CN104224633A - Pure peony skin-care essential oil and preparation method thereof - Google Patents
Pure peony skin-care essential oil and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a pure peony skin-care essential oil which is prepared from peony essential oil, flower fragrance essential oil, a functional component and an additive component, wherein the flower fragrance essential oil is prepared by distilling a mixture of peony petals and chionanthus retusus flowers with steam, and then by concentrating and drying; the functional component is prepared by adding absolute ethyl alcohol to dissolve 30-50 parts of an oligomerization stilbene compound, 15-20 parts of peony root and bark extract, 15-20 parts of rutin, 5-10 parts of vitamin E and 15-20 parts of arbutin, wherein the weight of the absolute ethyl alcohol is 3-5 times of the total weight of the above five components; the additive component consists of the following components in parts by weight: 40-60 parts of glycerinum and 40-60 parts of hyaluronic acid. The skin-care essential oil disclosed by the invention can relatively well relieve stain, reduce melanin sedimentation, whiten the skin, activate the human skin surface cells, delay aging, moisten, isolate the ultraviolet light, and the like, is applicable to various skin types and people, can be used as a daily care essential oil, and can also be used as a healthcare massage oil.
Description
Technical field
The invention belongs to peony product deep process technology field, relate generally to a kind of pure Paeonia suffruticosa heal-care essential oil and preparation method thereof.
Background technology
There are some to be that mankind itself can not synthesize in unsaturated fatty acid, a kind of fatty acid must drawn from food, are also referred to as " required unsaturated fatty acid ".Must several unsaturated fatty acid be had extremely important, as linoleic acid, linolenic acid, arachidonic acid etc. in unsaturated fatty acid.Only otherwise lack linoleic acid, just can synthesize other two kinds in vivo must unsaturated fatty acids for human body.Linoleic acid has very strong opposing Characteristics of Free Radicals Produced, has splendid aging resistance and helps the multifrequency natures such as injection Vitamin B_6 absorption, having the collagen protein in very strong protection human skin, and the effect such as anti-melanin precipitation.Peony seed oil contains multiple unsaturated fatty acid, and its unsaturated fatty acid content is greater than 80%, wherein three kinds of important unsaturated fatty acids: linolenic acid, and the content of linoleic plus oleic acid is respectively: 35.7%, and 22.19%, 27.24%.In addition in peony seed oil still containing the odd-numbered fatty acid with better active anticancer, be a kind of have exploitation future important oily resource.Containing abundant oligomeric stilbene compound in the seed of Flos Moutan shell obtained in seed of Flos Moutan oil expression process, this compounds has extraordinary antioxidation and antibacterial activity, has important research and development and is worth.
Summary of the invention
The object of this invention is to provide a kind of take peony seed oil as pure Paeonia suffruticosa heal-care essential oil of primary raw material and preparation method thereof; this heal-care essential oil can desalinate mottle, reduction melanin deposition, skin whitening, removal speckle, activating human body skin surface cell preferably, reduce wrinkle appearance, slow down aging, moisturizing, isolation ultraviolet etc.; be applicable to various skin quality and crowd; as daily nursing quintessence oil, also can be used as health-care massage oil.
The technical scheme that the present invention realizes above-mentioned purpose employing is: a kind of pure Paeonia suffruticosa heal-care essential oil, is made up: seed of Flos Moutan quintessence oil 80-90%, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6% according to mass percent of following composition;
Described seed of Flos Moutan quintessence oil be seed of Flos Moutan squeeze the seed of Flos Moutan crude oil that obtains through coming unstuck, deacidification, defat dewaxing treatment again obtains after decolouring and deodorize seed of Flos Moutan quintessence oil;
Described Rose Absolute is concentrated after vapor distillation, dry obtained by the mixture of peony petal and Diffuse Coptosapelta flower;
Described functional component, obtains after adding five gross weight 3-5 anhydrous alcohol solution doubly by oligomeric stilbene compound 30-50 part, moutan root bark extract 15-20 part, rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part according to parts by weight; Wherein, oligomeric stilbene compound is the dried powder obtained after extraction, enrichment and drying from seed of Flos Moutan shell; The filtration cakes torrefaction that moutan root bark extract is obtained after vapor distillation, crystallization, filtration by moutan root bark obtains;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight.
