CN108158861A - A kind of preparation method of the Essence containing peony essential oil - Google Patents
A kind of preparation method of the Essence containing peony essential oil Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of preparation methods of the Essence containing peony essential oil, include the following steps：Prepare peony essential oil；Glycerine, hyaluronic acid, water are mixed, is stirred evenly at 70 80 DEG C, obtains water phase liquid；Vitamin E, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, is stirred evenly at 70 80 DEG C, obtains oil phase liquid；Oil phase liquid is added in water phase liquid, homogeneous 15 20 minutes obtains the Essence containing peony essential oil.The Essence prepared using the method for the present invention can rapidly permeate into human skin, have the effects that tender white, crease-resistant, anti-aging, lighten the stain, enhance elasticity of skin.
Description
Technical field
The present invention relates to facial treatment essence liquid preparation field more particularly to a kind of preparation sides of the Essence containing peony essential oil
Method.
Background technology
With the progress of society and economic development and the continuous improvement of living standards of the people, people are to beauty and skin care
The requirement of cosmetic is also higher and higher, increasingly develops to the direction of " naturalization, nutrient laden, curative effect ".But currently on the market
Various beauty and skin care cosmetics in it is most of all containing harmful chemical substance, such as leaded, mercury venomous injurant
Matter, these skin care item easily cause people's skin allergy, and human organ and function are caused to damage.It is opened from the last century 80's
Begin, skin expert finds that, various natural materials are added in skin care item, there is good nourishing effect, and nontoxic pair to skin
Effect, effective component extracting, which is added in skin care item, particularly from plant has more remarkable effect.
Essence is also known as maintenance stoste, has the multiple efficacies such as reparation, anti-aging, crease-resistant, whitening, moisturizing, nti-freckle.It is applicable in
All kinds of skin problems caused by increasing because of the age, nursing the reasons such as improper.Essence extracts from high nutrient and its is dense
Contracting, usually contains more active constituent, molecule is small, and penetration is stronger.Essence type is various, such as moisturizing essence, anti-ageing
Always/the Essence that compacts, nti-freckle Essence, cleawhite over-night essences etc..Plants essential oil is all added in many Essences on the market
Ingredient, peony essential oil be extracted from peony it is isolated there is volatile oily liquids, wherein rich in a variety of ammonia
Base acid and trace element, have and resist sensitivity, improve blood circulation, and beautifying face and moistering lotion promotes cytothesis, alleviates skin ageing,
The effects that adjusting skin problem is the raw material of cosmetics.But essential oil impurity of the addition in Essence is more at present, and purity is not high,
And contain a large amount of synthetics.
Invention content
Technical problems based on background technology, the present invention propose a kind of preparation of the Essence containing peony essential oil
Method, the Essence prepared using the method for the present invention can rapidly permeate into human skin, have tender white, crease-resistant, anti-aging, desalination
The effects that color spot, enhancing elasticity of skin.
The present invention provides a kind of preparation methods of the Essence containing peony essential oil, include the following steps：
S1, fresh peony petal and water are mixed, by crushing, after ultrasonication, is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, after stirring 10-20 minutes, stands 20-30 minutes,
Obtain gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, obtains peony essential oil；
S4, in parts by weight, weigh 10-15 parts of glycerine, 8-12 parts of hyaluronic acids, 1-2 parts of vitamin Es, 5-8 parts of orange essential oils,
Peony essential oil obtained in 2-4 parts of rhodiola root essential oils, 6-9 parts of grape pip essential oils, 20-25 parts of water, 7-10 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 70-80 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, in 70-
80 DEG C stir evenly, and obtain oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 15-20 minutes is obtained containing tree peony
The Essence of essential oil.
Preferably, the raw material of super absorbent resin includes by weight in S2：12-15 parts of cornstarch, acrylic acid 65-70
Part, 5-8 parts of corn stalk powder, 0.5-0.7 parts of potassium peroxydisulfate, N, N ' -0.06-0.08 parts of methylene-bisacrylamide, quality point
Sodium hydroxide solution 85-95 part, water 15-17 part of the number for 26%-29%.
