CN105726387A - Skin whitening microemulsion - Google Patents

Skin whitening microemulsion Download PDF

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Publication number
CN105726387A
CN105726387A CN201610089251.0A CN201610089251A CN105726387A CN 105726387 A CN105726387 A CN 105726387A CN 201610089251 A CN201610089251 A CN 201610089251A CN 105726387 A CN105726387 A CN 105726387A
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Prior art keywords
oil
extract
whitening
quintessence oil
microemulsion
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CN201610089251.0A
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Inventor
胡喜芬
其他发明人请求不公开姓名
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Guangzhou hangmei Cosmetics Co. Ltd.
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Foshan Qianru Cosmetics Co Ltd
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Priority to CN201610089251.0A priority Critical patent/CN105726387A/en
Publication of CN105726387A publication Critical patent/CN105726387A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/925Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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Abstract

The invention discloses a skin whitening microemulsion. More specifically, the skin whitening microemulsion contains sorbitan sesquioleate and PEG-20 sorbitan oleate; one or more oily components selected from hydrocarbon oil, synthetic grease, animal or vegetable oil, silicone oil and a mixture of silicone oil; polyhydric alcohol and water; one or more water-soluble skin whitening raw materials. The prepared skin whitening microemulsion is a water-in-oil system, is good in stability, can be stored for a long term, has a good solubilization effect on the water-soluble skin whitening raw materials, and can be made into a product containing high effective ingredients.

Description

A kind of whitening microemulsion
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of whitening microemulsion.
Background technology
Bright and clean, pale, ruddy skin is always what Nails was pursued, the most in recent years China and Japan, the southeast The fashion that Ya Deng state women praises highly, whitening has become as one of emphasis of cosmetics research and development.Along with the progress of technology, people research and develop Going out whitening product miscellaneous, whitening essential oil is exactly the category that one of them is important.But there is the plant of white-skinned face function Active constituent content in quintessence oil is on the low side, will realize preferable whitening effect and need to add substantial amounts of plants essential oil, the plant of excess Quintessence oil interpolation often results in fragrance overrich, has a strong impact on use sense, and for promoting effect of whitening essential oil, usual way is interpolation one A little oil-soluble skin-lightening cosmetic raw materials, such as tetrahexyldecyl ascorbate, but, most whitening raw material belongs to insoluble In the water-soluble material of oil preparation, this causes being difficult to during whitening essential oil Formula Development apply water solublity whitening raw material, selectable former Material is restricted, it is difficult to realize good white-skinned face function.
Summary of the invention
Based on this, the main object of the present invention is water-soluble for being difficult to apply during the exploitation of whitening essential oil in prior art The problem of property whitening raw material provides a solution.
In order to solve above-mentioned technical problem, the present invention is achieved through the following technical solutions:
A kind of whitening microemulsion, contains:
(a) two kinds of nonionic emulsifiers: sorbitan sesquioleate and PEG-20 sorbitan monooleate;
B () one or more of oily components, selected from hydrocarbon ils, synthesis grease, vegetable and animals oils, silicone oil and mixture thereof;
(c) polynary alcohol and water;
(d) one or more of water solublity whitening raw material;Wherein sorbitan sesquioleate and PEG-20 anhydrous sorbitol oleic acid The ratio of ester is (3:1)-(5:1), and emulsifying agent is the dense of (1:1)-(3:1), emulsifying agent and oily components with the ratio of oily components Degree summation is more than 75wt%.
Preferably, the ratio of sorbitan sesquioleate and PEG-20 sorbitan monooleate is 5:1.5, emulsifying agent with The ratio of oily components is 2:1.
In a preferred embodiment of the invention, described hydrocarbon ils is white mineral oil, vaseline, C15-19 alkane, hydrogenates the poly-last of the ten Heavenly stems Alkene, 2-Methylpentadecane, polyethylene, Parleam, paraffin, Fancol ID, squalane, ceresine, the one of vaccenic acid or Plant above mixing.