The preparation method of described pure Paeonia suffruticosa heal-care essential oil, comprises the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get seed of Flos Moutan and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant of its weight 1-3% is added in peony seed oil, stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, then be cooled to 5-10 DEG C, place 4-6h, then use 200 mesh screen, discard filtering residue, and the distilled water adding its weight 8-12% in the oil after filtration washs, separatory, removing water layer, obtain elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add its weight 2-4 dehydrated alcohol doubly, extract 1h under agitation, under-5-0 DEG C of condition, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, add mixing petal weight 1-3 sodium chloride doubly to stir, pickle 20-40min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, adding its weight 10-12 mass percent is doubly 95% ethanol, extracts 30-50 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; In concentrated extract, add mass percent is that the ethanol of 20-30% dissolves, filter, filtrate absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add weight 3-5 acetone solution doubly, then use solvent soln weight 8-15 activated carbon adsorption doubly, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, add its weight 15-20 water doubly and distill, collect distillate, be placed on after leaving standstill 18-24h in 2-5 DEG C of refrigerator, filter, collect filter cake, obtain moutan root bark extract, for subsequent use;
Oligomeric stilbene compound 30-50 part obtained above, moutan root bark extract 15-20 part is got according to parts by weight, and then get rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part, after mix homogeneously, add five gross weight 3-5 anhydrous alcohol solution doubly, namely functional component is obtained, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight, low whipping speed is stir 30 more than min under the condition of 60-120 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil 80-90% that step one to step 4 obtains, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6% is got according to mass percent, low whipping speed is stir more than 2h under the condition of 60-120 r/min, then at room temperature ageing 30-60d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
Seed of Flos Moutan described in step one is the seed of Flos Moutan obtained after the seed shelling of phoenix Paeonia suffruticosa or Paeonia papaveracea.
Peony petal described in step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
Surfactant described in step one is one or more in dodecylbenzene sodium sulfonate, sucrose ester, sodium hexameta phosphate, Dodecyl Polyoxyethylene Ether sodium sulfate.
Macroporous adsorbent resin described in step 3 be HPD-100, HPD-600,801, HZ 806, one in HZ816 resin.
beneficial effect of the present invention
one,heal-care essential oil whitening provided by the invention, moisturizing, antibacterial, antioxidation and the effect such as free radical resisting, anti-ultraviolet are remarkable; mottle, reduction melanin deposition, skin whitening, removal speckle, activating human body skin surface cell can be desalinated preferably, reduce wrinkle appearance, slow down aging, moisturizing, isolation ultraviolet etc.; and effectively can improve the diseases such as skin is itched, redness, drying, pimples; nontoxic, have no side effect; be applicable to various skin quality and crowd; as daily nursing quintessence oil, also can be used as health-care massage oil.
They are two years old, base oil of the present invention is the pure peony seed oil through surfactant defat and alcohol extraction defat associating defat, by the combination of the defat of association list surface-active agent and alcohol extraction defatting technology, make the defat peony seed oil defat of preparation more thorough, the defat oil colours pool of preparation is yellowish, mobility is very good, be very easy to be absorbed by the body, thus make the quintessence oil of preparation very little to skin irritation, be applicable to various skin quality and crowd, especially easily itch, red and swollen, dry, inflammation, oiliness, anaphylaxis and the most tender and lovely infant skin, child, old people, anemia of pregnant woman or athlete all can use, applied widely, and Be very effective.
