CN105796468A - Preparation method of Vanilla peanigoeia Ancer toilet water - Google Patents
Preparation method of Vanilla peanigoeia Ancer toilet water Download PDFInfo
- Publication number
- CN105796468A CN105796468A CN201610377616.XA CN201610377616A CN105796468A CN 105796468 A CN105796468 A CN 105796468A CN 201610377616 A CN201610377616 A CN 201610377616A CN 105796468 A CN105796468 A CN 105796468A
- Authority
- CN
- China
- Prior art keywords
- herba
- filtrate
- weight
- distilled water
- peanigoeia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Plant Pathology (AREA)
- Biotechnology (AREA)
- Epidemiology (AREA)
- Zoology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Dermatology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Botany (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Emergency Medicine (AREA)
- Pest Control & Pesticides (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of Vanilla peanigoeia Ancer toilet water. The preparation method includes the steps of (1), storing edible alcohol and distilled water in containers respectively; (2), subjecting pods of Vanilla peanigoeia Ancer to freezing and unfreezing, soaking the pods of the Vanilla peanigoeia Ancer in an edible alcohol solution, and filtering to obtain first filtrate; (3), preparing extracts from Herba Elsholtziae, Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, galanga resurrectionlily rhizome, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, peppermint, calamus, Folium Perillae and Agastache Rugosus respectively; (4), screening and removing impurities from star anise, fennel and shedding phoenix tree bark, pulverizing the star anise, the fennel and the shedding phoenix tree bark, with the impurities removed, by a pulverizer prior to heating reflux extraction and blending extracting liquids; (5), boiling vespertilionum faeces and filtering the boiled vespertilionum faeces to obtain second filtrate; (6), uniformly mixing all the ingredients according to specific parts by weight so as to obtain the Vanilla peanigoeia Ancer toilet water. The Vanilla peanigoeia Ancer toilet water is remarkably effective in mosquito repellency and harmless to human health and is capable of relieving itching, diminishing swelling, soothing the nerves and improving eyesight and sleeping quality effectively.
Description
Technical field
The invention mainly relates to cosmetics of everyday use field, specifically the preparation method of a kind of Herba vanillae Planifoliae floral water.
Background technology
Mosquito needs to suck human blood and lays eggs, educates ovum, therefore brings many troubles to the mankind.Human body is by after mosquito bite, and skin can become red and swollen, and sufferings unbearably, have an effect on outward appearance.Additionally, mosquito bite also can affect sleep, propagation malaria, filaricide, epidemic encephalitis type B and leather steps on the diseases such as heat, human body health is totally unfavorable.
Herba vanillae Planifoliae floral water is that one can effectively prevent mosquito bite, containing anophelifuge, a small amount of essence, then is equipped with ethanol and a kind of perfume series products that water is made.Tradition has in the floral water of repelling effect, generally with the addition of the repellant of chemosynthesis, is coated on skin or spills on the ground, forms protecting film, makes the mosquito dare not be close.Although but the repellant of above-mentioned chemosynthesis has wide spectrum repellent action, most of hematophagus being had good effect, but long-term or a large amount of use there will be the problems such as skin allergy locally or systemically, skin lesion；It addition, summer, weather was scorching, it is easy to cause sleep quality bad, the phenomenon of of short duration dizziness, blurred vision occurs.
Summary of the invention
For solving deficiency of the prior art, the preparation method that the present invention provides a kind of Herba vanillae Planifoliae floral water, prepared floral water can effective anophelifuge, there is relieving itching and eliminating swelling effect, lossless health, it is also possible to calm the nerves eye-catching, effectively promote sleep quality.
