CN104398445A - Honeysuckle perfume - Google Patents
Honeysuckle perfume Download PDFInfo
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- CN104398445A CN104398445A CN201410756511.6A CN201410756511A CN104398445A CN 104398445 A CN104398445 A CN 104398445A CN 201410756511 A CN201410756511 A CN 201410756511A CN 104398445 A CN104398445 A CN 104398445A
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- flos lonicerae
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Abstract
The invention discloses honeysuckle perfume. 100 parts by volume of the perfume comprise the following ingredients in parts by volume: 1-2 parts of basic essential oil, 4-6 parts of honeysuckle essential oil, 5-10 parts of honeysuckle hydrolat, 0-1.5 parts of an oil emulsifier, and the balance of 95% ethanol, wherein the honeysuckle essential oil and the honeysuckle hydrolat are simultaneously extracted and obtained through a vapor distillation method; the honeysuckle essential oil extracted by the method is high in quality; the vapor distillation method is simple in equipment, simple and convenient to operate, and high in extraction efficiency and free of residual solvent. In the perfume disclosed by the invention, the main ingredients, namely the honeysuckle essential oil and the honeysuckle hydrolat are aromatic and elegant in flavor, and have the functions of moistening skin, removing freckles, delaying senescence, balancing secreted sebum and moisture, excreting moisture, promoting metabolism of a human body, regulating functions of the human body, enhancing the immunity, inhibiting bacteria, resisting inflammation and regulating the immunity; the perfume is full of floral flavor and fruit flavor, sweet and fragrant, light and elegant in color and luster, natural in fragrance, fresh and graceful, and long-lasting in fragrance, and has a high market value and a wide market prospect.
Description
Technical field
The present invention relates to a kind of perfume, be specifically related to a kind of Flos Lonicerae perfume.
Background technology
Flos Lonicerae, has another name called Radix Ophiopogonis (formal name used at school: Lonicera japonica).The shrub of the perennial half evergreen winding of gold silver Pittosporum and stolon." Flos Lonicerae " comes from Compendium of Material Medica, owing to opening as white at the beginning of Flos Lonicerae, after transfer yellow to, hence obtain one's name Flos Lonicerae.Medical material Flos Lonicerae is Caprifoliaceae woodbine Radix Ophiopogonis and congener dry flower or is with the flower just opened.Flos Lonicerae, March blooms, and five go out, micro-perfume (or spice), and redly, Hua Chukai then color is white for the base of a fruit, the then yellow skin through, two day, therefore named Flos Lonicerae.
Flos Lonicerae is described as the good medicine of heat-clearing and toxic substances removing from ancient times.Its property sweet cold fragrance, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Flos Lonicerae can dispelling wind-heat, also kind removing summer-heat blood poison, for various febrile disease, as fever of the body, dermexanthesis, sends out the diseases such as speckle, pyretic toxicity carbuncle sore, laryngopharynx swelling and pain, equal Be very effective.Modern study proves, Flos Lonicerae contains the pharmacological component such as chlorogenic acid, luteolin glycosides, stronger restraint is had to the various pathogens such as Hemolytic streptococcus, staphylococcus aureus and upper respiratory tract infection Causative virus etc., in addition also can enhancing immunity, antiearly pregnancy, hepatoprotective, antitumor, antiinflammatory, antipyretic, hemostasis (blood coagulation), suppress intestinal absorption cholesterol etc., its clinical application widely, can be used for the treatment of respiratory tract infection, bacillary dysentery, acute urinary, hypertension etc. more than 40 with other medicines compatibility and plant disease.
The common extracting process of current Flos Lonicerae quintessence oil has the microwave-assisted way of distillation, freezing compression method (milling process), chemical solvent to extract and supercritical CO
2abstraction techniques etc., it is of poor quality to there is extraction in these methods, and cost of equipment is expensive, complicated operation, and the problems such as extraction time is long, organic solvent residual are unfavorable to large scale application.
Summary of the invention
The object of the present invention is to provide a kind of method simultaneously extracting Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol, it is high that the method has extraction efficiency, and equipment is simple, easy and simple to handle, no solvent residue, and fragrance is graceful, the advantages such as lasting is lasting.The present invention also aims to provide a kind of Flos Lonicerae perfume being main component with Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol.
