Background technology
The mask product of conceptualization is now more and more, and as facial films such as whitening, moisturizing, speckle dispelling, from sales volume, consumer favors the obvious conceptualization facial film of this class effect directivity very much.But consumer, when a large amount of this series products of use, has also proposed some worries to the effect of this series products and security performance.Cleawhite pack as wider in audient's face, some bad producers are in order to reach significant whitening effect, in facial film, add the heavy metals such as plumbous and hydrargyrum, the existence of these heavy metals has the effect that makes skin bleach rapidly really, but heavy metal can cause the discomfort of skin, and life-time service can be accumulated in human body, causes chronic poisoning, the health of serious harm human body.How therefore the mask product of the outstanding safety non-toxic again of a kind of whitening effect, moderate cost be provided, and is that consumer urgently wishes the problem that production firm solves.
Beta glucan is that D-Glucose monomer is by the formed polysaccharide of bond of glycosidic bond.Due to D-Glucose residue in conjunction with the difference of pattern, be divided into each other multiple, can activating macrophage, bite the removings such as neutrophil cell and cause cell to decompose fragment by radiation, can make macrophage distinguish and destroy mutant.
Nicotiamide, i.e. vitamin B
3it is the generally acknowledged skin anti-aging composition in cosmetic dermatology field, more and more by people, paid attention in recent years, its most important effect aspect skin anti-aging is colour of skin dimness, jaundice, the famished look that alleviates and prevent skin to produce in aging course in early days, and the skin care item that contain nicotiamide have extremely strong lock water, moisture-keeping efficacy.Large-scale medicine clinical research proves: only have the concentration nicotiamide using more than 5% just to have above-mentioned effect.But niacinamide content, at more than 5% skin-protection product, easily causes most user skin allergy.Therefore how making mask product have whitening skin and preserving moisture effect, can guarantee that again the content of nicotiamide is lower than 5%, is the problem that needs primary study.
Soybean isoflavone is a kind of in flavone compound, mainly be present in leguminous plant, because be extracts from plant, there is analog structure with estrogen, therefore soybean isoflavone claims again phytoestrogen, can make up the defect of women's estrogen hyposecretion after 30 years old, improves moisture of skin and elasticity situation, alleviate climacteric syndrome and improve osteoporosis, making women reproduce youth glamour.
Hesperidin is flavanone glycosides compound, is that hesperetin is combined the glycoside forming with glucose and rhamnose.Hesperidin has the osmotic pressure of maintaining, and strengthens the effects such as blood capillary toughness, can be used as the Natural antioxidant in cosmetic industry.
Anthocyanidin is the antidotal supplementary of pure natural, and anthocyanidin, in Europe, is called as " oral cosmetics for skin ", especially vaccinium oxycoccus pigment, skin nutrition, strengthens skin immunization power, tackling various allergic conditions, is the most effective antioxidant of current nature.It not only can prevent generating ahead of time of wrinkle of skin, also can maintain that normal cell links, blood vessel stable, strengthen capillary vessel circulation, improve flowing of blood capillary and vein, and then reach the rapid healing of abnormal skin.
Formulated together by these material sciences how, and fully play the effect of various materials, makes a performance gentleness, antiallergic, anti-aging clean white moisture saver mask, is problem to be solved by this invention.
Summary of the invention
The object of the invention is to the deficiency existing for existing whitening moisturizing face masque, a kind of clean white moisture saver mask and preparation technology thereof are provided.This facial film whitening skin and preserving moisture is remarkably productive, and materials safety is nontoxic, and preparation technology is simple, is suitable for batch production.
For achieving the above object, the present invention adopts following technical scheme:
A clean white moisture saver mask, is divided into A agent and B agent, and described its component of A agent is counted by mass fraction: glycerol 5-15%, hyaluronate sodium 0.1-1.0%, beta glucan 1.0-10.0%, Flos Jasmini Sambac extract 1.0-9.0%, Radix Glycyrrhizae extract 1.0-9.0%, nicotiamide 1.0-
3.0%, vitamin B
60.1-1.0%, Hesperidin 0.1-1.0%, soybean isoflavone 0.3-1.0%, light Radix Glycyrrhizae pyridine 0.1-0.5%, glutathion 0.5-2.0%, phenoxyethanol 0.5-2.0%, vitamin C phosphoric ester sodium 1.0-2.0%, methyl hydroxybenzoate 0.1-0.5%, Margarita extract 1.0-3.0%, surplus is purified water; Above each component mass number sum is 100%;
Described B agent is vaccinium oxycoccus pigment; The quality of B agent is the 0.1-0.5% of A agent.
