CN107550824B - Herbal floral water with effects of refreshing, dispelling mosquitoes and relieving itching and preparation method of herbal floral water - Google Patents
Herbal floral water with effects of refreshing, dispelling mosquitoes and relieving itching and preparation method of herbal floral water Download PDFInfo
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Abstract
The invention discloses herbal floral water capable of refreshing, dispelling mosquitoes and relieving itching and a preparation method thereof, and relates to the field of pharmaceutical chemicals. A traditional Chinese herbal floral water with effects of refreshing, repelling mosquitoes and relieving itching comprises the following components in parts by weight: 30-40 parts of honeysuckle extract, 15-40 parts of rhizoma paridis extract, 0.5-1.2 parts of basil volatile oil, 0.1-0.3 part of folium artemisiae argyi volatile oil, 0.5-1.2 parts of mint volatile oil, 0.3-1.0 part of lotus volatile oil, 0.3-1.5 parts of sweet osmanthus essential oil, 0.1-0.3 part of divaricate saposhnikovia root essential oil and 0.5-1.0 part of glycerol. The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention has appropriate refreshing degree, is good in comfort, and has the effects of diminishing swelling and repelling mosquitoes.
Description
Technical Field
The invention relates to the field of pharmaceutical chemicals, in particular to herbal floral water capable of refreshing, dispelling mosquitoes and relieving itching and a preparation method thereof.
Background
In hot summer, many people choose to outrun or avoid summer heat in the open air, or blow air in a courtyard after dinner, but are often plagued by mosquito bites.
Patent publication No. CN101181425 discloses a Chinese medicinal liniment for external use, which is prepared by mixing natural plant essential oil and tea oil extract of Chinese medicines, and is characterized in that:
(1) the compositions are:
camphor salicylic acid methyl ester turpentine
Peppermint oil clove basil oil camphor oil
Oleum Anisi Stellati, oleum Cinnamomi, and Borneolum Syntheticum
An extract of the oil of menthol, eucalyptus oil and tea,
(2) the tea oil extract is prepared by extracting from a traditional Chinese medicine composition at least comprising the following components in parts by weight:
herba Selaginellae and herba Centipedae Hibisci Mutabilis
Radix Angelicae Dahuricae (radix Cynanchi Paniculati) of flos Magnoliae
Flos Lonicerae cortex Ilicis Rotundae
White semiliquidambar cathayensis herba ephedrae
Paris polyphylla herringbone grass golden thread wind
The golden earring is a cloud with yellow color.
The Chinese medicinal liniment for external use is used for treating cold, headache, mosquito bite, innominate toxic swelling and boat and vehicle vertigo. However, the invention has the following disadvantages: has multiple and mixed components, unobvious main medicines and insignificant mosquito repellent effect.
The patent with publication number CN 103989595A discloses a natural children floral water, which is prepared from the following raw materials in parts by weight: 8-18 parts of honeysuckle, 10-30 parts of aloe, 12-30 parts of eucalyptus leaves, 7-15 parts of lavender, 5-15 parts of green foeniculum, 11-30 parts of cacumen biotae, 10-20 parts of elsholtzia, 15-40 parts of sweet wormwood, 7-15 parts of notopterygium root, 10-18 parts of frankincense, 5-18 parts of mint, 10-25 parts of liquorice, 12-30 parts of borneol and 90-200 parts of distilled water. The natural and non-irritant toilet water is prepared by homogenizing plant extracted essential oil prepared from lavender, Lvjinxiang, elsholtzia, frankincense and mint and supernate prepared from honeysuckle, aloe, eucalyptus leaves, cacumen biotae, sweet wormwood, notopterygium root and liquorice together. However, the invention has the defects of insignificant mosquito repelling and itching relieving effects and the like.
Patent publication No. CN103989612A discloses prickly heat powder which is prepared from the following components: 11-20 parts of pearl powder, 20-40 parts of honeysuckle, 15-30 parts of aloe, 10-25 parts of sweet osmanthus, 12-20 parts of mint, 5-10 parts of plant essential oil, 0.5-2 parts of salicylic acid, 0.1-1 part of titanium dioxide and 7-15 parts of borneol. The prickly heat powder disclosed by the invention has the characteristics of wide raw material source, naturalness, no stimulation, good prickly heat removing and itching relieving effects and low price. But the product has no obvious mosquito repellent effect.