Object of the present invention is achieved through the following technical solutions:
The method simultaneously extracting Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol is a steam distillation, specifically comprises the steps:
(1) pulverize: honeysuckle fresh flower is joined mass percentage concentration be 2 ~ 4% without in iodine common salt water through pulverizer pulverize, obtain Flos Lonicerae starch.
(2) distill: Flos Lonicerae slurry adds distillating still and obtains oil mixing with water gas through steam distillation, obtains the fraction of oil water mixture through spiral cooler condensation.
(3) oil-water separation: the fraction of oil water mixture collects the Flos Lonicerae hydrosol of the rough Flos Lonicerae quintessence oil in upper strata and lower floor after oil water separator is separated.
(4) purification: rough Flos Lonicerae quintessence oil obtains proof gold Flos Lonicerae quintessence oil through molecular distillation purification.
Honeysuckle fresh flower described in step (1) is preferably 0.1 ~ 0.5:1 with the mass ratio without iodine common salt water.
The condition of the distillation described in step (2) is preferably: temperature 105 DEG C ~ 120 DEG C, steam pressure 0.1 ~ 0.5Mpa, distillation time 100 ~ 180 minutes.
The condition of the molecular distillation described in step (4) is preferably: temperature 30 DEG C ~ 40 DEG C, pressure 5 ~ 10Pa.
A kind of Flos Lonicerae perfume, the volume component of every 100 these perfume of parts by volume is: basic quintessence oil 1 ~ 2 part, the Flos Lonicerae quintessence oil obtained by said extracted method 4 ~ 6 parts, Flos Lonicerae hydrosol 5 ~ 10 parts, and emulsifier 0 ~ 1.5 part, adds the ethanol to 100 part of 95%; Wherein, every 100 parts by volume basis quintessence oils are mixed by following parts by volume component: Oleum menthae 5 parts, oil of Cymbopogon winterianus 10 parts, oleum bergamottae 10 parts, sweet orange oil 5 parts, Cananga odorata quintessence oil 5 parts, grapefruit essential oil 10 parts, jasmin quintessence oil 20 parts, tea tree ethereal oil 5 parts, Herba Lysimachiae foenum-graeci quintessence oil 3 parts, Flos Rosae Rugosae quintessence oil 20 parts, chamomile essential oil 7 parts.
The invention has the advantages that: the present invention is extracted by steam distillation simultaneously and obtains Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol, and it is high that the method has extraction efficiency, equipment is simple, and easy and simple to handle, the advantages such as no solvent residue, are worthy of popularization.Flos Lonicerae perfume of the present invention with Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol for main component, with other plant or flowers quintessence oil coordinate and obtain a kind of Flos Lonicerae perfume.Main component Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol fragrant odour simple and elegant, moistening skin and eliminating spot, slow down aging, balance sebum and moisture content secretion, excretion moisture content, can promote human metabolism, regulates bodily fuctions, improve immunity, have the effects such as antibacterial, antiinflammatory, immunity moderation.Flos Lonicerae perfume of the present invention is full of the fragrance of a flower and fruital aromatic, the fragrant and sweet fragrance of a flower, and color and luster is simple and elegant, and fragrance nature, distributes pure and fresh gracefulness, lasting fragrance, have very high using value and wide market prospect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
Embodiment 1
Preparation 2000mL Flos Lonicerae perfume, each volume components is: basic quintessence oil 20mL, Flos Lonicerae quintessence oil 100mL, Flos Lonicerae hydrosol 100mL, emulsifier 0mL, add the ethanol of 95% to 2000mL; Wherein, basic quintessence oil is mixed by Oleum menthae 1.0mL, oil of Cymbopogon winterianus 2.0mL, oleum bergamottae 2.0mL, sweet orange oil 1.0mL, Cananga odorata quintessence oil 1.0mL, grapefruit essential oil 2.0mL, jasmin quintessence oil 4.0mL, tea tree ethereal oil 1.0mL, Herba Lysimachiae foenum-graeci quintessence oil 0.6mL, Flos Rosae Rugosae quintessence oil 4.0mL, foreign glycosides chrysanthemum quintessence oil 1.4mL.