Preferably, in the raw material of super absorbent resin, the water content of corn stalk powder is 5%-8%, and granularity is 60-80 mesh
Preferably, the preparation method of super absorbent resin includes the following steps in S2：
Step 1: cornstarch is added in 70-80 DEG C of water, constant temperature stirs 40-50 minutes, the starch solution A being gelatinized；
Step 2: acrylic acid is added in sodium hydroxide solution, stirs 20-30 minutes, add corn stalk powder, persulfuric acid
Potassium, N, N '-methylene-bisacrylamide, stir evenly, and obtain mixed solution B；
Step 3: the mixed solution B obtained in the starch solution A and step 2 that are obtained in step 1 is uniformly mixed, it is put into micro-
Microwave treatment 3-5 minutes, microwave power 250-300W in wave reactor, dry, crushing obtains being used to prepare peony essential oil
Super absorbent resin.
Preferably, temperature dry in step 3 is 70-80 DEG C, and the time is 15-20 hours.
Preferably, the super absorbent resin granularity for being used to prepare peony essential oil that step 3 obtains after crushing is 70-80 mesh.
Preferably, the weight ratio of fresh peony petal and water is 1 in S1:1-1.3.
Preferably, the additive amount of super absorbent resin is 0.02-0.04 times of peong flower juice weight in S2.
Preferably, S3, which surpasses, closes in carbon dioxide abstraction, and the pressure of extraction is 23-35Mpa, and extraction temperature is 35-45 DEG C,
Extraction time is 50-90 minutes, carbon dioxide flow 15-18L/h.
Preferably, S3, which surpasses, closes in carbon dioxide abstraction, the supercritical carbon dioxide extracting instrument used there are two separating still,
The pressure of first separating still is 8-10Mpa, and temperature is 40-45 DEG C, and the pressure of the second separating still is 3-5Mpa, temperature 30-35
℃。
Preferably, surpass in S3 and close on carbon dioxide abstraction and use cyclohexane as entrainer.
Preferably, surpass in S3 and close on carbon dioxide abstraction, the flow of entrainer cyclohexane is the 6%- of carbon dioxide flow
8%。
Preferably, the ultrasonic power of ultrasonication is 200-300w, frequency 28-32Hz, ultrasonic time 15- in S1
20min。
Preferably, the agitation revolution of homogeneous is 2800-3200rpm in S7.
Contain peony essential oil, orange essential oil, rhodiola root essential oil, grape pip essence in the Essence prepared using the method for the present invention
The natural components such as oil, non-stimulated to human skin, the Essence of the compositions such as cooperation glycerine, hyaluronic acid can rapidly permeate into human body
Skin has the effects that tender white, crease-resistant, anti-aging, lighten the stain, enhance elasticity of skin.
The effects that peony essential oil has anti-oxidant, delay skin aging, inhibits color spot, prevents acne, bright and clean skin quality；Orange
Essential oil has antibacterial, toxin expelling, lightens the stain, the pH-value of balance skin, and collagen is helped to be formed, help the growth of skin tissue with
The effect of reparation, the fragrance of orange essential oil can expel intense strain and pressure, improve insomnia caused by anxiety, make one mood
It is optimistic, it rejuvenates；Rhodiola root essential oil can clearing heat and detoxicating, vital energy regualting and blood circulation-promoting, only need minimal amount just can resist aoxidize caused by it is dim sink
With colour of skin unevenness, improve dry, water shortage status, enhance the elasticity and vigor of skin, skin can be allowed tender pale；Grape seed oil has
Two kinds of very important elements, linolenic acid and proanthocyanidin, linolenic acid can resist free radical, anti-aging, help to absorb
Vitamin C and E strengthen the elasticity of the circulatory system, reduce the injury of ultraviolet light, protect the collagen in skin, improve vein
Swelling and oedema prevent melanin deposition, and proanthocyanidin has protection blood vessel elasticity, protects skin afflicting with great suffering torment from ultraviolet light, in advance
The destruction of anti-collagenous fibres and elastomer makes skin keep due elasticity and tension, and skin sagging and wrinkle is avoided to generate.