Disclosure of Invention
Based on the defects of the prior art, the invention provides the herbal floral water with the effects of cooling, repelling mosquitoes and relieving itching, and the herbal floral water has appropriate cooling degree, good comfort, and effects of diminishing swelling and repelling mosquitoes.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
a traditional Chinese herbal floral water with effects of refreshing, repelling mosquitoes and relieving itching comprises the following components in parts by weight: 30-40 parts of honeysuckle extract, 15-40 parts of rhizoma paridis extract, 0.5-1.2 parts of basil volatile oil, 0.1-0.3 part of folium artemisiae argyi volatile oil, 0.5-1.2 parts of mint volatile oil, 0.3-1.0 part of lotus volatile oil, 0.3-1.5 parts of sweet osmanthus essential oil, 0.1-0.3 part of divaricate saposhnikovia root essential oil and 0.5-1.0 part of glycerol.
Preferably, the herbal mosquito-repellent itching-relieving toilet water comprises the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.1 part of divaricate saposhnikovia root essential oil, 0.5 part of sweet osmanthus flower essential oil and 0.5 part of glycerol.
Preferably, the herbal mosquito-repellent itching-relieving toilet water also comprises the following components in parts by weight: 4.5-10 parts of anophelifuge.
Preferably, the herbal mosquito-repellent itching-relieving toilet water comprises the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus essential oil, 0.1 part of divaricate saposhnikovia root essential oil, 0.5 part of glycerol and 5.0 parts of anophelifuge.
Preferably, the herbal mosquito-repellent itching-relieving toilet water also comprises the following components in parts by weight: 0.5-1.0 part of borneol.
Preferably, the herbal mosquito-repellent itching-relieving toilet water comprises the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus essential oil, 0.1 part of divaricate saposhnikovia root essential oil, 0.5 part of glycerol, 5.0 parts of anophelifuge and 0.8 part of borneol.
Preferably, the preparation method of the herbal floral water with effects of cooling, repelling mosquitoes and relieving itching comprises the following steps:
step 1: mixing flos Lonicerae leaching solution and rhizoma paridis leaching solution to obtain mixed solution I,
step 2: adding folium artemisiae argyi volatile oil, basil volatile oil, mint volatile oil, lotus flower volatile oil, sweet osmanthus flower essential oil, divaricate saposhnikovia root essential oil and glycerin into the obtained mixed solution I, and performing volume fixing by using distilled water to obtain mixed solution II;
and step 3: heating the mixed solution II in a water bath kettle to completely dissolve;
and 4, step 4: standing, and filtering to obtain the final product.
Preferably, the temperature of the water bath in step 3 is 35 ℃.
Preferably, the standing time in the step 4 is 3-5 days.
Compared with the prior art, the invention has the following beneficial effects:
the invention provides herbal floral water capable of refreshing, dispelling mosquitoes and relieving itching, which is prepared from honeysuckle extract, paris polyphylla extract, basil volatile oil, folium artemisiae argyi volatile oil, mint volatile oil, lotus flower volatile oil, sweet osmanthus flower essential oil, divaricate saposhnikovia root essential oil and a proper amount of glycerol.
