CN104013547A - Toothpaste for stopping bleeding, brightening and refreshing breath and preparation method thereof - Google Patents
Toothpaste for stopping bleeding, brightening and refreshing breath and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a toothpaste for stopping bleeding, brightening and refreshing breath and a preparation method thereof. The toothpaste for stopping bleeding, brightening and refreshing breath contains the following materials: olive oil, palm oil, grape seed oil, silica, a universal self emulsified composite emulsifier, a general emulsifier, polyethylene glycol 6000, sodium dodecyl sulfate, sorbitol, a coconut extract, a bletilla striata extract, an Eclipta alba extract, a peppermint extract, a pyracantha fortuneana extract, glycerin, saturated salt water, sodium cyclamate, propylene glycol, distilled water and ethylparaben. Compared with the prior art, the toothpaste contains additional natural plant extracts, has mild property, high safety, powerful effects of removing bad breath, making the mouth breath fragrant and refreshing oral cavity, good foamability and good hemostatic effect; in addition, the toothpaste also has anti-inflammatory effect to prevent inner heat and control inflammation, and can repair mucous membrane tissue wound and enhance the oral mucosal resistance.
Description
Technical field
The present invention relates to a kind of toothpaste and preparation method thereof, particularly a kind of hemostasis brilliant white fresh breath type toothpaste and preparation method thereof.
Background technology
In a state-owned proverb " bread is the staff of life ", " food taking tooth as first ", what visible oral health was inseparable with quality of life is related to that people are recognized morning.Along with the raising of quality of life, the supply of high-carbohydrate food is abundant, and all kinds of odontopathies also display gradually, and gingival hemorrhage is also one of modal odontopathy.
Gingival hemorrhage is the too early physiology degradation phenomena of the one of gingiva tissue, to thoroughly solve a difficult problem for gingival hemorrhage, or will be from start with at all, to supplement gingiva nutrition as basic, the nutrition that can allow gingiva directly absorb is provided, make the gingiva tissue of degenerating again improve immunity, could fundamentally solve a series of teeth oral cavity problems that gingival hemorrhage brings.
Along with the raising of quality of life, people also strengthen day by day to implication attention degree.Implication roughly can be divided into that following three aspects: causes, the first is in oral cavity, to form putrefaction because food remains in, if any not brushing teeth before sleeping etc.The second is in oral cavity, to have inflammation, as periodontitis etc.The third is exactly " the intestines and stomach heat, stomach-fire prosperous " it has often been said, this reason allows people have a headache most, no matter be that herbal tea is brushed teeth, drunk to duty, or pathogenic fire purging bowel relieving stomach is all of no avail, has therefore long-term halitosis of many people, is difficult to cure.
For above dental problems, we solve with toothpaste at most selection, and therefore toothpaste also becomes a part inseparable in life.What most people used is all the toothpaste that contains pure chemistry composition, but may hide and endanger.Recently, multiple famous brand name whitening toothpastes are exposed to the sun contains bleach, life-time service unsoundness hidden danger.Therefore there is strong demand for a kind of natural non-stimulated toothpaste again with remarkable efficacy composition.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of hemostasis brilliant white fresh breath type toothpaste that contains natural component extract.
The present invention also provides the preparation method of described toothpaste.
A kind of hemostasis brilliant white fresh breath type toothpaste, contains following material in 135g toothpaste:
Described Cortex cocois radicis extracting solution is to prepare by the following method:
Cortex cocois radicis is peeled off, get coconut meat 10-50g, adding distil water 3-7 doubly measures, and squeezes coconut juice with juice extractor, and four layers of filtered through gauze are for subsequent use.
Described Rhizoma Bletillae extraction solution is to prepare by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, pulverize, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and get final product.
Described Herba Ecliptae extracting solution is to prepare by the following method:
Take Herba Ecliptae appropriate, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 8-14 times of water gaging the 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Herba Ecliptae weight, filters and get final product.
Described Herba Menthae extracting solution is prepared by the following method:
Take Herba Menthae a certain amount of, and add 8-12 distilled water doubly, be positioned in electric jacket, after 5-6 hour, be cooled to room temperature by volatile oil extractor reflux, extract,, with double gauze filtration.
Described pyracantha fortuneana extracting solution is to prepare by the following method:
Take pyracantha fortuneana appropriate, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of pyracantha fortuneana weight, filters and get final product.
Described essence is peach flavor, green cucumber essence, jasmin essence.