In this heal-care essential oil, three, with the addition of two kinds of floral perfumes, by first by peony petal and the mixing of Diffuse Coptosapelta flower, salt adding prepares quintessence oil by the method that vapor distillation prepares essence after pickling process again, make the quintessence oil fragrance nature of preparation, pure, strong, fragrance is unique, and fragrance is pleasant.The fragrance of a flower fragrance that existing Diffuse Coptosapelta flower essential oil is pure, has again the fragrance of Flos Moutan uniqueness, and these two kinds of quintessence oils also have good antibacterial action.In the functional component of adding, the Gnetin H obtained is extracted from seed of Flos Moutan shell, to skin whitening and moistening effect especially remarkable, also to improving melanotic nevus, freckle has good improvement curative effect, also has the effects such as antiinflammatory, reducing swelling and alleviating pain, antiallergic, antiviral, and mildly can remove the cutin of skin surface, allow skin be rich in life, there is effect of tender skin.
Detailed description of the invention
A kind of pure Paeonia suffruticosa heal-care essential oil, is made up of following composition according to mass percent: seed of Flos Moutan quintessence oil 80-90%, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6%;
Described seed of Flos Moutan quintessence oil be seed of Flos Moutan squeeze the seed of Flos Moutan crude oil that obtains through coming unstuck, deacidification, defat dewaxing treatment again obtains after decolouring and deodorize seed of Flos Moutan quintessence oil;
Described Rose Absolute is concentrated after vapor distillation, dry obtained by the mixture of peony petal and Diffuse Coptosapelta flower;
Described functional component, obtains after adding five gross weight 3-5 anhydrous alcohol solution doubly by oligomeric stilbene compound 30-50 part, moutan root bark extract 15-20 part, rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part according to parts by weight; Wherein, oligomeric stilbene compound is the dried powder obtained after extraction, enrichment and drying from seed of Flos Moutan shell; The filtration cakes torrefaction that moutan root bark extract is obtained after vapor distillation, crystallization, filtration by moutan root bark obtains;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight.
The preparation method of described pure Paeonia suffruticosa heal-care essential oil, comprises the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get seed of Flos Moutan and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant of its weight 1-3% is added in peony seed oil, stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, then be cooled to 5-10 DEG C, place 4-6h, then use 200 mesh screen, discard filtering residue, and the distilled water adding its weight 8-12% in the oil after filtration washs, separatory, removing water layer, obtain elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add its weight 2-4 dehydrated alcohol doubly, extract 1h under agitation, under-5-0 DEG C of condition, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, add mixing petal weight 1-3 sodium chloride doubly to stir, pickle 20-40min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, adding its weight 10-12 mass percent is doubly 95% ethanol, extracts 30-50 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; In concentrated extract, add mass percent is that the ethanol of 20-30% dissolves, filter, filtrate absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add weight 3-5 acetone solution doubly, then use solvent soln weight 8-15 activated carbon adsorption doubly, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, add its weight 15-20 water doubly and distill, collect distillate, be placed on after leaving standstill 18-24h in 2-5 DEG C of refrigerator, filter, collect filter cake, obtain moutan root bark extract, for subsequent use;
Oligomeric stilbene compound 30-50 part obtained above, moutan root bark extract 15-20 part is got according to parts by weight, and then get rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part, after mix homogeneously, add five gross weight 3-5 anhydrous alcohol solution doubly, namely functional component is obtained, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight, low whipping speed is stir 30 more than min under the condition of 60-120 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil 80-90% that step one to step 4 obtains, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6% is got according to mass percent, low whipping speed is stir more than 2h under the condition of 60-120 r/min, then at room temperature ageing 30-60d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
Seed of Flos Moutan described in step one is the seed of Flos Moutan obtained after the seed shelling of phoenix Paeonia suffruticosa or Paeonia papaveracea.
Peony petal described in step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
Surfactant described in step one is one or more in dodecylbenzene sodium sulfonate, sucrose ester, sodium hexameta phosphate, Dodecyl Polyoxyethylene Ether sodium sulfate.
Macroporous adsorbent resin described in step 3 be HPD-100, HPD-600,801, HZ 806, one in HZ816 resin.
below in conjunction with specific embodiment, the present invention will be further described:
embodiment 1:
A kind of pure Paeonia suffruticosa heal-care essential oil, is made up of following composition according to mass percent: seed of Flos Moutan quintessence oil 80%, Rose Absolute 6%, functional component 8% and adding ingredient 6%;
Described functional component, obtains after adding the anhydrous alcohol solution of five gross weight 3 times by oligomeric stilbene compound 30 parts, moutan root bark extract 15 parts, rutin 15 parts, vitamin E 5 parts and arbutin 15 parts according to parts by weight; Described adding ingredient is made up of glycerol 40 parts and hyaluronic acid 60 parts according to parts by weight.