The raw materials and the mechanism of the floral water are as follows: honeysuckle flower: is dried flower bud or flower with initial blossom of Lonicera japonica Thunb of Caprifoliaceae. Collected before blooming in summer and dried. Sweet in nature and taste and cold in nature. It enters lung, heart and stomach meridians. The functions and indications are as follows: clear heat and remove toxicity, disperse wind-heat. Can be used for treating carbuncle, swelling and sore, pharyngitis, erysipelas, toxic heat, dysentery, wind-heat type common cold, epidemic febrile disease, and fever;
rhizoma paridis: is dried rhizome of plant of Paris of Liliaceae, and has bitter and slightly cold taste. It enters heart, lung and liver meridians. Has the effects of clearing away heat and toxic materials, relieving swelling and pain, cooling liver, and arresting convulsion. It is commonly used for furuncle, carbuncle, swelling and sore throat, snake and insect bite, traumatic injury, pain, convulsion and convulsion;
basil: is an annual plant of Labiatae, also called as herba Ocimi, JIUZHA, flos Caryophylli, and herb Hierochloes Adoratae, and has effects of dispelling pathogenic wind, relieving exterior syndrome, removing toxic substance, relieving swelling, activating qi-flowing, promoting blood circulation, eliminating dampness, regulating stomach, tonifying heart, tranquilizing, etc., and can be used for treating common cold due to wind-cold, headache, dyspepsia, stomach and abdomen distending pain, menoxenia, traumatic injury, asthma, bronchitis, and cardiovascular diseases;
folium artemisiae argyi: is dried leaf of Artemisia argyi L.of Compositae. Pungent and bitter taste, warm nature; spleen, liver and kidney meridians entered; fragrant warm powder, can be raised and lowered; has the effects of warming channels, stopping bleeding, dispelling cold, relieving pain, reducing dampness and killing parasites; mainly treats irregular menstruation, dysmenorrheal, infertility caused by cold womb, threatened abortion and the like;
mint: is dry aerial part of Mentha haplocalyx of Labiatae, has pungent taste, cold nature and no toxicity, enters lung and liver channels, has effects of dispelling pathogenic wind and heat, clearing heat, relieving exterior syndrome, dispelling pathogenic wind, relieving swelling, relieving sore throat, and relieving pain, and is often used for wind-heat type common cold, wind-heat type headache, conjunctival congestion pain, sore throat, etc.;
lotus flower: is bud of Nymphaeaceae plant flos Nelumbinis. Collecting large buds or open flowers containing bud in 6-7 months, and drying in the shade. Bitter in nature and taste; sweet; and (7) flattening. Meridian tropism; the liver meridian. The functional indications are as follows: stasis dissipating and bleeding stopping; to remove dampness and dispel wind. Major damage to hematemesis; blood stranguria; metrorrhagia and metrostaxis and bleeding; eczema of the upper part of the body; itch of scabies;
sweet osmanthus: dried flower of Olea Europaea of Oleaceae. The nature and taste are warm and pungent. It enters lung, spleen and kidney meridians. The efficacy and the effect are as follows: warm lung and resolve retained fluid, dispel cold and alleviate pain. Can be used for treating phlegm retention, cough and asthma, abdominal psychroalgia, intestinal wind and bloody dysentery, amenorrhea, dysmenorrhea, cold hernia, abdominal pain, toothache, and halitosis;
wind prevention: is root of Saposhnikovia divaricata (Turcz.) Schischk of Umbelliferae. Pungent and sweet in nature and slightly warm in nature. Enter bladder, liver and spleen meridians. Has effects in expelling pathogenic wind, relieving exterior syndrome, eliminating dampness, relieving pain, and relieving spasm.
The formula mechanism of the cool mosquito-repellent itching-relieving toilet water is as follows: the flos Lonicerae leaching solution and rhizoma paridis leaching solution have detumescence and itching relieving effects, and also have mosquito repellent effect, and are monarch drugs; the basil and sweet osmanthus flower volatile oil has the effects of repelling mosquitoes and diminishing swelling, the lotus flower volatile oil has the effects of repelling mosquitoes and relieving itching, and the basil and sweet osmanthus flower volatile oil, the basil and sweet osmanthus flower volatile oil and the lotus flower volatile oil are mosquito-repelling and antibacterial active ingredients and are ministerial drugs; the folium artemisiae argyi volatile oil and the radix saposhnikoviae volatile oil have the effect of relieving itching, the mint volatile oil has the effects of cooling and relieving pain, and the three components are main components for relieving itching and swelling and are adjuvant drugs; glycerol has effects of keeping moisture, moistening and protecting skin, and is used as auxiliary component. The cool mosquito-repelling itching-relieving toilet water prepared by the nine substances through scientific compatibility has good mosquito-repelling effect, can effectively relieve the spasm, itching and red swelling caused by mosquito biting, adopts natural mosquito-repelling itching-relieving raw materials, is pleasant in smell, is safe to human bodies, and has no toxic or side effect after long-term use. The above starting materials are either commercially available or can be prepared according to methods well known to those skilled in the art.
