CN110051593A - A kind of peony essence dew and preparation method thereof - Google Patents
A kind of peony essence dew and preparation method thereof Download PDFInfo
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- CN110051593A CN110051593A CN201910452777.4A CN201910452777A CN110051593A CN 110051593 A CN110051593 A CN 110051593A CN 201910452777 A CN201910452777 A CN 201910452777A CN 110051593 A CN110051593 A CN 110051593A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a kind of peony essence dew and preparation method thereof, reveal in peony essence dew in essence and Peony show and peony extract are added in common ingredient, active component content is up to 15% in peony water and peony extract, Skin Cell free radical can effectively be removed, aging is resisted, the activity of the intracorporal TYR enzyme of people is effectively eliminated, reduces the generation of melanin, mitigate pigment deposition, enhances the anti-senescence function of skin.The peony essence dew in peony water and peony extract purification process in, peony petal is refrigerated at low ambient temperatures first, and the moisture of peony petal is removed using frozen drying, while obtaining peony petal water, the peony petal dried, by, to the active material extraction in roseleaf, being effectively guaranteed the activity of the extract in peony petal under the conditions of 40~50 DEG C, use effect of peony extract is improved.
Description
[technical field]
The invention belongs to maintain skin care field, it is related to a kind of peony essence dew and preparation method thereof.
[background technique]
Skin to the first line of defence of external environment, has as body and protects body from various physics, chemistry and micro-
The effect of the factors such as biology invasion.Sebum level caused by a variety of causes is abnormal, and lipid components or ratio change, can all lead
Cause skin barrier impaired, so as to cause the generation for changing even related skin complaints of skin type.
In addition to heredity, age, the physically or chemically factors such as stimulation, disease and drug；Environmental factor (as dry, cold) is right
The influence of human skin also increasingly aggravates；With the air pollution and increasingly increased life pressure of modern society's sharp deterioration
Power, due to the bad intervention of external environment, the free radical balance of the skin surface of more and more people is destroyed, and body will produce therewith
Raw excessive free radical, accelerates the aging of skin, and it is excessive wrinkle, drying, tarnish and color spot occur so as to cause skin
The feature of the agings such as deposition.
The skin condition of good health is the target that people from modern society especially women pursues, and in addition to diet and is moved to skin
Outside skin state is brought change and promoted, the effect of skin care item also should not be underestimated.People are very heavy to daily skin nursing maintenance
Depending on, the small molecule contained in daily skin care item used resists the substance that free radical generates, can by direct contact with the skin,
Osmotic absorption enters skin lining, directly effectively understands above-mentioned polyradical excessively, inhibits the activity of TYR enzyme, antibacterial disappears
The phenomenon that inflammation reaches the equilibrium state for maintaining skin surface bacterium colony, with the generation of delaying skin surface layer wrinkle and crosses presenility.
In the use process of skin care products, essence takes on important role, contains in essence and fundamentally solves skin
The substance of problem, the face cleaning of preamble and the use of toner are provided to make the state of skin surface, including cleannes and soda acid
Value reaches the state that a suitable essential ingredient absorbs, to be more convenient the use of essence and the efficient absorption of essential ingredient.
Peony is rich in polyphenols, amino acid, fatty acid, vitamin and the essential trace elements of the human body etc., is
A kind of preferable natural nutrition health care resource.Some researches show that peony petal extracts brilliant oxidation resistance, this is right
In it is anti crease and anti senile it is old for be a kind of excellent ingredient, and the cultivated area of tree peony is being expanded with swift and violent speed, but people
Mostly used using the oil of tree peony and ornamental value, and ignore the preparation of tree peony correlation skin care item, the especially harvesting of peony
Do not conflict with tree peony as both skin care item, the deep processing of peony not only can adequately utilize Peony Resource, but also can be more
The further good development for promoting tree peony industry.
The extraction process of many essence products all not can avoid this process of high temperature, so that many plant extracts
Photosensitive and heat-sensitive substance in matter is destroyed.
[summary of the invention]
It is an object of the invention to overcome the above-mentioned prior art, a kind of peony essence dew and its preparation side are provided
Method.Essence dew can effectively remove Skin Cell free radical, resist aging, effectively eliminate the work of the intracorporal TYR enzyme of people
Property, the generation of melanin is reduced, pigment deposition is mitigated, enhances the anti-senescence function of skin.