The peony essential oil used in the method for the present invention is using fresh peony petal as raw material, first breaks fresh peony petal
Broken, supersonic wave wall breaking makes the derived essential oil in peony be released from cell.Peong flower juice is absorbed with super absorbent resin
After carry out supercritical carbon dioxide extracting, super absorbent resin has very strong absorbability and water-retaining property, several by external pressure
Do not lose moisture.Super absorbent resin is different to the binding ability of hydrone with derived essential oil, and carbon dioxide is by absorbing
During the super absorbent resin of peong flower juice, volatile oil components therein are taken away, moisture and impurity then stay in high water absorption
Property resin in, realize water-oil separating, pure essential oil can be directly recovered to from separating still.Super absorbent resin can be repeatedly
Water suction, recycling reduce production cost.In supercritical carbon dioxide extracting using cyclohexane as entrainer, extraction can be improved
The efficiency taken.The method of this kind extraction peony essential oil can extract the derived essential oil in peony, essential oil purity to greatest extent
Height, free from admixture are remained without extractant, are easily absorbed, and are a kind of methods that peony essential oil efficiently, is quickly extracted from peony.
Specific embodiment
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
The present invention provides a kind of preparation methods of the Essence containing peony essential oil, include the following steps：
S1, by weight ratio be 1:1.2 fresh peony petal and water mixing, crushed 20 mesh, be 240w with ultrasonic power, frequency
After 30Hz ultrasonications 17min, it is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, the additive amount of super absorbent resin is peong flower juice
0.028 times of weight after stirring 13 minutes, stands 26 minutes, obtains gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 27Mpa, and extraction temperature is 42 DEG C, and extraction time is 71 minutes, carbon dioxide flow 16.8L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 8.9Mpa, and temperature is 42 DEG C, second point
Pressure from kettle is 3.6Mpa, and temperature is 33 DEG C；Surpass in S3 and close on carbon dioxide abstraction and use cyclohexane as entrainer, cyclohexane
Flow for 1.13L/h, the extract of the first separating still and the second separating still is merged, obtains peony essential oil；
S4, in parts by weight, weigh 12 parts of glycerine, 10 parts of hyaluronic acids, 1.4 parts of vitamin Es, 6.2 parts of orange essential oils, 2.2 parts
Peony essential oil obtained in rhodiola root essential oil, 6.9 parts of grape pip essential oils, 23 parts of water, 8.1 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 76 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, at 76 DEG C
It stirs evenly, obtains oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 17 divides under 3000rpm agitation revolutions
Clock obtains the Essence containing peony essential oil.
Wherein, the raw material of super absorbent resin includes by weight in S2：13 parts of cornstarch, 67 parts of acrylic acid, corn
6.8 parts of straw powder, 0.62 part of potassium peroxydisulfate, N, N ' -0.074 part of methylene-bisacrylamide, the hydroxide that mass fraction is 27%
86 parts of sodium solution, 15.8 parts of water.The water content of corn stalk powder is 5.4%, and granularity is 70 mesh.
The preparation method of super absorbent resin includes the following steps：
Step 1: cornstarch is added in 76 DEG C of water, constant temperature stirs 43 minutes, the starch solution A being gelatinized；
Step 2: acrylic acid is added in sodium hydroxide solution, stirs 27 minutes, add corn stalk powder, potassium sulfate, N,
N '-methylene-bisacrylamide, stirs evenly, and obtains mixed solution B；
Step 3: the mixed solution B obtained in the starch solution A and step 2 that are obtained in step 1 is uniformly mixed, it is put into micro-
Microwave treatment 4.3 minutes in wave reactor, microwave power 280W is 18 hours dry at 76 DEG C, crushed 70 mesh sieve, obtains height
Water-absorbing resins.