Detailed Description
In order to better understand the present invention, the following examples are further provided to clearly illustrate the contents of the present invention, but the contents of the present invention are not limited to the following examples. In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present invention. It will be apparent, however, to one skilled in the art, that the present invention may be practiced without one or more of these specific details.
Example 1
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of divaricate saposhnikovia root essential oil and 0.5 part of glycerol.
As a specific implementation mode of the invention, the method for extracting the honeysuckle leaching liquor comprises the following steps:
step 301: pulverizing flos Lonicerae decoction pieces, and sieving;
step 302: taking 450 g of honeysuckle, precisely weighing, dividing into 3 parts, and respectively placing in 3 conical flasks with the same volume;
step 303: respectively adding 500ml of alcohol into the conical flask, sealing the conical flask, and cold soaking;
step 304: standing, collecting supernatant I, adding 300ml of dealdehydized alcohol into the residue, standing, and collecting supernatant II;
step 305: mixing the clear liquid I and the clear liquid II, and rapidly performing suction filtration by using a vacuum pump;
step 306: adding dealdehyding alcohol to reach volume of 3000 ml.
The rotation speed of the crushing in the step 301 is 25000 r/min.
And the crushing time in the step 301 is 3-5 min.
The screening in step 301 is through a six-mesh screen.
In step 303, the alcohol is dideal alcohol.
The standing time in step 304 is 24 h.
The number of suction filtration in step 305 is 3.
In the invention, the extraction method of the paris polyphylla leaching liquor is the same as that of the honeysuckle leaching liquor, and the details are not repeated.
As a specific embodiment of the invention, the method for extracting the folium artemisiae argyi volatile oil comprises the following steps:
step 101: taking 100g of naturally dried folium artemisiae argyi decoction pieces, and grinding the decoction pieces;
step 102: placing the pulverized folium Artemisiae Argyi in 1000ml round flask, adding distilled water, and cold soaking;
step 103: adding a plurality of glass beads into the round-bottom flask, shaking and mixing, and connecting a volatile oil tester and a reflux condenser tube;
step 104: adding water from the upper end of the reflux condenser pipe to fill the scale part of the volatile oil detector and overflow the volatile oil into the round-bottom flask;
step 105: slowly heating the round-bottom flask in an electric heating jacket until the round-bottom flask is boiled, keeping slight boiling until the oil amount is not increased any more, stopping heating, and standing;
step 106: opening the piston at the lower end of the volatile oil tester to slowly discharge water to separate out volatile oil.
Step 107: adding small amount of anhydrous sodium sulfate, and drying to obtain folium Artemisiae Argyi volatile oil.
The addition amount of the distilled water in the step 102 is 8 times of that of the folium artemisiae argyi decoction pieces in the step 1.
The time of the cold soaking in the step 102 is 2 hours.
The time for the microboiling in step 105 was 4 hours.
As a specific embodiment of the invention, the extraction method of the mint volatile oil comprises the following steps:
step 201: opening a compressed air valve, checking whether a slag discharge door is freely opened and closed, checking whether a leakage phenomenon exists, checking a pressure value, and whether a safety valve is normal, and feeding and producing materials after an extraction tank is normal;
step 202: adopting a steam distillation method, putting dry mint decoction pieces, setting the temperature, starting a multifunctional extractor, heating for continuous reflux, allowing steam to enter a condenser for condensation, allowing condensate to enter an oil-water separator for oil-water separation;
step 203: the drainage valve is used for adjusting the liquid level of an oil layer in the oil-water separator, so that the oil layer can be drained from the oil drainage pipe, and water in the oil-water separator can be drained from a drain outlet at the bottom of the oil-water separator;
step 204: and cleaning equipment according to GMP requirements, wherein the cleaning conditions are as follows:
cleaning with clear water: circulating clear water until the clear water is clear;
hot water circulation: and circularly washing with hot water at 60-75 ℃ for 5 min.
Step 205: the method is used for obtaining the mint volatile oil by times.
The temperature is set to 98 ℃ in step 202.
The refluxing time in step 202 is 4 hours.
In the invention, the extraction method of basil volatile oil is the same as that of mint volatile oil, and the details are not repeated.