In order to achieve the above objectives, the present invention is achieved by the following scheme:
A kind of peony essence dew, in terms of mass fraction, is made of following raw material: 42~50 parts of water, 9~12 parts of propylene glycol,
5~8 parts of saualane, 6~9 parts of dipotassium glycyrrhizinate, 0.1~0.5 part of hyaluronic acid, 0.1~1 part of allantoin, 1~5 part of niacinamide,
3~10 parts of oat extract, 1~5 part of Hydrolyzed Collagen, 0.1~0.5 part of carbomer, 0.2~0.5 part of triethanolamine, fourth two
5~10 parts of alcohol, 0.2~5 part of tocopherol, 10~12 parts of peony water, 1~5 part of peony extract, Phenoxyethanol 0.1~1
Part.
A further improvement of the present invention is that:
Preferably, peony water is that freeze-drying peony petal is made in the process.
Preferably, peony extract is made by the peony petal supercritical extract after being freeze-dried.
A kind of preparation method of peony essence dew, comprising the following steps: by 42~50 parts of water, 9~12 parts of propylene glycol,
5~8 parts of saualane, 6~9 parts of dipotassium glycyrrhizinate, 0.1~1 part of allantoin, 1~5 part of niacinamide, 0.1~0.5 part
Carbomer, 5~10 parts of butanediol, 10~12 parts of peony water be mixed to prepare mixture A, will be stirred after mixture A heating
It mixes uniformly, mixture B is made, the temperature of mixture B starts to stir, mixture C is made after stirring, mixture C is set after reducing
In emulsion pot, 0.2~5 part of tocopherol is added, mixture D is made after homogeneous, stirring；After the temperature of mixture D is reduced,
0.1~0.5 part of hyaluronic acid, 3~10 parts of oat extract, 1~5 part of Hydrolyzed Collagen, 1~5 part male is added
Simultaneously mixture E is made in red flower extract and 0.2~0.5 part of triethanolamine, homogeneous after mixing evenly；Reduce the temperature of mixture E
0.1~1 part of Phenoxyethanol is added after degree, peony essence dew is made after mixing evenly.
Preferably, mixture A is warming up to 75~95 DEG C, and mixture B is made after mixing evenly；The temperature of mixture B reduces
Start to stir to 60~75 DEG C.
Preferably, in mixture C be added tocopherol after 10~15min of homogeneous, at 65~75 DEG C stir 10~15min
Mixture D is made.
Preferably, mixture D is vacuumized and is cooled to 50~60 DEG C, hyaluronic acid, oat extract, hydrolytic collagen is added
Mixture E is made in albumen, peony extract and triethanolamine, 3~5min of homogeneous after mixing evenly；Reduce the temperature of mixture E
It spends to 35~45 DEG C of addition Phenoxyethanols.
Preferably, the preparation process of peony water are as follows: 3h is refrigerated after cleaning up peony petal in -80 DEG C, it will be cold
Peony petal behind hiding, which is placed in low-temperature freeze-drying machine, to be freeze-dried, and peony water is made in drying process.
Preferably, the preparation process of peony extract are as follows: 3h is refrigerated after cleaning up peony petal in -80 DEG C,
Peony petal after refrigeration is placed in low-temperature freeze-drying machine and is freeze-dried；Peony petal after drying be crushed into 80 mesh
Sieve, is obtained by extraction peony extract from the peony petal after sieving.
Preferably, extraction process are as follows: the peony petal after sieving is obtained into peony by supercritical carbon dioxide extracting
Extract, extraction time 90min, extracting pressure 350mbar, extraction temperature are 40 DEG C, CO in extraction process2Flow is
1.5L/min。
Compared with prior art, the invention has the following advantages:
The invention discloses a kind of peony essence dew, reveals in common ingredient in peony essence dew in essence and tree peony is added
Flower fair and peony extract, active component content can be removed effectively up to 15% in peony water and peony extract
Skin Cell free radical resists aging, effectively eliminates the activity of the intracorporal TYR enzyme of people, reduce the generation of melanin, mitigates
Pigment deposition enhances the anti-senescence function of skin.