Described Flos Jasmini Sambac extract main component is volatile oil, extracting method is: dried jasmine flower is pulverized, after alcohol solution dipping 4 ~ 6h with 60 ~ 70wt%, with the ethanol water-bath reflux, extract, 1h of 60 ~ 70wt%, sucking filtration, residue is used the alcohol solution dipping reflux, extract, 30min of 60 ~ 70wt% again, sucking filtration, merges filtrate, centrifugal, centrifugal liquid merges, concentrated.
Described Radix Glycyrrhizae extract main component is flavone compound, the whitening function of Radix Glycyrrhizae extract is mainly by the activity of restraint of tyrosinase and dopachrome interconvertible enzyme (TRP-2), hinders 5, the polymerization of 6-dihydroxy indole, with this, stop melanic formation, thereby reach the effect of skin whitening; There is the composition of sun-proof usefulness to be generally chromocor compound, ultraviolet light and visible ray are all shown to strong absorption.Compare with synthetic sunscreen, Radix Glycyrrhizae extract need not add antioxidant as sunscreen in formula, Diazolidinyl Urea not, and stable absorption ability is strong.
Described Margarita extract main component is flavone compound, and extracting method is by Margarita lixiviate 2 ~ 3 times in 70 ~ 80 ℃ of water, and extracting solution is merged, and filters, and then that filtrate is centrifugal, centrifugal liquid merges, concentrated.
A technique of preparing clean white moisture saver mask as above, the preparation technology of A agent comprises the following steps:
(1) soybean isoflavone is dissolved in 40 ~ 50 ℃ of water, after drop to room temperature, filter standby;
(2) appropriate purified water is added in agitator, is heated to 85 ~ 90 ℃, insulation cools to 35 ~ 40 ℃ after half an hour, under stirring, adds methyl hydroxybenzoate, after dissolving completely, adds hyaluronate sodium, and swelling is complete;
(3) under stirring, add glycerol, beta glucan, Flos Jasmini Sambac extract, Radix Glycyrrhizae extract, nicotiamide, vitamin B
6, Hesperidin, the pyridine of light Radix Glycyrrhizae, glutathion, phenoxyethanol, vitamin C phosphoric ester sodium, Margarita extract, mix homogeneously;
(4) in the solution of step (3), add soybean isoflavone solution, stir mix homogeneously;
(5) after ageing 20 ~ 30h, filter, make the A agent of facial mask liquid.
A kind of using method of clean white moisture saver mask as above is: silkworm silk cloth is soaked in A agent after 5 ~ 7min, adds B agent, then by soaking silkworm silk cloth later, apply face 15 ~ 20min.
Beneficial effect of the present invention is:
(1) generally speaking, when the consumption of nicotiamide surpasses 5% in cosmetics, just have obvious whitening skin and preserving moisture effect, but nicotiamide consumption surpasses 5%, the skin of most people is easily irritated; But the present invention has added soybean isoflavone, Hesperidin, nicotiamide (B in facial film simultaneously
3), vitamin B
6deng, flavone compound and nicotiamide (B
3), vitamin B
6combine, there is synergism, can significantly strengthen whitening effect, and because the synergism between material, when reaching identical whitening effect, the consumption of nicotiamide has significantly reduced, and has so just greatly reduced the risk that this mask product makes application on human skin allergy;
(2) raw material sources safety of the present invention, Flos Jasmini Sambac, Radix Glycyrrhizae, the Margarita of pure natural of take is raw material, its extract is made an addition in facial film, be equipped with again the soybean isoflavone of the title that have " phytoestrogen ", and the vaccinium oxycoccus pigment that have the title of " oral cosmetics ", make facial film performance gentle, to skin without injury;
(3) vaccinium oxycoccus pigment, as antidotal nutrient, can be absorbed fast by skin, performance effect; This is separately packed A agent and B agent, remixes together during use; So more can give prominence to the effect of vaccinium oxycoccus pigment, use more scientific and effective, effect Yi Gengjia.