Embodiment 2
The present invention provides a kind of preparation methods of the Essence containing peony essential oil, include the following steps：
S1, by weight ratio be 1：1.1 fresh peony petal and water mixing, crushed 20 mesh, be 280w with ultrasonic power, frequency
After 29Hz ultrasonications 16min, it is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, the additive amount of super absorbent resin is peong flower juice
0.033 times of weight after stirring 15 minutes, stands 22 minutes, obtains gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 33Mpa, and extraction temperature is 37 DEG C, and extraction time is 86 minutes, carbon dioxide flow 15.4L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 8.3Mpa, and temperature is 43 DEG C, second point
Pressure from kettle is 4.2Mpa, and temperature is 31 DEG C；Surpass in S3 and close on carbon dioxide abstraction and use cyclohexane as entrainer, cyclohexane
Flow for 1.20 L/h, the extract of the first separating still and the second separating still is merged, obtains peony essential oil；
S4, in parts by weight, weigh 13 parts of glycerine, 9 parts of hyaluronic acids, 1.6 parts of vitamin Es, 7.8 parts of orange essential oils, 3.3 parts it is red
Peony essential oil obtained in red-spotted stonecrop essential oil, 7.6 parts of grape pip essential oils, 21 parts of water, 8.9 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 72 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, at 78 DEG C
It stirs evenly, obtains oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 18 divides under 2900rpm agitation revolutions
Clock obtains the Essence containing peony essential oil.
Wherein, the raw material of super absorbent resin includes by weight in S2：12 parts of cornstarch, 68 parts of acrylic acid, corn
7.7 parts of straw powder, 0.53 part of potassium peroxydisulfate, N, N ' -0.066 part of methylene-bisacrylamide, the hydroxide that mass fraction is 26%
91 parts of sodium solution, 16.2 parts of water.The water content of corn stalk powder is 5.8%, and granularity is 65 mesh.
The preparation method of super absorbent resin includes the following steps：
Step 1: cornstarch is added in 73 DEG C of water, constant temperature stirs 48 minutes, the starch solution A being gelatinized；
Step 2: acrylic acid is added in sodium hydroxide solution, stir 24 minutes, add corn stalk powder, potassium peroxydisulfate,
N, N '-methylene-bisacrylamide, stir evenly, and obtain mixed solution B；
Step 3: the mixed solution B obtained in the starch solution A and step 2 that are obtained in step 1 is uniformly mixed, it is put into micro-
Microwave treatment 3.4 minutes in wave reactor, microwave power 260W is 19.4 hours dry at 73 DEG C, crushed 75 mesh sieve, obtains
Super absorbent resin.
Embodiment 3
The present invention provides a kind of preparation methods of the Essence containing peony essential oil, include the following steps：
S1, by weight ratio be 1：1 fresh peony petal and water mixing, crushed 20 mesh, with ultrasonic power be 210w, frequency is
After 31Hz ultrasonications 19min, it is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, the additive amount of super absorbent resin is peong flower juice
0.023 times of weight after stirring 19 minutes, stands 29 minutes, obtains gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 24Mpa, and extraction temperature is 44 DEG C, and extraction time is 54 minutes, carbon dioxide flow 16.1L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 9.7Mpa, and temperature is 41 DEG C, second point
Pressure from kettle is 4.8Mpa, and temperature is 34 DEG C；Surpass in S3 and close on carbon dioxide abstraction and use cyclohexane as entrainer, cyclohexane
Flow for 1.01L/h, the extract of the first separating still and the second separating still is merged, obtains peony essential oil；
S4, in parts by weight, weigh 11 parts of glycerine, 11 parts of hyaluronic acids, 1.2 parts of vitamin Es, 5.4 parts of orange essential oils, 2.7 parts
Peony essential oil obtained in rhodiola root essential oil, 8.8 parts of grape pip essential oils, 22 parts of water, 7.3 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 78 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, at 74 DEG C
It stirs evenly, obtains oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 19 divides under 3100rpm agitation revolutions
Clock obtains the Essence containing peony essential oil.