The preparation of toothpaste provided by the invention, comprises the following steps:
A) take olive oil 3.5-7.0g, Petiolus Trachycarpi oil 3.0-5.5g, Oleum Vitis viniferae 1.4-4.0g in beaker A, take again general-purpose self emulsifying mixed emulsifier 3.7-7.5g, unemul 0.5-3.2g in beaker A, be placed in 70-90 DEG C of water-bath heating and melting using material in beaker A as oil phase;
B) measure distilled water 5.0-30ml in beaker B, take polyethylene glycol 6000 4.5-7.0g, sodium lauryl sulphate 4.0-13.0g, sorbitol 4.0-7.0g, cyclamate 0.01-1.0g in beaker B, be placed in 70-90 DEG C of water-bath heating and melting using material in beaker B as water;
C) treat that in beaker A and beaker B, material melts completely, while reaching uniform temp, material in beaker B is slowly joined in beaker A, and be constantly stirred to completely and mix, there is not lamination in standing 5-15min, by its cool to room temperature, add successively Cortex cocois radicis extracting solution 0.6-9.0g, Rhizoma Bletillae extraction solution 1.0-12.0g, Herba Ecliptae extracting solution 1.0-2.0g, Herba Menthae extracting solution 0.5-10.0g, pyracantha fortuneana extracting solution 1.0-5.0g, glycerol 6.0-15.0ml again, constantly stir and become paste;
D) get appropriate Sal and be dissolved in and in distilled water, form saturated brine, and get 3.5-8.0g and join in beaker B, carry out stirring and adjusting denseness, take ethyl hydroxybenzoate 0.01-1.0g, add 1-12ml propylene glycol, heating is dissolved it, joins in beaker B, stirs;
E) pour part content in beaker B into mortar, add silicon dioxide 4.5-20.0g, be fully ground to pasty state, then add remaining content in beaker B, continue grinding and evenly obtain hemostasis brilliant white fresh breath type toothpaste.
Various compositions in the present invention are as follows:
Cortex cocois radicis not only can kill the antibacterial that causes dental caries, and can not improve the medicine resistance ability of " tooth worm ", and is free from side effects, and may will become the important component of tooth-care article of new generation.Unique component in Cortex cocois radicis can be resisted the main bacteria-Streptococcus mutans that causes dental caries, and not only anti-caries effect is good, and is free from side effects.
The Pseudobulbus Bletillae (Rhizoma Bletillae), containing bletilla mannan, has obvious anastalsis.The Pseudobulbus Bletillae (Rhizoma Bletillae) has antibacterial action, softening calculus, and the stimulation that diminishes inflammation and bring, alleviates red swelling of gingiva and suppresses gingival hemorrhage, improves the microcirculation of gingiva.
Herba Ecliptae energy the kidney invigorating tonifying YIN, cooling blood for hemostasis, for odontoseisis etc.It has bacteriostasis to staphylococcus aureus, typhoid fever stalk bacterium, dysentery bacterium, bacillus pyocyaneus; Have good haemostatic effect, water extract also has remarkable anastalsis.
Herba Menthae is cool in nature, nontoxic, makes people's implication delicate fragrance, contains menthol, can wind-dispelling heat-dissipating, and refresh oneself, throat, dispersing the stagnated live-QI to relieve the stagnation of QI, rash are antipruritic, anti-inflammatory analgesic, cure mainly all diseases of the abilities to speak such as toothache.Long-term brush teeth with the mentha leave drying, can make your teeth whitening, breath freshening.
In pyracantha fortuneana, contain the active substance that suppresses dental caries, to human teeth, control has positive effect, is again the quality raw materials of making toothpaste.It is rich in vitamin C, organic acid, protein, aminoacid, vitamin and multiple mineral element, can prevent gingival atrophy, hemorrhage.In pyracantha fortuneana, contain biology and brighten material, can effectively suppress the vigor of various pigment enzymes in human body.
Olive oil can improve the metabolic function of organism, promotes bone growth, promotes the generation of ore deposit agent and the absorption of calcium, effectively prevents the generation of deciduous teeth dental caries, plays an important role aspect osteoporosis in the bone growth phase and preventing.
The balanced proportion that Petiolus Trachycarpi oil contains satisfied fatty acid and unsaturated fatty acid.In Petiolus Trachycarpi oil, be rich in natural vitamin e, carotenoid and linoleic acid very useful to the health of human body, not containing cholesterol.
Oleum Vitis viniferae has preventive and therapeutic action to dental caries and gingivitis, has anti-allergic effects, gos deep into the release that cell fundamentally suppresses sensitizing factor " histamine ", improves the toleration of cell to anaphylactogen, antiinflammatory, antiallergic.