As a specific embodiment of the invention, the lotus flower essential oil, the osmanthus flower essential oil and the divaricate saposhnikovia root essential oil are all purchased from the market.
The preparation method of the herbal floral water with effects of cooling, repelling mosquitoes and relieving itching comprises the following steps:
step 1: respectively preparing a honeysuckle extract and a paris polyphylla extract, and mixing the honeysuckle extract and the paris polyphylla extract to obtain a mixed solution I;
step 2: respectively preparing folium artemisiae argyi volatile oil and mint volatile oil, adding the folium artemisiae argyi volatile oil, basil volatile oil, mint volatile oil, lotus flower volatile oil, sweet osmanthus flower essential oil, divaricate saposhnikovia root essential oil and glycerin into the mixed solution I, and performing volume fixing by using distilled water to obtain a mixed solution II;
and step 3: heating the mixed solution II in a water bath kettle to completely dissolve;
and 4, step 4: standing, and filtering to obtain the final product.
The temperature of the water bath in step 3 was 35 ℃.
The standing time in the step 4 is 3-5 days.
Example 2
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 30 parts of honeysuckle extract, 15 parts of rhizoma paridis extract, 0.5 part of basil volatile oil, 0.2 part of argy wormwood leaf volatile oil, 0.5 part of mint volatile oil, 0.3 part of lotus flower volatile oil, 0.3 part of osmanthus essential oil, 0.2 part of divaricate saposhnikovia root essential oil and 0.7 part of glycerol.
Example 3
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 35 parts of honeysuckle extract, 30 parts of rhizoma paridis extract, 1.2 parts of basil volatile oil, 0.3 part of argy wormwood leaf volatile oil, 1.2 parts of mint volatile oil, 1.0 part of lotus flower volatile oil, 1.5 parts of osmanthus essential oil, 0.3 part of divaricate saposhnikovia root essential oil and 1.0 part of glycerol.
Example 4
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.5 part of glycerol and 5.0 parts of anophelifuge.
The preparation method of the herbal floral water with effects of cooling, repelling mosquitoes and relieving itching in the embodiment comprises the following steps of 1-4 in the embodiment 1: and (4) mixing the anophelifuge with the mixed liquid obtained by filtering in the step (4) to obtain a finished product.
Example 5
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 30 parts of honeysuckle extract, 15 parts of rhizoma paridis extract, 0.5 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.5 part of mint volatile oil, 0.3 part of lotus flower volatile oil, 0.3 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.5 part of glycerol and 4.5 parts of anophelifuge.
Example 6
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.2 parts of basil volatile oil, 0.3 part of argy wormwood leaf volatile oil, 1.2 parts of mint volatile oil, 1.0 part of lotus flower volatile oil, 1.5 parts of osmanthus essential oil, 0.3 part of ledebouriella essential oil, 1.0 part of glycerol and 10 parts of anophelifuge.
Example 7
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 35 parts of honeysuckle extract, 30 parts of rhizoma paridis extract, 0.9 part of basil volatile oil, 0.2 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.6 part of lotus flower volatile oil, 0.9 part of osmanthus essential oil, 0.2 part of ledebouriella essential oil, 0.7 part of glycerol and 7 parts of anophelifuge.
Example 8
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 32 parts of honeysuckle extract, 23 parts of rhizoma paridis extract, 0.6 parts of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.7 part of mint volatile oil, 0.4 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.6 part of glycerol and 6 parts of anophelifuge.
Example 9
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 38 parts of honeysuckle extract, 35 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.2 part of argy wormwood leaf volatile oil, 1.0 part of mint volatile oil, 0.9 part of lotus flower volatile oil, 1.2 parts of osmanthus essential oil, 0.2 part of divaricate saposhnikovia root essential oil, 0.9 part of glycerol and 8 parts of anophelifuge.
Example 10
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.5 part of glycerol, 5.0 parts of anophelifuge and 0.8 part of borneol.
The preparation method of the herbal floral water with effects of cooling, repelling mosquitoes and relieving itching in the embodiment comprises the following steps of 1-4 in the embodiment 1: and (4) mixing the anophelifuge and the borneol with the mixed solution obtained by filtering in the step (4) to obtain a finished product.
