CN104887555A - Honeysuckle flower toothpaste and preparation method thereof - Google Patents
Honeysuckle flower toothpaste and preparation method thereof Download PDFInfo
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- CN104887555A CN104887555A CN201510226246.5A CN201510226246A CN104887555A CN 104887555 A CN104887555 A CN 104887555A CN 201510226246 A CN201510226246 A CN 201510226246A CN 104887555 A CN104887555 A CN 104887555A
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Abstract
The invention discloses a honeysuckle flower toothpaste and a preparation method thereof, which belongs to the technical field of toothpaste. The honeysuckle flower toothpaste is prepared by silica, carragheenan, xanthan gum, sorbitol, sodium dodecyl sulfate, menthol, sodium benzoate, essential oil, water-soluble artificial food coloring, deionized water and a honeysuckle flower extract product. The toothpaste is prepared by the honeysuckle flower extract, the honeysuckle flower essential oil and sodium benzoate, three substrates have good synergism, can enlarge antibiosis, antiviral and bacteriostasis effects of honeysuckle flower, and have good efficacy for clearing heat to decrease internal heat, cleaning tooth and refreshing breath.
Description
Technical field
The present invention relates to technical field of toothpaste, specifically, relate to a kind of Flos Lonicerae odontopathy paste and preparation method thereof.
Background technology
Toothpaste is the articles for use of cleaning teeth in daily life, is the necessary of protection human oral cavity health and human-body safety.Common toothpaste usually by abrasivus (as calcium carbonate, calcium hydrogen phosphate, calcium pyrophosphate, silicon dioxide, aluminium hydroxide), wetting agent is (as glycerol, sorbitol, propylene glycol, Polyethylene Glycol and water), surfactant is (as sodium lauryl sulfate, 2 ~ acyl-oxygen base key sodium sulfonate, sodium lauroyl sarcosine), thickening agent is (as carboxymethyl cellulose, Cornu Cervi pectin, hydroxyethyl-cellulose, xanthan gum, guar gum, carrageenin etc.), sweeting agent is (as glycerol, cyclohexylamine sulfonic acid sodium, saccharin sodium etc.), antiseptic (as sorbic acid potassium salt and sodium benzoate), active additive is (as chlorophyll, fluoride) and color element, essence etc. mix.Ordinary toothpaste has the effect of cleaning oral cavity, but the poor effect in its protection oral cavity.Illness finds its way in by the mouth, the kind of present people's diet is more and more come more, and tooth plays mastication in people's diet processes, easily be subject to from infringements such as the antibacterials in food, the odontopathies such as dental caries, decayed tooth, anaphylaxis dentine, gingivitis, periodontitis have had influence on our daily life deeply, among many people are just enduring the worries of can't have dinner because having a toothache to the fullest extent and decoct.Especially in Guizhou province, because dampness is heavier, everybody likes eating maror, and maror easily causes getting angry, especially blocked shot in the winter time, the people of more than 90% can often get angry, and get angry and can bring misery to people's diet, serious gets angry, and can cause pharyngodynia with dryness, angular chilitis and toothache etc.The difficult demand meeting people of the common abstersive toothpaste of only tool, therefore, studies and a kind ofly has the toothpaste improving oral problem and have important practical significance.
Summary of the invention
In view of this, the object of this invention is to provide a kind of Flos Lonicerae odontopathy paste and preparation method thereof, to solve effect that existing ordinary toothpaste does not have good protection oral cavity, be difficult to meet the demand of people and the deficiency existed.
The present invention solves the problems of the technologies described above by the following technical programs:
A kind of Flos Lonicerae odontopathy paste, is prepared from by the raw material of following weight portion:
Preferably, described Flos Lonicerae odontopathy paste is prepared from by the raw material of following weight portion:
More preferably, described Flos Lonicerae odontopathy paste is prepared from by the raw material of following weight portion:
The preparation method of described Flos Lonicerae odontopathy paste, first by sodium benzoate, deionized water, Mentholum and after water solublity food coloring mix and blend a period of time, obtains aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, a period of time is stirred under certain rotating speed, after adding aqueous solution continuation stirring a period of time, add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions with after certain rotating speed stirring reaction a period of time, then add quintessence oil, stir a period of time with certain rotating speed under vacuum conditions, last fill, to obtain final product.