This toothpaste, by antibacterial, the anastalsis of the Pseudobulbus Bletillae (Rhizoma Bletillae) and Herba Menthae, has been controlled growing of tooth bacterium effectively; In pyracantha fortuneana, contain biology and brighten material, can effectively suppress the vigor of various pigment enzymes in human body, reach teeth whitening effect; The Pseudobulbus Bletillae (Rhizoma Bletillae) can be softened calculus, and the stimulation that diminishes inflammation and bring is alleviated red swelling of gingiva and suppresses gingival hemorrhage, improves the microcirculation of gingiva; Olive oil can improve the metabolic function of organism, promotes bone growth, promotes the generation of ore deposit agent and the absorption of calcium, effectively prevents the generation of deciduous teeth dental caries; Oleum Vitis viniferae stops the destruction of radical pair human body cell, and dental caries and gingivitis are had preventive and therapeutic action, have anti-allergic effects.
In a word, the present invention compared with prior art, has added the composition of natural plant extracts, has character gentleness, safe, potent removal halitosis, makes implication fragrance, oral cavity refreshing, there is antiinflammatory action simultaneously, prevent and treat the inflammation infringement of getting angry, repair mucosal tissue wound surface, strengthen oral mucosa resistance.
The made toothpaste of the present invention is creamy white, and viscosity is suitable, and foam is smooth suitable, and evenly fine and smooth, stretchability is good.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Olive oil of the present invention, Oleum Vitis viniferae, Petiolus Trachycarpi oil, silicon dioxide are commercially available.
Embodiment 1
The preparation of 1.1 Cortex cocois radicis extracting solution
Cortex cocois radicis is peeled off, get coconut meat 50g, 6 times of amounts of adding distil water, squeeze coconut juice with juice extractor, and four layers of filtered through gauze are for subsequent use;
The preparation of 1.2 Rhizoma Bletillae extraction solution
Take Pseudobulbus Bletillae (Rhizoma Bletillae) 150g, after pulverizing, soak 0.5h, decoct and extract 3 times in 95 DEG C of heating, add 8 times of water gagings the 1st time, extract 1.5h, add 6 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 5 times of g/ml of Fructus Sapindi Mukouossi weight.
The preparation of 1.3 Herba Ecliptae extracting solution
Take Herba Ecliptae 70g, soak 0.5h, decoct and extract 3 times in 100 DEG C of heating, add 14 times of water yields the 1st time, extract 1.5h, 10 times of water yields of the 2nd use, extract 1.5h, 8 times of water yields of the 3rd use, extract 1h, filter with double gauze at every turn, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times of g/ml of Herba Ecliptae weight.
The preparation of 1.4 Herba Menthae extracting solution
Take Herba Menthae 50g, put in round-bottomed flask, and add the distilled water of 9 times, be positioned in electric jacket, after 5 hours, be cooled to room temperature by volatile oil extractor reflux, extract,, filter to obtain extracting solution with double gauze, stand-by.
The preparation of 1.5 pyracantha fortuneana extracting solution
Take pyracantha fortuneana 90g, decoct and extract 3 times in 90 DEG C of heating, add 8 times of water yields the 1st time, extract 1.5h, 6 times of water yields of the 2nd use, extract 1.0h, and 6 times of water yields of the 3rd use are extracted 1.0h, filter with double gauze at every turn, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times of g/ml of pyracantha fortuneana weight.
The preparation of 1.6 toothpaste
A) take olive oil 4.0g, Petiolus Trachycarpi oil 3.5g, Oleum Vitis viniferae 2.4g in beaker A, take again general-purpose self emulsifying mixed emulsifier (Ac-402) 4.0g, unemul (LUXE) 0.8g in beaker A, be placed in 75 DEG C of water-bath heating and melting using material in beaker A as oil phase;
B) measure distilled water 15.0ml in beaker B, take PEG60005.0g, K
124.5g, sorbitol 4.0g, cyclamate 0.2g, in beaker B, are placed in 75 DEG C of water-bath heating and melting using material in beaker B as water;
C) treat that in beaker A and beaker B, material melts completely, while all reaching 75 DEG C, material in beaker B is slowly joined in beaker A, and be constantly stirred to emulsion bases form, add successively Cortex cocois radicis extracting solution 0.6g, Rhizoma Bletillae extraction solution 2.0g, Herba Ecliptae extracting solution 3.0g, Herba Menthae extracting solution 0.5g, pyracantha fortuneana extracting solution 1.5g, glycerol 8.0ml, constantly stir and become paste;
D) get appropriate Sal and be dissolved in and in distilled water, form saturated brine, and get 3.5g saturated brine and join in beaker A, carry out stirring and adjusting denseness, take ethyl hydroxybenzoate 0.01g, add 4ml propylene glycol, heating is dissolved it, joins in beaker B, stirs;
E) pour part content in beaker B into mortar, add silica 1 1.0g, be fully ground to pasty state, then add remaining content in beaker B, continue grinding and evenly obtain hemostasis brilliant white fresh breath type toothpaste.