The present invention for achieving the above object, is achieved through the following technical solutions:
The preparation method of a kind of Herba vanillae Planifoliae floral water, comprises the following steps:
(1): take edible ethanol, distilled water and put to container preservation respectively；
(2): take bean pod of Herba vanillae Planifoliae chilled, thaw, after using distilled water cleaning, pulverizing, add in 70%～75% edible alcohol solution by weight 1: 2～10, soak 5～10 days；Filter to get filtrate one；
(3): respectively Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis are dried, put respectively to container again, then be separately added into the distilled water of 10 times of weight, afterwards respectively 80-100 DEG C reflux, extract, 8-24 hour；Then, cooled and filtered, more respectively weight is concentrated into 1/10th, obtain each component extract；
null(4): by anise、Fructus Foeniculi、Naturally the Firmiana platanifolia (Linn. f.) Marsili bark screening and removing impurities come off，Then clear water washing by soaking is used，Then by the Firmiana platanifolia (Linn. f.) Marsili bark of washes clean、Anistree、Fructus Foeniculi is dried，Dry temperature not higher than 80 degrees Celsius，Use pulverizer is pulverized，Powder particle diameter controls to pass through No. 1 sieve，To the anise after pulverizing、Fructus Foeniculi、Bark heating and refluxing extraction 3 times，The distilled water reflux, extract, of 4～7 times of volumes of first time use 2～4 hours，70%～75% alcohol reflux of second time 4～6 times of volumes of use 4～6 hours，80%～95% alcohol reflux of third time 2～4 times of volumes of use 1～2.5 hour，United extraction liquid，Increase concentration of alcohol successively，To anise、Fructus Foeniculi and the cell wall of Firmiana platanifolia (Linn. f.) Marsili bark naturally come off progressively permeate，Anophelifuge substance is conducive to be fully extracted；
(5): take and after Faeces Vespertilionis is ground into powder, put into container, add the distilled water of 2 times of weight, obtain filtrate two after cooling after boiling, filtration, then the weight of filtrate two is concentrated into 1/10th；
(6): namely following components mix homogeneously by weight is obtained Herba vanillae Planifoliae floral water: edible ethanol 60%-75%, wetting agent 2%-5%, filtrate one 5%-7%, Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, each 1%-2% of Herba Pogostemonis extract, filtrate two 2%-5%, distilled water surplus after concentration.
Also include chelating agen 0.1%-0.3%, antioxidant 0.1%-0.5% and sun-proof alcohol-soluble pigment 0.1%-0.3%.
Also include solubilizing agent 0.1%-0.5%.
After step (5) is boiled, cool down after making water boiling 0.5-2h, be conducive to the chemical substance in Faeces Vespertilionis fully to discharge, the filtrate two of filtration.
Effect of described natural Chinese medicinal herb is as follows:
Herba vanillae Planifoliae: control pyretic toxicity, skin infection, innominate toxic swelling, eczema, scabies, worm venom.
Herba Moslae: Herba Moslae energy relieving the exterior syndrome by diaphoresis, removing dampness for regulating stomach, inducing diuresis to remove edema, has a headache and fever, and aversion to cold is lossless, and the feeling of stuffiness in chest is suffered from abdominal pain, vomiting and diarrhoea.
The Radix Angelicae Dahuricae: the functions such as the dehumidifying that gets rid of illness, evacuation of pus granulation promoting, promoting blood circulation and stopping pain.
Rhizoma Chuanxiong: blood-activating and qi-promoting, wind-expelling pain-stopping, the pungent temperature of Rhizoma Chuanxiong is fragrant dry, blood circulation promoting and blood stasis dispelling.
Rutin: block peripheroneural esthesiodic effect, and the skin reaching antipruritic effect inflammation infection has good restitution, skin antibacterial, clean, release skin are infected by the virus simultaneously.
Folium Artemisiae Argyi: dispersing cold for relieving pain；External removing dampness to relieve itching, abnormal smells from the patient can anophelifuge.
Rhizoma Kaempferiae: warming middle-JIAO for eliminating dampness, promoting the circulation of QI to relieve pain.
Herba Lycopi: invigorate blood circulation, inducing diuresis to remove edema.
Flos Magnoliae: dispersing wind and cold.
Flos Caryophylli: heat clearing away, removing toxic substances, antifungal.
Flos Lonicerae: energy dispelling wind-heat, also kind removing summer-heat blood poison, for various febrile diseases, such as fever of the body, dermexanthesis, send out the diseases such as speckle, pyretic toxicity carbuncle sore, laryngopharynx swelling and pain.
Herba Menthae: can releasing skin pruritus, erythra and eczema, clear away heart-fire improving eyesight.
Rhizoma Acori Graminei: there is the effect eliminated the phlegm, dissipate the medicine of wind hearing-improing and eyesight improving, damp eliminating removing toxic substances.
Folium Perillae: there are expelling wind and cold pathogens, regulate the flow of vital energy and in effect.
Herba Pogostemonis: have the effect such as dispelling summer-heat from superficies of the body, removing dampness to restore normal function of the stomach, has loose bowels for summertime flu, cold and heat headache, vomiting.
Faeces Vespertilionis: having effect for the treatment of conjunctival congestion and swelling pain, subconjuctival hemorrhage, inside and outside cataracta, the phenomenon well alleviating temporary blurred vision has mosquito repellent function simultaneously.