The preparation method of described pure Paeonia suffruticosa heal-care essential oil, comprises the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get phoenix seed of Flos Moutan and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant sodium dodecyl base benzene sulfonic acid sodium salt of its weight 1% is added in peony seed oil, stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, then be cooled to 5 DEG C, place 4h, then use 200 mesh screen, discard filtering residue, and the distilled water adding its weight 8% in the oil after filtration washs, separatory, removing water layer, obtain elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add the dehydrated alcohol of its weight 2 times, extract 1h under agitation, under-5 DEG C of conditions, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh tree peony peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, the sodium chloride adding mixing petal weight 1 times stirs, pickle 20min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, the mass percent adding its weight 10 times is 95% ethanol, extracts 30 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; Add in concentrated extract mass percent be 20% ethanol dissolve, filter, filtrate uses HPD-100 absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add the acetone solution of weight 3 times, then use solvent soln weight 8-activated carbon adsorption doubly, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, the water adding its weight 15 times distills, and collects distillate, is placed on after leaving standstill 18h in 2 DEG C of refrigerators, filters, collect filter cake, obtain moutan root bark extract, for subsequent use;
Get oligomeric stilbene compound obtained above, moutan root bark extract according to parts by weight, and then get rutin, vitamin E and arbutin, after mix homogeneously, add the anhydrous alcohol solution of five gross weight 3 times, namely obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol and hyaluronic acid according to parts by weight, low whipping speed is stir 30 more than min under the condition of 60 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil, Rose Absolute, functional component and the adding ingredient that step one to step 4 obtains is got according to above-mentioned mass percent, low whipping speed is stir more than 2h under the condition of 60r/min, then at room temperature ageing 30d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
embodiment 2:
A kind of pure Paeonia suffruticosa heal-care essential oil, is made up of following composition according to mass percent: seed of Flos Moutan quintessence oil 90%, Rose Absolute 3%, functional component 4% and adding ingredient 3%;
Described functional component, obtains after adding the anhydrous alcohol solution of five gross weight 5 times by oligomeric stilbene compound 50 parts, moutan root bark extract 20 parts, rutin 20 parts, vitamin e1 0 part and arbutin 20 parts according to parts by weight; Described adding ingredient is made up of glycerol 60 parts and hyaluronic acid 40 parts according to parts by weight.
The preparation method of described pure Paeonia suffruticosa heal-care essential oil, comprises the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get paeonia rockii seed and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant of its weight 3% is added in peony seed oil, surfactant is weight ratio is the sucrose ester of 1:1 and the mixture of sodium hexameta phosphate, and stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, is then cooled to 10 DEG C, place 6h, use 200 mesh screen again, discard filtering residue, and the distilled water adding its weight 12% in the oil after filtration washs, separatory, removing water layer, obtains elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add the dehydrated alcohol of its weight 4 times, extract 1h under agitation, under 0 DEG C of condition, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh ROUFURONG peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, the sodium chloride adding mixing petal weight 3 times stirs, pickle 40min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, the mass percent adding its weight 12 times is 95% ethanol, extracts 50 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; Add in concentrated extract mass percent be 30% ethanol dissolve, filter, filtrate is with HZ 806 absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add the acetone solution of weight 5 times, then use the activated carbon adsorption of solvent soln weight 15 times, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, the water adding its weight 20 times distills, and collects distillate, is placed on after leaving standstill 24h in 5 DEG C of refrigerators, filters, collect filter cake, obtain moutan root bark extract, for subsequent use;
Get oligomeric stilbene compound obtained above, moutan root bark extract according to parts by weight, and then get rutin, vitamin E and arbutin, after mix homogeneously, add the anhydrous alcohol solution of five gross weight 5 times, namely obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 60 parts and hyaluronic acid 40 parts according to parts by weight, low whipping speed is stir 30 more than min under the condition of 120 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil, Rose Absolute, functional component and the adding ingredient that step one to step 4 obtains is got according to mass percent, low whipping speed is stir more than 2h under the condition of 120 r/min, then at room temperature ageing 60d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
embodiment 3:
A kind of pure Paeonia suffruticosa heal-care essential oil, is made up of following composition according to mass percent: seed of Flos Moutan quintessence oil 85%, Rose Absolute 4%, functional component 6% and adding ingredient 5%;
Described functional component, obtains after adding the anhydrous alcohol solution of five gross weight 4 times by oligomeric stilbene compound 40 parts, moutan root bark extract 18 parts, rutin 18 parts, vitamin E 8 parts and arbutin 18 parts according to parts by weight; Described adding ingredient is made up of glycerol 50 parts and hyaluronic acid 50 parts according to parts by weight.