Described Flos Lonicerae quintessence oil, Flos Lonicerae hydrosol are extracted by the method comprised the steps and obtain:
(1) pulverize: in honeysuckle fresh flower be that honeysuckle fresh flower to be added mass percentage concentration be 2 ~ 4% pulverize through pulverizer without iodine common salt water for the ratio of 0.1 ~ 0.5:1 without the mass ratio of the iodine common salt water yield, obtain Flos Lonicerae and starch.
(2) distill: Flos Lonicerae slurry adds distillating still and obtains oil mixing with water gas through steam distillation, distillation time 100 ~ 180 minutes, and control steam pressure is 0.1 ~ 0.5Mpa, vapo(u)rizing temperature is 105 DEG C ~ 120 DEG C; Through spiral cooler, obtain the fraction of oil water mixture with tap water condensation.
(3) oil-water separation: the fraction of oil water mixture, through oil water separator, leaves standstill, and collects the Flos Lonicerae hydrosol obtaining the rough Flos Lonicerae quintessence oil in upper strata and lower floor after profit layering through oil water separator;
(4) purification: Flos Lonicerae quintessence oil temperature be 30 DEG C ~ 40 DEG C, pressure obtains proof gold Flos Lonicerae quintessence oil through molecular distillation purification under being the condition of 5 ~ 10Pa.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from spirit of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (5)
1. extract a method for Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol simultaneously, it is characterized in that comprising the steps:
(1) pulverize: honeysuckle fresh flower is joined mass percentage concentration be 2 ~ 4% without in iodine common salt water through pulverizer pulverize, obtain Flos Lonicerae starch;
(2) distill: Flos Lonicerae slurry adds distillating still and obtains oil mixing with water gas through steam distillation, obtains the fraction of oil water mixture through spiral cooler condensation;
(3) oil-water separation: the fraction of oil water mixture collects the Flos Lonicerae hydrosol of the rough Flos Lonicerae quintessence oil in upper strata and lower floor after oil water separator is separated;
(4) purification: rough Flos Lonicerae quintessence oil obtains proof gold Flos Lonicerae quintessence oil through molecular distillation purification.
2. the method simultaneously extracting Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol according to claim 1, is characterized in that: the honeysuckle fresh flower described in step (1) is 0.1 ~ 0.5:1 with the mass ratio without iodine common salt water.
3. the method simultaneously extracting Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol according to claim 1, it is characterized in that: the condition of the distillation described in step (2) is: temperature 105 DEG C ~ 120 DEG C, steam pressure 0.1 ~ 0.5Mpa, distillation time 100 ~ 180 minutes.
4. the method simultaneously extracting Flos Lonicerae quintessence oil and Flos Lonicerae hydrosol according to claim 1, is characterized in that: the condition of the molecular distillation described in step (4) is: temperature 30 DEG C ~ 40 DEG C, pressure 5 ~ 10Pa.
