CN103494747B - Compound peony skin-caring essential oil and preparation method thereof - Google Patents
Compound peony skin-caring essential oil and preparation method thereof Download PDFInfo
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Abstract
The invention mainly relates to compound peony skin-caring essential oil and a preparation method thereof. The essential oil is composed of the following components in percentage by weight: 80%-90% of basic oil, 5%-10% of flower aroma essential oil, 4%-8% of functional components and 1%-5% of adding components. The preparation method comprises the preparation steps: preparing the basic oil, the flower aroma essential oil, the functional components and the adding components; then mixing, aging and filtering to prepare the peony compound essential oil. The peony compound skin-caring essential oil provided by the invention has the obvious effects of fading stains, reducing melanin sediments, whitening the skin, removing flecks, activating superficial cells of the skin of a human body, reducing wrinkles, delaying aging, preserving moisture and nourishing, isolating ultraviolet light and the like, can effectively improve the symptoms of itching, red and swollen and dry skin, face blisters and the like, has no toxic and side effects, and is applicable to people with various skin types.
Description
Technical field
The invention belongs to peony product deep process technology field, relate generally to a kind of Paeonia suffruticosa compound heal-care essential oil and preparation method thereof.
Background technology
Paeonia suffruticosa originates in the western part of China Qinling Mountains and Daba Mountain one is with mountain area, is perennial machaka, poor growth, and plant type is little.Paeonia suffruticosa is the distinctive woody rare flower of China, has the artificial culture history of the self-sow of thousands of years and more than 2,000 year.Paeonia suffruticosa have " aromatic ", " king's in spending " laudatory title.Paeonia suffruticosa whole body is precious, and Flos Moutan can be for viewing and admiring, and Flos Moutan can also be made peony flower tea, Flos Moutan quintessence oil; Moutan root bark is Chinese medicine " Cortex Moutan "; Paeonia suffruticosa leaf can extract flavone; Peony seed oil contains multiple unsaturated fatty acid, and especially rare odd-numbered fatty acid is a kind of edible oil and fat source that important exploitation is worth that has.On March 22nd, 2011, Ministry of Health of the People's Republic of China approval from phoenix Paeonia suffruticosa (
paeonia ostiit.Hong et J.X.Zhang) and Paeonia papaveracea (
paeonia rockii) the peony seed oil made through techniques such as transmission from one meridian to another squeezing, decolouring, deodorizes of seed core can produce as new resource food and edible [Ministry of Health of the People's Republic of China's bulletin, 2011 No. 9: Ministry of Public Health is the bulletin as new resource food about approval Acer Truncatum Buge seed oil and peony seed oil].
Due to the high nutritive value of peony seed oil, its unsaturated fatty acid content is greater than 80%, wherein three kinds of important unsaturated fatty acids: linolenic acid, the content of linoleic plus oleic acid is respectively: 35.7%, 22.19%, 27.24%.Different from other several base oils, the linolenic acid content of peony seed oil is higher, but oleic acid and linoleic acid content are lower.In peony seed oil, still containing in addition the odd-numbered fatty acid with better active anticancer, is a kind of important oily resource that has exploitation future.
Oleum Vitis viniferae, is a kind of conventional base oil, contains more linoleic acid (content is greater than 70%), and Oleum Vitis viniferae key property is its material such as fatty acid, fructose that contains abundant vitamin, trace mineral, needed by human.The procyanidin that Oleum Vitis viniferae also contains can be protected the elasticity of human vas, and protection human skin is avoided ultraviolet injury etc.Therefore make it have antioxidation, desalination mottle, reduces melanin deposition, skin whitening, removal speckle, activating human body skin cells of superficial layer, reduces the appearance of wrinkle, the effects such as slow down aging.Oleum Vitis viniferae no side effects, adapt to be suitable for crowd comprise child, old people, anemia of pregnant woman or athlete all can, subject range is very wide.