Embodiment 4
The present invention provides a kind of preparation methods of the Essence containing peony essential oil, include the following steps：
S1, by weight ratio be 1：1.3 fresh peony petal and water mixing, crushed 20 mesh, ultrasonic power 260w, frequency are
After 28Hz ultrasonications 18min, it is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, the additive amount of super absorbent resin is peong flower juice
0.037 times of weight after stirring 17 minutes, stands 24 minutes, obtains gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 31Mpa, and extraction temperature is 39 DEG C, and extraction time is 62 minutes, carbon dioxide flow 17.7L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 9.4Mpa, and temperature is 44 DEG C, second point
Pressure from kettle is 3.2Mpa, and temperature is 32 DEG C, and the extract of the first separating still and the second separating still is merged, and obtains tree peony essence
Oil；
S4, in parts by weight, weigh 14 parts of glycerine, 8 parts of hyaluronic acids, 1.8 parts of vitamin Es, 7.1 parts of orange essential oils, 3.6 parts it is red
Peony essential oil obtained in red-spotted stonecrop essential oil, 6.3 parts of grape pip essential oils, 24 parts of water, 9.7 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 74 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, at 72 DEG C
It stirs evenly, obtains oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 16 divides under 3200rpm agitation revolutions
Clock obtains the Essence containing peony essential oil.
Embodiment 5
The preparation method of the Essence containing peony essential oil in embodiment 1, wherein, surpass in S3 and close on carbon dioxide abstraction entrainment
The flow of agent cyclohexane can also be 1.21L/h.
Embodiment 6
The preparation method of the Essence containing peony essential oil in embodiment 1, wherein, the raw material of super absorbent resin is by weight in S2
Amount part can also include：14 parts of cornstarch, 66 parts of acrylic acid, 5.2 parts of corn stalk powder, 0.57 part of potassium peroxydisulfate, N, N '-Asia
0.078 part of bisacrylamide, 88 parts of the sodium hydroxide solution that mass fraction is 29%, 15.3 parts of water.Corn stalk powder contains
Water is 6.9%, and granularity is 75 mesh.
Embodiment 7
The preparation method of the Essence containing peony essential oil in embodiment 1, wherein, the raw material of super absorbent resin is by weight in S2
Amount part can also include：15 parts of cornstarch, 69 parts of acrylic acid, 6.1 parts of corn stalk powder, 0.68 part of potassium peroxydisulfate, N, N '-Asia
0.062 part of bisacrylamide, 93 parts of the sodium hydroxide solution that mass fraction is 28%, 16.7 parts of water.Corn stalk powder contains
Water is 7.8%, and granularity is 80 mesh.
Embodiment 8
The preparation method of the Essence containing peony essential oil in embodiment 1, wherein, the preparation method of super absorbent resin may be used also
To include the following steps：
Step 1: cornstarch is added in 78 DEG C of water, constant temperature stirs 46 minutes, the starch solution A being gelatinized；
Step 2: acrylic acid is added in sodium hydroxide solution, stir 22 minutes, add corn stalk powder, potassium peroxydisulfate,
N, N '-methylene-bisacrylamide, stir evenly, and obtain mixed solution B；
Step 3: the mixed solution B obtained in the starch solution A and step 2 that are obtained in step 1 is uniformly mixed, it is put into micro-
Microwave treatment 4.8 minutes in wave reactor, microwave power 270W is 16.4 hours dry at 79 DEG C, crushed 80 mesh sieve, obtains
Super absorbent resin.
Existing device on the market can be selected in microwave reactor involved in the present invention, as long as required function of the present invention can be realized
, preferred Nanjing optically-active Science and Technology Ltd. LWMC-201 type microwave reactors.