The invention also discloses a kind of preparation method of peony essence dew, pass through emulsion pot in the preparation process of essence dew
Mixed raw material obtains uniformly and the product of high-quality so that material is sufficiently mixed under vacuum conditions；Wherein Dan Huashui and male
In the purification process of red flower extract, peony petal is refrigerated first at low ambient temperatures, and is removed using frozen drying
The moisture for removing peony petal, while obtaining peony petal water, the peony petal dried, by 40~50 DEG C of conditions
Under to the active material extraction in roseleaf, be effectively guaranteed the activity of the extract in peony petal, improve peony
Use effect of extract.
[specific embodiment]
Below with reference to specific steps, the invention will be described in further detail, and the invention discloses a kind of peony essence dew
Preparation method, specifically includes the following steps:
Step 1, the pretreatment of peony petal
Selection just opens the phase to the fresh peony flower of phase in full bloom, just opens the judgment criteria of phase are as follows: the expansion of outer layer petal, it is interior to multilayer
Petal is loose, and internal layer petal still closes up；The judgment criteria of phase in full bloom are as follows: the expansion of internal layer petal, stamen are completely exposed；Picking is simultaneously
After removing peony petal, peony petal is cleaned up, peony petal is placed in -80 DEG C and refrigerates 3h；
Step 2, the drying of peony petal and the preparation of peony water
Peony petal after refrigeration is taken out, is placed in low-temperature freeze-drying machine and is freeze-dried, drying temperature is 25 DEG C, is done
Dry 24~36h of time, peony water cryo-conservation at -4 DEG C obtained in drying process is spare, and the petal after drying is crushed
Cross 80 meshes.
Step 3, peony extract is prepared
It is passed through carbon dioxide in supercritical extraction reactor, raises simultaneously extraction kettle internal temperature and pressure, until titanium dioxide
Carbon becomes supercriticality；Peony petal after pulverizing and sieving is put into extraction kettle, 90min is extracted, extracting pressure is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, and gained is peony extract.
Step 4, preparation peony essence dew
Prepare raw material, in terms of mass fraction, 42~50 parts of water, 9~12 parts of propylene glycol, 5~8 parts of saualane, glycyrrhizic acid
6~9 parts of dipotassium, 0.1~0.5 part of hyaluronic acid, 0.1~1 part of allantoin, 1~5 part of niacinamide, 3~10 parts of oat extract,
1~5 part of Hydrolyzed Collagen, 0.1~0.5 part of carbomer, 0.2~0.5 part of triethanolamine, 5~10 parts of butanediol, tocopherol
0.2~5 part, 10~12 parts of peony water, 1~5 part of peony extract, 0.1~1 part of Phenoxyethanol.
By the water in above-mentioned raw material, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, fourth two
Mixture A is made after pure and mild peony water mixing, mixture A is warming up to 75~95 DEG C, mixture B is made after mixing evenly,
Mixture B is cooled to 60~75 DEG C, and stirring to particle and powder reagent is dissolved in solvent, no particle and powder, until having dissolved
Obtained mixture C, is pumped into emulsion pot for mixture C after complete；Then tocopherol, 10~15min of homogeneous, 65~75 are slowly pumped into
Mixture D is made at DEG C after 10~15min of insulated and stirred, vacuumizes cooling；When temperature is 50~60 DEG C, addition hyaluronic acid,
Mixing is made in oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, 3~5min of homogeneous after mixing evenly
Object E；When temperature is 35~45 DEG C, Phenoxyethanol is added, stirs evenly and obtains peony essence dew.
Embodiment 1
The fresh peony flower for just opening the phase to the phase in full bloom is won to clean up peony petal after removing peony petal, be placed in-
3h is refrigerated in 80 DEG C, is freeze-dried after refrigeration, and peony water cryo-conservation at -4 DEG C obtained in drying process is spare, will do
Petal after dry crushed 80 meshes；Peony petal is put into supercritical extraction reactor and extracts 90min, the pressure of extraction process is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, obtains peony extract；
In terms of mass fraction, prepare 42 parts of water, 10 parts of propylene glycol, 8 parts of saualane, 6 parts of dipotassium glycyrrhizinate, hyaluronic acid
0.5 part, 0.5 part of allantoin, 5 parts of niacinamide, 3 parts of oat extract, 1 part of Hydrolyzed Collagen, 0.5 part of carbomer, three ethyl alcohol
0.5 part of amine, 5 parts of butanediol, 3 parts of tocopherol, 11 parts of peony water, 3 parts of peony extract, 1 part of Phenoxyethanol.