Embodiment 2
The preparation of 2.1 Cortex cocois radicis extracting solution
Cortex cocois radicis is peeled off, get coconut meat 40g, 4 times of amounts of adding distil water, squeeze coconut juice with juice extractor, and four layers of filtered through gauze are for subsequent use;
The preparation of 2.2 Pseudobulbus Bletillae (Rhizoma Bletillae) extracts
Take Pseudobulbus Bletillae (Rhizoma Bletillae) 100g, after pulverizing, soak 0.5h, decoct and extract 3 times in 98 DEG C of heating, add 9 times of water gagings the 1st time, extract 1h, add 7 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 3 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight.
The preparation of 2.3 Herba Ecliptae extracting solution
Take Herba Ecliptae 70g, soak 0.6h, decoct and extract 3 times in 95 DEG C of heating, add 10 times of water yields the 1st time, extract 1.5h, 10 times of water gagings of the 2nd use, extract 1h, 8 times of water yields of the 3rd use, extract 1h, filter with double gauze at every turn, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times of g/ml of Herba Ecliptae weight.
The preparation of 2.4 Herba Menthae extracting solution
Take Herba Menthae 50g, put in round-bottomed flask, add the distilled water of 9 times, be positioned in electric jacket, after 5.5 hours, be cooled to room temperature by volatile oil extractor reflux, extract,, filter extracting solution with double gauze, stand-by.
The preparation of 2.5 pyracantha fortuneana extracting solution
Take pyracantha fortuneana 80g, extract 3 times, decoct and extract 3 times in 100 DEG C of heating, add 10 times of water yields the 1st time, extract 1.5h, 8 times of water yields of the 2nd use, extract 1.5h, 6 times of water yields of the 3rd use, extract 1.0h, filter with double gauze at every turn, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 3 times of g/ml of pyracantha fortuneana weight
The preparation of 2.6 toothpaste
A) take olive oil 6.0g, Petiolus Trachycarpi oil 5.5g, Oleum Vitis viniferae 1.4g in beaker A, take again general-purpose self emulsifying mixed emulsifier (Ac-402) 5.0g, unemul (LUXE) 1.5g in beaker A, using material in beaker A as oil phase as for heating and melting in 85 DEG C of water-baths;
B) measure distilled water 25.0ml in beaker B, take PEG60004.5g, K126.0g, sorbitol 5.0g, cyclamate 0.3g in beaker B, using material in beaker B as water as for heating and melting in 85 DEG C of water-baths;
C) treat that in beaker A and beaker B, material melts completely, while reaching uniform temp, material in beaker B is slowly joined in beaker A, and be constantly stirred to completely and mix, there is not lamination in standing 10min, by its cool to room temperature, add successively Cortex cocois radicis extracting solution 1.0g, Rhizoma Bletillae extraction solution 3.0g, Herba Ecliptae to extract 2.5g, Herba Menthae extracting solution 0.3g, pyracantha fortuneana extracting solution 2.0g, glycerol 10.0ml again, constantly stir and become paste;
D) get appropriate Sal and be dissolved in and in distilled water, form saturated brine, and get 5.0g and join in beaker B, carry out stirring and adjusting denseness, take ethyl hydroxybenzoate 0.1g, add 8ml propylene glycol, heating is dissolved it, joins in beaker B, stirs;
E) pour part content in beaker B into mortar, add silica 1 0.0g, be fully ground to pasty state, then add remaining content in beaker B, continue grinding and evenly obtain hemostasis brilliant white fresh breath type toothpaste.
Embodiment 3:
The physical and chemical index of embodiment 1,2 is as follows:
3.1 character
This product is that viscosity is suitable, and foam is smooth suitable, evenly fine and smooth, the milky toothpaste that stretchability is good.
3.2PH value checks
Dip a small amount of toothpaste with the PH reagent paper of moistening, PH is 6-7.