In a preferred embodiment of the invention, described synthesis grease is that myristyl alcohol myristinate, caprylic/capric are sweet Oil three esters, isopropyl myristate, isononyl isononanoate, ethylhexyl palmitate, glycol distearate, glycerol three (second Base caproic acid) ester, spermol ethylhexoate, Dermol DIPS, Dermol 105, three different nonyl essences, dicaprylyl carbonate, C12-15 alcohol benzoate, propylene glycol carbonate, one or more mixing of isopropyl isostearate.
In a preferred embodiment of the invention, described vegetable and animals oils is lanoline, fat of Oromaius norvaehollandeae, horse fat, Oleum Hippophae, Rhizoma Zingiberis Recens Root oil, soybean oil, safflower oil, olive oil, Radix Oenotherae erythrosepalae oil, Rosehips oil, American Avocado Tree oil, Jojoba oil, Oleum Vitis viniferae, Bai Chihua Seed oil, deep-sea two save shepherd's purse seed oil, Butyrospermum parkii fruit fatty oil, cocoa seed fat, macadimia nut seed oil, camellia seed oil, Petiolus Trachycarpi oil, Petiolus Trachycarpi A kind of in core oil, camellia seed oil, Rosa Canina fruit oil, Semen Tritici aestivi germ oil, Semen pruni armeniacae oil or their mixing.
In a preferred embodiment of the invention, described silicone oil is ring five polydimethylsiloxane, trimethyl silicane alkoxyl Esters of silicon acis, polydimethylsiloxane, dimethiconol, phenyl trimethicone, cetyl polydimethylsiloxanes Alkane, caprylyl methicone, one or more mixing of stearyl dimethione.
In a preferred embodiment of the invention, described polyhydric alcohol be glycerol, propylene glycol, butanediol, pentanediol, oneself two Alcohol, sorbitol, ethanol, PEG-8, Polyethylene Glycol-32, dipropylene glycol, diglycerol, glycerin polyether-26, Natrulon H-10, One or more mixing of polyglycereol-8.
In a preferred embodiment of the invention, described water solublity whitening raw material is ascorbic acid glucoside, 3-o-ethoxy Base ascorbic acid, Trenaxmine, nicotiamide, glabridin, alpha-arbutin, β-arbutin, Symwhite-337, resveratrol, Phloretin, lactobacillus fermentation lysate, yogurt extract, Fructus Phyllanthi extract, daisy extract, Azelaic Acid glycine two Potassium, Herba Centellae extract, sodium ascorbyl phosphate, vitamin C, vitamin C phosphoric ester potassium, yeast extract, Radix Mori skin extract Thing, Radix Sangusorbae extract, Rhizoma Saururi extract, Rhizoma Atractylodis Macrocephalae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, Agkistrodon Diffusa extract, Folium Ginkgo extract, Radix Ginseng Rubra extract, Radix Glycyrrhizae extract, Rhizoma Alismatis extract, the one of Herba Asari extract or Plant above mixing.
Preferably, described water solublity whitening raw material contains daisy extract, Herba Hedyotidis Diffusae extract and Radix Sangusorbae extract, The addition of described daisy extract is 0.1-0.5wt%, and the addition of described Herba Hedyotidis Diffusae extract is 0.1- 0.5wt%, the addition of described Radix Sangusorbae extract is 0.1-0.5wt%.
The inventors found that daisy extract, Herba Hedyotidis Diffusae extract and Radix Sangusorbae extract are significant due to it Synergistic function, the lightening compositions obtained has the whitening effect being obviously improved.
It is further preferred that described water solublity whitening raw material can also contain Radix Ginseng Rubra extract and Radix Angelicae Sinensis extract, described The addition of Radix Ginseng Rubra extract be 0.1-0.5wt%, the addition of described Radix Angelicae Sinensis extract is 0.1-0.5wt%.
The inventors found that the mixing of Radix Ginseng Rubra extract and Radix Angelicae Sinensis extract has good promotion to white-skinned face function Effect.
The microemulsion of the present invention can be prepared by conventional production technology, following preparation method, preparation technology bag Include following steps: the mixing of sorbitan sesquioleate, PEG-20 sorbitan monooleate and oily components is constituted oil by (1) Phase, is heated to 85 DEG C, stirring and dissolving by oil phase;The mixing of polyhydric alcohol, water and water solublity whitening raw material is constituted aqueous phase, aqueous phase is added Hot to 85 DEG C, stirring and dissolving;(2) under quickly stirring (mixing speed 50rpm), aqueous phase is slowly added to oil phase, stirs; (3) ultrasonic Treatment using frequency to be 1kHZ 5 minutes, are cooled to room temperature.