The content of Linoleic Acid in Safflower Oil is greater than 80%, is that in known plants, content is the highest, is therefore described as " king of linoleic acid ".Safflower oil can maintain cell softness, strengthens elasticity and activity, the softness exquisiteness that skin is become, and can promote hair growth.In addition, another feature of safflower oil is in oil, to be rich in natural Vitamin E, and average content, in 800mgDL left and right, is that in all plants, content is the highest, and therefore Flos Carthami is described as " hat of vitamin E ".Vitamin E in safflower oil is pure natural, the natural Vitamin E with vital activity.Vitamin E is a kind of very strong reducing agent, has extremely strong antioxidation.It also has antidotal effect, and aging, old and feeble cell and tissue are got increasingly vigorous.Vitamin E is that one can improve body immunity, eliminates free radical, the nutrient substance of prophylaxis of cancer.
Semen pruni armeniacae oil belongs to neutral base oil, is squeezed and is obtained by apricot fruit, and its main feature is oleic acid content high (content is greater than 70%), and Semen pruni armeniacae oil has opsonic action to pimples skin, and the sensitive skin of rich and honour hands is also had to protection effect.It and any vegetable oil all can be in harmonious proportion mutually, are also therefore the most widely used base oils.Semen pruni armeniacae oil is rich in the materials such as polybasic unsaturated fatty acid, vitamin D, E and protein, can soft skin, moisturizing, crease-resistant, whitening, healing cicatrix, promote tissue regeneration, specially control that skin is itched, red and swollen, dry and pimples.There is good skin-friendly, be applicable to various skin quality, especially easily itch, red and swollen, dry, inflammation, oiliness, anaphylaxis and the most tender and lovely infant skin.Also having the ultraviolet effect of isolation, is also therefore the most widely used base oil.
In unsaturated fatty acid, having some is that mankind itself can not synthesize, and must from food, draw, and is called essential unsaturated fatty acid.Must in unsaturated fatty acid, there be several unsaturated fatty acids extremely important, as linoleic acid, linolenic acid, arachidonic acid etc.Only otherwise lack linoleic acid, just can synthesize in vivo other two kinds must unsaturated fatty acids for human body.Therefore, linoleic acid is most important unsaturated fatty acid in human body, is the basic substance of life.Because unsaturated fatty acid is very easily oxidized, while eating them, should increase in right amount the intake of vitamin E.Linoleic acid has very strong opposing Characteristics of Free Radicals Produced, has splendid aging resistance and helps the multifrequency natures such as vitamin C, E absorption, has the collagen protein in very strong protection human skin, improves the effect such as passages through which vital energy circulates swelling and anti-melanin precipitation.
Alpha-linolenic acid has extremely important effect for the mankind's health.Alpha-linolenic acid is a kind of polyunsaturated fatty acid, is a kind of essential fatty acid.Alpha-linolenic acid is a kind of life core substance, is to form human body brain cell and histiocytic important component, and be a kind of nutrient that the mankind need in life every day.In alpha-linolenic acid molecule, there are three conjugated double bonds; so there is very strong reproducibility; high temperature, airborne oxygen, ultraviolet and some heavy metal ion can be oxidized; therefore being rich in the edible oil of alpha-linolenic acid should lucifuge, sealing is preserved; when use, avoid high temperature frying as far as possible, in oil, add appropriate vitamin E to do protective effect simultaneously.
Paeonol is a kind of extract that derives from moutan root bark, has the effects such as calmness, hypnosis, antibacterial, antiinflammatory, antioxidation, blood pressure lowering.Paeonol can suppress O in cell
2 -free-radical generating, promotes skin of face blood circulation, activates old and feeble epidermis cell, smoothes away wrinkles, and removes speckle, moistening skin beautifying.Can make skin whitening, by fossil pigments Reduction fading in skin, silt dissipating rashes disappears; Also there is the effects such as antiinflammatory, reducing swelling and alleviating pain, antiallergic, antiviral simultaneously.Mottle, myalgia, skin pruritus, psoriasis, zona shingles, eczema are had to good treatment and health-care effect.
Rutin has antioxidation and anti-radical action, is the easily problem of oxidation of unsaturated fatty acid in natural, safe effectively improvement system of antioxidant.Rutin can also effectively absorb the ultraviolet in the sun simultaneously, is good UV absorbent, therefore can be used as sunscreen.
