CN108785166A - A method of producing edible cosmetics using paeonia rockii seed - Google Patents

A method of producing edible cosmetics using paeonia rockii seed Download PDF

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CN108785166A
CN108785166A CN201810745195.0A CN201810745195A CN108785166A CN 108785166 A CN108785166 A CN 108785166A CN 201810745195 A CN201810745195 A CN 201810745195A CN 108785166 A CN108785166 A CN 108785166A
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paeonia
valve
peony seeds
peony
gas
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CN108785166B (en
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芦玉君
冉烔
窦永位
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Gansu Changyuan Ecological Agriculture Technology Co Ltd
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Gansu Changyuan Ecological Agriculture Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/12Fermented milk preparations; Treatment using microorganisms or enzymes
    • A23C9/13Fermented milk preparations; Treatment using microorganisms or enzymes using additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G1/00Preparation of wine or sparkling wine
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/92Oral administration

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Abstract

The invention discloses a kind of methods producing edible cosmetics using paeonia rockii seed, belong to cosmetics technical field.The edible cosmetics raw material of the present invention is prepared by paeonia rockii seed, fresh Paeonia papaveracea petal, pistil, new fresh-rose.Production this method of the present invention extracts at low temperature, ensure that natural original active constituent of raw material does not destroy, the nutritional ingredient of paeonia rockii seed.Product quality produced by the invention is high, and nutrition is comprehensive, does not generate harmful substance, does not generate the three wastes substantially, all recycling utilizes waste residue again, does not pollute the environment, simple production process is easy to operate.Low energy consumption for preparation process of the present invention, and production cost is low, and process units takes up an area few.Product yield is high, can save resource.

Description

A method of producing edible cosmetics using paeonia rockii seed
Technical field
The invention belongs to cosmetics technical fields, and in particular to a kind of to produce edible health care using paeonia rockii seed The method of cosmetics.
Background technology
The main place of production of Paeonia papaveracea is the peculiar kind of China in Gansu the Northwest, it be in Chinese Tree Peony Cultivars most Excellent kind.Paeonia papaveracea complete stool is all precious, and especially its seed, flower, pistil have more unique nutritive value.Purple plague purpura is male The nutritive value of the health products oil of red seed production is:It contains alpha-linolenic acid 42%, contains linoleic acid 27%, contains oleic acid 23%, in addition Also contain the nutritional ingredients such as vitamin A, vitamin C, vitamin E and biological polyphenol.
Take paeonia rockii seed oil have effects that it is following:1) effect for reducing body's cholesterol, can reduce human blood-pressure, Blood fat is reduced, cardiovascular and cardiovascular and cerebrovascular disease risk can be reduced;2) prevent diabetes and its complication;3) people can be enhanced The immunocompetence of body;4) has effects that anti-aging and oxidation resistant;5) have effects that clear up harmful substance in blood;6) have The effect of improving man memory ability;7) have effects that prevent multiple sclerosis;8) with anti-treating rheumatic arthritis Effect;9) there is the effect of prevention skin tinea or wet disease.
The nutritive value of Paeonia papaveracea and pistil:Paeonia papaveracea petal and pollen contain several amino of needed by human ten Acid, vitamin E and general flavone.There is beautifying face and moistering lotion, reducing blood lipid, blood pressure lowering, hypoglycemic, promoting blood circulation and removing blood stasis, improvement to sleep, is clear for it Fiery improving eyesight, promote longevity, improve anaemia, blood-nourishing protect liver, mitigate chloasma faciei, delay middle-aged and the old's climacteric and prevention before The multi-efficiency of row gland disease.
The nutritive value of rose:The Major Nutrient of rose be geraniol, citronellol, nerol, benzyl carbinol, nonyl alcohol, Linalool, haematochrome and carrotene.It has effects that beautifying face and moistering lotion and slows down aging.Currently, the oil expression method of peony oil by Three kinds below:1) mechanical pressing method, this method squeezing oil recovery rate is low, and the oil quality squeezed out is unstable;2) mechanical presses method:It should The damp deep, unstable quality of oil colours that method squeezes out, the component of fragile bad oil;3) solvent leaching:The product of leaching dissolution There is peculiar smell, there is dissolvent residual, small size solvent.How to avoid and overcomes the shortcomings of that the above peony oil oil expression and defect become currently urgently Problem to be solved.Currently, people live in densely populated, seriously polluted, environmental degradation, diet is bad, and operating pressure is big Under state, there are many body inferior health person crowd, and it is a first-class selection to select tree peony health food.