Present invention also offers a kind of whitening massage quintessence oil, including the component of following mass percent:
There is the plants essential oil 0.01-1% of white-skinned face function
Vitamin E acetate 0.1-1%
Butylated hydroxytoluene 0.05-0.2%
Above-mentioned whitening microemulsion 0.1-5%
Vegetable oil surplus.
In a preferred embodiment of the invention, the described plants essential oil with white-skinned face function is Herba Lysimachiae foenum-graeci quintessence oil, lemon Lemon grass quintessence oil, Bergamot, cumin essential oil, sandalwood essential oil, Peppermint essential oil, P-Cymene, five-leaved chaste tree quintessence oil, Acotus illicioides essence Oil, Basil Essential, eryngo quintessence oil, Fructus Citri Limoniae quintessence oil, Bergamot, clove oil, cinnamon essential oil, shellflower leaf essential oil, gorgeous mountain Rhizoma Zingiberis Recens seed quintessence oil, Rhizoma Alpiniae Officinarum quintessence oil, Rhizoma Curcumae Longae essential oil, Rhizoma Curcumae quintessence oil, ginger essential oil, Fructus Citri grandis quintessence oil, blue or green lemon quintessence oil, Basil Essential, Zingiber casumnar quintessence oil, Flos Rosae Rugosae quintessence oil, Dianthus carryophyllus quintessence oil, hyacinth quintessence oil, Aleppo pine quintessence oil, Radix Oenotherae erythrosepalae quintessence oil, Semen Armeniacae Amarum One or more mixing of quintessence oil.
Preferably, described plants essential oil is the mixing of lemon grass (Cymbopogon citratus) quintessence oil and Rhizoma Curcumae Longae essential oil, described lemon grass (Cymbopogon citratus) quintessence oil and The mass ratio of Rhizoma Curcumae Longae essential oil is (1-10): (1-10).
In a preferred embodiment of the invention, described vegetable oil is Oleum Hippophae, Ginger Root oil, soybean oil, Semen Flos Carthami Shepherd's purse seed is saved at oil, olive oil, Radix Oenotherae erythrosepalae oil, Rosehips oil, American Avocado Tree oil, Jojoba oil, Oleum Vitis viniferae, white Limnanthes Alba Seed Oil, deep-sea two Oil, Butyrospermum parkii fruit fatty oil, cocoa seed fat, macadimia nut seed oil, camellia seed oil, Petiolus Trachycarpi oil, palm-kernel oil, camellia seed oil, certain herbaceous plants with big flowers A kind of in flower seed oil, Rosa Canina fruit oil, Semen Tritici aestivi germ oil, Semen pruni armeniacae oil or their mixing.
Preferably, described vegetable oil is the mixing of Oleum Helianthi, Jojoba oil and Oleum Vitis viniferae, described sunflower seed The mass ratio of oil, Jojoba oil and Oleum Vitis viniferae is (1-10): (1-10): (1-10).Oleum Helianthi, Jojoba oil and Semen Vitis viniferae The use sense that can play of mixture of oil, and rich in nutritional labeling can play skin care, promote the metabolism of skin Deng skin effect, white-skinned face function there is facilitation.
Compared with prior art, the method have the advantages that: the microemulsion of the present invention has good stability, can be long-term Storage;Water solublity whitening raw material there is is good solubilization, the product higher containing functional component can be made;The present invention is made Standby microemulsion is water-in-oil system, can be used alone, and is also added in oil-type skin-lightening cosmetic, easy to use;This Bright preparation technology is simple, it is easy to produce.
Detailed description of the invention
For a more detailed description to the present invention below in conjunction with detailed description of the invention, but embodiments of the present invention are not limited to This, for the technological parameter indicated the most especially or condition, can refer to routine techniques and carry out.
