CN104072777B - 一种107胶的提纯精制工艺 - Google Patents
一种107胶的提纯精制工艺 Download PDFInfo
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- CN104072777B CN104072777B CN201410290637.9A CN201410290637A CN104072777B CN 104072777 B CN104072777 B CN 104072777B CN 201410290637 A CN201410290637 A CN 201410290637A CN 104072777 B CN104072777 B CN 104072777B
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- glue
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- 238000000034 method Methods 0.000 title abstract description 15
- 238000007670 refining Methods 0.000 title abstract 2
- 239000003292 glue Substances 0.000 claims abstract description 28
- 239000000047 product Substances 0.000 claims abstract description 23
- 239000012043 crude product Substances 0.000 claims abstract description 8
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims description 20
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 20
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 20
- -1 polydimethylsiloxane Polymers 0.000 claims description 20
- 238000000746 purification Methods 0.000 claims description 17
- 239000003463 adsorbent Substances 0.000 claims description 16
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 15
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 9
- GQIUQDDJKHLHTB-UHFFFAOYSA-N trichloro(ethenyl)silane Chemical compound Cl[Si](Cl)(Cl)C=C GQIUQDDJKHLHTB-UHFFFAOYSA-N 0.000 claims description 9
- 239000005050 vinyl trichlorosilane Substances 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 7
- 150000002978 peroxides Chemical class 0.000 claims description 6
- 108010010803 Gelatin Proteins 0.000 claims description 5
- 239000008346 aqueous phase Substances 0.000 claims description 5
- 238000007664 blowing Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 239000003999 initiator Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000012071 phase Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 claims description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 claims 1
- 239000005052 trichlorosilane Substances 0.000 claims 1
- 238000001179 sorption measurement Methods 0.000 abstract description 16
- 239000011347 resin Substances 0.000 abstract description 4
- 229920005989 resin Polymers 0.000 abstract description 4
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical group [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 8
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- 238000004519 manufacturing process Methods 0.000 description 5
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- 229920002379 silicone rubber Polymers 0.000 description 3
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- 239000004342 Benzoyl peroxide Substances 0.000 description 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 1
- 241000370738 Chlorion Species 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 235000019400 benzoyl peroxide Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000013058 crude material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- ZHPNWZCWUUJAJC-UHFFFAOYSA-N fluorosilicon Chemical compound [Si]F ZHPNWZCWUUJAJC-UHFFFAOYSA-N 0.000 description 1
- 239000000413 hydrolysate Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000002210 silicon-based material Substances 0.000 description 1
- 229920005573 silicon-containing polymer Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Abstract
Description
实施例 | 低分子吸附率见% |
1 | 91 |
2 | 83 |
3 | 95 |
4 | 93 |
5 | 91 |
对比例1 | 72 |
对比例2 | 71 |
对比例3 | 56 |
Claims (3)
Priority Applications (1)
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CN201410290637.9A CN104072777B (zh) | 2014-06-13 | 2014-06-13 | 一种107胶的提纯精制工艺 |
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CN201410290637.9A CN104072777B (zh) | 2014-06-13 | 2014-06-13 | 一种107胶的提纯精制工艺 |
Publications (2)
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CN104072777A CN104072777A (zh) | 2014-10-01 |
CN104072777B true CN104072777B (zh) | 2017-01-25 |
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CN201410290637.9A Active CN104072777B (zh) | 2014-06-13 | 2014-06-13 | 一种107胶的提纯精制工艺 |
