CN103421608B - Preparation method of essence containing natural honeysuckle extract and toothpaste containing essence - Google Patents
Preparation method of essence containing natural honeysuckle extract and toothpaste containing essence Download PDFInfo
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Abstract
The invention relates to oral hygiene products, in particular to a preparation method of essence containing natural honeysuckle extract and a toothpaste containing the essence. The method includes: weighing honeysuckle, ethanol and purified water for mixing, soaking under negative pressure, heating for decoction, and filtering to obtain filtrate and residue; decoloring the filtrate, and concentrating to obtain honeysuckle extract; well mixing natural menthol, dementholized peppermint oil, fennel oil, eugenol and spearmint oil with the honeysuckle extract, and standing to obtain the honeysuckle extract essence. The honeysuckle extract essence is rich, stable and lasting in fragrance, capable of decreasing swelling to relieve pain, activating blood to scatter stasis, removing prickly heat to stop itching and refreshing. The toothpaste containing the essence is capable of clearing heat, decreasing internal heat, diminishing inflammation, removing bad breath, and the like, and especially capable of well relieving gum swelling and bleeding. Due to the fact that the ingredients of the toothpaste are the natural extract, natural inflammation diminishing, pain easing and bleeding stopping functions are provided without any side effects.
Description
Technical field
The present invention relates to dental care products, specifically relate to a kind of essence and the toothpaste preparation method that contain natural honeysuckle extract.
Background technology
Toothpaste is used from cleaning teeth with toothbrush one, and protection oral hygiene, to a kind of daily necessities of human-body safety, has very long history.Along with the progress of society, various types of toothpaste is come out one after another, and natural extract is applied in toothpaste as activeconstituents and solves related oral problem, has become market mainstream focus.
Japanese Honeysuckle is the general designation of Chinese medicinal materials and plant.Plant honeysuckle has another name called honeysuckle, is the perennial half evergreen winding bejuco of Caprifoliaceae." Japanese Honeysuckle " one comes from Compendium of Material Medica, owing to opening as white at the beginning of Flos Lonicerae, after transfer yellow to, hence obtain one's name Japanese Honeysuckle.Medicinal material Japanese Honeysuckle is Caprifoliaceae woodbine honeysuckle and belongs to together, plant drying Alabastrum or just opened flower.Japanese Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times.Its property sweet cold air fragrance, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Japanese Honeysuckle can dispelling wind-heat, removing summer-heat blood poison, for various febrile disease, as the disease such as body heat, dermexanthesis, spot, hot carbuncle carbuncle, swelling and pain in the throat, and equal Be very effective.
Summary of the invention
An object of the present invention be to provide a kind ofly have that swelling and pain relieving, promoting blood circulation to remove blood stasis, miliaria of dispelling are antipruritic, the natural honeysuckle extract essence of effect that produces refreshing effect to the mind and preparation method thereof.
In order to realize this object, the technical solution adopted in the present invention is: a kind of preparation method of natural honeysuckle extract essence, comprises the steps:
1., take is Japanese Honeysuckle by weight proportion: ethanol: pure water=0.6 ~ 1.25: the raw material of 0.45 ~ 0.85: 3.5 ~ 4.5;
2., by Japanese Honeysuckle, ethanol, pure water mixing, be soak 36 ~ 48h under the condition of-0.050 ~-0.060MPa in vacuum tightness, reheat decoction 4 ~ 5h, filter to get filtrate and filter residue;
3., by filtrate decolour, and be that 80 ~ 120: 1 (being 80 ~ 120L before such as concentrating, is 1L after concentrated) concentrates by volume, obtain Flos Lonicerae extract;
4., according to parts by weight, Natural menthol 18 ~ 25 parts, Peppermint Oil 30 ~ 36 parts, olium anisi 0.8 ~ 1.2 part, Eugenol 0.4 ~ 0.6 part, Oleum Menthae Rotundifoliae 0.5 ~ 1 part and Flos Lonicerae extract 10 ~ 15 parts are stirred, leave standstill 12 ~ 36h, obtain natural honeysuckle extract essence.