Mixing water, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, butanediol and peony water
It is warming up to 75 DEG C after mixing, after mixing evenly, keeps the temperature to 65 DEG C, stirring is pumped into emulsion pot to after being completely dissolved, tocopherol is added,
Homogeneous 15min, the insulated and stirred 11min at 65 DEG C, vacuumizes cooling；When temperature is 59 DEG C, by ready addition hyalomitome
Acid, oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, homogeneous 3min, stir evenly；When temperature is 43
DEG C when, be added Phenoxyethanol, stir evenly obtain peony essence dew.
Embodiment 2
The fresh peony flower for just opening the phase to the phase in full bloom is won to clean up peony petal after removing peony petal, be placed in-
3h is refrigerated in 80 DEG C, is freeze-dried after refrigeration, and peony water cryo-conservation at -4 DEG C obtained in drying process is spare, will do
Petal after dry crushed 80 meshes；Peony petal is put into supercritical extraction reactor and extracts 90min, the pressure of extraction process is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, obtains peony extract；
In terms of mass fraction, prepare 48 parts of water, 9 parts of propylene glycol, 5 parts of saualane, 9 parts of dipotassium glycyrrhizinate, hyaluronic acid 0.1
Part, 1 part of allantoin, 1 part of niacinamide, 3 parts of oat extract, 3 parts of Hydrolyzed Collagen, 0.3 part of carbomer, triethanolamine 0.3
Part, 7 parts of butanediol, 0.2 part of tocopherol, 12 parts of peony water, 1 part of peony extract, 0.1 part of Phenoxyethanol.
Mixing water, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, butanediol and peony water
It is warming up to 95 DEG C after mixing, after mixing evenly, keeps the temperature to 75 DEG C, stirring is pumped into emulsion pot to after being completely dissolved, tocopherol is added,
Homogeneous 10min, the insulated and stirred 15min at 75 DEG C, vacuumizes cooling；When temperature is 60 DEG C, by ready addition hyalomitome
Acid, oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, homogeneous 5min, stir evenly；When temperature is 45
DEG C when, be added Phenoxyethanol, stir evenly obtain peony essence dew.
Embodiment 3
The fresh peony flower for just opening the phase to the phase in full bloom is won to clean up peony petal after removing peony petal, be placed in-
3h is refrigerated in 80 DEG C, is freeze-dried after refrigeration, and peony water cryo-conservation at -4 DEG C obtained in drying process is spare, will do
Petal after dry crushed 80 meshes；Peony petal is put into supercritical extraction reactor and extracts 90min, the pressure of extraction process is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, obtains peony extract；
With mass fraction, prepare 43 parts of water, 12 parts of propylene glycol, 6 parts of saualane, 7 parts of dipotassium glycyrrhizinate, hyaluronic acid 0.3
Part, 0.1 part of allantoin, 3 parts of niacinamide, 7 parts of oat extract, 5 parts of Hydrolyzed Collagen, 0.1 part of carbomer, triethanolamine
0.2 part, 5 parts of butanediol, 0.2 part of tocopherol, 10 parts of peony water, 1 part of peony extract, 1 part of Phenoxyethanol.
Mixing water, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, butanediol and peony water
It is warming up to 80 DEG C after mixing, after mixing evenly, keeps the temperature to 60 DEG C, stirring is pumped into emulsion pot to after being completely dissolved, tocopherol is added,
Homogeneous 13min, the insulated and stirred 10min at 65 DEG C, vacuumizes cooling；When temperature is 50 DEG C, by ready addition hyalomitome
Acid, oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, homogeneous 4min, stir evenly；When temperature is 35
DEG C when, be added Phenoxyethanol, stir evenly obtain peony essence dew.