The preparation method of described pure Paeonia suffruticosa heal-care essential oil, comprises the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get paeonia rockii seed and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant Dodecyl Polyoxyethylene Ether sodium sulfate of its weight 2% is added in peony seed oil, stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, then be cooled to 7 DEG C, place 5h, then use 200 mesh screen, discard filtering residue, and the distilled water adding its weight 10% in the oil after filtration washs, separatory, removing water layer, obtain elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add the dehydrated alcohol of its weight 3 times, extract 1h under agitation, under-3 DEG C of conditions, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh tree peony peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, the sodium chloride adding mixing petal weight 2 times stirs, pickle 30min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, the mass percent adding its weight 11 times is 95% ethanol, extracts 40 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; Add in concentrated extract mass percent be 30% ethanol dissolve, filter, filtrate uses HZ816 absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add the acetone solution of weight 4 times, then use the activated carbon adsorption of solvent soln weight 12 times, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, the water adding its weight 18 times distills, and collects distillate, is placed on after leaving standstill 22h in 3 DEG C of refrigerators, filters, collect filter cake, obtain moutan root bark extract, for subsequent use;
Get oligomeric stilbene compound obtained above, moutan root bark extract according to parts by weight, and then get rutin, vitamin E and arbutin, after mix homogeneously, add the anhydrous alcohol solution of five gross weight 4 times, namely obtain functional component, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol and hyaluronic acid according to parts by weight, low whipping speed is stir 30 more than min under the condition of 90 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil, Rose Absolute, functional component and the adding ingredient that step one to step 4 obtains is got according to mass percent, low whipping speed is stir more than 2h under the condition of 90 r/min, then at room temperature ageing 45d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
test data
1. the heal-care essential oil bacteriostatic test that prepared by the present invention is studied
(1) bacterial strain:
antibacterial:staphylococcus aureus
s. aureas, bacillus subtilis
bacillus subtilis, escherichia coli
e. agalactiae, Salmonella
samonellal;
mycete:aspergillus niger: Aspergillus niger;
yeast:candida albicans Candida Albicans
(2) configuration of bacterium liquid
By each inoculation in corresponding culture medium, antibacterial cultivates 36-48 hour at 37 DEG C, and the appropriate bacterium colony of picking is mixed homogeneously with physiological saline solution respectively, and be mixed with certain density plastc ring, mixed cell suspension total concentration is about 1.0*10
8cfu/mL, the refrigerator being placed in 4 DEG C is for subsequent use.Mycete is cultivated 120 hours in 27 DEG C of constant incubators, yeast is cultivated 24 hours under similarity condition, the appropriate yeast and mold bacterium colony of picking mix homogeneously in physiological saline solution, makes certain density plastc ring, and mixing yeast and mold total concentration is about 1.0*10
7cfu/mL, the refrigerator being placed in 4 DEG C is for subsequent use.