Invention content
It is an object of the invention to overcome the shortcomings of and avoid prior art and defect, designs and research and develop and is a kind of novel The technique stream of edible cosmetics is made of paeonia rockii seed, Paeonia papaveracea petal, Paeonia papaveracea pistil and roseleaf Journey.
In order to achieve the above object, the present invention is achieved by the following scheme.
A kind of to produce edible cosmetics using paeonia rockii seed, raw material is by paeonia rockii seed, fresh Paeonia papaveracea Petal, pistil, new fresh-rose are formed by following weight fraction:Paeonia rockii seed 87%~91%, Paeonia papaveracea petal 6%~ 8%, Paeonia papaveracea pistil 2%~5%, new fresh-rose 1%~2%.
The present invention is multicomponent mixture system, and each component role is as follows in system:
1) paeonia rockii seed, Paeonia papaveracea petal, Paeonia papaveracea pistil:Specific Varieties of Peony production is in Gansu, Qinghai, Ningxia And and the production of the ground such as Henan paeonia rockii seed, Paeonia papaveracea petal and Paeonia papaveracea pistil.
1. paeonia rockii seed:Paeonia rockii seed extract oil is that the current world preferably obtains my vegetable oil, it is full of nutrition, meets Absorption of human body, and have medical care effect, paeonia rockii seed oil is up to 92% or more, predominantly flax containing unsaturated fatty acid Acid, linoleic acid, oleic acid, it provides unsaturated fatty acid to product in systems.
2. Paeonia papaveracea petal:Paeonia papaveracea contains many amino acid of a large amount of tare weight, protein and vitamin E, it In systems amino acid and vitamin E are provided to product.
3. Paeonia papaveracea pistil:Paeonia papaveracea pistil contains a large amount of amino acid, protein and vitamin E, it is in system In to product provide amino acid and vitamin E.
2) new fresh-rose:It is the brackish water rose of specific Yongdeng County, Gansu Province production;It contains citronellol, nerol, benzene second The substances such as alcohol, nonyl alcohol, linalool, haematochrome and carrotene.Its effect in systems is to be had additional nutrients with product and fragrance, Improve product mouthfeel.
The method for producing edible cosmetics using paeonia rockii seed, includes the following steps:
1) entire process units edible vegetable oil is clean, it must not be by any type of greasy dirt and grease;CO will be housed2Steel cylinder with System is connected, and closes valve A, valve B and valve C is opened, by CO2It is put into cryoliquifier, cryoliquifier external application -25 DEG C frozen liq, by CO2Temperature is reduced to -5 DEG C, will be cooled to -5 DEG C of CO2It is sent into buffer;
2) valve D is opened, by CO2It is sent into pressuring machine;The CO that will be pressurizeed in pressuring machine2It is sent into heater, heater adds The hot water heating that 60 DEG C of heat pipe external application;By paeonia rockii seed powder, Paeonia papaveracea pollen, Flos Rosae Rugosas pollen, Paeonia papaveracea pollen press than Example mixing is added in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower;
3) valve E is opened, by CO2It is put into multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower;Control multilayer analysis 20~the 25MPa of pressure for flowing inclined plate gas-solid-liquid phase reverse flow extraction tower 28, controls 38~50 DEG C of its temperature;Control valve E, control The gas liquid scale of construction of multilayer analysis stream inclined plate processed, by paeonia rockii seed powder, Paeonia papaveracea pollen, Flos Rosae Rugosas pollen, Paeonia papaveracea pistil Powder is added from the top of extraction tower;
4) 28 top valve F of extraction tower is opened, under stress the CO of liquid and gas2It is mixed into CO with extracting2Gas The paeonia rockii seed oil ingredient of phase liquid phase, Paeonia papaveracea component, rose component, Paeonia papaveracea pistil component with liquid phase with Gas phase CO2Enter tower aftercooler, 15 DEG C of cooling water coolings of cooler after being filtered;
5) CO come out from cooler2Gas phase, citronellol, nerol, benzyl carbinol, nonyl alcohol, linalool, haematochrome and Hu Luo The mixture for extracting product component is opened valve G by Bu Su liquid phases, into pre-separator, by the tea product of mixture point From temperature is controlled at 30~40 DEG C, the CO in mixture2Liquid phase is presented in all gasifications, most of product, and the product in case is pressed to beat Pre-separator valve J is opened, product enters in semi-finished product storage tank;
