CN107308021B - Cool and refreshing type jasmine sambac essential oil and preparation method thereof - Google Patents
Cool and refreshing type jasmine sambac essential oil and preparation method thereof Download PDFInfo
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- CN107308021B CN107308021B CN201710406989.XA CN201710406989A CN107308021B CN 107308021 B CN107308021 B CN 107308021B CN 201710406989 A CN201710406989 A CN 201710406989A CN 107308021 B CN107308021 B CN 107308021B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a cool type jasmine sambac essential oil with light spots and a preparation method thereof, wherein the cool type jasmine essential oil with light spots is prepared from the following components in percentage by mass: 35-50% of jasmine essential oil, 10-15% of honeysuckle essential oil, 3-8% of cooling agent, 7-15% of mint essential oil, 6-10% of frankincense oil, 1-2% of surfactant and the balance of pure water, wherein the preparation method comprises the following steps: preparing base oil; preparing flower essential oil; adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for more than 4 hours at the stirring speed of 80-200r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum sambac essential oil. The invention has the advantages of good effect, no toxic or side effect and the like.
Description
Technical Field
The invention relates to the field of daily chemicals, and particularly relates to cool type jasminum grandiflorum essential oil and a preparation method thereof.
Background
The essential oil skin care is from France, the essential oil skin care is popular in two years, the face cleaning with the essential oil can deeply remove dirt in pores, can also promote blood circulation of facial skin, discharge in vivo waste toxin, enable the face to be full of gloss, and achieve the effects of face cleaning, moisture preservation and tender care.
With the development of society and the continuous improvement of living standard, beauty lovers can use skin care essential oil, some spot-removing cosmetics on the market are mixed in types of fish and dragon, the quality is different, the price is generally higher, and even some cosmetics can generate side effects on skin after being used, so further improvement is needed.
Disclosure of Invention
The invention aims to overcome the defects of large side effect and poor using effect in the prior art and provide the cool type jasminum grandiflorum essential oil and the preparation method thereof.
The technical scheme provided by the invention for solving the technical problems is as follows: the invention discloses a cool type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 35-50% of jasmine essential oil, 10-15% of honeysuckle essential oil, 3-8% of cooling agent, 7-15% of mint essential oil, 6-10% of frankincense oil, 1-2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 36-48% of jasmine essential oil, 11-14% of honeysuckle essential oil, 4-7% of cooling agent, 8-14% of mint essential oil, 7-9% of frankincense oil, 1-2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 42% of jasmine essential oil, 12% of honeysuckle essential oil, 5% of cooling agent, 11% of mint essential oil, 8% of frankincense oil, 1% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 50% of jasmine essential oil, 10% of honeysuckle essential oil, 8% of cooling agent, 7% of mint essential oil, 10% of frankincense oil, 2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 35% of jasmine essential oil, 15% of honeysuckle essential oil, 3% of cooling agent, 15% of mint essential oil, 6% of frankincense oil, 1.5% of surfactant and the balance of pure water.
Preferably, the cooling agent is one or more of N,2, 3-trimethyl-2-isopropyl butanamide, N-ethyl-p-menthyl-3-carboxamide, and N-ethyl-p-menthyl-3-carboxamide.
Preferably, the surfactant is one of phospholipid surfactant, amino acid surfactant, liposome compound, lanolin and its derivatives.
Preferably, the invention also discloses a preparation method of the cooling type jasminum grandiflorum essential oil, which specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 2-4.5h under the condition that the stirring speed is 80-200r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 30-50min, keeping the temperature for 3-5h, slowly heating to room temperature, then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh gold and silver petals, adding sodium chloride 4-10 times of the weight of the petals, stirring, pickling for 45-90min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain flos Lonicerae essential oil;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for more than 4 hours at the stirring speed of 80-200r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum sambac essential oil.