The methods of being uniformly mixed, stirring evenly, centrifuging involved in the present invention, homogeneous be this field it is known often
Know, details are not described herein.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of preparation method of the Essence containing peony essential oil, which is characterized in that include the following steps：
S1, fresh peony petal and water are mixed, by crushing, after ultrasonication, is centrifugally separating to obtain peong flower juice；
Super absorbent resin is added in S2, the peong flower juice obtained in S1, after stirring 10-20 minutes, stands 20-30 minutes,
Obtain gel peony extract；
S3, supercritical carbon dioxide extracting is carried out to obtaining gel peony extract in S2, obtains peony essential oil；
S4, in parts by weight, weigh 10-15 parts of glycerine, 8-12 parts of hyaluronic acids, 1-2 parts of vitamin Es, 5-8 parts of orange essential oils,
Peony essential oil obtained in 2-4 parts of rhodiola root essential oils, 6-9 parts of grape pip essential oils, 20-25 parts of water, 7-10 parts of S3, it is spare；
S5, the glycerine weighed in S4, hyaluronic acid, water are mixed, is stirred evenly at 70-80 DEG C, obtain water phase liquid；
S6, the vitamin E weighed in S4, orange essential oil, rhodiola root essential oil, grape pip essential oil, peony essential oil are mixed, in 70-
80 DEG C stir evenly, and obtain oil phase liquid；
S7, the oil phase liquid obtained in S6 is added in the water phase liquid obtained in S5, homogeneous 15-20 minutes is obtained containing tree peony
The Essence of essential oil.
A kind of 2. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S2
The raw material of middle super absorbent resin includes by weight：12-15 parts of cornstarch, 65-70 parts of acrylic acid, corn stalk powder 5-8
Part, 0.5-0.7 parts of potassium peroxydisulfate, N, N ' -0.06-0.08 parts of methylene-bisacrylamide, the hydrogen-oxygen that mass fraction is 26%-29%
Change 85-95 parts of sodium solution, 15-17 parts of water.
A kind of 3. preparation method of Essence containing peony essential oil according to claim 2, which is characterized in that the S2
The preparation method of middle super absorbent resin includes the following steps：
Step 1: cornstarch is added in 70-80 DEG C of water, constant temperature stirs 40-50 minutes, the starch solution A being gelatinized；
Step 2: acrylic acid is added in sodium hydroxide solution, stirs 20-30 minutes, add corn stalk powder, persulfuric acid
Potassium, N, N '-methylene-bisacrylamide, stir evenly, and obtain mixed solution B；
Step 3: the mixed solution B obtained in the starch solution A and step 2 that are obtained in step 1 is uniformly mixed, it is put into micro-
Microwave treatment 3-5 minutes, microwave power 250-300W in wave reactor, dry, crushing obtains super absorbent resin.
A kind of 4. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S1
In the weight ratio of fresh peony petal and water be 1:1-1.3.
A kind of 5. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S2
The additive amount of middle super absorbent resin is 0.02-0.04 times of peong flower juice weight.
A kind of 6. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S3
Super to close in carbon dioxide abstraction, the pressure of extraction is 23-35Mpa, and extraction temperature is 35-45 DEG C, and extraction time is 50-90 points
Clock, carbon dioxide flow 15-18L/h.
A kind of 7. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S3
Super to close in carbon dioxide abstraction, there are two separating still, the pressure of the first separating still for the supercritical carbon dioxide extracting instrument used
For 8-10Mpa, temperature is 40-45 DEG C, and the pressure of the second separating still is 3-5Mpa, and temperature is 30-35 DEG C.
A kind of 8. preparation method of Essence containing peony essential oil according to claim 1, which is characterized in that the S3
In surpass and close on carbon dioxide abstraction and use cyclohexane as entrainer, the 6%-8% of the flow of cyclohexane for carbon dioxide flow.
A kind of 9. preparation method of Essence containing peony essential oil according to claim 8, which is characterized in that the S1
The ultrasonic power of middle ultrasonication is 200-300w, frequency 28-32Hz, ultrasonic time 15-20min.
10. the preparation method of a kind of Essence containing peony essential oil according to claim 1, which is characterized in that described
The agitation revolution of homogeneous is 2800-3200rpm in S7.
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