6) tail gas of top out in pre-separator is sent into aftercooler, tail gas is cooled down, cooler is with 15 DEG C cooling water cooling;Valve H is opened, tail gas is entered in postposition separator, the waste material in tail gas is detached, opens valve K, it will It is sent into semi-finished product storage tank;Valve B is closed, valve C and A is opened, the tail gas at the top of postposition separator is sent to Low Temperature Liquid Change in device;
7) after the completion of the extraction work in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower, system pressure is reduced, The slag-drip opening for opening bottom, slag is recycled;Pre-separator, bottom deslagging, drain valve are opened successively;Postposition separator is opened, Bottom deslagging, drain valve;Semi-finished product storage tank is opened, valve L, semi-finished product enter multilayer ultra-fine filling material filter-press, by product In contaminant filter it is clean, impurity screening from top recycle, finished product open valve M, into finished product basin, open valve N, packet It fills up to the cosmetics.
The processing method of the paeonia rockii seed powder, includes the following steps:
1) select that fuller, impurity is few, maturity is high, as black as jet peony seeds are put into rotary screen, removes husky Soil and other impurities, the paeonia rockii seed for removing screening impurity enter storage bin(hopper) storage;Then by the Paeonia papaveracea of bin stock quarrel Seed is loaded with sack to be freezed 40 hours in the freezer for be put into -10 DEG C, and then that the purple plague purpura that 40 hours are freezed in warehouse is male Red seed is added hulling machine and shells;
2) peony seeds benevolence that shell will have been taken off with elevator is promoted Multi-stage screening machine is added, by changing colour in peony seeds benevolence, mould Become, unhulled unqualified peony seeds are picked out, the discoloration in screening removing peony seeds, the peony seeds benevolence gone mouldy;It will screening Good paeonia rockii seed benevolence is slowly added to drum-type with peony seeds benevolence charger and rotates long cylinder air-flow peony seeds benevolence drying machine, with day Right gas is heating raw material, lights hot-blast stove, and combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation Filter removes the air in dust, and by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown air by wind turbine pressurization Enter drum-type and rotate long cylinder air-flow peony seeds benevolence drying machine, by the moisture of paeonia rockii seed benevolence into one under the conditions of 60 DEG C ± 2 DEG C Drying is walked, control moisture is 2%~3%;
3) peony seeds benevolence after drying flows automatically to dry peony seeds benevolence hold-up tank, first, playing the role of storage, second is that ensureing Its natural cooling is cooled to 35 DEG C or less.The dry peony seeds of peony seeds benevolence for temperature being reduced to 35 DEG C of following temperature feed Machine is added peony seeds benevolence pulverizer, is crushed to 30~40 mesh, the peony seeds benevolence powder after crushing is detached by cyclone separator.
The processing method of the Paeonia papaveracea petal, includes the following steps:
1) by the no disease and pests harm of select, the Paeonia papaveracea petal in full bloom not lost is rinsed well with clear water;Then it is put On fresh peony flower charger, be homogeneously added into drum-type and rotate in long cylinder air-flow peony drying machine, use natural gas as Fuel is heated, hot-blast stove is lighted, combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation filter Remove the air in dust, for air by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown into drum by wind turbine pressurization Formula rotates in long cylinder air-flow peony drying machine, and by Paeonia papaveracea drying under conditions of 50 DEG C ± 2 DEG C, controlling its moisture is 4%~5%;
2) peony after drying flows automatically to dry peony seeds benevolence hold-up tank, first, playing the role of storage, second is that ensureing it Natural cooling is cooled to 32 DEG C or less.Temperature is reduced to the dry peony charger of peony seeds benevolence of 32 DEG C of following temperature, The broken machine of dried flower is added, is crushed to 30~40 mesh, the peony pollen after crushing is detached by cyclone separator.