Preferably, described step 1. in the volumn concentration of ethanol be 40 ~ 75%.
Preferably, described step 2. middle decocting time is 4.5h, and decocting temperature is 65 ~ 85 DEG C.
Preferably, described step 3. in concentrated be to carry out at 100: 1 by volume, and thickening temperature is 70 ~ 100 DEG C.
Preferably, described step 4. in time of repose be 24h.
In addition, the invention also discloses a kind of natural honeysuckle extract essence according to preparing described in above-mentioned preparation method.
Another object of the present invention is to provide a good drug efficacy, without any side effects, heat-clearing can be played, fall fire, anti-inflammatory, the effect such as antihalitosis, red and swollen for gum especially and gingival hemorrhage have the toothpaste of good remission effect.
In order to realize this object, the technical solution adopted in the present invention is: the toothpaste containing natural honeysuckle extract essence, is the natural honeysuckle extract essence of 1.5 ~ 2.5% in its lotion total composition containing weight ratio.
As a kind of preferred implementation of the toothpaste containing natural honeysuckle extract essence of the present invention, this toothpaste also comprises following component:
Three of object of the present invention is the preparation method providing this toothpaste a kind of, comprises the steps:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, heating 5 ~ 10min, forms mixture D 3;
D, mixed with mixture D 2 by sorbyl alcohol, heating 5 ~ 10min, forms mixture D 4;
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stir 3 ~ 5min under vacuum, make lotion, be filled into multiple-unit tube.
Preferably, described step c Heating temperature is 50 ~ 70 DEG C, and steps d Heating temperature is 60 ~ 70 DEG C.
The present invention contains essence and the toothpaste preparation method of natural honeysuckle extract, and its beneficial effect shows:
1, the natural honeysuckle extract essence of preparation give off a strong fragrance, stable and stay length, and have can antipruritic, the effect that produces refreshing effect to the mind of swelling and pain relieving, promoting blood circulation to remove blood stasis, miliaria of dispelling.
2, preparation containing the toothpaste of natural honeysuckle extract essence, heat-clearing can be played, fall fire, anti-inflammatory, the effect such as antihalitosis, red and swollen for gum especially and gingival hemorrhage have good remission effect.Because main component is natural extract, there is natural anti-inflammatory, analgesia, hemostatic function, without any side effects.Meanwhile, old and young women and children are all suitable, and life-time service is useful and harmless.
3, the manufacture craft of toothpaste is simple, is applicable to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated, it should be noted that, various raw material is delicatessen food level, or obtain according to prior art preparation.
Embodiment 1
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 416g (after drying, lower with), 70% ethanol 283g and pure water 1500g mix, be soak 48h under the condition of-0.050MPa in vacuum tightness.
2., be heated to 85 DEG C of decoction 4.5h, filter to get filtrate and filter residue.
3., by filtrate decolour with gac (weight percent is not higher than 5%), 100 DEG C of constant temperature are concentrated into 20g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 37g, Peppermint Oil 47g, olium anisi 1.7g, Eugenol 0.8g and Oleum Menthae Rotundifoliae 1.3g, stir, leave standstill 24h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table (in 100g, lower same)
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 2.5 | Sodium monoflurophosphate | 1 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.5 |
| Silicon-dioxide | 17 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 50 DEG C of heating 10min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 70 DEG C of heating 10min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 5min under vacuum, make lotion, be filled into multiple-unit tube.
Embodiment 2
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 400g, 65% ethanol 275g and pure water 1400g mix, be soak 45h under the condition of-0.060MPa in vacuum tightness.
2., be heated to 75 DEG C of decoction 4h, filter to get filtrate and filter residue.
3., by filtrate decolour, 95 DEG C of constant temperature are concentrated into 19g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 36g, Peppermint Oil 45g, olium anisi 1.6g, Eugenol 0.7g and Oleum Menthae Rotundifoliae 1.2g, stir, leave standstill 18h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 2.2 | Sodium monoflurophosphate | 0.9 |
| Sorbyl alcohol | 68 | Tertiary sodium phosphate | 0.45 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 60 DEG C of heating 7min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 65 DEG C of heating 5min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 4min under vacuum, make lotion, be filled into multiple-unit tube.