Compared with the prior art, the invention has the following beneficial advantages:
the cool type light spot jasmine essential oil prepared by the invention has the characteristics of coolness and no greasiness by adding a freshener, is called as the king of the essential oil, is very expensive due to extremely low yield of the jasmine essential oil, has elegant smell, can relieve depression, revive spirit, promote self-confidence, and can nurse and improve the conditions of skin dryness, water shortage, oil passing and sensitivity, lighten striae gravidarum and scars, increase skin elasticity, make skin feel soft and tender, and can achieve the purpose of activating blood and channels and collaterals by dropping a few drops of jasmine essential oil into hot water for soaking feet;
the honeysuckle essential oil can moisten skin, remove freckles, delay aging, balance sebum and water secretion and excrete water on the skin;
the surfactant is a substance which can remarkably reduce the surface tension of the solution and change the interface state of the system by adding a small amount;
in addition, all the raw materials adopted by the invention are natural raw materials, so that the traditional Chinese medicine composition has no toxic or side effect and has a good effect;
the essential oil is worthy of caring skin from the aspects of functional maintenance such as whitening, moisturizing, acne treatment and the like, or mental rehabilitation such as relaxation and relaxation, and can quickly permeate into blood circulation through skin due to the characteristics of small molecules, easiness in permeation and the like of the essential oil, so that the essential oil has the function of conditioning the skin, and the effect of beautifying the skin is achieved;
the essential oil is volatile aromatic substances extracted from flowers, leaves, stems, roots or fruits of plants by a steam distillation method, an extrusion method, a cold soaking method or a solvent extraction method, but can not directly act on the skin, the essential oil needs to be added for dilution and then used, as the base oil generally has higher viscosity, the skin can generate greasy feeling after being smeared, and people can feel uncomfortable especially in summer with higher temperature, so that the use is influenced, N,2, 3-trimethyl-2-isopropyl butanamide, N-ethyl-p-menthyl-3-formamide, N-ethyl-p-menthyl-3-carboxamide and other menthyl formamide compounds are cooling agents with good quality, have higher cooling activity and no side effects such as burning, numbness, irritation and the like, and are mainly used as cooling agents for candies such as candies, In oral care, medicine;
the surfactant is a substance which can remarkably reduce the surface tension of the solution and change the interface state of the system by adding a small amount;
the natural surface additive mainly comprises phospholipid surfactants, amino acid surfactants, liposome compounds, lanolin and derivatives thereof, wherein lecithin has the most representative and wide application in the phospholipid surfactants, and as an amphoteric surfactant, lecithin is non-toxic, high in safety coefficient and good in surface performance, so that the lecithin is more and more emphasized in the application of cosmetics.
Detailed Description
The present invention will be further described with reference to specific examples, but the present invention is not limited to these examples.
The invention discloses a cool type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 35-50% of jasmine essential oil, 10-15% of honeysuckle essential oil, 3-8% of cooling agent, 7-15% of mint essential oil, 6-10% of frankincense oil, 1-2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 36-48% of jasmine essential oil, 11-14% of honeysuckle essential oil, 4-7% of cooling agent, 8-14% of mint essential oil, 7-9% of frankincense oil, 1-2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 42% of jasmine essential oil, 12% of honeysuckle essential oil, 5% of cooling agent, 11% of mint essential oil, 8% of frankincense oil, 1% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 50% of jasmine essential oil, 10% of honeysuckle essential oil, 8% of cooling agent, 7% of mint essential oil, 10% of frankincense oil, 2% of surfactant and the balance of pure water.
Preferably, the invention discloses cool and refreshing type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 35% of jasmine essential oil, 15% of honeysuckle essential oil, 3% of cooling agent, 15% of mint essential oil, 6% of frankincense oil, 1.5% of surfactant and the balance of pure water.
Preferably, the cooling agent is one or more of N,2, 3-trimethyl-2-isopropyl butanamide, N-ethyl-p-menthyl-3-carboxamide, and N-ethyl-p-menthyl-3-carboxamide.
Preferably, the surfactant is one of phospholipid surfactant, amino acid surfactant, liposome compound, lanolin and its derivatives.
Preferably, the invention also discloses a preparation method of the cooling type jasminum grandiflorum essential oil, which specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 2-4.5h under the condition that the stirring speed is 80-200r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 30-50min, keeping the temperature for 3-5h, slowly heating to room temperature, then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh gold and silver petals, adding sodium chloride 4-10 times of the weight of the petals, stirring, pickling for 45-90min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain flos Lonicerae essential oil;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for more than 4 hours at the stirring speed of 80-200r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum sambac essential oil.
Example 1
The invention discloses a cool type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 42% of jasmine essential oil, 12% of honeysuckle essential oil, 5% of cooling agent, 11% of mint essential oil, 8% of frankincense oil, 1% of surfactant and the balance of pure water.
The cooling agent adopts N-ethyl-p-menthyl-3-carboxamide.
The surfactant is amino acid surfactant.
The invention also discloses a preparation method of the cool type jasminum grandiflorum essential oil, which specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 4.5 hours under the condition that the stirring speed is 150r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 40 minutes, keeping the temperature for 4 hours, slowly heating to room temperature, and then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh honeysuckle petals, adding sodium chloride 6 times of the weight of the honeysuckle petals, uniformly stirring, pickling for 60min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain honeysuckle essential oil for later use;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for 6 hours at a stirring speed of 110r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum grandiflorum essential oil.
Example 2
The invention discloses a cool type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 50% of jasmine essential oil, 10% of honeysuckle essential oil, 8% of cooling agent, 7% of mint essential oil, 10% of frankincense oil, 2% of surfactant and the balance of pure water.
The cooling agent adopts N,2, 3-trimethyl-2-isopropyl butanamide.
The surfactant is lanolin and its derivative.
The invention also discloses a preparation method of the cool type jasminum grandiflorum essential oil, which specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 4.5 hours under the condition that the stirring speed is 200r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 30 minutes, keeping the temperature for 5 hours, slowly heating to room temperature, and then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh honeysuckle petals, adding sodium chloride 10 times of the weight of the petals, uniformly stirring, pickling for 90min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain honeysuckle essential oil for later use;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for 7 hours at the stirring speed of 80r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum grandiflorum essential oil.