Compared with prior art, advantageous effects of the invention:
1) products material of the invention has selected unique formula, technological process to select supercritical extraction process, will Extraction tower is designed as the smaller slender type multilayer analysis of major diameter and stays inclined plate gas-solid-liquid phase reverse flow extraction tower.
2) method of the invention can replace the techniques such as current mechanical pressing method, mechanical presses method, solvent dissolution.This hair Bright purpose is a set of energy-saving and environmental protection of design, efficient, low consumption, safety, the novel process and device for not consuming solvent.
3) technological process of the invention is solved the problems, such as containing the green element of aspergillus flavus in product, main that color selector is selected to remove change Long paeonia rockii seed, in addition technical process control not will produce aflatoxins.
4) production this method of the invention extracts at low temperature, ensure that natural original active constituent of raw material is not broken It is bad, the nutritional ingredient of paeonia rockii seed.
5) product quality produced by the invention is high, and nutrition is comprehensive, does not generate harmful substance, does not generate the three wastes, waste residue substantially All recycling utilizes again, does not pollute the environment, simple production process is easy to operate.
6) in the present invention between logistics gas phase, liquid phase, solid phase due to increasing inclined plate, increase gas phase, liquid phase, solid phase it Between time of contact, increase contact area, accelerate rate of extraction, reduce extraction time, improve productivity.Energy consumption Low, production cost is low, and process units takes up an area few.Product yield is high, can save resource.
Description of the drawings
Fig. 1 is paeonia rockii seed powder processing process upstream figure of the present invention.
Fig. 2 is paeonia rockii seed powder processing downstream process figure of the present invention.
Fig. 3 is Paeonia papaveracea rose drying disintegrating process figure of the present invention.
Fig. 4 is Paeonia papaveracea pistil disintegrating process figure of the present invention.
Fig. 5 is solid (S) liquid (L) phase reverse flow supercritical extract paeonia rockii seed of multilayer analysis stream inclined plate gas (G) of the present invention Powder, flower, pistil, rose health products cosmetic material artwork.
1- rotary screens in figure, 2- storage bin(hopper)s, 3- freezers, 4- hulling machines, 5- elevators, 6- multistage color selectors, 7- are infrared Burn hot-blast stove, 8- wind turbines, and 9- dries peony seeds benevolence storagetank, and 10- dries peony seeds charger, 11- shelling paeonia rockii seeds Benevolence charger, 12- peony seeds benevolence pulverizers, 13- paeonia rockii seed benevolence powder packaging, 14- drum-types rotate long cylinder air-flow peony seeds Benevolence drying machine, 15- cyclone separators, 16- dried flower storagetanks, 17- dried flower chargers, 18- tree peony-rose fresh flower chargers, 19- Dried flower pulverizer, 20- petal powder packaging, 21- peony bud pulverizers, 22- pistil powder packaging, 23-CO2Steel cylinder, 24- Low Temperature Liquids Change cooler, 25- buffers, 26- pressuring machines, 27- heaters, 28- multilayers, which are analysed, flows inclined plate gas-solid-liquid phase reverse flow extraction tower, 29- tower aftercoolers, 30- pre-separators, 31- aftercoolers, 32- semi-finished product basins, 33- postposition separators, 34- multilayers Ultra-fine filling material filter-press, 35- filters, 36- stirring rod.
Specific implementation mode
Below by specific embodiment, technical scheme of the present invention is further illustrated.It should be appreciated that this hair Bright embodiment is not limited to the following examples, and accommodation and/or change in any form made for the present invention all will Fall into protection scope of the present invention.