Example 11
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 30 parts of honeysuckle extract, 15 parts of rhizoma paridis extract, 0.5 part of basil volatile oil, 0.2 part of argy wormwood leaf volatile oil, 0.5 part of mint volatile oil, 0.3 part of lotus flower volatile oil, 0.3 part of osmanthus essential oil, 0.2 part of ledebouriella essential oil, 0.7 part of glycerol, 4.5 parts of anophelifuge and 0.5 part of borneol.
Example 12
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching disclosed by the invention is composed of the following components in parts by weight: 35 parts of honeysuckle extract, 30 parts of rhizoma paridis extract, 1.2 parts of basil volatile oil, 0.3 part of argy wormwood leaf volatile oil, 1.2 parts of mint volatile oil, 1.0 part of lotus flower volatile oil, 1.5 parts of osmanthus essential oil, 0.3 part of ledebouriella essential oil, 1.0 part of glycerol, 10 parts of anophelifuge and 1.0 part of borneol.
Comparative example 1
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus flower essential oil, 0.1 part of divaricate saposhnikovia root essential oil and 0.5 part of glycerol.
This comparative example compared to example 1, omitting the use of peppermint volatile oil.
Comparative example 2
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 4.5 parts of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.5 part of glycerol, 5.0 parts of anophelifuge and 0.3 part of borneol.
Compared with the example 10, the content of the mint volatile oil and the borneol is adjusted.
Comparative example 3
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 1.5 parts of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.1 part of ledebouriella essential oil, 0.5 part of glycerol, 5.0 parts of anophelifuge and 1.2 parts of borneol.
Compared with the example 10, the content of the mint volatile oil and the borneol is adjusted.
Comparative example 4
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle leaching liquor, 1.0 part of basil volatile oil, 0.1 part of argyi leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus flower essential oil, 0.1 part of divaricate saposhnikovia root essential oil and 0.5 part of glycerol.
This comparative example compared to example 1, the use of the paris polyphylla leaching solution was omitted.
Comparative example 5
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus flower essential oil and 0.5 part of glycerol.
This comparative example compared to example 1, omitting the use of essential oil of ledebouriella seseloides.
Comparative example 6
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle leaching liquor, 1.0 part of basil volatile oil, 0.1 part of argyi leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus flower essential oil and 0.5 part of glycerol.
This comparative example compared to example 1, omitting the use of the paris polyphylla leaching solution and the ledebouriella essential oil.
Comparative example 7
The herbal floral water capable of refreshing, repelling mosquitoes and relieving itching is prepared from the following components in parts by weight: 40 parts of honeysuckle extract, 10 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of osmanthus essential oil, 0.5 part of divaricate saposhnikovia root essential oil and 0.5 part of glycerol.
Compared with example 1, the content of the rhizoma paridis leaching solution and the radix sileris essential oil is adjusted in the comparative example.
Evaluation of the effects:
1. cooling degree experiment of herbal cool, mosquito-repellent and itching-relieving floral water of the invention
The test method comprises the following steps: selecting 20 volunteers, and evaluating according to the test results of the volunteers, wherein the results are shown in table 1:
TABLE 1 Cool degree test results
As can be seen from table 1, the cooling degree improvement rates of examples 1 to 3 are more than 70%, the cooling degree improvement rates of examples 10 to 12 are more than 80%, and the cooling degree improvement rates of comparative examples 1, 2 and 3 are respectively 25%, 35% and 40%, which are significantly reduced compared with the cooling degree effect of the floral water of the present invention, and thus it is demonstrated that the mint volatile oil and borneol in the floral water composition of the present invention are effectively blended, and cooperate with other components to obtain a good cooling effect, and have a certain effect of relieving summer heat.
2. Comfort level experiment of herbal cool, mosquito-repellent and itching-relieving floral water
The test method comprises the following steps: selecting 20 volunteers, and evaluating according to the test results of the volunteers, wherein the results are shown in table 2:
table 2 comfort test results
As can be seen from table 2, the comfort level of example 10 is the best, and next, examples 11 to 12 are good, the comfort level of examples 1 to 3 is the worst, the comfort level of comparative example 1 is the worst, and comparative examples 2 and 3 are poor, which shows that the toilet water of the present invention can bring a significant comfort feeling to people.