3.3 caloric test
Toothpaste is packaged in transparent dressing product bottle, within about one week, observes without lamination in the refrigerator cold-storages of 4 DEG C.In the calorstat of 55 DEG C, put 24h, without layering, spoiled phenomenon.
3.4 centrifugal test
Toothpaste is packaged in tool plug test tube, and the centrifugal 20min of 3000r/min, without lamination.
3.5 zests, anaphylaxis experiment
White mice back cuts off hair, smears respectively by the toothpaste of embodiment 1,2 preparation in cutting plucked position, and is not coated with position and compares, and result does not have zest and anaphylaxis.
Get 1 gram of embodiment and be applied in volunteer (25-50 year, 80 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.
3.6 room temperatures are placed experiment
Embodiment 1,2 made toothpaste are placed in to bottle for cosmetics, and room temperature leaves standstill investigates 6 months, and without lamination, unchanged with aftersensation, abnormal smells from the patient is unchanged.
3.7 toothpaste trial effects
Choose volunteer (25-50 year, 80 people) and brush teeth with prepared toothpaste, find that foam is smooth, be easy to remove, generally feel breath freshening with rear volunteer, taste is better, alleviation sensitivity of tooth.Through the continuous use of month, reduce bacteria breed in mouth, dental haemorrhage, flavescence, halitosis phenomenon obviously reduces.
Embodiment 4:
This toothpaste resultant effect is investigated
Below utilize effect of feeling to come the toothpaste that Evaluation operation example 1,2 produces on probation.Adopt public-opinion poll point system, choose people's object on probation of 80 25-50 year age bracket, be divided into arbitrarily two groups, brush teeth with toothpaste prepared by embodiment 1,2 respectively.Sooner or later used twice every day, and be two months service time.Every result of use total score is 5 points: 5 are divided into best result, represents fine, very satisfied; 4 are divided into better; 3 are divided into and can accept; 3 points is bad below, can not accept.It is below every average.The results are shown in Table 1:
Table 1 resultant effect is investigated
| Result of use | The every average of embodiment 1 | The every average of embodiment 2 |
| Hemostatic | 4.8 | 4.9 |
| Whitening | 4.8 | 4.7 |
| Refrigerant property | 5 | 5 |
| Foaming characteristic | 5 | 5 |
| Pure and fresh property | 4.9 | 4.9 |
In sum, the potent removal halitosis of the prepared toothpaste of the present invention, makes implication fragrance, and oral cavity refreshing, has good foaming characteristic, and haemostatic effect is better.
Claims (8)
1. a hemostasis brilliant white fresh breath type toothpaste, is characterized in that, in 135g toothpaste, contain with
2. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described Cortex cocois radicis extracting solution is to prepare by the following method:
Cortex cocois radicis is peeled off, get coconut meat 10-50g, adding distil water 3-7 doubly measures, and squeezes coconut juice with juice extractor, and four layers of filtered through gauze are for subsequent use.
3. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described Rhizoma Bletillae extraction solution is to prepare by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, pulverize, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and get final product.
4. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described Herba Ecliptae extracting solution is to prepare by the following method:
Take Herba Ecliptae appropriate, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 8-14 times of water gaging the 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Herba Ecliptae weight, filters and get final product.
5. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described Herba Menthae extracting solution is prepared by the following method:
Take Herba Menthae a certain amount of, and add 8-12 distilled water doubly, be positioned in electric jacket, after 5-6 hour, be cooled to room temperature by volatile oil extractor reflux, extract,, with double gauze filtration.
6. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described pyracantha fortuneana extracting solution is to prepare by the following method:
Take pyracantha fortuneana appropriate, soak 0.15-0.8h, decoct and extract 3 times in 90-100 DEG C of heating, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of pyracantha fortuneana weight, filters and get final product.
7. hemostasis brilliant white fresh breath type toothpaste according to claim 1, is characterized in that, described essence is peach flavor, green cucumber essence, jasmin essence.