It is a kind of to produce edible cosmetics using paeonia rockii seed with paeonia rockii seed, fresh Paeonia papaveracea Valve, pistil, new fresh-rose produce new health food and cosmetics for raw material, are mainly made of the raw material of following percentage, It is specific as follows:
Embodiment 1:Curative effect class cosmetics are wiped to prepare, dosage is as follows:
Paeonia rockii seed 90% (is calculated) with butt
Paeonia papaveracea petal 6% (is calculated) with butt
Paeonia papaveracea pistil 2% (is calculated) with butt
New fresh-rose 2% (being calculated with butt)
The following production stage of the present invention:
1. the machining process of paeonia rockii seed powder and steps are as follows:
1) select that fuller, impurity is few, maturity is high, as black as jet peony seeds.Paeonia rockii seed is put into Rotary screen removes sandy soil and other impurities, and the paeonia rockii seed for removing screening impurity enters storage bin(hopper) storage.By bin stock quarrel Paeonia rockii seed is loaded in the freezer for be put into -10 DEG C with sack and is freezed 40 hours, the purpose of freezing be it is chilled after just In shelling.It freezes 40 hours paeonia rockii seed addition hulling machines in warehouse to shell, the purpose of shelling is to improve purple plague purpura Peony seeds oil yield improves product quality.
2) peony seeds benevolence that shell will have been taken off with elevator is promoted Multi-stage screening machine is added, by changing colour in peony seeds benevolence, mould Become, unhulled unqualified peony seeds are picked out, the discoloration in screening removing peony seeds, the peony seeds benevolence gone mouldy;It will screening Good paeonia rockii seed benevolence is slowly added to drum-type with peony seeds benevolence charger and rotates long cylinder air-flow peony seeds benevolence drying machine, with day Right gas is heating raw material, lights hot-blast stove, and combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation Filter removes the air in dust, and by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown air by wind turbine pressurization Enter drum-type and rotate long cylinder air-flow peony seeds benevolence drying machine, by the moisture of paeonia rockii seed benevolence into one under the conditions of 60 DEG C ± 2 DEG C Drying is walked, control moisture is 2%~3%;
3) peony seeds benevolence after drying flows automatically to dry peony seeds benevolence hold-up tank, first, playing the role of storage, second is that ensureing Its natural cooling is cooled to 35 DEG C or less.The dry peony seeds of peony seeds benevolence for temperature being reduced to 35 DEG C of following temperature feed Machine is added peony seeds benevolence pulverizer, is crushed to 30~40 mesh, the peony seeds benevolence powder after crushing is detached by cyclone separator.
2. the drying and crushing technical process brief introduction of Paeonia papaveracea
By the no disease and pests harm of select, the Paeonia papaveracea petal in full bloom not lost is rinsed well with clear water;It is then placed on It on fresh peony flower charger, is homogeneously added into drum-type and rotates in long cylinder air-flow peony drying machine, use natural gas as adding Hot fuel, lights hot-blast stove, and combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation filter and remove Fall the air in dust, for air by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown into drum-type by wind turbine pressurization It rotates in long cylinder air-flow peony drying machine, by Paeonia papaveracea drying under conditions of 50 DEG C ± 2 DEG C, controlling its moisture is 4%~5%;
2) peony after drying flows automatically to dry peony seeds benevolence hold-up tank, first, playing the role of storage, second is that ensureing it Natural cooling is cooled to 32 DEG C or less.Temperature is reduced to the dry peony charger of peony seeds benevolence of 32 DEG C of following temperature, The broken machine of dried flower is added, is crushed to 30~40 mesh, the peony pollen after crushing is detached by cyclone separator.
3. the drying and crushing technical process brief introduction of rose
Drying and crushing technique of the drying and crushing technique of rose with Paeonia papaveracea.
4. the disintegrating process process brief introduction of Paeonia papaveracea pistil:
Paeonia papaveracea pistil is manually put into peony bud pulverizer, is crushed to 30~40 mesh or so, the tree peony after crushing Pistil is separated by cyclone separator.