The specific embodiment
The present invention further illustrates the present invention with the following example, but protection scope of the present invention is not limited to the following example.
embodiment 1
A clean white moisture saver mask, is divided into A agent and B agent, and described its component of A agent is counted by mass fraction: glycerol 5%, hyaluronate sodium 0.1%, beta glucan 5.0%, Flos Jasmini Sambac extract 4.0%, Radix Glycyrrhizae extract 4.0%, nicotiamide 2.0%, vitamin B
60.5%, Hesperidin 0.5%, soybean isoflavone 0.6%, light Radix Glycyrrhizae pyridine 0.3%, glutathion 1.0%, phenoxyethanol 0.5%, vitamin C phosphoric ester sodium 1.0%, methyl hydroxybenzoate 0.3%, Margarita extract 1.0%, surplus is purified water; Above each component mass number sum is 100%;
Described B agent is vaccinium oxycoccus pigment; The quality of B agent is 0.1% of A agent.
Described Flos Jasmini Sambac extract main component is volatile oil, extracting method is: dried jasmine flower is pulverized, after alcohol solution dipping 4h with 60wt%, with the ethanol water-bath reflux, extract, 1h of 60wt%, sucking filtration, residue is used the alcohol solution dipping reflux, extract, 30min of 60wt% again, sucking filtration, merges filtrate, centrifugal, centrifugal liquid merges, concentrated;
Described Radix Glycyrrhizae extract main component is flavone compound, the whitening function of Radix Glycyrrhizae extract is mainly by the activity of restraint of tyrosinase and dopachrome interconvertible enzyme (TRP-2), hinders 5, the polymerization of 6-dihydroxy indole, with this, stop melanic formation, thereby reach the effect of skin whitening; There is the composition of sun-proof usefulness to be generally chromocor compound, ultraviolet light and visible ray are all shown to strong absorption.Compare with synthetic sunscreen, Radix Glycyrrhizae extract need not add antioxidant as sunscreen in formula, Diazolidinyl Urea not, and stable absorption ability is strong.Radix Glycyrrhizae extracting method is: extracting liquorice powder 1g, the 40ml that adds diethyl ether, reflux 1 hour, filter, medicinal residues add methanol 30ml, reflux 1 hour, filter, filtrate evaporate to dryness, residue adds water 40ml to be made to dissolve, and uses n-butanol extraction 3 times, each 20ml, merge n-butyl alcohol liquid, wash evaporate to dryness with water 3 times.
Described Margarita extract main component is flavone compound, and extracting method is by Margarita lixiviate 3 times in 70 ℃ of water, and extracting solution is merged, and filters, and then that filtrate is centrifugal, centrifugal liquid merges, concentrated.
The technique of preparing clean white moisture saver mask as above, the preparation technology of A agent comprises the following steps:
(1) soybean isoflavone is dissolved in 40 ℃ of water, after drop to room temperature, filter standby;
(2) appropriate purified water is added in agitator, is heated to 85 ℃, insulation cools to 35 ℃ after half an hour, under stirring, adds methyl hydroxybenzoate, after dissolving completely, adds hyaluronate sodium, and swelling is complete;
(3) under stirring, add glycerol, beta glucan, Flos Jasmini Sambac extract, Radix Glycyrrhizae extract, nicotiamide, vitamin B
6, Hesperidin, the pyridine of light Radix Glycyrrhizae, glutathion, phenoxyethanol, vitamin C phosphoric ester sodium, Margarita extract, mix homogeneously;
(4) in the solution of step (3), add soybean isoflavone solution, stir mix homogeneously;
(5) after ageing 20h, filter, make the A agent of facial mask liquid.