The result of combining table 1~ table 2 can know, and this application floral water matched stack is reasonable, has obviously reached and has given people cool and refreshing, the anticipated effect of comfort, and cool degree is suitable moreover, and the comfort level is good.
3. Experiment for mosquito repellent effect of herbal cool, mosquito repellent, itching relieving toilet water
Experimental floral water: the floral water prepared in example 1, example 4, example 10, and comparative examples 1 to 7, the control group was pure water,
experiment mosquito: breeding Aedes albopictus indoors; feeding conditions are as follows: the temperature is 26 +/-1) DEG C, the relative humidity is 65 +/-5 percent,
the experimental method comprises selecting 100 volunteers, randomly dividing into 10 groups, collecting skin area of 5cm × 5cm of human hand, covering the rest skin, and smearing 1ml/cm on the exposed skin of left hand2The method comprises the steps of coating experimental floral water with a dosage, extending hands into cages for 100s 10min after coating, testing for 1 time every 2.5h for 4 times, and calculating an effective protection rate (%) according to the number of aedes albopictus staying on arms, wherein the effective protection rate (%) is not larger than (the number of control group stopping-falling mosquitoes is one experimental group stopping-falling mosquito number)/the number of control group stopping-falling mosquitoes is × 100%, and the number of the control group stopping-falling mosquitoes is ×%, and the number of the control group stopping-falling mosquitoes is larger than that of the aedes albopictusThe results are shown in table 3:
TABLE 3 mosquito repelling effect test results
The results in table 3 show that the effective protection rates of the toilet water in example 1 within 5 hours are 78.28%, 80.08% and 81.62%, respectively, and the mosquito repellent effect is remarkable. The mosquito repellent effects of comparative examples 1 to 7 are reduced, wherein the toilet water of comparative example 1 omits the use of the mint volatile oil compared with example 1, the effective protection rate within 2.5 hours is only 72.52%, the mosquito repellent effect within 2.5 hours is obviously reduced compared with example 1 by 89.15%, the mint volatile oil is used for achieving the cool and comfortable effects at the beginning of use, but the mosquito repellent effect is obviously influenced by the combination of the mint volatile oil and the components of the mosquito repellent composition in a mosquito repellent experiment. Compared with the embodiment 10, the toilet water in the comparative examples 2 and 3 has the advantages that the contents of the mint volatile oil and the borneol are adjusted, the mosquito repellent effect is obviously reduced compared with the embodiment 10, and the use of the mint volatile oil and the borneol has an obvious influence on the mosquito repellent effect of the toilet water. Comparative example 4 and comparative example 5 the use of the paris polyphylla leaching liquor and the ledebouriella root essential oil is omitted in comparison with example 1, and the mosquito repellent effect is reduced in comparison with example 1, which shows that the use of the paris polyphylla leaching liquor and the ledebouriella root essential oil affects the mosquito repellent effect of the floral water. Compared with the embodiment 1, the comparative example 6 omits the use of the paris polyphylla leaching liquor and the divaricate saposhnikovia root essential oil, and the mosquito repellent effect is obviously reduced compared with the embodiment 1. Comparative example 7 compared with example 1, the content of the paris polyphylla leaching liquor and the content of the saposhnikovia divaricata essential oil are simultaneously adjusted, the mosquito repellent effect is reduced, and the proportion of the paris polyphylla leaching liquor and the saposhnikovia divaricata essential oil is reasonable, so that the mosquito repellent effect of floral water is improved.
4. Experiment on anti-inflammatory and detumescent effects of herbal cooling, mosquito repelling and itching relieving toilet water
The experimental method comprises the following steps: 160 mice are taken and randomly divided into 8 groups according to mass balance, each group is 20 mice and marked by picric acid, a blank control group is given with 10ml of physiological saline for each time, a positive control group is sequentially given with equal amount of floral water in the invention, the floral water is given for 1 time every day, the floral water is given for 3 days, 0.04ml of dimethylbenzene is smeared on the right ear of the mice after 1 hour of last administration, the cervical vertebra of each group of animals is dislocated and killed after 1 hour, then the ears are symmetrically punched by a puncher with the diameter of 6mm, and the ears are weighed. The mass was recorded and the swelling degree was calculated, and the intensity of the anti-inflammatory action was expressed in terms of swelling degree, and the results are shown in table 4, in which:
degree of swelling = right ear mass-left ear mass,
swelling rate = (right ear mass-left ear mass)/left ear mass 100%.