The abnormal smells from the patient that anise, Fructus Foeniculi, the extract of Firmiana platanifolia (Linn. f.) Marsili bark that naturally comes off distribute has good repelling effect.
Compared with the products such as existing Herba vanillae Planifoliae floral water, the present invention has advantage highlighted below:
The preparation method that the present invention adopts bean pod of Herba vanillae Planifoliae extract, has cooling effect containing Folium Menthae extract, containing anophelifuge substance: Folium Artemisiae Argyi extract, star anise extract, phoenix tree peel extract；Removing dampness material: Radix Angelicae Dahuricae extract, Rhizoma Kaempferiae extract, Herba Moslae extract, Rhizoma Acori Graminei extract, containing analgesic substance: Rhizoma Chuanxiong extract, Herba Lycopi extract；Containing antifungal substance: Flos Caryophylli extract, alleviation can be imitated because of miliaria, scorching hot and the discomfort that mosquito bite produces, again can long-acting mosquito-driving, Herba vanillae Planifoliae extract is wherein added adding, Flos Magnoliae extract, Herba vanillae Planifoliae is senior flavorant, there is the title of " king of flavorant ", not only nontoxic but also there is natural fragrance, and pharmacological evaluation proves, Herba vanillae Planifoliae extract can control pyretic toxicity, eczema, mosquito is bitten, there is natural flower aroma, the floral water prepared can effective anophelifuge, there is relieving itching and eliminating swelling effect, choose from natural Chinese medicinal herb, without toxic chemical substance, utilize the mutual synergism of Chinese medicine, lossless health, can also calm the nerves eye-catching, effectively promote sleep quality.
Making liquid distilled from honeysuckle flowers or lotus leaves edible ethanol concentration is 60%-75%, and this proportioning is easily penetrated into inside antibacterial, makes the protein in protoplasm and nucleus become irreversible curdled appearance, thus playing bactericidal action.Thus sterilization is strong.In order to prevent precipitation, it is possible to be aided with a small amount of chelating agen (sodium citrate), antioxidant (ditertbutylparacresol) and sun-proof alcohol-soluble pigment.
The using method of described Herba vanillae Planifoliae floral water is as follows:
The human body exposure portion such as opponent, foot, can be sprayed on product the human body exposure portion such as hands, foot, then smear uniformly with palm；To the exposure portion such as face, neck, first product can be sprayed on palm, then the exposure portion such as face, neck be smeared uniformly, it is also possible to product is sprayed directly on indoor or medicated clothing and carry out anophelifuge.
Detailed description of the invention
In conjunction with specific embodiments, the invention will be further described.Should be understood that these embodiments are merely to illustrate the present invention rather than restriction the scope of the present invention.In addition, it is to be understood that after having read the content that the present invention lectures, the present invention can be made various changes or modifications by those skilled in the art, and these equivalent form of values fall within the application appended claims limited range equally.
Embodiment 1:
(1): take edible ethanol, distilled water and put to container preservation respectively；
(2): take bean pod of Herba vanillae Planifoliae chilled, thaw, after using distilled water cleaning, pulverizing, add in 70% edible alcohol solution by weight 1: 2, soak 5 days；Filter to get filtrate one；
(3): respectively Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis are dried, put respectively to container again, then the distilled water of 10 times of weight it is separately added into, afterwards respectively 80 DEG C of reflux, extract, 8 hours, then, cooled and filtered, more respectively weight is concentrated into 1/10th, obtaining each component extract, backflow makes extract be fully extracted；
(4): by anise, Fructus Foeniculi, the Firmiana platanifolia (Linn. f.) Marsili bark screening and removing impurities that naturally comes off, then use clear water washing by soaking, then the Firmiana platanifolia (Linn. f.) Marsili bark of washes clean, anise, Fructus Foeniculi are dried, dry temperature 80 degrees Celsius, remove impurity；Use pulverizer is pulverized, powder particle diameter controls to pass through No. 1 sieve, to the anise after pulverizing, Fructus Foeniculi, bark heating and refluxing extraction 3 times, the distilled water reflux, extract, of 4 times of volumes of first time use 2 hours, 70% alcohol reflux of second time 4 times of volumes of use 4 hours, 80% alcohol reflux of third time 2 times of volumes of use 1 hour, united extraction liquid；
(5): take and after Faeces Vespertilionis is ground into powder, put into container, the distilled water of 2 times of weight of addition, boils and obtains filtrate two after cooling, filtration after cooling after making water boiling 0.5h, then the weight of filtrate two is concentrated into 1/10th；
(6): namely following components mix homogeneously by weight is obtained Herba vanillae Planifoliae floral water:
Edible ethanol 60%, wetting agent 2%, filtrate one 5%, Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis extract each 1%, filtrate 2 2%, distilled water surplus after concentration.