Embodiment 3
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 380g, 60% ethanol 275g and pure water 1400g mix, be soak 40h under the condition of-0.060MPa in vacuum tightness.
2., be heated to 75 DEG C of decoction 5h, filter to get filtrate and filter residue.
3., by filtrate decolour, 90 DEG C of constant temperature are concentrated into 17g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 34g, Peppermint Oil 43g, olium anisi 1.4g, Eugenol 0.7g and Oleum Menthae Rotundifoliae 1.1g, stir, leave standstill 30h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 2 | Sodium monoflurophosphate | 0.8 |
| Sorbyl alcohol | 67 | Tertiary sodium phosphate | 0.35 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 65 DEG C of heating 5min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 60 DEG C of heating 10min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 3min under vacuum, make lotion, be filled into multiple-unit tube.
Embodiment 4
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 360g, 50% ethanol 260g and pure water 1300g mix, be soak 38h under the condition of-0.050MPa in vacuum tightness.
2., be heated to 73 DEG C of decoction 4h, filter to get filtrate and filter residue.
3., by filtrate decolour, 80 DEG C of constant temperature are concentrated into 16g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 26g, Peppermint Oil 38g, olium anisi 1.2g, Eugenol 0.6g and Oleum Menthae Rotundifoliae 1g, stir, leave standstill 12h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 1.8 | Sodium monoflurophosphate | 0.7 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.25 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 70 DEG C of heating 8min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 70 DEG C of heating 5min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 3min under vacuum, make lotion, be filled into multiple-unit tube.
Embodiment 5
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 320g, 45% ethanol 250g and pure water 1200g mix, be soak 37h under the condition of-0.055MPa in vacuum tightness.
2., be heated to 72 DEG C of decoction 5h, filter to get filtrate and filter residue.
3., by filtrate decolour, 80 DEG C of constant temperature are concentrated into 13g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 21g, Peppermint Oil 33g, olium anisi 1g, Eugenol 0.5g and Oleum Menthae Rotundifoliae 0.7g, stir, leave standstill 36h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 1.7 | Sodium monoflurophosphate | 0.6 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.15 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 55 DEG C of heating 5min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 60 DEG C of heating 8min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 4min under vacuum, make lotion, be filled into multiple-unit tube.
Embodiment 6
1, the preparation of natural honeysuckle extract essence
1., extracting honeysuckle 200g, 40% ethanol 150g and pure water 1000g mix, be soak 36h under the condition of-0.055MPa in vacuum tightness.
2., be heated to 65 DEG C of decoction 4h, filter to get filtrate and filter residue.
3., by filtrate decolour, 80 DEG C of constant temperature are concentrated into 10g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 18g, Peppermint Oil 30g, olium anisi 0.8g, Eugenol 0.4g and Oleum Menthae Rotundifoliae 0.5g, stir, leave standstill 25h, obtain natural honeysuckle extract essence.
The preparation of the toothpaste 2, containing natural honeysuckle extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural honeysuckle extract essence | 1.5 | Sodium monoflurophosphate | 0.55 |
| Sorbyl alcohol | 50 | Tertiary sodium phosphate | 0.1 |
| Silicon-dioxide | 21 | Xylo-Mucine | 1.2 |
| Lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, 65 DEG C of heating 9min, form mixture D 3.
D, mixed with mixture D 2 by sorbyl alcohol, 65 DEG C of heating 5min, form mixture D 4.
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stirring 5min under vacuum, make lotion, be filled into multiple-unit tube.
Comparative example 1
Only be with the difference of embodiment 1, when preparing toothpaste, do not add natural honeysuckle extract essence, other component and content identical with embodiment 1 (supplying less than 100g pure water).
Clinical trial result
Test method: choose there are gingival hemorrhage, gum red and swollen symptom experimenter 90 people tests, each half of men and women, the age from 18 ~ 59 years old, 30 years old mean age.Be divided into 2 groups at random, the toothpaste (being added with natural honeysuckle extract essence) that experimental group uses embodiment 1 to prepare, the toothpaste (not adding natural honeysuckle extract essence) that control group uses comparative example 1 to prepare, every morning, evening respectively brush teeth once.