Embodiment 1
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 3kg, PEG-20 anhydrous sorbitol oleic acid Ester 1kg, Fancol ID 2kg, glycerol 1kg, nicotiamide 0.1kg, water 0.5kg;
Preparation technology: the mixing of sorbitan sesquioleate, PEG-20 sorbitan monooleate and Fancol ID is constituted by (1) Oil phase, is heated to 85 DEG C, stirring and dissolving by oil phase;The mixing of glycerol, water and Herba portulacae extract is constituted aqueous phase, by heated aqueous To 85 DEG C, stirring and dissolving;(2) under quickly stirring (mixing speed 50rpm), aqueous phase is slowly added to oil phase, stirs;(3) The ultrasonic Treatment using frequency to be 1kHZ 5 minutes, is cooled to room temperature.
Embodiment 2
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, Herba Asari extract 0.5kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 3
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 4kg, PEG-20 anhydrous sorbitol oleic acid Ester 1kg, Jojoba oil 2kg, horse fat 0.1kg, phenyl trimethicone 0.2kg, hydrogenated polydecene 2.7kg, propylene glycol 1kg, arbutin 0.1kg, Radix Mori peel extract 0.1kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 4
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1kg, polydimethylsiloxane 0.1kg, caprylic/capric triglyceride 0.4kg, Radix Oenotherae erythrosepalae oil 0.5kg, butanediol 0.5kg, white And extract 0.3kg, water 0.6kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 5
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, daisy extract 0.5kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 6
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, Herba Hedyotidis Diffusae extract 0.5kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 7
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, Radix Sangusorbae extract 0.5kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 8
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, Radix Sangusorbae extract 0.1kg, daisy extract 0.1kg, spend in vain Herba Hedyotidis Diffusae extract 0.3kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 9
A kind of microemulsion, it includes the component of following quality: sorbitan sesquioleate 5kg, PEG-20 anhydrous sorbitol oleic acid Ester 1.5kg, isononyl isononanoate 3kg, PEG-8 1.5kg, Radix Sangusorbae extract 0.1kg, daisy extract 0.1kg, spend in vain Herba Hedyotidis Diffusae extract 0.3kg, Radix Ginseng Rubra extract 0.1kg, Radix Angelicae Sinensis extract 0.1kg, water 0.5kg;
Preparation technology: similar embodiment 1, does not repeats them here.
Embodiment 10
A kind of whitening massage quintessence oil, including the component of following mass percent:
Herba Lysimachiae foenum-graeci quintessence oil 0.01%
Basil Essential 0.5%
Vitamin E acetate 1%
Butylated hydroxytoluene 0.05%
Whitening microemulsion 5% prepared by embodiment 1
Oleum Hippophae surplus.
Preparation technology: butylated hydroxytoluene is mixed with Oleum Hippophae, heating for dissolving, then it is cooled to room temperature, sequentially adds Whitening microemulsion prepared by Herba Lysimachiae foenum-graeci quintessence oil, Vitamin E acetate, embodiment 5, stirs.
Embodiment 11
A kind of whitening massage quintessence oil, including the component of following mass percent:
Sandalwood essential oil 1%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 0.1% prepared by embodiment 2
Olive oil 20%
Camellia seed oil surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 12
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.5%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 5
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 13
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.5%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 6
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 14
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.5%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 7
Oleum Helianthi surplus.
Preparation technology similar embodiment 15, does not repeats them here.
Embodiment 15
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.5%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 8
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 16
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.5%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 9
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 17
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.2%
Sandalwood essential oil 0.3%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 9
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 18
A kind of whitening massage quintessence oil, including the component of following mass percent:
Lemon grass (Cymbopogon citratus) quintessence oil 0.2%
Sandalwood essential oil 0.3%
Vitamin E acetate 0.1%
Butylated hydroxytoluene 0.2%
Whitening microemulsion 1% prepared by embodiment 9
Jojoba oil 30%
Oleum Vitis viniferae 20%
Oleum Helianthi surplus.
Preparation technology similar embodiment 10, does not repeats them here.
Embodiment 19
Experiment one, stability test
Whitening microemulsion obtained by embodiment 1-9 is carried out stability test.Method of testing: test object is placed on-15 DEG C, place respectively one month under room temperature and 45 DEG C of environment after observe, with invariant color, without Precipitation, free from extraneous odour as criterion of acceptability. Experimental result: observed after 1 month, finds that the whitening microemulsion obtained by embodiment 1-9 is the most qualified.As can be seen here, this Bright prepared microemulsion is stable.