Embodiment 2:
(1): take edible ethanol, distilled water and put to container preservation respectively；
(2): take bean pod of Herba vanillae Planifoliae chilled, thaw, after using distilled water cleaning, pulverizing, add in 70%～75% edible alcohol solution by weight 1: 10, soak 10 days；Filter to get filtrate one；
(3): respectively Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis are dried, put respectively to container again, then the distilled water of 10 times of weight it is separately added into, afterwards respectively 100 DEG C of reflux, extract, 24 hours；Then, cooled and filtered, more respectively weight is concentrated into 1/10th, obtain each component extract；
(4): by anise, Fructus Foeniculi, naturally the Firmiana platanifolia (Linn. f.) Marsili bark screening and removing impurities come off, then clear water washing by soaking is used, then by the Firmiana platanifolia (Linn. f.) Marsili bark of washes clean, anistree, Fructus Foeniculi is dried, dry temperature 60 degrees Celsius, use pulverizer is pulverized, powder particle diameter controls to pass through No. 1 sieve, to the anise after pulverizing, Fructus Foeniculi, bark heating and refluxing extraction 3 times, the distilled water reflux, extract, of 7 times of volumes of first time use 4 hours, 75% alcohol reflux of second time 6 times of volumes of use 6 hours, 95% alcohol reflux of third time 4 times of volumes of use 2.5 hours, united extraction liquid；
(5): take and after Faeces Vespertilionis is ground into powder, put into container, add the distilled water of 2 times of weight, boil and obtain filtrate two after cooling, filtration after making water boiling 2h, then the weight of filtrate two is concentrated into 1/10th；
(6): namely following components mix homogeneously by weight is obtained Herba vanillae Planifoliae floral water:
Edible ethanol 75%, wetting agent 5%, filtrate one 7%, Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis extract each 2%, filtrate 2 5% after concentration, also include chelating agen 0.3%, antioxidant 0.5%, sun-proof alcohol-soluble pigment 0.3% and solubilizing agent 0.5%, distilled water surplus.
Embodiment 3:
(1): take edible ethanol, distilled water and put to container preservation respectively；
(2): take bean pod of Herba vanillae Planifoliae chilled, thaw, after using distilled water cleaning, pulverizing, add in 73% edible alcohol solution by weight 1: 6, soak 8 days；Filter to get filtrate one；
(3): respectively Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis are dried, put respectively to container again, then the distilled water of 10 times of weight it is separately added into, afterwards respectively 90 DEG C of reflux, extract, 12 hours；Then, cooled and filtered, more respectively weight is concentrated into 1/10th, obtain each component extract；
(4): by anise, Fructus Foeniculi, naturally the Firmiana platanifolia (Linn. f.) Marsili bark screening and removing impurities come off, then clear water washing by soaking is used, then by the Firmiana platanifolia (Linn. f.) Marsili bark of washes clean, anistree, Fructus Foeniculi is dried, dry temperature 70 degrees Celsius, use pulverizer is pulverized, powder particle diameter controls to pass through No. 1 sieve, to the anise after pulverizing, Fructus Foeniculi, bark heating and refluxing extraction 3 times, the distilled water reflux, extract, of 6 times of volumes of first time use 3 hours, 73% alcohol reflux of second time 5 times of volumes of use 5 hours, 90% alcohol reflux of third time 3 times of volumes of use 1.5 hours, united extraction liquid；
(5): take and after Faeces Vespertilionis is ground into powder, put into container, add the distilled water of 2 times of weight, boil and obtain filtrate two after cooling, filtration after making water boiling 1.5h, then the weight of filtrate two is concentrated into 1/10th；
(6): namely following components mix homogeneously by weight is obtained Herba vanillae Planifoliae floral water:
Edible ethanol 70%, wetting agent 3%, filtrate one 4%, Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis extract each 1.5%, filtrate 2 3.5% after concentration, also include chelating agen 0.1%, antioxidant 0.1%, sun-proof alcohol-soluble pigment 0.1% and solubilizing agent 0.1%, distilled water surplus.
Embodiment 4:(tests the drug effect of Herba vanillae Planifoliae floral water)
Aedes albopictus, indoor feeding normal lines, after emergence, 4～5 days female adult mosquitos are for measuring.