Using method is: silkworm silk cloth is soaked in A agent after 5min, adds B agent, then by soaking silkworm silk cloth later, apply face 15min.
embodiment 2
A clean white moisture saver mask, is divided into A agent and B agent, and described its component of A agent is counted by mass fraction: glycerol 15%, hyaluronate sodium 0.5%, beta glucan 1.0%, Flos Jasmini Sambac extract 1.0%, Radix Glycyrrhizae extract 9.0%, nicotiamide 1.0%, vitamin B
61.0%, Hesperidin 0.1%, soybean isoflavone 0.3%, light Radix Glycyrrhizae pyridine 0.5%, glutathion 2.0%, phenoxyethanol 1.0%, vitamin C phosphoric ester sodium 1.5%, methyl hydroxybenzoate 0.5%, Margarita extract 2.0%, surplus is purified water; Above each component mass number sum is 100%;
Described B agent is vaccinium oxycoccus pigment; The quality of B agent is 0.3% of A agent.
The technique of preparing clean white moisture saver mask as above, the preparation technology of A agent comprises the following steps:
(1) soybean isoflavone is dissolved in 50 ℃ of water, after drop to room temperature, filter standby;
(2) appropriate purified water is added in agitator, is heated to 90 ℃, insulation cools to 37 ℃ after half an hour, under stirring, adds methyl hydroxybenzoate, after dissolving completely, adds hyaluronate sodium, and swelling is complete;
(3) under stirring, add glycerol, beta glucan, Flos Jasmini Sambac extract, Radix Glycyrrhizae extract, nicotiamide, vitamin B
6, Hesperidin, the pyridine of light Radix Glycyrrhizae, glutathion, phenoxyethanol, vitamin C phosphoric ester sodium, Margarita extract, mix homogeneously;
(4) in the solution of step (3), add soybean isoflavone solution, stir mix homogeneously;
(5) after ageing 25h, filter, make the A agent of facial mask liquid.
A kind of using method of clean white moisture saver mask as above is: silkworm silk cloth is soaked in A agent after 7min, adds B agent, then by soaking silkworm silk cloth later, apply face 20min.
embodiment 3
A clean white moisture saver mask, is divided into A agent and B agent, and described its component of A agent is counted by mass fraction: glycerol 10%, hyaluronate sodium 1.0%, beta glucan 10.0%, Flos Jasmini Sambac extract 9.0%, Radix Glycyrrhizae extract 1.0%, nicotiamide 3.0%, vitamin B
60.1%, Hesperidin 1.0%, soybean isoflavone 1.0%, light Radix Glycyrrhizae pyridine 0.1%, glutathion 0.5%, phenoxyethanol 2.0%, vitamin C phosphoric ester sodium 2.0%, methyl hydroxybenzoate 0.1%, Margarita extract 3.0%, surplus is purified water; Above each component mass number sum is 100%;
Described B agent is vaccinium oxycoccus pigment; The quality of B agent is 0.5% of A agent.
A technique of preparing clean white moisture saver mask as above, the preparation technology of A agent comprises the following steps:
(1) soybean isoflavone is dissolved in 45 ℃ of water, after drop to room temperature, filter standby;
(2) appropriate purified water is added in agitator, is heated to 87 ℃, insulation cools to 40 ℃ after half an hour, under stirring, adds methyl hydroxybenzoate, after dissolving completely, adds hyaluronate sodium, and swelling is complete;
(3) under stirring, add glycerol, beta glucan, Flos Jasmini Sambac extract, Radix Glycyrrhizae extract, nicotiamide, vitamin B
6, Hesperidin, the pyridine of light Radix Glycyrrhizae, glutathion, phenoxyethanol, vitamin C phosphoric ester sodium, Margarita extract, mix homogeneously;
(4) in the solution of step (3), add soybean isoflavone solution, stir mix homogeneously;
(5) after ageing 30h, filter, make the A agent of facial mask liquid.
A kind of using method of clean white moisture saver mask as above is: silkworm silk cloth is soaked in A agent after 6min, adds B agent, then by soaking silkworm silk cloth later, apply face 17min.
The foregoing is only preferred embodiment of the present invention, all equalizations of doing according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.