Experiment two, whitening effect test
Whitening essential oil prepared by embodiment 12-18 is carried out efficacy assessments, and with commercially available whitening essential oil for comparative example 1.Test Object: each experimental group is 10 women, 30-55 year, it is possible to by Normalization rule cosmetics, and cooperating personnel are the completeest Become appraisal, there is certain expressive faculty, the impression after energy actual response use;Test zone: facial skin;Use: every It uses twice, uses 48 days continuously;Evaluation criterion: effective, effectively, invalid, concrete, by the 0th day and the photograph of the 48th day The judgement substantially bleached that compares is effective;It is effective for having, by the photograph contrast of the 0th day and the 48th day, the judgement necessarily bleached; Bleaching inconspicuous by the photograph contrast of the 0th day and the 48th day, it is invalid to be judged as.Concrete test result is shown in Table 1.
Table 1 whitening test result table
Effective Effectively Invalid
Embodiment 12 4 3 3
Embodiment 13 3 3 4
Embodiment 14 5 2 3
Embodiment 15 7 2 1
Embodiment 16 8 2 0
Embodiment 17 9 1 0
Embodiment 18 10 0 0
Comparative example 1 3 3 4
Knowable to upper table 1, the whitening massage quintessence oil prepared by embodiment 12-18 and commercially available prod comparative example 1 efficacy test result Relatively understanding, the whitening massage oil obtained by the present invention has good whitening effect;Embodiment 15 and the whitening of embodiment 12-14 Test result contrast understands, and daisy extract, Herba Hedyotidis Diffusae extract and Radix Sangusorbae extract have significant Synergistic and make With, the lightening compositions obtained has the whitening effect being obviously improved;Embodiment 16 and 15 whitening test result understands, and Radix Ginseng Rubra carries The mixing taking thing and Radix Angelicae Sinensis extract has good facilitation to white-skinned face function.Embodiment 17 and 16 whitening test result can Knowing, the mixing of lemon grass (Cymbopogon citratus) quintessence oil and Rhizoma Curcumae Longae essential oil can promote whitening effect further.Embodiment 18 and 17 whitening test result can Know, the further whitening facilitation effect that is mixed with of Oleum Helianthi, Jojoba oil and Oleum Vitis viniferae is described.
The above, be only presently preferred embodiments of the present invention, and the present invention not does any pro forma restriction, therefore All contents without departing from technical solution of the present invention, any simply repair made for any of the above embodiments according to the technical spirit of the present invention Change, equivalent variations and modification, all still fall within the range of technical solution of the present invention.

Claims (10)

1. a whitening microemulsion, it is characterised in that contain:
(a) two kinds of nonionic emulsifiers: sorbitan sesquioleate and PEG-20 sorbitan monooleate;
B () one or more of oily components, selected from hydrocarbon ils, synthesis grease, vegetable and animals oils, silicone oil and mixture thereof;
(c) polynary alcohol and water;
(d) one or more of water solublity whitening raw material;Wherein sorbitan sesquioleate and PEG-20 anhydrous sorbitol oleic acid The ratio of ester is (3:1)-(5:1), and emulsifying agent is the dense of (1:1)-(3:1), emulsifying agent and oily components with the ratio of oily components Degree summation is more than 75wt%.
Whitening microemulsion the most according to claim 1, it is characterised in that described sorbitan sesquioleate and PEG-20 The ratio of sorbitan monooleate is 5:1.5, and emulsifying agent is 2:1 with the ratio of oily components.
Whitening microemulsion the most according to claim 1, it is characterised in that described water solublity whitening raw material is ascorbic acid Glucoside, 3-o-ethoxy ascorbic acid, Trenaxmine, nicotiamide, glabridin, alpha-arbutin, β-arbutin, phenethyl isophthalic Diphenol, resveratrol, phloretin, lactobacillus fermentation lysate, yogurt extract, Fructus Phyllanthi extract, daisy extract, Azelaic Acid glycine dipotassium, Herba Centellae extract, sodium ascorbyl phosphate, vitamin C, vitamin C phosphoric ester potassium, yeast carry Take thing, Radix Mori peel extract, Radix Sangusorbae extract, Rhizoma Saururi extract, Rhizoma Atractylodis Macrocephalae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, white And extract, Herba Hedyotidis Diffusae extract, Folium Ginkgo extract, Radix Ginseng Rubra extract, Radix Glycyrrhizae extract, Rhizoma Alismatis extract, Herba Asari One or more mixing of extract.