Method of testing: put into 200 Aedes albopictus in the mosquito cage that length, width and height are 35cm × 30cm × 35cm; after mosquito normal activity; the back of the hand of volunteer is exposed 4cm × 5cm skin; remainder tightly covers; hands stretches in mosquito cage and places 3 minutes, and the mosquito coming to stop falling is qualified for attack more than 30 persons.
Repellency test: the skin area respectively drawing 5cm × 5cm at volunteer's (being numbered 1#, 2#, 3#) left hand and right hand back that 3 attacks are qualified is test block, remainder uses medicated clothing to block, the test block of right hand the back of the hand is blank, the Herba vanillae Planifoliae floral water that the test block uniform application embodiment 3 of left hand the back of the hand prepares, tightly covers remainder.After smearing Herba vanillae Planifoliae floral water 2 hours, hands is stretched in mosquito cage 2 minutes, observe with or without mosquito bite, once every test in 1 hour, as long as there being 1 mosquito to come to bite and namely judge that anophelifuge lost efficacy later.
Result of the test: see following table:
As can be seen from the above table, Aedes albopictus is had certain repelling effect by the Herba vanillae Planifoliae floral water described in embodiment 3, and effective protecting time can reach 4～8 hours.
Claims (4)
1. the preparation method of a Herba vanillae Planifoliae floral water, it is characterised in that: comprise the following steps
(1): take edible ethanol, distilled water and put to container preservation respectively；
(2): take bean pod of Herba vanillae Planifoliae chilled, thaw, after using distilled water cleaning, pulverizing, add in 70%～75% edible alcohol solution by weight 1: 2～10, soak 5～10 days；Filter to get filtrate one；
(3): respectively Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, rutin, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, Herba Pogostemonis are dried, put respectively to container again, then be separately added into the distilled water of 10 times of weight, afterwards respectively 80-100 DEG C reflux, extract, 8-24 hour；Then, cooled and filtered, more respectively weight is concentrated into 1/10th, obtain each component extract；
(4): by anise, Fructus Foeniculi, naturally the Firmiana platanifolia (Linn. f.) Marsili bark screening and removing impurities come off, then clear water washing by soaking is used, then by the Firmiana platanifolia (Linn. f.) Marsili bark of washes clean, anistree, Fructus Foeniculi is dried, dry temperature not higher than 80 degrees Celsius, use pulverizer is pulverized, powder particle diameter controls to pass through No. 1 sieve, to the anise after pulverizing, Fructus Foeniculi, bark heating and refluxing extraction 3 times, the distilled water reflux, extract, of 4～7 times of volumes of first time use 2～4 hours, 70%～75% alcohol reflux of second time 4～6 times of volumes of use 4～6 hours, 80%～95% alcohol reflux of third time 2～4 times of volumes of use 1～2.5 hour, united extraction liquid；
(5): take and after Faeces Vespertilionis is ground into powder, put into container, add the distilled water of 2 times of weight, obtain filtrate two after cooling after boiling, filtration, then the weight of filtrate two is concentrated into 1/10th.
(6): namely following components mix homogeneously by weight is obtained Herba vanillae Planifoliae floral water:
Edible ethanol 60%-75%, wetting agent 2%-5%, filtrate one 5%-7%, Herba Moslae, the Radix Angelicae Dahuricae, Rhizoma Chuanxiong, Folium Artemisiae Argyi, Rhizoma Kaempferiae, Herba Lycopi, Flos Magnoliae, Flos Caryophylli, Flos Lonicerae, Herba Menthae, Rhizoma Acori Graminei, Folium Perillae, each 1%-2% of Herba Pogostemonis extract, filtrate two 2%-5%, distilled water surplus.
2. the preparation method of a kind of Herba vanillae Planifoliae floral water according to claim 1, it is characterised in that: it is characterized in that: also include chelating agen 0.1%-0.3%, antioxidant 0.1%-0.5% and sun-proof alcohol-soluble pigment 0.1%-0.3%.
3. the preparation method of a kind of Herba vanillae Planifoliae floral water according to claim 1, it is characterised in that: also include solubilizing agent 0.1%-0.5%.