Example 3
The invention discloses a cool type jasminum grandiflorum essential oil which is prepared from the following components in percentage by mass: 35% of jasmine essential oil, 15% of honeysuckle essential oil, 3% of cooling agent, 15% of mint essential oil, 6% of frankincense oil, 1.5% of surfactant and the balance of pure water.
The cooling agent adopts N-ethyl-p-menthyl-3-carboxamide.
The surfactant is phospholipid surfactant.
The invention also discloses a preparation method of the cool type jasminum grandiflorum essential oil, which specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 2 hours under the condition that the stirring speed is 160r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 50 minutes, keeping the temperature for 3 hours, slowly heating to room temperature, and then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh honeysuckle petals, adding sodium chloride 10 times of the weight of the petals, uniformly stirring, pickling for 60min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain honeysuckle essential oil for later use;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for 5 hours at the stirring speed of 100r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum grandiflorum essential oil.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Any person skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.
Claims (6)
1. The preparation method of the cool and refreshing type jasminum grandiflorum essential oil comprises the following components in percentage by mass: 35-50% of jasmine essential oil, 10-15% of honeysuckle essential oil, 3-8% of cooling agent, 7-15% of mint essential oil, 6-10% of frankincense oil, 1-2% of surfactant and the balance of pure water; the surfactant is one of phospholipid surfactant, amino acid surfactant, humor compound, lanolin and its derivative, and features that: the method specifically comprises the following steps:
step one, preparing base oil:
according to the mass percentage, adding jasmine essential oil, mint essential oil, frankincense oil and pure water into a reactor, firstly stirring for 2-4.5h under the condition that the stirring speed is 80-200r/min, then adding a surfactant, stirring and mixing uniformly, then slowly cooling to 0 ℃ within 30-50min, keeping the temperature for 3-5h, slowly heating to room temperature, then filtering by using a filter to obtain filtrate, namely base oil for later use;
step two, preparing the flower essential oil:
collecting fresh gold and silver petals, adding sodium chloride 4-10 times of the weight of the petals, stirring, pickling for 45-90min, extracting in a steam distillation device, extracting the obtained distillate with ethyl acetate, and drying with anhydrous sodium carbonate to obtain flos Lonicerae essential oil;
step three:
adding the flower fragrance essential oil and the cooling agent into the base oil prepared in the first step according to the mass percentage, stirring for more than 4 hours at the stirring speed of 80-200r/min, then filtering by using a filter with a filter screen of 1000 meshes at room temperature, collecting filtrate, and subpackaging to obtain the cool type jasminum sambac essential oil.
2. The preparation method of the cool and refreshing jasminum grandiflorum essential oil according to claim 1, which is characterized by comprising the following steps: the jasmine faint-patch essential oil is prepared from the following components in percentage by mass: 36-48% of jasmine essential oil, 11-14% of honeysuckle essential oil, 4-7% of cooling agent, 8-14% of mint essential oil, 7-9% of frankincense oil, 1-2% of surfactant and the balance of pure water.
3. The preparation method of the cool and refreshing jasminum grandiflorum essential oil according to claim 1, which is characterized by comprising the following steps: the jasmine faint-patch essential oil is prepared from the following components in percentage by mass: 42% of jasmine essential oil, 12% of honeysuckle essential oil, 5% of cooling agent, 11% of mint essential oil, 8% of frankincense oil, 1% of surfactant and the balance of pure water.
4. The preparation method of the cool and refreshing jasminum grandiflorum essential oil according to claim 1, which is characterized by comprising the following steps: the jasmine faint-patch essential oil is prepared from the following components in percentage by mass: : 50% of jasmine essential oil, 10% of honeysuckle essential oil, 8% of cooling agent, 7% of mint essential oil, 10% of frankincense oil, 2% of surfactant and the balance of pure water.
5. The preparation method of the cool and refreshing jasminum grandiflorum essential oil according to claim 1, which is characterized by comprising the following steps: the jasmine faint-patch essential oil is prepared from the following components in percentage by mass: 35% of jasmine essential oil, 15% of honeysuckle essential oil, 3% of cooling agent, 15% of mint essential oil, 6% of frankincense oil, 1.5% of surfactant and the balance of pure water.
6. The preparation method of the cooling type jasminum grandiflorum essential oil according to any one of claims 1 to 5, wherein the preparation method comprises the following steps: the cooling agent adopts one or more of N,2, 3-trimethyl-2-isopropyl butanamide, N-ethyl-p-menthyl-3-formamide and N-ethyl-p-menthyl-3-carboxamide in any proportion.
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CN105456063A (en) * | 2015-12-14 | 2016-04-06 | 安徽丰乐香料有限责任公司 | Cool and refreshing skin-caring essential oil |
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CN105686981A (en) * | 2014-11-25 | 2016-06-22 | 郭亚萍 | Acne removing and whitening essential oil |
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