Above procedure completes the processing process of Paeonia papaveracea pistil, this process part Figure of description 3:
5. the preparation method of Paeonia papaveracea health products and cosmetics is as follows:
1) entire process units edible vegetable oil is clean, it must not be by any type of greasy dirt and grease.CO will be housed2Steel cylinder with System is connected.Valve A is closed, valve B and valve C is opened, by CO2It is put into cryoliquifier, cryoliquifier external application -25 DEG C frozen liq, by CO2Temperature is reduced to -5 DEG C.- 5 DEG C of CO will be cooled to2It is sent into buffer.
2) valve D is opened, by CO2It is sent into pressuring machine 4, increases its pressure.The CO that will be pressurizeed in pressuring machine 42It is sent into heating In device, the hot water heating of 60 DEG C of heater heating tube external application.By the paeonia rockii seed powder in Fig. 1, Fig. 2, Fig. 3, Paeonia papaveracea Powder, Flos Rosae Rugosas pollen, Paeonia papaveracea pollen mix in proportion to be added in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower.
3) valve E is opened, by CO2It is put into multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower.Control multilayer analysis Flow inclined plate gas-solid-liquid phase reverse flow extraction tower 20~25MPa of pressure, control 38~50 DEG C of historical relic between.Control valve E, control The gas liquid scale of construction of multilayer analysis stream inclined plate processed, convenient for paeonia rockii seed powder, Paeonia papaveracea pollen, rose is added from the top of extraction tower Rare pollen, Paeonia papaveracea pistil powder, slowly decline, and analysis stream inclined plate is especially increased out of extraction tower, greatly reduces solid phase The decrease speed of material increases the contact area of gas-solid liquid phase, increases the time of contact of gas-solid liquid phase, makes extraction yield substantially Degree improves.
4) valve F at the top of extraction tower is opened, under stress the CO of liquid and gas2It is mixed into CO with extracting2Gas phase The paeonia rockii seed oil ingredient of liquid phase, Paeonia papaveracea component, rose component, Paeonia papaveracea pistil component is with liquid phase and gas Phase CO2Enter tower aftercooler, 15 DEG C of cooling water coolings of cooler after being filtered.
5) CO come out from cooler2Gas phase, citronellol, nerol, benzyl carbinol, nonyl alcohol, linalool, haematochrome and Hu Luo The mixture for extracting product component is opened valve G by Bu Su liquid phases, and into pre-separator, the tea product of mixture are detached Get off, temperature controls the condition at 30~40 DEG C, the CO in mixture2Liquid phase is presented in all gasifications, most of product, presses in case Product open pre-separator valve J, product enters in semi-finished product storage tank.
6) tail gas of top out travels further into aftercooler in pre-separator, and tail gas is further cooled down, 15 DEG C of cooling water coolings of cooler.Valve H is opened, tail gas is entered in postposition separator, the product in tail gas is further The product separated opens valve K, into semi-finished product storage tank.Tail gas at the top of postposition separator removes cryoliquifier In, concrete operation method:Valve B is closed, valve C and A are opened, tail gas recycles in systems always.
7) after the completion of the extraction work in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower, by the pressure in system It lowers, opens the slag-drip opening of bottom, slag is recycled.Pre-separator, bottom deslagging, drain valve are opened successively;Open postposition Separator, bottom deslagging, drain valve.The processing method of semi-finished product:Semi-finished product storage tank is opened, valve L, it is super that semi-finished product enter multilayer Flour filler filter-press, the contaminant filter in product is clean, and impurity screening is recycled from top, and finished product opens valve M, is entered In finished product basin.Valve N is opened, is packed up to the product.
This process is shown in that Figure of description 4, solid (S) liquid (L) the phase reverse flow supercritical extract of multilayer analysis stream inclined plate gas (G) are purple Spot peony seeds powder, flower, pistil, rose health products cosmetic material process flow chart.
Embodiment 2:Face oil is wiped to prepare, increases the dosage of paeonia rockii seed.
Embodiment 3:To prepare perfumed soap, the dosage of Paeonia papaveracea petal is increased.
Embodiment 4:To prepare shower cream, the dosage of Paeonia papaveracea pistil is increased.
Embodiment 5:To prepare facial mask, the dosage of roseleaf is increased.