(3) method
Adopt the method for American Pharmacopeia Microbial Challenge testing inspection preservative effectiveness.Take the obtained heal-care essential oil 100 grams of embodiment 1 as test sample, load in appropriate container, add appropriate plastc ring respectively, make every gram of sample finally containing amount of bacteria (1-5) * 10
6cfu/mL, yeast and mold amount is (1-5) * 10
5cfu/mL, abundant mix homogeneously, is placed in 37 DEG C of incubators respectively and cultivates.At 0 day of inoculation, 3 days, 7 days, 14 days, within 21 days and 28 days, sample and carry out bacterium component analysis, result was as shown in table 1.
Table 1: colony counts change list
2. cosmetics result of use investigation:
(1) whitening and freckle effect
Crowd on probation: (1) 18-28 year crowd, women 50 people; (2) 28-40 year crowd, female 50 people; (3) 40-55 year crowd, women 50 people.
Using method: smear these skin care item after clean of crowd's morning and evening every day on probation, use and add up effect after 20 days.
Effect assessment: before comparatively using after use, skin becomes pale exquisiteness, mottle is desalinated, and is successful; Otherwise, for not obvious; Statistical result is as shown in table 2:
Table 2:
(2) moistening effect
Number on probation: (1) 18-28 year crowd, women 50 people; (2) 28-40 year crowd, women 50 people; (3) 40-55 year crowd, women 50 people.
Using method: smear these skin care item after clean of crowd's morning and evening every day on probation, use and add up effect after 10 days.
Effect assessment: before comparatively using after use, skin becomes moistening exquisiteness, has elastic force, dried bark on the face disappears, and is successful; Otherwise, be DeGrain; Statistical result is as shown in table 3:
Table 3:
(3) to comedo action effect
Number on probation: (1) 16-28 year crowd, women 50 people; Male 50 people.
Using method: smear these skin care item after clean of crowd's morning and evening every day on probation, use and add up effect after 20 days.
Effect assessment: before comparatively using after use, comedo original pox print of skin alleviates thin out, and does not grow comedo having smallpox and tail off, and is successful; Otherwise, be DeGrain; Statistical result is as shown in table 4:
Table 4:
Claims (6)
1. a pure Paeonia suffruticosa heal-care essential oil, is characterized in that: be made up of following composition according to mass percent: seed of Flos Moutan quintessence oil 80-90%, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6%;
Described seed of Flos Moutan quintessence oil be seed of Flos Moutan squeeze the seed of Flos Moutan crude oil that obtains through coming unstuck, deacidification, defat dewaxing treatment again obtains after decolouring and deodorize seed of Flos Moutan quintessence oil;
Described Rose Absolute is concentrated after vapor distillation, dry obtained by the mixture of peony petal and Diffuse Coptosapelta flower;
Described functional component, obtains after adding five gross weight 3-5 anhydrous alcohol solution doubly by oligomeric stilbene compound 30-50 part, moutan root bark extract 15-20 part, rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part according to parts by weight; Wherein, oligomeric stilbene compound is the dried powder obtained after extraction, enrichment and drying from seed of Flos Moutan shell; The filtration cakes torrefaction that moutan root bark extract is obtained after vapor distillation, crystallization, filtration by moutan root bark obtains;
Described adding ingredient is made up of glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight.