5. a Flos Lonicerae perfume, it is characterized in that: the volume component of every 100 these perfume of parts by volume is: basic quintessence oil 1 ~ 2 part, the Flos Lonicerae quintessence oil obtained by the method described in any one of claim 1-4 4 ~ 6 parts, Flos Lonicerae hydrosol 5 ~ 10 parts, emulsifier 0 ~ 1.5 part, adds the ethanol to 100 part of 95%; Wherein, every 100 parts by volume basis quintessence oils are mixed by following parts by volume component: Oleum menthae 5 parts, oil of Cymbopogon winterianus 10 parts, oleum bergamottae 10 parts, sweet orange oil 5 parts, Cananga odorata quintessence oil 5 parts, grapefruit essential oil 10 parts, jasmin quintessence oil 20 parts, tea tree ethereal oil 5 parts, Herba Lysimachiae foenum-graeci quintessence oil 3 parts, Flos Rosae Rugosae quintessence oil 20 parts, chamomile essential oil 7 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410756511.6A CN104398445A (en) | 2014-12-10 | 2014-12-10 | Honeysuckle perfume |
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| CN201410756511.6A CN104398445A (en) | 2014-12-10 | 2014-12-10 | Honeysuckle perfume |
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| CN104398445A true CN104398445A (en) | 2015-03-11 |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104784079A (en) * | 2015-04-29 | 2015-07-22 | 绥阳县吉帮金银花科技发展有限公司 | Flos lonicerae perfume and preparation method thereof |
| CN104825348A (en) * | 2015-04-14 | 2015-08-12 | 张徐徐 | Plant essential oil color cosmetic |
| CN105561730A (en) * | 2015-12-16 | 2016-05-11 | 无锡吉进环保科技有限公司 | Plant-type air purifying agent |
| CN106256344A (en) * | 2016-08-30 | 2016-12-28 | 郭清辉 | A kind of Flos Lonicerae quintessence oil dew and preparation method thereof |
| CN106963837A (en) * | 2017-05-24 | 2017-07-21 | 廖建军 | Skin trauma nursing essential oil and its preparation method and application |
| CN107213061A (en) * | 2017-06-07 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | One kind releive moisturizing flower water |
| CN107213087A (en) * | 2017-06-07 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | A kind of sun-proof repair spends water |
| CN107308021A (en) * | 2017-06-02 | 2017-11-03 | 安徽安龙基因医学检验所有限公司 | A kind of light spot refined jasmine oil of cold-type yellow (clear) and preparation method thereof |
| CN107858205A (en) * | 2017-11-05 | 2018-03-30 | 成重任 | A kind of hydrosol liquid, processing method and the application of cordyceps sinensis ginseng |
| CN107982174A (en) * | 2017-12-22 | 2018-05-04 | 陈彦蓉 | A kind of distillation and preparation method thereof of clearing heat for detumescence, Whitening, spot |
| CN109602624A (en) * | 2019-01-30 | 2019-04-12 | 普宁市嘉宝日用化工有限公司 | A kind of male vigorously perfume and preparation method thereof |
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| CN101845365A (en) * | 2010-05-17 | 2010-09-29 | 袁主平 | Method for manufacturing plant essential oil |
| CN102406575A (en) * | 2011-11-21 | 2012-04-11 | 江西金乔园林有限公司 | Sweet osmanthus perfume |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104825348A (en) * | 2015-04-14 | 2015-08-12 | 张徐徐 | Plant essential oil color cosmetic |
| CN104784079A (en) * | 2015-04-29 | 2015-07-22 | 绥阳县吉帮金银花科技发展有限公司 | Flos lonicerae perfume and preparation method thereof |
| CN105561730A (en) * | 2015-12-16 | 2016-05-11 | 无锡吉进环保科技有限公司 | Plant-type air purifying agent |
| CN106256344A (en) * | 2016-08-30 | 2016-12-28 | 郭清辉 | A kind of Flos Lonicerae quintessence oil dew and preparation method thereof |
| CN106963837A (en) * | 2017-05-24 | 2017-07-21 | 廖建军 | Skin trauma nursing essential oil and its preparation method and application |
| CN107308021A (en) * | 2017-06-02 | 2017-11-03 | 安徽安龙基因医学检验所有限公司 | A kind of light spot refined jasmine oil of cold-type yellow (clear) and preparation method thereof |
| CN107308021B (en) * | 2017-06-02 | 2021-04-23 | 安徽安龙基因科技有限公司 | Cool and refreshing type jasmine sambac essential oil and preparation method thereof |
| CN107213061A (en) * | 2017-06-07 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | One kind releive moisturizing flower water |
| CN107213087A (en) * | 2017-06-07 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | A kind of sun-proof repair spends water |
| CN107858205A (en) * | 2017-11-05 | 2018-03-30 | 成重任 | A kind of hydrosol liquid, processing method and the application of cordyceps sinensis ginseng |
| CN107982174A (en) * | 2017-12-22 | 2018-05-04 | 陈彦蓉 | A kind of distillation and preparation method thereof of clearing heat for detumescence, Whitening, spot |
| CN109602624A (en) * | 2019-01-30 | 2019-04-12 | 普宁市嘉宝日用化工有限公司 | A kind of male vigorously perfume and preparation method thereof |
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Application publication date: 20150311 |