Ursolic acid is a stronger antioxidant, can suppress 5-LO in arachidonic acid metabolic process, Cycloxygenase activity, stops prostaglandin and leukotriene to generate, and this may be the reason of the reaction of ursolic acid inflammation-inhibiting, inhibition lipid peroxide.Defying age, skin speckle dispelling, the dispel pigment of the antioxidation of ursolic acid to human body has positive role.Ursolic acid stable in properties, color and abnormal smells from the patient do not change in time, and have good touch sense, therefore in cosmetics and skincare product, are widely used.
Summary of the invention
The object of this invention is to provide a kind of Paeonia suffruticosa compound heal-care essential oil and preparation method thereof, the effects such as this quintessence oil desalination mottle, reduction melanin deposition, skin whitening, removal speckle, activating human body skin cells of superficial layer, the appearance of minimizing wrinkle, slow down aging, moisturizing, isolation ultraviolet are remarkable, and can effectively improve the diseases such as skin is itched, red and swollen, dry, pimples, nontoxic, have no side effect, be applicable to various skin quality and crowd.
The technical scheme that the present invention realizes above-mentioned purpose employing is: a kind of Paeonia suffruticosa compound heal-care essential oil, made by following composition according to mass percent: base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and adding ingredient 1-5%;
Described base oil is made up of raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight;
Described Rose Absolute is made up of Flos Moutan quintessence oil 50-70 part and Diffuse Coptosapelta flower essential oil 30-50 part according to parts by weight;
Described functional component is according to parts by weight by Cortex Moutan extract 30-40 part, and Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part, obtain after adding four gross weight 2-5 anhydrous alcohol solution doubly; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight.
A preparation method for Paeonia suffruticosa compound heal-care essential oil, comprises the following steps:
The preparation of step 1, base oil
Get raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight, add in reactor, under the condition that first low whipping speed is 60-120r/min, stir 1-5h, add again surfactant, be uniformly mixed, then in 20-30min slow cooling to-5 DEG C, after insulation 4-8h, be slowly warming up to room temperature, then filter with 200 mesh sieves, filter the filtrate obtaining and be base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh peony petal, add its weight 2-7 sodium chloride doubly to stir, pickle 20-100min, then be placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, after dried over anhydrous sodium carbonate, obtain Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get above-mentioned Flos Moutan quintessence oil 50-70 part making according to parts by weight and Diffuse Coptosapelta flower essential oil 30-50 part is placed in agitator, under the condition that low whipping speed is 60-120r/min, stir 1-3h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add its weight 15-20 water doubly to distill, collect distillate, be placed in 2-5 DEG C of refrigerator and leave standstill after 18-24h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add peony petal raw material weight 15-20 ethyl acetate doubly to soak 8-10d, taking out peony petal is placed in the baking oven of 60-80 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; In dry peony petal, add its weight 8-12 edible ethanol doubly, the mass concentration of edible ethanol is 80-95 %, after soaking 8-12d, filter, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, be Flos Moutan extract, for subsequent use;
Get above-mentioned Cortex Moutan extract 30-40 part making, Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part according to parts by weight, then add four gross weight 2-5 dehydrated alcohol doubly to dissolve, obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight, more than stirring 30min under the condition that low whipping speed is 60-120r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to mass percent base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and the adding ingredient 1-5% that step 1 to step 4 obtains, low whipping speed be under the condition of 60-120r/min, stir 2h more than, then ageing 30-60d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
Described peony seed oil is that the seed core of phoenix Paeonia suffruticosa or Paeonia papaveracea obtains through cold press.
The raw material of preparing Flos Moutan quintessence oil in described step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
The surfactant adopting in described step 1 is one or both in the synthetic alkyl polyglucoside of natural fat alcohol and glucose or fatty alcohol-polyoxyethylene ether non-ionic surface active agent.