2. the preparation method of a kind of pure Paeonia suffruticosa heal-care essential oil as claimed in claim 1, is characterized in that: comprise the following steps:
The preparation of step one, seed of Flos Moutan quintessence oil
Get seed of Flos Moutan and squeeze the seed of Flos Moutan crude oil obtained, come unstuck, deacidification, after decolouring and deodorize process, obtain peony seed oil, for subsequent use; The surfactant of its weight 1-3% is added in peony seed oil, stirring and emulsifying 1h under temperature is no more than 30 DEG C of conditions, then be cooled to 5-10 DEG C, place 4-6h, then use 200 mesh screen, discard filtering residue, and the distilled water adding its weight 8-12% in the oil after filtration washs, separatory, removing water layer, obtain elementary dewaxed oil, for subsequent use; In elementary dewaxed oil, add its weight 2-4 dehydrated alcohol doubly, extract 1h under agitation, under-5-0 DEG C of condition, leave standstill 30min after extraction terminates, separatory, gets subnatant, namely obtains seed of Flos Moutan quintessence oil, for subsequent use;
The preparation of step 2, Rose Absolute
Get fresh peony petal and Diffuse Coptosapelta flower raw material, according to the ratio mixing that peony petal and Diffuse Coptosapelta flower weight ratio are 1:3, add mixing petal weight 1-3 sodium chloride doubly to stir, pickle 20-40min, be then placed in vapor distillation device and extract, the distillation obtained is extracted with ethyl acetate, extract reclaims ethyl acetate, the concentrated extract obtained is adopted dried over anhydrous sodium carbonate, obtains Rose Absolute, for subsequent use;
The preparation of step 3, functional component
Get seed of Flos Moutan shell raw material, adding its weight 10-12 mass percent is doubly 95% ethanol, extracts 30-50 min under ultrasound condition, filters, collect extracting solution, then repeat supersound extraction and filter operation 2 times, merge the extracting solution of three times, be concentrated into solvent-free, obtain extracting extractum, for subsequent use; In concentrated extract, add mass percent is that the ethanol of 20-30% dissolves, filter, filtrate absorption with macroporous adsorbent resin, then the ethanol elution gradient elution of 20%, 30%, 40%, 50%, 60%, 80% and 95% is followed successively by with mass percent, collect the fraction that mass percent is the ethanol elution of 50%, be concentrated into solvent-free, obtain function extractum, for subsequent use; In function extractum, add weight 3-5 acetone solution doubly, then use solvent soln weight 8-15 activated carbon adsorption doubly, filter, filtrate decompression reclaims acetone, and the dried powder obtained is oligomeric stilbene compound, for subsequent use;
Get moutan root bark raw material, add its weight 15-20 water doubly and distill, collect distillate, be placed on after leaving standstill 18-24h in 2-5 DEG C of refrigerator, filter, collect filter cake, obtain moutan root bark extract, for subsequent use;
Oligomeric stilbene compound 30-50 part obtained above, moutan root bark extract 15-20 part is got according to parts by weight, and then get rutin 15-20 part, vitamin E 5-10 part and arbutin 15-20 part, after mix homogeneously, add five gross weight 3-5 anhydrous alcohol solution doubly, namely functional component is obtained, for subsequent use;
The preparation of step 4, adding ingredient
Get raw material glycerol 40-60 part and hyaluronic acid 40-60 part according to parts by weight, low whipping speed is stir 30 more than min under the condition of 60-120 r/min, and namely obtained adding ingredient, for subsequent use;
The preparation of step 5, pure Paeonia suffruticosa heal-care essential oil
Seed of Flos Moutan quintessence oil 80-90% that step one to step 4 obtains, Rose Absolute 3-6%, functional component 4-8% and adding ingredient 3-6% is got according to mass percent, low whipping speed is stir more than 2h under the condition of 60-120 r/min, then at room temperature ageing 30-60d, filter screen is adopted to be that 1000 object filters filter again, collect filtrate, subpackage, namely completes the preparation of pure Paeonia suffruticosa heal-care essential oil.
3. the preparation method of a kind of pure Paeonia suffruticosa heal-care essential oil as claimed in claim 2, is characterized in that: the seed of Flos Moutan described in step one is the seed of Flos Moutan obtained after the seed shelling of phoenix Paeonia suffruticosa or Paeonia papaveracea.
4. the preparation method of a kind of pure Paeonia suffruticosa heal-care essential oil as claimed in claim 2, is characterized in that: the peony petal described in step 2 is the petal of Zhao's pink peony or ROUFURONG Flos Moutan.
5. the preparation method of a kind of pure Paeonia suffruticosa heal-care essential oil as claimed in claim 2, is characterized in that: the surfactant described in step one is one or more in dodecylbenzene sodium sulfonate, sucrose ester, sodium hexameta phosphate, Dodecyl Polyoxyethylene Ether sodium sulfate.
6. the preparation method of a kind of pure Paeonia suffruticosa heal-care essential oil as claimed in claim 2, is characterized in that: the macroporous adsorbent resin described in step 3 be HPD-100, HPD-600,801, HZ 806, one in HZ816 resin.
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