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Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105294954B (zh) * | 2015-11-30 | 2017-10-17 | 王金明 | 一种α、ω二羟基聚二甲基硅氧烷的吸附纯化方法 |
CN105732694B (zh) * | 2016-03-04 | 2018-07-13 | 张玲 | 一种吸附提纯1,1,1,3,5,5,5-七甲基三硅氧烷的方法 |
CN107159161A (zh) * | 2017-06-04 | 2017-09-15 | 张玲 | 一种二甲基硅油纯化剂的制备方法 |
CN107082884A (zh) * | 2017-06-04 | 2017-08-22 | 王金桢 | 一种吸附提纯二甲基硅油的方法 |
CN107243329A (zh) * | 2017-08-02 | 2017-10-13 | 王金桢 | 一种合成织物用二甲基羟基硅油吸附剂的制备方法 |
CN114672279A (zh) * | 2022-04-20 | 2022-06-28 | 江门市胜鹏化工实业有限公司 | 一种基于107胶的胶黏剂组合物制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5621061A (en) * | 1994-06-29 | 1997-04-15 | Wacker-Chemie Gmbh | Process for stabilizing organopolysiloxanes |
CN101343037A (zh) * | 2007-07-10 | 2009-01-14 | 中国石油天然气股份有限公司 | 一种脱除有机硅生产中水解盐酸中的微量硅氧烷的方法 |
CN102079816A (zh) * | 2009-11-27 | 2011-06-01 | 威海赛奥新材料科技有限公司 | 高纯度硅油的制备方法 |
CN102206349A (zh) * | 2011-04-23 | 2011-10-05 | 茂名市信翼化工有限公司 | 一种α、ω二羟基聚二甲基硅氧烷的纯化方法 |
-
2014
- 2014-06-13 CN CN201410290637.9A patent/CN104072777B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5621061A (en) * | 1994-06-29 | 1997-04-15 | Wacker-Chemie Gmbh | Process for stabilizing organopolysiloxanes |
CN101343037A (zh) * | 2007-07-10 | 2009-01-14 | 中国石油天然气股份有限公司 | 一种脱除有机硅生产中水解盐酸中的微量硅氧烷的方法 |
CN102079816A (zh) * | 2009-11-27 | 2011-06-01 | 威海赛奥新材料科技有限公司 | 高纯度硅油的制备方法 |
CN102206349A (zh) * | 2011-04-23 | 2011-10-05 | 茂名市信翼化工有限公司 | 一种α、ω二羟基聚二甲基硅氧烷的纯化方法 |
Non-Patent Citations (2)
Title |
---|
吸附法脱除浓盐酸中微量硅氧烷的研究;王桂英等;《吉林化工学院学报》;20110531;第28卷(第5期);全文 * |
大孔离子交换树脂及新型吸附树脂的结构与性能;何炳林等;《高分子通报》;20050830(第4期);全文 * |
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CN104072777A (zh) | 2014-10-01 |
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Address after: 315042 Zhejiang province Jiangdong District of Ningbo City Road 265 Lane 17 No. 104 Min'an room Applicant after: Wang Jinming Address before: 322000 Zhejiang province Yiwu City Binwang zipper Street 5 District No. 3 room 602 Applicant before: Wang Jinming |
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Effective date of registration: 20180425 Address after: 324123 Jiangshan District, Jiangshan, Jiangshan District, Jiangshan District, Zhejiang, 2 85 Patentee after: JIANGSHAN HUASHUN ORGANIC SILICONE CO.,LTD. Address before: 542899 No. 25 Jianzhong Road, Hezhou, the Guangxi Zhuang Autonomous Region. Patentee before: Yang Gaolin |
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Denomination of invention: Process for purifying and refining 107 gel Effective date of registration: 20190627 Granted publication date: 20170125 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN HUASHUN ORGANIC SILICONE CO.,LTD. Registration number: 2019330000180 |
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Denomination of invention: Process for purifying and refining 107 gel Effective date of registration: 20200709 Granted publication date: 20170125 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN HUASHUN ORGANIC SILICONE Co.,Ltd. Registration number: Y2020330000463 |
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Denomination of invention: Purification process of 107 gum Effective date of registration: 20210708 Granted publication date: 20170125 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN HUASHUN ORGANIC SILICONE Co.,Ltd. Registration number: Y2021330000840 |
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Denomination of invention: Purification process of 107 glue Effective date of registration: 20220720 Granted publication date: 20170125 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN HUASHUN ORGANIC SILICONE CO.,LTD. Registration number: Y2022330001455 |
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Denomination of invention: A Purification and Refining Process for 107 Gum Effective date of registration: 20230707 Granted publication date: 20170125 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN HUASHUN ORGANIC SILICONE CO.,LTD. Registration number: Y2023330001354 |
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