Beneficial effect of the present invention:
One, the invention provides a kind of taking oil peony seed oil as main foundation oil, Flos Moutan quintessence oil is main Rose Absolute, peony extract is a kind of Paeonia suffruticosa compound heal-care essential oil of major function composition and preparation method thereof, belong to Paeonia suffruticosa deep processing studying technological domain, develop significant to the further further investigation of Paeonia suffruticosa Related product.In peony seed oil, contain abundant linolenic acid, but oleic acid wherein and linoleic acid content are lower, by adding the higher Semen pruni armeniacae oil of oleic acid content, the Oleum Vitis viniferae that linoleic acid content is higher, make the balanced proportion of the fatty acid in this heal-care essential oil, be applicable to human body and use.Add safflower oil not only contain abundant natural Vitamin E, and effectively oil-control go bad.And add Oleum Vitis viniferae, Semen pruni armeniacae oil Flos Carthami seed oil, make this heal-care essential oil desalination mottle, reduce melanin deposition, skin whitening, remove speckle, activating human body skin cells of superficial layer, reducing wrinkle occurs, slow down aging, moisturizing, the effects such as isolation ultraviolet are remarkable, and can effectively improve skin itches, red and swollen, dry, the diseases such as pimples, nontoxic, have no side effect, be applicable to various skin quality and crowd, especially easily itch, red and swollen, dry, inflammation, oiliness, anaphylaxis and the most tender and lovely infant skin, child, old people, anemia of pregnant woman or athlete all can use, applied widely, and effect is remarkable.
Two, two kinds of floral perfumes in this heal-care essential oil, are added, Flos Moutan quintessence oil gives off a strong fragrance, and especially selects the petal of the minority Flos Moutan such as Zhao's pink peony or ROUFURONG Paeonia suffruticosa, and the content of its quintessence oil is lower, production cost is higher, but fragrance uniqueness, fragrant pleasant; Diffuse Coptosapelta flower essential oil fragrance is natural, quality is pure, and add in heal-care essential oil and make quintessence oil lasting at human body skin lasting, lingering, and also these two kinds of quintessence oils also have good antibacterial action.
Three, in the functional component of adding, the effective ingredient that Cortex Moutan extracts is paeonol, has calmness, hypnosis, antibacterial, antiinflammatory, antioxidation, blood pressure lowering, promote skin of face blood circulation, activate old and feeble epidermis cell, smooth away wrinkles, remove speckle, moistening skin beautifying; Flos Moutan extract effective ingredient is flavone, has absorption ultraviolet, the effects such as antioxidation; Rutin and ursolic acid have good antioxidation, can further effectively suppress the oxidation of multiple unsaturated fatty acid in heal-care essential oil, extend the expiration date.Meanwhile, rutin and ursolic acid also have good biological activity: rutin has antioxidation and anti-radical action, can effectively improve skin aging, extend cell ageing, natural, safety; Rutin can also effectively absorb the ultraviolet in the sun, and sun-proof result is remarkable.Defying age, skin speckle dispelling, the dispel pigment of ursolic acid to human body has positive role, and ursolic acid stable in properties, and color and abnormal smells from the patient do not change in time, touches sense good.So, the present invention is to provide a kind of skin protection moisturizing essential oil with whitening, moisturizing, antibacterial, antioxidation and the effect such as free radical resisting, anti-ultraviolet.
Detailed description of the invention
A kind of Paeonia suffruticosa compound heal-care essential oil, is made up of following composition according to mass percent: base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and adding ingredient 1-5%;
Described base oil is made up of raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight;
Described Rose Absolute is made up of Flos Moutan quintessence oil 50-70 part and Diffuse Coptosapelta flower essential oil 30-50 part according to parts by weight;
Described functional component is according to parts by weight by Cortex Moutan extract 30-40 part, and Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part, obtain after adding four gross weight 2-5 anhydrous alcohol solution doubly; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight.