Embodiment 4
The fresh peony flower for just opening the phase to the phase in full bloom is won to clean up peony petal after removing peony petal, be placed in-
3h is refrigerated in 80 DEG C, is freeze-dried after refrigeration, and peony water cryo-conservation at -4 DEG C obtained in drying process is spare, will do
Petal after dry crushed 80 meshes；Peony petal is put into supercritical extraction reactor and extracts 90min, the pressure of extraction process is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, obtains peony extract；
With mass fraction, prepare 42 parts of water, 9 parts of propylene glycol, 5 parts of saualane, 6 parts of dipotassium glycyrrhizinate, hyaluronic acid 0.2
Part, 0.1 part of allantoin, 1 part of niacinamide, 10 parts of oat extract, 1 part of Hydrolyzed Collagen, 0.1 part of carbomer, triethanolamine
0.2 part, 10 parts of butanediol, 0.2 part of tocopherol, 10 parts of peony water, 5 parts of peony extract, 0.2 part of Phenoxyethanol.
Mixing water, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, butanediol and peony water
It is warming up to 85 DEG C after mixing, after mixing evenly, keeps the temperature to 70 DEG C, stirring is pumped into emulsion pot to after being completely dissolved, tocopherol is added,
Homogeneous 12min, the insulated and stirred 12min at 70 DEG C, vacuumizes cooling；When temperature is 52 DEG C, by ready addition hyalomitome
Acid, oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, homogeneous 5min, stir evenly；When temperature is 40
DEG C when, be added Phenoxyethanol, stir evenly obtain peony essence dew.
Embodiment 5
The fresh peony flower for just opening the phase to the phase in full bloom is won to clean up peony petal after removing peony petal, be placed in-
3h is refrigerated in 80 DEG C, is freeze-dried after refrigeration, and peony water cryo-conservation at -4 DEG C obtained in drying process is spare, will do
Petal after dry crushed 80 meshes；Peony petal is put into supercritical extraction reactor and extracts 90min, the pressure of extraction process is
350mbar, extraction temperature are 40 DEG C, the CO of extraction process2Flow is 1.5L/min, obtains peony extract；
In terms of mass fraction, prepare 50 parts of water, 9 parts of propylene glycol, 5 parts of saualane, 6 parts of dipotassium glycyrrhizinate, hyaluronic acid 0.5
Part, 1 part of allantoin, 1 part of niacinamide, 3 parts of oat extract, 1 part of Hydrolyzed Collagen, 0.5 part of carbomer, triethanolamine 0.5
Part, 5 parts of butanediol, 5 parts of tocopherol, 10 parts of peony water, 0.5 part of peony extract, 0.5 part of Phenoxyethanol.
Mixing water, propylene glycol, saualane, dipotassium glycyrrhizinate, allantoin, niacinamide, carbomer, butanediol and peony water
It is warming up to 90 DEG C after mixing, after mixing evenly, keeps the temperature to 73 DEG C, stirring is pumped into emulsion pot to after being completely dissolved, tocopherol is added,
Homogeneous 11min, the insulated and stirred 13min at 73 DEG C, vacuumizes cooling；When temperature is 55 DEG C, by ready addition hyalomitome
Acid, oat extract, Hydrolyzed Collagen, peony extract, triethanolamine, homogeneous 3min, stir evenly；When temperature is 37
DEG C when, be added Phenoxyethanol, stir evenly obtain peony essence dew.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of peony essence dew, which is characterized in that in terms of mass fraction, be made of following raw material: 42~50 parts of water, propylene glycol
9~12 parts, 5~8 parts of saualane, 6~9 parts of dipotassium glycyrrhizinate, 0.1~0.5 part of hyaluronic acid, 0.1~1 part of allantoin, nicotinoyl
1~5 part of amine, 3~10 parts of oat extract, 1~5 part of Hydrolyzed Collagen, 0.1~0.5 part of carbomer, triethanolamine 0.2~
0.5 part, 5~10 parts of butanediol, 0.2~5 part of tocopherol, 10~12 parts of peony water, 1~5 part of peony extract, benzene oxygen second
0.1~1 part of alcohol.
2. peony essence dew according to claim 1, which is characterized in that peony water is freeze-drying peony petal process
In be made.
3. peony essence dew according to claim 1, which is characterized in that peony extract is by the tree peony after being freeze-dried
Petal supercritical extract is made.