Brush teeth before test, first record the gingival hemorrhage of experimenter, the red and swollen symptom of gum.
Brush teeth test after the 7th day, then the gingival hemorrhage of unified inspection experimenter, the red and swollen symptom variation of gum.
Criterion: after test of brushing teeth, experimenter's gingival hemorrhage reduce or eliminate, gum redness alleviates or eliminates be effective, otherwise, unchanged or gingival hemorrhage increase and gum redness add severe one be all considered as invalid.
Check after experimenter uses seven days, result is as follows:
From the assay of experimenter, the toothpaste containing natural honeysuckle extract essence of the present invention, for alleviating gingival hemorrhage symptom efficient 84.4%, being 82.2% for alleviating the red and swollen symptom of gum efficient, being all obviously better than the statistic data of control group.Therefore, the toothpaste containing natural honeysuckle extract essence of the present invention, all has good prevention and therapy effect for gingival hemorrhage, gum redness.
Above content is only conceive example and explanation to the present invention; affiliated those skilled in the art make various amendment to described specific embodiment or supplement or adopt similar mode to substitute; only otherwise depart from the design of invention or surmount this scope as defined in the claims, protection scope of the present invention all should be belonged to.
Claims (7)
1. the toothpaste containing natural honeysuckle extract essence, is characterized in that, be made up of the component of following weight percent:
The preparation method of described natural honeysuckle extract essence comprises the steps:
1., take is Japanese Honeysuckle by weight proportion: ethanol: pure water=0.6 ~ 1.25: the raw material of 0.45 ~ 0.85: 3.5 ~ 4.5;
2., by Japanese Honeysuckle, ethanol, pure water mixing, be soak 36 ~ 48h under the condition of-0.050 ~-0.060MPa in vacuum tightness, reheat decoction 4 ~ 5h, filter to get filtrate and filter residue;
3., by filtrate decolour, and be to concentrate at 80 ~ 120: 1 by volume, obtain Flos Lonicerae extract;
4., according to parts by weight, Natural menthol 18 ~ 25 parts, Peppermint Oil 30 ~ 36 parts, olium anisi 0.8 ~ 1.2 part, Eugenol 0.4 ~ 0.6 part, Oleum Menthae Rotundifoliae 0.5 ~ 1 part and Flos Lonicerae extract 10 ~ 15 parts are stirred, leave standstill 12 ~ 36h, obtain natural honeysuckle extract essence.
2. the toothpaste containing natural honeysuckle extract essence according to claim 1, is characterized in that, described step 1. in the volumn concentration of ethanol be 40 ~ 75%.
3. the toothpaste containing natural honeysuckle extract essence according to claim 1, is characterized in that, described step 2. middle decocting time is 4.5h, and decocting temperature is 65 ~ 85 DEG C.
4. the toothpaste containing natural honeysuckle extract essence according to claim 1, is characterized in that, described step 3. in concentrated be to carry out at 100: 1 by volume, and thickening temperature is 70 ~ 100 DEG C.
5. the toothpaste containing natural honeysuckle extract essence according to claim 1, is characterized in that, described step 4. middle time of repose is 24h.
6. a preparation method for the toothpaste containing natural honeysuckle extract essence as described in any one of Claims 1 to 5, is characterized in that, comprise the steps:
A, lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 mixed, heating 5 ~ 10min, forms mixture D 3;
D, mixed with mixture D 2 by sorbyl alcohol, heating 5 ~ 10min, forms mixture D 4;
E, mixture D 3, D4 to be added in emulsification pot, add natural honeysuckle extract essence and mix, stir 3 ~ 5min under vacuum, make lotion, be filled into multiple-unit tube.
7. the preparation method of the toothpaste containing natural honeysuckle extract essence according to claim 6, it is characterized in that, described step c Heating temperature is 50 ~ 70 DEG C, and steps d Heating temperature is 60 ~ 70 DEG C.
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