A preparation method for Paeonia suffruticosa compound heal-care essential oil, comprises the following steps:
The preparation of step 1, base oil
Get raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight, add in reactor, under the condition that first low whipping speed is 60-120r/min, stir 1-5h, add again surfactant, be uniformly mixed, then in 20-30min slow cooling to-5 DEG C, after insulation 4-8h, be slowly warming up to room temperature, then filter with 200 mesh sieves, filter the filtrate obtaining and be base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh peony petal, add its weight 2-7 sodium chloride doubly to stir, pickle 20-100min, then be placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, after dried over anhydrous sodium carbonate, obtain Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get above-mentioned Flos Moutan quintessence oil 50-70 part making according to parts by weight and Diffuse Coptosapelta flower essential oil 30-50 part is placed in agitator, under the condition that low whipping speed is 60-120r/min, stir 1-3h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add its weight 15-20 water doubly to distill, collect distillate, be placed in 2-5 DEG C of refrigerator and leave standstill after 18-24h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add peony petal raw material weight 15-20 ethyl acetate doubly to soak 8-10d, taking out peony petal is placed in the baking oven of 60-80 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; In dry peony petal, add its weight 8-12 edible ethanol doubly, the mass concentration of edible ethanol is 80-95 %, after soaking 8-12d, filter, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, be Flos Moutan extract, for subsequent use;
Get above-mentioned Cortex Moutan extract 30-40 part making, Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part according to parts by weight, then add four gross weight 2-5 dehydrated alcohol doubly to dissolve, obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight, more than stirring 30min under the condition that low whipping speed is 60-120r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to mass percent base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and the adding ingredient 1-5% that step 1 to step 4 obtains, low whipping speed be under the condition of 60-120r/min, stir 2h more than, then ageing 30-60d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
Described peony seed oil is that the seed core of phoenix Paeonia suffruticosa or Paeonia papaveracea obtains through cold press.
The raw material of preparing Flos Moutan quintessence oil in described step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
The surfactant adopting in described step 1 is one or both in the synthetic alkyl polyglucoside of natural fat alcohol and glucose or fatty alcohol-polyoxyethylene ether non-ionic surface active agent.
Below in conjunction with specific embodiment, the present invention will be further described:
Embodiment 1:
A kind of Paeonia suffruticosa compound heal-care essential oil, is made up of following composition according to mass percent: base oil 90%, Rose Absolute 5%, functional component 4% and adding ingredient 1%;
Described base oil is made up of 10 parts of 10 parts of Flos Carthami seeds oil of 40 parts of raw material Paeonia ostii peony seed oils, 20 parts of Oleum Vitis viniferaes, Semen pruni armeniacae oil according to parts by weight;
Described Rose Absolute is made up of with 30 parts of Diffuse Coptosapelta flower essential oils 50 parts of tree peony Flos Moutan quintessence oils according to parts by weight;
Described functional component, obtains after adding the anhydrous alcohol solution of 2 times of four gross weights by 10 parts of 30 parts of Cortex Moutan extracts, 30 parts of Flos Moutan extracts, 10 parts of rutins and ursolic acids according to parts by weight; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of with 20 parts of hyaluronic acids 40 parts of glycerol according to parts by weight.
A preparation method for Paeonia suffruticosa compound heal-care essential oil, comprises the following steps:
The preparation of step 1, base oil
Get raw material Paeonia ostii peony seed oil, Oleum Vitis viniferae, Semen pruni armeniacae oil Flos Carthami seed oil according to above-mentioned parts by weight, add in reactor, under the condition that first low whipping speed is 60r/min, stir 1h, add again the synthetic alkyl polyglucoside of surfactant natural fat alcohol and glucose, be uniformly mixed, then in 20min slow cooling to-5 DEG C, after insulation 4h, be slowly warming up to room temperature, then filter with 200 mesh sieves, filter the filtrate obtaining and be base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh tree peony peony petal, add the sodium chloride of 2 times of its weight to stir, pickle 20min, be then placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, and after dried over anhydrous sodium carbonate, obtains Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get the above-mentioned Flos Moutan quintessence oil making according to the parts by weight in above-mentioned formula and Diffuse Coptosapelta flower essential oil is placed in agitator, under the condition that low whipping speed is 60r/min, stir 1h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add the water of 15 times of its weight to distill, collect distillate, be placed in 2 DEG C of refrigerators and leave standstill after 18h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the tree peony peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add the ethyl acetate of 15 times of peony petal raw material weights to soak 8d, taking out peony petal is placed in the baking oven of 60 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; To the edible ethanol that adds 8 times of its weight in dry peony petal, the mass concentration of edible ethanol is 80 %, filters after soaking 8d, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, Flos Moutan extract, for subsequent use;