8. the preparation method of a kind of brilliant white fresh breath type toothpaste that stops blooding claimed in claim 1, is characterized in that, comprises the following steps:
A) take olive oil 3.5-7.0g, Petiolus Trachycarpi oil 3.0-5.5g, Oleum Vitis viniferae 1.4-4.0g in beaker A, take again general-purpose self emulsifying mixed emulsifier 3.7-7.5g, unemul 0.5-3.2g in beaker A, be placed in 70-90 DEG C of water-bath heating and melting using material in beaker A as oil phase;
B) measure distilled water 5.0-30ml in beaker B, take polyethylene glycol 6000 4.5-7.0g, sodium lauryl sulphate 4.0-13.0g, sorbitol 4.0-7.0g, cyclamate 0.01-1.0g in beaker B, be placed in 70-90 DEG C of water-bath heating and melting using material in beaker B as water;
C) treat that in beaker A and beaker B, material melts completely, while reaching uniform temp, material in beaker B is slowly joined in beaker A, and be constantly stirred to completely and mix, there is not lamination in standing 5-15min, by its cool to room temperature, add successively Cortex cocois radicis extracting solution 0.6-9.0g, Rhizoma Bletillae extraction solution 1.0-12.0g, Herba Ecliptae extracting solution 1.0-2.0g, Herba Menthae extracting solution 0.5-10.0g, pyracantha fortuneana extracting solution 1.0-5.0g, glycerol 6.0-15.0ml again, constantly stir and become paste;
D) get appropriate Sal and be dissolved in and in distilled water, form saturated brine, and get 3.5-8.0g and join in beaker B, carry out stirring and adjusting denseness, take ethyl hydroxybenzoate 0.01-1.0g, add 1-12ml propylene glycol, heating is dissolved it, joins in beaker B, stirs;
E) pour part content in beaker B into mortar, add silicon dioxide 4.5-20.0g, be fully ground to pasty state, then add remaining content in beaker B, continue grinding and evenly obtain hemostasis brilliant white fresh breath type toothpaste.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105055038A (en) * | 2015-08-27 | 2015-11-18 | 佛山市禾才科技服务有限公司 | Toothpick capable of undergoing irreversible discoloration and preparation method thereof |
| CN105213053A (en) * | 2015-08-27 | 2016-01-06 | 佛山市禾才科技服务有限公司 | A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof |
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| CN105943478A (en) * | 2016-05-10 | 2016-09-21 | 芜湖亮晶晶生物科技有限公司 | Toothpaste with efficacies of brightening and whitening teeth and diminishing inflammation and preparation method of toothpaste |
| CN105997774A (en) * | 2016-05-10 | 2016-10-12 | 芜湖亮晶晶生物科技有限公司 | Hemostatic and anti-inflammatory toothpaste and preparation method thereof |
| CN106109344A (en) * | 2016-08-17 | 2016-11-16 | 林少英 | A kind of Fructus Citri Limoniae fresh breath toothpaste |
| CN106137853A (en) * | 2016-08-17 | 2016-11-23 | 林少英 | A kind of fresh breath toothpaste |
| CN110787090A (en) * | 2019-12-03 | 2020-02-14 | 重庆食品工业研究所 | Pyracantha fortuneana toothpaste and preparation method thereof |
| CN112137901A (en) * | 2020-10-16 | 2020-12-29 | 清远市华宝生物科技有限公司 | Anti-inflammation hemostasis whitening toothpaste and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055038A (en) * | 2015-08-27 | 2015-11-18 | 佛山市禾才科技服务有限公司 | Toothpick capable of undergoing irreversible discoloration and preparation method thereof |
| CN105213053A (en) * | 2015-08-27 | 2016-01-06 | 佛山市禾才科技服务有限公司 | A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof |
| CN105213052A (en) * | 2015-08-27 | 2016-01-06 | 佛山市禾才科技服务有限公司 | A kind of have toothpick of antibacterial hemostasia effect and preparation method thereof |
| CN105943478A (en) * | 2016-05-10 | 2016-09-21 | 芜湖亮晶晶生物科技有限公司 | Toothpaste with efficacies of brightening and whitening teeth and diminishing inflammation and preparation method of toothpaste |
| CN105997774A (en) * | 2016-05-10 | 2016-10-12 | 芜湖亮晶晶生物科技有限公司 | Hemostatic and anti-inflammatory toothpaste and preparation method thereof |
| CN106109344A (en) * | 2016-08-17 | 2016-11-16 | 林少英 | A kind of Fructus Citri Limoniae fresh breath toothpaste |
| CN106137853A (en) * | 2016-08-17 | 2016-11-23 | 林少英 | A kind of fresh breath toothpaste |
| CN110787090A (en) * | 2019-12-03 | 2020-02-14 | 重庆食品工业研究所 | Pyracantha fortuneana toothpaste and preparation method thereof |
| CN112137901A (en) * | 2020-10-16 | 2020-12-29 | 清远市华宝生物科技有限公司 | Anti-inflammation hemostasis whitening toothpaste and preparation method thereof |
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