Whitening microemulsion the most according to claim 3, it is characterised in that described water solublity whitening raw material contains Bellis perennis and carries Taking thing, Herba Hedyotidis Diffusae extract and Radix Sangusorbae extract, the addition of described daisy extract is 0.1-0.5wt%, described The addition of Herba Hedyotidis Diffusae extract is 0.1-0.5wt%, and the addition of described Radix Sangusorbae extract is 0.1-0.5wt%.
Whitening microemulsion the most according to claim 4, it is characterised in that described water solublity whitening raw material can also contain Radix Ginseng Rubra extract and Radix Angelicae Sinensis extract, the addition of described Radix Ginseng Rubra extract is 0.1-0.5wt%, described Radix Angelicae Sinensis extract Addition be 0.1-0.5wt%.
6. the preparation method of the whitening microemulsion described in an any one of claim 1-5, it is characterised in that described preparation side Method comprises the following steps: (1) is by sorbitan sesquioleate, PEG-20 sorbitan monooleate and oily components mixing structure Become oil phase, oil phase is heated to 85 DEG C, stirring and dissolving;The mixing of polyhydric alcohol, water and water solublity whitening raw material is constituted aqueous phase, by water Heat phase to 85 DEG C, stirring and dissolving;(2) aqueous phase being slowly added under quickly stirring (mixing speed 50rpm) oil phase, stirring is all Even;(3) ultrasonic Treatment using frequency to be 1kHZ 5 minutes, are cooled to room temperature.
7. a whitening massage quintessence oil, including the component of following mass percent:
There is the plants essential oil 0.01-1% of white-skinned face function
Vitamin E acetate 0.1-1%
Butylated hydroxytoluene 0.05-0.2%
The whitening microemulsion 0.1-5% of any one of claim 1-5
Vegetable oil surplus.
Whitening the most according to claim 7 massage quintessence oil, it is characterised in that the described plants essential oil with white-skinned face function For Herba Lysimachiae foenum-graeci quintessence oil, lemon grass (Cymbopogon citratus) quintessence oil, Bergamot, cumin essential oil, sandalwood essential oil, Peppermint essential oil, P-Cymene, five-leaved chaste tree essence Oil, Acotus illicioides quintessence oil, Basil Essential, eryngo quintessence oil, Fructus Citri Limoniae quintessence oil, Bergamot, clove oil, cinnamon essential oil, gorgeous mountain Folium Zingiberis quintessence oil, shellflower seed quintessence oil, Rhizoma Alpiniae Officinarum quintessence oil, Rhizoma Curcumae Longae essential oil, Rhizoma Curcumae quintessence oil, ginger essential oil, Fructus Citri grandis quintessence oil, blue or green lemon essence Oil, Basil Essential, zingiber casumnar quintessence oil, Flos Rosae Rugosae quintessence oil, Dianthus carryophyllus quintessence oil, hyacinth quintessence oil, Aleppo pine quintessence oil, see by the moon Grass quintessence oil, one or more mixing of Semen Armeniacae Amarum quintessence oil.
Whitening the most according to claim 8 massage quintessence oil, it is characterised in that described plants essential oil be lemon grass (Cymbopogon citratus) quintessence oil and The mixing of Rhizoma Curcumae Longae essential oil, described lemon grass (Cymbopogon citratus) quintessence oil and the mass ratio of Rhizoma Curcumae Longae essential oil are (1-10): (1-10).
Whitening the most according to claim 7 massage quintessence oil, it is characterised in that described vegetable oil be Oleum Helianthi, flash Bar oil and the mixing of Oleum Vitis viniferae, the mass ratio of described Oleum Helianthi, Jojoba oil and Oleum Vitis viniferae is (1-10): (1- 10): (1-10).
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