Get the above-mentioned Cortex Moutan extract making, Flos Moutan extract, rutin and ursolic acid according to the parts by weight in above-mentioned formula, then add the dehydrated alcohol of 2 times of four gross weights to dissolve, obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol and hyaluronic acid according to the parts by weight in above-mentioned formula, more than stirring 30min under the condition that low whipping speed is 60r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to the mass percent in above-mentioned formula base oil, Rose Absolute, functional component and the adding ingredient that step 1 to step 4 obtains, low whipping speed be under the condition of 60r/min, stir 2h more than, then ageing 30d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
Embodiment 2:
A kind of Paeonia suffruticosa compound heal-care essential oil, is made up of following composition according to mass percent: base oil 80%, Rose Absolute 10%, functional component 7.5% and adding ingredient 2.5%;
Described base oil is made up of 20 parts of 20 parts of Flos Carthami seeds oil of 50 parts of raw material Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil, 30 parts of Oleum Vitis viniferaes, Semen pruni armeniacae oil according to parts by weight;
Described Rose Absolute is made up of with 50 parts of Diffuse Coptosapelta flower essential oils 70 parts of ROUFURONG Flos Moutan quintessence oils according to parts by weight;
Described functional component, obtains after adding the anhydrous alcohol solution of 5 times of four gross weights by 20 parts of 40 parts of Cortex Moutan extracts, 40 parts of Flos Moutan extracts, 20 parts of rutins and ursolic acids according to parts by weight; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of with 30 parts of hyaluronic acids 60 parts of glycerol according to parts by weight.
A preparation method for Paeonia suffruticosa compound heal-care essential oil, comprises the following steps:
The preparation of step 1, base oil
Get raw material Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil, Oleum Vitis viniferae, Semen pruni armeniacae oil Flos Carthami seed oil according to the parts by weight in above-mentioned formula, add in reactor, under the condition that first low whipping speed is 120r/min, stir 5h, add again fatty alcohol-polyoxyethylene ether non-ionic surface active agent, be uniformly mixed, then in 30min slow cooling to-5 DEG C, after insulation 8h, be slowly warming up to room temperature, then filter with 200 mesh sieves, filter the filtrate obtaining and be base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh ROUFURONG peony petal, add the sodium chloride of 7 times of its weight to stir, pickle 100min, then be placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, after dried over anhydrous sodium carbonate, obtain Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get 70 parts of the above-mentioned Flos Moutan quintessence oils making according to the parts by weight in above-mentioned formula and be placed in agitator with 50 parts of Diffuse Coptosapelta flower essential oils, under the condition that low whipping speed is 120r/min, stir 3h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add the water of 20 times of its weight to distill, collect distillate, be placed in 5 DEG C of refrigerators and leave standstill after 24h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the ROUFURONG peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add the ethyl acetate of 20 times of peony petal raw material weights to soak 10d, taking out peony petal is placed in the baking oven of 80 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; To the edible ethanol that adds 12 times of its weight in dry peony petal, the mass concentration of edible ethanol is 95 %, filters after soaking 12d, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, Flos Moutan extract, for subsequent use;
Get the above-mentioned Cortex Moutan extract making according to the parts by weight in above-mentioned formula, Flos Moutan extract, rutin and ursolic acid, then add the dehydrated alcohol of 5 times of four gross weights to dissolve, and obtains functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol and hyaluronic acid according to the parts by weight in above-mentioned formula, more than stirring 30min under the condition that low whipping speed is 120r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to the mass percent in above-mentioned formula base oil, Rose Absolute, functional component and the adding ingredient that step 1 to step 4 obtains, low whipping speed be under the condition of 120r/min, stir 2h more than, then ageing 60d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
Embodiment 3:
A kind of Paeonia suffruticosa compound heal-care essential oil, is made up of following composition according to mass percent: base oil 84.5%, Rose Absolute 5%, functional component 6% and adding ingredient 4.5%;
Described base oil is made up of 15 parts of 15 parts of Flos Carthami seeds oil of 45 parts of raw material Paeonia ostii peony seed oils, 25 parts of Oleum Vitis viniferaes, Semen pruni armeniacae oil according to parts by weight;
Described Rose Absolute is made up of with 40 parts of Diffuse Coptosapelta flower essential oils 60 parts of ROUFURONG Flos Moutan quintessence oils according to parts by weight;
Described functional component, obtains after adding the anhydrous alcohol solution of 3.5 times of four gross weights by 15 parts of 35 parts of Cortex Moutan extracts, 35 parts of Flos Moutan extracts, 15 parts of rutins and ursolic acids according to parts by weight; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of with 25 parts of hyaluronic acids 50 parts of glycerol according to parts by weight.