The dosage of each product is determined according to the content of above example, as shown in table 1:
Project Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Paeonia rockii seed 91% 87% 87% 88%
Paeonia papaveracea petal 6% 8% 7% 6%
Paeonia papaveracea pistil 2% 4% 5% 4%
Fresh roseleaf 1% 1% 1% 2%
The preparation method is the same as that of Example 1 for embodiment 2~5.
The application method of this product
Product produced by the invention mainly has two large effects and purposes:First, for making general cosmetics;Second is that for doing Edible cosmetics.
One, the application method of edible cosmetics
1. cooking:When cooking Hot dishes, the vegetable fried takes the dish out of the pot after sabot, and surface waters 5~6ml and mixes that it can be served thoroughly.Cold dish Also 5~6ml is watered per assorted cold dishes surface mix that it can be served thoroughly with the method.
2. directly drinking:Be grown up 3~4ml, 2~3ml of child for each person every day.
3. being added when Baoshang a little.
4. frying:This product deep fried foodstuff can be used.
5. wheaten food additive can be done, soft dose.
6. when cooking rice can per kilogram add 30~60g.
It is drunk 7. being added in grape wine, lemon juice, yoghurt.
Two, the application method of general cosmetics
Face oil is wiped 1. can do.
2. facial mask solvent can be made of it.
3. perfumed soap can be made.
4. shampoo, shower cream can be done.
The present invention can be summarized with others without prejudice to the concrete form of the spirit or essential characteristics of the present invention.No matter from which From the point of view of a bit, the embodiment above of the invention can only all be considered the description of the invention and cannot limit the present invention, right Claim indicates the scope of the present invention, therefore, with the comparable meaning and scope of claims of the present invention in it is any Change, is all considered as being included within Claims scope.

Claims (2)

1. a kind of producing edible cosmetics using paeonia rockii seed, it is characterised in that raw material is by paeonia rockii seed, new Light violet spot peony petal, pistil, new fresh-rose are formed by following weight fraction:Paeonia rockii seed 87%~91%, purple plague purpura are male Red petal 6%~8%, Paeonia papaveracea pistil 2%~5%, new fresh-rose 1%~2%.
2. a kind of method producing edible cosmetics using paeonia rockii seed according to claim 1, feature It is to include the following steps:
1) paeonia rockii seed powder is processed
1. selecting, fuller, impurity is few, and maturity is high, as black as jet peony seeds are put into rotary screen, remove sandy soil and Other impurities, the paeonia rockii seed for removing screening impurity enter storage bin(hopper) storage;Then the paeonia rockii seed of bin stock quarrel is used Sack loads to be freezed 40 hours in the freezer for be put into -10 DEG C, and 40 hours paeonia rockii seeds and then will be freezed in warehouse Hulling machine is added to shell;
2. with elevator will take off shell peony seeds benevolence promoted be added Multi-stage screening machine, by peony seeds benevolence discoloration, go mouldy, not The unqualified peony seeds of shelling are picked out, and screening removes the discoloration in peony seeds, the peony seeds benevolence gone mouldy;The purple that will have been screened Spot peony seeds benevolence is slowly added to drum-type with peony seeds benevolence charger and rotates long cylinder air-flow peony seeds benevolence drying machine, is with natural gas Raw material is heated, hot-blast stove is lighted, combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation filter Remove the air in dust, for air by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown into drum by wind turbine pressurization Formula rotates long cylinder air-flow peony seeds benevolence drying machine, and the moisture of paeonia rockii seed benevolence is further dried under the conditions of 60 DEG C ± 2 DEG C, It is 2%~3% to control moisture;
3. the peony seeds benevolence after dry flows automatically to dry peony seeds benevolence hold-up tank, natural cooling is cooled to 35 DEG C or less;Temperature It is reduced to the dry peony seeds charger of peony seeds benevolence of 35 DEG C of following temperature, peony seeds benevolence pulverizer is added, it is crushed to 30~ 40 mesh, the peony seeds benevolence powder after crushing are detached by cyclone separator.
