大赛璐化学工业株式会社 制备醋酸的方法
CN100582076C (zh) * 2004-12-06 2010-01-20 大赛璐化学工业株式会社 蒸馏方法

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1350726A (en) 1919-08-05 1920-08-24 Haapanen Henry Waldemar Brake attachment for automobiles
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US4039395A (en) 1975-08-11 1977-08-02 Monsanto Company Purification of acetic acid
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
US4894477A (en) 1986-10-14 1990-01-16 Hoechst Celanese Corporation Process for regenerating a carbonylation catalyst solution to remove corrosion metals and carbonylation of methanol to acetic acid
US5334755A (en) 1992-04-24 1994-08-02 Chiyoda Corporation Process for the production of acetic acid from methanol and carbon monoxide using supported rhodium catalyst
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
US5554790A (en) * 1994-04-04 1996-09-10 Daicel Chemical Industries, Ltd. Process for producing acetic anhydride and acetic acid
JP3244385B2 (ja) 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
US5625095A (en) 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
GB9521501D0 (en) * 1995-10-20 1995-12-20 Bp Chem Int Ltd Process
IN192600B (cg-RX-API-DMAC7.html) 1996-10-18 2004-05-08 Hoechst Celanese Corp
US6211405B1 (en) 1998-10-23 2001-04-03 Celanese International Corporation Addition of iridium to the rhodium/inorganic iodide catalyst system
US6303813B1 (en) 1999-08-31 2001-10-16 Celanese International Corporation Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile
JP2004131389A (ja) * 2002-10-08 2004-04-30 Daicel Chem Ind Ltd カルボン酸の製造方法及び製造システム
US7208624B2 (en) 2004-03-02 2007-04-24 Celanese International Corporation Process for producing acetic acid
JP4489487B2 (ja) * 2004-04-02 2010-06-23 ダイセル化学工業株式会社 ヨウ化水素の分離方法
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
CN101223124B (zh) 2005-07-14 2011-05-04 大赛璐化学工业株式会社 生产羧酸的方法
US7820855B2 (en) * 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
CN102131758A (zh) 2008-06-28 2011-07-20 Aa保费投资公司 用于生产羧酸的组合物及其制备方法和使用方法
US7790920B2 (en) 2008-09-11 2010-09-07 Lyondell Chemical Technology, L.P. Preparation of acetic acid
CN105111067B (zh) 2010-05-18 2018-02-06 国际人造丝公司 通过除去高锰酸盐还原化合物纯化乙酸物流的方法
EP2598467B1 (en) 2010-07-26 2017-09-06 Daicel Corporation Process for producing acetic acid
JP5488358B2 (ja) 2010-09-10 2014-05-14 トヨタ自動車株式会社 内燃機関の制御装置
MY161174A (en) 2010-12-15 2017-04-14 Daicel Corp Process for producing acetic acid
US8629298B2 (en) 2011-02-28 2014-01-14 Lyondell Chemical Technology, L.P. Acetic acid production process
US8637699B2 (en) 2011-04-15 2014-01-28 Lyondell Chemical Technology, L.P. Process for the manufacture of acetic acid
CN102681276B (zh) 2012-02-28 2014-07-09 京东方科技集团股份有限公司 阵列基板及其制造方法以及包括该阵列基板的显示装置
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
US8859810B2 (en) 2012-08-21 2014-10-14 Celanese International Corporation Process for recovering permanganate reducing compounds from an acetic acid production process
ES2807618T3 (es) 2014-11-14 2021-02-23 Celanese Int Corp Procesos para producir ácido acético a partir de un medio de reacción que tiene bajo contenido de yoduro de etilo

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3791935A (en) * 1971-11-10 1974-02-12 Monsanto Co Purification of carboxylic acids
CN1067372C (zh) * 1995-04-27 2001-06-20 大赛璐化学工业株式会社 制备醋酸的方法
CN100582076C (zh) * 2004-12-06 2010-01-20 大赛璐化学工业株式会社 蒸馏方法

Also Published As

Publication number Publication date
EP2826767B2 (en) 2021-03-31
JPWO2013137236A1 (ja) 2015-08-03
MX343501B (es) 2016-11-07
EP2826767A4 (en) 2015-12-23
MY166788A (en) 2018-07-23
CN104169249A (zh) 2014-11-26
MX2014010995A (es) 2014-10-13
US9006483B2 (en) 2015-04-14
USRE48855E1 (en) 2021-12-21
JP6158788B2 (ja) 2017-07-05
KR102040693B1 (ko) 2019-11-05
US20150025270A1 (en) 2015-01-22
BR112014022682B1 (pt) 2020-04-14
KR20140135239A (ko) 2014-11-25
SG11201404601QA (en) 2014-10-30
EP2826767A1 (en) 2015-01-21
EP2826767B1 (en) 2017-08-09
TWI547477B (zh) 2016-09-01
ES2640292T5 (es) 2021-10-14
ES2640292T3 (es) 2017-11-02
TW201348193A (zh) 2013-12-01
WO2013137236A1 (ja) 2013-09-19
MY187113A (en) 2021-09-01
IN2014DN06541A (cg-RX-API-DMAC7.html) 2015-06-12

Similar Documents

Publication Publication Date Title
CN104169249B (zh) 乙酸的制备方法
KR101851035B1 (ko) 아세트산의 제조 방법
KR101879006B1 (ko) 아세트산의 제조 방법
RU2508162C2 (ru) Способ и установка для карбонилирования метанола с обогащенным уксусной кислотой потоком мгновенного испарения
RU2493142C1 (ru) Получение уксусной кислоты посредством карбонилирования с повышенной реакционной способностью и мгновенным испарением
CN103249705B (zh) 乙酸的制造方法
JP5662269B2 (ja) 酢酸の製造方法
US11014867B2 (en) Processes for producing an acetic acid product having low butyl acetate content
EP2150519A1 (en) Method and apparatus for making acetic acid with improved light ends column productivity
TW201302310A (zh) 含有腐蝕金屬污染物之羰基化製程流中胺類化合物之移除
JP6039781B2 (ja) 低いヨウ化エチル含量を有する反応媒体から酢酸を製造する方法
CN106715379B (zh) 用于生产乙酸的方法
US8455685B2 (en) Acetic anhydride production by way of carbonylation with enhanced reaction and flashing
EP3356321B1 (en) Process to produce acetic acid with recycle of water
WO2016076970A1 (en) Processes for producing acetic acid from a reaction medium having low ethyl iodide content
CN110234621A (zh) 乙酸的制备方法
CN110114331A (zh) 乙酸的制备方法
HK1147473A (en) Method and apparatus for making acetic acid with improved purification

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160330

Termination date: 20210312

CF01 Termination of patent right due to non-payment of annual fee
IW01 Full invalidation of patent right

Decision date of declaring invalidation: 20170503

Decision number of declaring invalidation: 32082

Granted publication date: 20160330

IW01 Full invalidation of patent right