A preparation method for Paeonia suffruticosa compound heal-care essential oil, comprises the following steps:
The preparation of step 1, base oil
Get raw material Paeonia ostii peony seed oil, Oleum Vitis viniferae, Semen pruni armeniacae oil Flos Carthami seed oil according to the parts by weight in above-mentioned formula, add in reactor, under the condition that first low whipping speed is 90r/min, stir 3h, adding mass ratio is the synthetic alkyl glucoside surfactant of natural fat alcohol and glucose of 1:1 again, be uniformly mixed, then in 25min slow cooling to-5 DEG C, after insulation 6h, be slowly warming up to room temperature, then filter with 200 mesh sieves, the filtrate that filtration obtains is base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh ROUFURONG peony petal, add the sodium chloride of 5 times of its weight to stir, pickle 60min, then be placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, after dried over anhydrous sodium carbonate, obtain Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get the above-mentioned Flos Moutan quintessence oil making according to the parts by weight in above-mentioned formula and Diffuse Coptosapelta flower essential oil is placed in agitator, under the condition that low whipping speed is 90r/min, stir 2h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add the water of 18 times of its weight to distill, collect distillate, be placed in 4 DEG C of refrigerators and leave standstill after 21h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the ROUFURONG peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add the ethyl acetate of 18 times of peony petal raw material weights to soak 9d, taking out peony petal is placed in the baking oven of 70 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; To the edible ethanol that adds 10 times of its weight in dry peony petal, the mass concentration of edible ethanol is 90 %, filters after soaking 10d, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, Flos Moutan extract, for subsequent use;
Get the above-mentioned Cortex Moutan extract making, Flos Moutan extract, rutin and ursolic acid according to the parts by weight in above-mentioned formula, then add the dehydrated alcohol of 3.5 times of four gross weights to dissolve, obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol and hyaluronic acid according to the parts by weight in above-mentioned formula, more than stirring 30min under the condition that low whipping speed is 90r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to the mass percent in above-mentioned formula base oil, Rose Absolute, functional component and the adding ingredient that step 1 to step 4 obtains, low whipping speed be under the condition of 90r/min, stir 2h more than, then ageing 45d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
Claims (5)
1. a Paeonia suffruticosa compound heal-care essential oil, is characterized in that: be made up of following composition according to mass percent: base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and adding ingredient 1-5%;
Described base oil is made up of raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight;
Described Rose Absolute is made up of Flos Moutan quintessence oil 50-70 part and Diffuse Coptosapelta flower essential oil 30-50 part according to parts by weight;
Described functional component, obtains after adding four gross weight 2-5 anhydrous alcohol solution doubly by Cortex Moutan extract 30-40 part, Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part according to parts by weight; Wherein Cortex Moutan extract is that the distillate of Cortex Moutan after vapor distillation filters the filter cake obtaining; Flos Moutan extract be by extract that Flos Moutan after quintessence oil obtains with ethanol extraction without solution extractum;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight.