2) Paeonia papaveracea petal is processed
1. by the no disease and pests harm of select, the Paeonia papaveracea petal in full bloom not lost is rinsed well with clear water;It is then placed on male On red fresh flower charger, it is homogeneously added into drum-type and rotates in long cylinder air-flow peony drying machine, use natural gas as heating Fuel, lights hot-blast stove, and combustion tail gas heats hot-blast stove tubulation, the combustion gas of heat is led in tubulation, manages outer promoting menstruation filter and remove Air in dust, for air by being heated when the tubulation of hot-blast stove, the hot-air of heating is blown into drum-type rotation by wind turbine pressurization Turn in long cylinder air-flow peony drying machine, by Paeonia papaveracea drying under conditions of 50 DEG C ± 2 DEG C, it is 4% to control its moisture ~5%;
2. the peony after dry flows automatically to dry peony seeds benevolence hold-up tank, natural cooling is cooled to 32 DEG C or less;Temperature is dropped As low as the dry peony charger of peony seeds benevolence of 32 DEG C of following temperature, the broken machine of dried flower is added, is crushed to 30~40 mesh, crushes Peony pollen afterwards is detached by cyclone separator.
3) finished product is processed
1. entire process units edible vegetable oil is clean, it must not be by any type of greasy dirt and grease;CO will be housed2Steel cylinder and system It is connected, closes valve A, valve B and valve C is opened, by CO2It is put into cryoliquifier, -25 DEG C of cryoliquifier external application is cold Freeze liquid, by CO2Temperature is reduced to -5 DEG C, will be cooled to -5 DEG C of CO2It is sent into buffer;
2. valve D is opened, by CO2It is sent into pressuring machine;The CO that will be pressurizeed in pressuring machine2It is sent into heater, heater heating tube The hot water heating that 60 DEG C of external application;Paeonia rockii seed powder, Paeonia papaveracea point, Flos Rosae Rugosas pollen, Paeonia papaveracea point are mixed in proportion It closes and is added in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower;
3. valve E is opened, by CO2It is put into multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower;Control multilayer analysis stream inclined plate 20~25MPa of pressure of gas-solid-liquid phase reverse flow extraction tower, controls 38~50 DEG C of its temperature;Control valve E, control multilayer analysis The gas liquid scale of construction for flowing inclined plate, by paeonia rockii seed powder, Paeonia papaveracea pollen, Flos Rosae Rugosas pollen, Paeonia papaveracea pistil powder from extraction The top of tower is added;
4. opening valve F at the top of extraction tower, under stress the CO of liquid and gas2It is mixed into CO with extracting2Gas phase liquid phase Paeonia rockii seed oil ingredient, Paeonia papaveracea component, rose component, Paeonia papaveracea pistil component is with liquid phase and gas phase CO2Enter tower aftercooler, 15 DEG C of cooling water coolings of cooler after being filtered;
5. the CO come out from cooler2Gas phase, citronellol, nerol, benzyl carbinol, nonyl alcohol, linalool, haematochrome and carrotene liquid The mixture for extracting product component is opened valve G by phase, into pre-separator, the tea product of mixture is detached, temperature Control is at 30~40 DEG C, the CO in mixture2Liquid phase is presented in all gasifications, most of product, presses the product in case to open preposition Separator valve J, product enter in semi-finished product storage tank;
6. the tail gas of top out in pre-separator 30 is sent into aftercooler, tail gas is cooled down, cooler is with 15 DEG C Cooling water cooling;Valve H is opened, tail gas is entered in postposition separator, the waste material in tail gas is detached, valve K is opened, by it It is sent into semi-finished product storage tank;Valve B is closed, valve C and A is opened, the tail gas at the top of postposition separator is sent to low-temperature liquefaction In device;
7. after the completion of the extraction work in multilayer analysis stream inclined plate gas-solid-liquid phase reverse flow extraction tower, system pressure is reduced, is opened The slag-drip opening of bottom, slag is recycled;Pre-separator, bottom deslagging, drain valve are opened successively;Open postposition separator, bottom Deslagging, drain valve;Semi-finished product storage tank, valve L are opened, semi-finished product enter multilayer ultra-fine filling material filter-press, will be in product Contaminant filter is clean, and impurity screening is recycled from top, and finished product opens valve M, into finished product basin, opens valve N, packaging is Obtain the cosmetics.
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