4. a kind of preparation method of peony essence dew, which comprises the following steps: by 42~50 parts of water, 9~12 parts
Propylene glycol, 5~8 parts of saualane, 6~9 parts of dipotassium glycyrrhizinate, 0.1~1 part of allantoin, 1~5 part of niacinamide,
0.1~0.5 part of carbomer, 5~10 parts of butanediol, 10~12 parts of peony water are mixed to prepare mixture A, by mixture
It is stirred evenly after A heating, mixture B is made, the temperature of mixture B starts to stir after reducing, and mixture C is made after stirring, will
Mixture C is placed in emulsion pot, and 0.2~5 part of tocopherol is added, and mixture D is made after homogeneous, stirring；By the temperature of mixture D
After degree reduces, 0.1~0.5 part of hyaluronic acid, 3~10 parts of oat extract, 1~5 part of Hydrolyzed Collagen, 1 is added
Simultaneously mixture E is made in~5 parts of peony extract and 0.2~0.5 part of triethanolamine, homogeneous after mixing evenly；It reduces mixed
0.1~1 part of Phenoxyethanol is added after the temperature of conjunction object E, peony essence dew is made after mixing evenly.
5. the preparation method of peony essence dew according to claim 4, which is characterized in that mixture A is warming up to 75~95
DEG C, mixture B is made after mixing evenly；The temperature of mixture B is reduced to 60~75 DEG C to start to stir.
6. the preparation method of peony essence dew according to claim 4, which is characterized in that fertility is added in mixture C
10~15min of homogeneous after phenol stirs 10~15min at 65~75 DEG C and mixture D is made.
7. the preparation method of peony essence dew according to claim 4, which is characterized in that mixture D is vacuumized cooling
To 50~60 DEG C, hyaluronic acid, oat extract, Hydrolyzed Collagen, peony extract and triethanolamine, homogeneous 3 is added
Mixture E is made in~5min after mixing evenly；The temperature of mixture E is reduced to 35~45 DEG C of addition Phenoxyethanols.
8. the preparation method of peony essence dew according to claim 4, which is characterized in that the preparation process of peony water
Are as follows: 3h is refrigerated after cleaning up peony petal in -80 DEG C, the peony petal after refrigeration is placed in low-temperature freeze-drying machine
It is freeze-dried, peony water is made in drying process.
9. the preparation method of peony essence dew according to claim 4, which is characterized in that the preparation of peony extract
Journey are as follows: refrigerate 3h after cleaning up peony petal in -80 DEG C, the peony petal after refrigeration is placed in low-temperature freeze-drying machine
Middle freeze-drying；Peony petal after drying be crushed into 80 meshes, peony is obtained by extraction from the peony petal after sieving
Extract.
10. the preparation method of peony essence dew according to claim 9, which is characterized in that extraction process are as follows: after sieving
Peony petal peony extract, extraction time 90min are obtained by supercritical carbon dioxide extracting, extracting pressure is
350mbar, extraction temperature are 40 DEG C, CO in extraction process2Flow is 1.5L/min.
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| CN201910452777.4A CN110051593A (en) | 2019-05-28 | 2019-05-28 | A kind of peony essence dew and preparation method thereof |
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| CN111658583A (en) * | 2020-06-15 | 2020-09-15 | 西北农林科技大学 | Preparation method of peony moistening anti-inflammatory essence and essence |
| CN111849642A (en) * | 2020-07-16 | 2020-10-30 | 菏泽瑞璞牡丹产业科技发展有限公司 | Peony fresh flower water and preparation method thereof |
| CN113952266A (en) * | 2021-09-29 | 2022-01-21 | 中科瑞莱茵(北京)生物科技有限公司 | Preparation method and application of peony water |
| CN116159009A (en) * | 2023-03-17 | 2023-05-26 | 北京迷奇生物科技有限公司 | Peony petal toner and preparation method thereof |
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| CN111658583A (en) * | 2020-06-15 | 2020-09-15 | 西北农林科技大学 | Preparation method of peony moistening anti-inflammatory essence and essence |
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| CN113952266A (en) * | 2021-09-29 | 2022-01-21 | 中科瑞莱茵(北京)生物科技有限公司 | Preparation method and application of peony water |
| CN113952266B (en) * | 2021-09-29 | 2023-10-13 | 中科瑞莱茵(北京)生物科技有限公司 | Preparation method and application of peony flower water |
| CN116159009A (en) * | 2023-03-17 | 2023-05-26 | 北京迷奇生物科技有限公司 | Peony petal toner and preparation method thereof |
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