4. the preparation method of a kind of Herba vanillae Planifoliae floral water according to claim 1, it is characterised in that: after step (5) is boiled, make the filtrate two of cold filtration after water boiling 0.5-2h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610377616.XA CN105796468A (en) | 2016-05-31 | 2016-05-31 | Preparation method of Vanilla peanigoeia Ancer toilet water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610377616.XA CN105796468A (en) | 2016-05-31 | 2016-05-31 | Preparation method of Vanilla peanigoeia Ancer toilet water |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105796468A true CN105796468A (en) | 2016-07-27 |
Family
ID=56427973
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610377616.XA Pending CN105796468A (en) | 2016-05-31 | 2016-05-31 | Preparation method of Vanilla peanigoeia Ancer toilet water |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105796468A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105123815A (en) * | 2015-09-21 | 2015-12-09 | 杰恩斯·沙比提 | Traditional Chinese medicine sachet capable of repelling mosquitoes and other insects |
| CN109203163A (en) * | 2018-08-24 | 2019-01-15 | 湖州汇德集团有限公司 | The production method of mosquito repellent wood floor |
-
2016
- 2016-05-31 CN CN201610377616.XA patent/CN105796468A/en active Pending
Non-Patent Citations (2)
| Title |
|---|
| 中华人民共和国卫生部: "化妆品禁用组分", 《化妆品卫生规范》 * |
| 吴海大: "化妆品及其原料的安全性", 《日用化学品科学》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105123815A (en) * | 2015-09-21 | 2015-12-09 | 杰恩斯·沙比提 | Traditional Chinese medicine sachet capable of repelling mosquitoes and other insects |
| CN109203163A (en) * | 2018-08-24 | 2019-01-15 | 湖州汇德集团有限公司 | The production method of mosquito repellent wood floor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103655718B (en) | Traditional Chinese medicine composition, preparation, and floral water and application method thereof | |
| CN103655245B (en) | Mosquito repelling flora water | |
| CN105724462A (en) | Electric mosquito-repellent incense liquid and preparation method | |
| CN109221260A (en) | A kind of mosquito repellent sachet | |
| CN105853263A (en) | Traditional Chinese medicinal mosquito repelling liquid and preparation method thereof | |
| CN106214571B (en) | Melia azedarach mosquito-repellent composition and preparation method and application thereof | |
| CN105796468A (en) | Preparation method of Vanilla peanigoeia Ancer toilet water | |
| KR20120009192A (en) | Oriental herbal bathing material and manufacturing method thereof | |
| CN104510641A (en) | Natural water lily eczema-removing baby oil | |
| CN103720841A (en) | Chinese medicinal preparation for treating chronic suppurative otitis media and preparation method thereof | |
| CN106377604A (en) | Antibacterial inflammation diminishing and itching relieving traditional Chinese medicine ointment and preparation method thereof | |
| CN104206444B (en) | A kind of electric liquid device fragrant containing lavender natural and preparation method | |
| CN103341044B (en) | Itching-relieving compound preparation and preparation method thereof | |
| CN102772626A (en) | Anti-inflammation detoxification sterilization medicine composition | |
| CN112891504A (en) | Four-season skin-care epidemic-prevention ginger paste with ginger decoction dregs as base materials and preparation method | |
| CN112022947A (en) | Bacteriostatic agent based on traditional Chinese herbal medicines and small molecular compounds, and preparation method and application thereof | |
| CN104784394A (en) | Traditional Chinese medicine sachet with capability of improving immunity and preparation method of traditional Chinese medicine sachet | |
| CN104922449A (en) | Traditional Chinese medicine disinfection solution and preparation method thereof | |
| CN104186571A (en) | Electric heating liquid mosquito-repellent incense with sweet marjoram fragrance and preparation method thereof | |
| CN109432244A (en) | A kind of Chinese medicine preparation and its preparation method and application improving sensitive skin state | |
| CN108434268A (en) | A kind of Chinese medicine preparation and preparation method thereof for treating dermatitis | |
| CN105079425A (en) | Composition preparation for treating infantile hand-foot-mouth disease, and preparation method of composition preparation | |
| CN105267457A (en) | Traditional Chinese medicine preparation for treating neonatal diaper dermatitis and method for preparing traditional Chinese medicine preparation | |
| CN106176414A (en) | A kind of ecological, environmental protective natural plants mosquito-repellent water | |
| CN105362522A (en) | Oral drug specially for treating male balanitis and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20161230 Address after: 224005 Yancheng City Institute of pharmaceutical industry, Yancheng, Career Technical College,, Jiangsu Applicant after: Yancheng industry Vocationl Technical College Address before: 224005 Yancheng City Institute of pharmaceutical industry, Yancheng, Career Technical College,, Jiangsu Applicant before: Xu Jingjing |
|
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160727 |
|
| RJ01 | Rejection of invention patent application after publication |