2. the preparation method of a kind of Paeonia suffruticosa compound heal-care essential oil as claimed in claim 1, is characterized in that: comprise the following steps:
The preparation of step 1, base oil
Get raw material peony seed oil 40-50 part, Oleum Vitis viniferae 20-30 part, Semen pruni armeniacae oil 10-20 part Flos Carthami seed oil 10-20 part according to parts by weight, add in reactor, under the condition that first low whipping speed is 60-120r/min, stir 1-5h, add again surfactant, be uniformly mixed, then in 20-30min slow cooling to-5 DEG C, after insulation 4-8h, be slowly warming up to room temperature, then filter with 200 mesh sieves, filter the filtrate obtaining and be base oil, for subsequent use;
The preparation of step 2, Rose Absolute
Gather fresh peony petal, add its weight 2-7 sodium chloride doubly to stir, pickle 20-100min, then be placed in vapor distillation device and extract, the distillation obtaining is extracted with ethyl acetate, after dried over anhydrous sodium carbonate, obtain Flos Moutan quintessence oil, for subsequent use;
Adopt Diffuse Coptosapelta flower to make Diffuse Coptosapelta flower essential oil according to the preparation method same with Flos Moutan quintessence oil, for subsequent use;
Then get above-mentioned Flos Moutan quintessence oil 50-70 part making according to parts by weight and Diffuse Coptosapelta flower essential oil 30-50 part is placed in agitator, under the condition that low whipping speed is 60-120r/min, stir 1-3h, make Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get Cortex Moutan raw material, add its weight 15-20 water doubly to distill, collect distillate, be placed in 2-5 DEG C of refrigerator and leave standstill after 18-24h, filter, collect filter cake, obtain Cortex Moutan extract, for subsequent use;
Getting the peony petal extracting after Flos Moutan quintessence oil in step 2 is raw material, petal is spread out, place at room temperature dry in the shade to moisture be 10-15%, then add peony petal raw material weight 15-20 ethyl acetate doubly to soak 8-10d, taking out peony petal is placed in the baking oven of 60-80 DEG C to be dried to moisture is 5-8%, obtain dry peony petal, for subsequent use; In dry peony petal, add its weight 8-12 edible ethanol doubly, the mass concentration of edible ethanol is 80-95 %, after soaking 8-12d, filter, the filtrate that filtration obtains temperature be less than 60 DEG C, vacuum be under 0.1MPa condition distilling under reduced pressure to without solution, obtain extractum, be Flos Moutan extract, for subsequent use;
Get above-mentioned Cortex Moutan extract 30-40 part making, Flos Moutan extract 30-40 part, rutin 10-20 part and ursolic acid 10-20 part according to parts by weight, then add four gross weight 2-5 dehydrated alcohol doubly to dissolve, obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 20-30 part according to parts by weight, more than stirring 30min under the condition that low whipping speed is 60-120r/min, make adding ingredient, for subsequent use;
The preparation of step 5, Paeonia suffruticosa compound heal-care essential oil
Get according to mass percent base oil 80-90%, Rose Absolute 5-10%, functional component 4-8% and the adding ingredient 1-5% that step 1 to step 4 obtains, low whipping speed be under the condition of 60-120r/min, stir 2h more than, then ageing 30-60d at room temperature, adopting filter screen is that 1000 object filters filter again, collect filtrate, subpackage, completes the preparation of Paeonia suffruticosa compound heal-care essential oil.
3. the preparation method of a kind of Paeonia suffruticosa compound heal-care essential oil as claimed in claim 2, is characterized in that: described peony seed oil is that the seed core of phoenix Paeonia suffruticosa or Paeonia papaveracea obtains through cold press.
4. the preparation method of a kind of Paeonia suffruticosa compound heal-care essential oil as claimed in claim 2, is characterized in that: the raw material of preparing Flos Moutan quintessence oil in described step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
5. the preparation method of a kind of Paeonia suffruticosa compound heal-care essential oil as claimed in claim 2, being characterised in that: the surfactant adopting in described step 1 is one or both in the synthetic alkyl polyglucoside of natural fat alcohol and glucose or fatty alcohol-polyoxyethylene ether non-ionic surface active agent.
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| JP2012144497A (en) * | 2011-01-13 | 2012-08-02 | Angelux Planning:Kk | Method of using paeoniae radix essence in massage, and paeoniae radix oil |
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