TABLE 4 anti-inflammatory and repercussive effects
As can be seen from the results in table 4, the swelling degree results of examples 1, 4 and 10 are significantly different from those of the blank control group, which indicates that the floral water of the present invention can significantly reduce the swelling degree of mice. The swelling degree results of comparative examples 4, 5 and 6 show that the omission of one or both of the paris polyphylla leaching solution and the saposhnikovia divaricata essential oil can reduce the swelling diminishing effect, and the decrease of the swelling diminishing effect of the omission of the paris polyphylla leaching solution and the saposhnikovia divaricata essential oil is more remarkable, which indicates that the paris polyphylla leaching solution and the saposhnikovia divaricata essential oil have the synergistic effect in the invention. Comparative example 7 adjusts the contents of the rhizoma paridis leaching solution and the ledebouriella root essential oil, and other components and contents are kept unchanged, so that the difference is obvious compared with the anti-inflammatory effect of example 1, and the proper proportion also influences the exertion of the anti-inflammatory effect of the toilet water.
In conclusion, the herbal refreshing mosquito-repellent itching-relieving toilet water disclosed by the invention is appropriate in refreshing degree, good in comfort level and remarkable in mosquito-repellent effect, can effectively resist inflammation and reduce swelling, can meet the requirements of cooling, relieving summer heat, relieving itching and reducing swelling of the public, and also has a remarkable mosquito-repellent effect.
From the above, the toilet water of the present invention is a preferred embodiment, and several modifications and alterations can be made without departing from the principle of the present invention, and all of them are included in the protection scope of the present invention.
Claims (5)
1. A herbal floral water with effects of refreshing, dispelling mosquitoes and relieving itching, which is characterized by comprising the following components in parts by weight: 30-40 parts of honeysuckle extract, 15-40 parts of paris polyphylla extract, 0.5-1.2 parts of basil volatile oil, 0.1-0.3 part of argyi leaf volatile oil, 0.5-1.2 parts of mint volatile oil, 0.3-1.0 part of lotus flower volatile oil, 0.3-1.5 parts of sweet osmanthus essential oil, 0.1-0.3 part of divaricate saposhnikovia root essential oil, 0.5-1.0 part of glycerol, 4.5-10 parts of mosquito repellent ester and 0.5-1.0 part of borneol.
2. The herbal refreshing mosquito-repellent itching-relieving toilet water as claimed in claim 1, which is characterized by comprising the following components in parts by weight: 40 parts of honeysuckle extract, 40 parts of rhizoma paridis extract, 1.0 part of basil volatile oil, 0.1 part of argy wormwood leaf volatile oil, 0.8 part of mint volatile oil, 0.5 part of lotus flower volatile oil, 0.5 part of sweet osmanthus essential oil, 0.1 part of divaricate saposhnikovia root essential oil, 0.5 part of glycerol, 5.0 parts of anophelifuge and 0.8 part of borneol.
3. The preparation method of the herbal floral water for refreshing, repelling mosquitoes and relieving itching according to claim 1 or 2, comprising the following steps:
step 1: mixing flos Lonicerae leaching solution and rhizoma paridis leaching solution to obtain mixed solution I,
step 2: adding folium artemisiae argyi volatile oil, basil volatile oil, mint volatile oil, lotus flower volatile oil, sweet osmanthus flower essential oil, divaricate saposhnikovia root essential oil and glycerin into the mixed solution I, and fixing the volume by using distilled water to obtain mixed solution II;
and step 3: heating the mixed solution II in a water bath kettle to completely dissolve;
and 4, step 4: standing, filtering, and mixing anophelifuge and Borneolum with the filtered mixture to obtain the final product.
4. The preparation method of the herbal mosquito-repellent itching-relieving toilet water according to claim 3, wherein the temperature of the water bath in step 3 is 35 ℃.
5. The preparation method of the herbal refreshing mosquito-repellent itching-relieving toilet water according to claim 3, wherein the standing time in the step 4 is 3-5 days.
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