Preferably, the preparation method of described Flos Lonicerae odontopathy paste, by sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 20 ~ 60min, obtains aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1000 ~ 2000r/min, after reaction 20 ~ 30min, then adds aqueous solution continuation stirring 10 ~ 20min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 15 ~ 20min, then add quintessence oil, stir 12 ~ 18min under vacuum conditions, last fill, to obtain final product.
Vacuum under described vacuum state is more than 0.096MPa.
Described quintessence oil is Flos Lonicerae quintessence oil.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 40 ~ 50min of 50 ~ 60 DEG C, carry out decoction 2 ~ 3h, filter and filtrate is concentrated into the clear paste that relative density is 1.1 ~ 1.2, by clear paste and ethanol with (20 ~ 30): after the mass ratio of (70 ~ 80) fully mixes, reflux, extract, 1 ~ 2 time at the temperature of 70 ~ 80 DEG C, leave standstill 8 ~ 10h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6 ~ 7, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: with parts by weight, gets 100 parts of honeysuckle fresh flowers, adds 1400 ~ 1600 parts of water, add 45 ~ 55 parts of normal hexane again, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Described carrageenan, also known as antler glue, carrageenin, Irish Herba corydalis edulis glue, is a kind of general designation of the polysaccharide extracted from marine red alga (comprising Chondrus, Eucheuma, China fir Trentepohlia and husky Lepidium etc.).
Described xanthan gum is also known as Xanthan gum, HANSHENGJIAO, Xanthan Gum, it is a kind of monospore polysaccharide of generation of being fermented by false xanthomonas, be primary raw material by cabbage black rot xanthomonas campestris with carbohydrate, through aerobic fermentation biotechnology, cut off 1,6 ~ glycosidic bond, after opening side chain, by the outer heteropolysaccharide of the acid born of the same parents of the one of Isosorbide-5-Nitrae ~ be bonded to straight chain composition.
Described Sorbitol, another name sorbitol is white hygroscopic powder or crystalline powder, lamellar or granule, odorless.Have refrigerant sweet taste, Sorbitol character: colorless needle crystals, or white crystalline powder, odorless, have refrigerant sweet taste, soluble in water, be insoluble in organic solvent, it is acidproof, and heat resistance is good, and with aminoacid, protein etc. not easily play Maillard reaction.
Described sodium lauryl sulphate, white or faint yellow powdery, water-soluble, to alkali and hard water insensitive, there is the foaming power of decontamination, emulsifying and excellence.
Described Mentholum system extracted by the leaf of Herba Menthae and stem, has another name called menthol, Mentholum, white crystal, has refrigerant itching-relieving action, for oral administrationly can be used as carminative.
Described sodium benzoate is mostly white particle, and odorless or micro-band Benzoinum abnormal smells from the patient, taste is micro-sweet, has convergence, and sodium benzoate is not only good acid antiseptic, also has sterilization and bacteriostasis effect.
Described edible synthesized coloring matter is generally bright in colour, strong coloring force, good stability, odorless, tasteless, and quality is homogeneous, is easy to dissolve and colorant match, and with low cost,
Containing a large amount of neochlorogenic acid, caffeic acid and chlorogenic acid in described Flos Lonicerae extract, there is antibacterial, antiviral and bacteriostasis preferably.
Described Flos Lonicerae quintessence oil has the effect that slow down aging, balance sebum and moisture are secreted.
Beneficial effect of the present invention is:
1. the present invention is by being used for preparing toothpaste by Flos Lonicerae extractive solution, Flos Lonicerae quintessence oil and sodium benzoate, and these three kinds of materials have good synergism, can expand antibacterial, antiviral and the bacteriostasis of Flos Lonicerae, obtain effect of good resolving heat and reducing pathogenic fire.
2. the present invention is by comprehensively allocating silicon dioxide, carrageenan, xanthan gum, sorbitol, sodium lauryl sulphate, Mentholum, sodium benzoate, Flos Lonicerae quintessence oil, water solublity food coloring, deionized water and Flos Lonicerae extract, make the toothpaste outward appearance of production better, color is that Herba Menthae is green, and taste good, for mint aroma, the favor of consumers in general can be obtained.
3. technique of the present invention is simple, and convenient operation, production procedure is short, and production efficiency is high, is suitable for large-scale batch production.Meanwhile, this technique, due to the response time of the sequencing that strictly controls material and add and material, is conducive to the performance of effect of various raw material, makes to produce effect that Flos Lonicerae odontopathy paste has good resolving heat and reducing pathogenic fire, cleaning teeth and fresh breath.
Detailed description of the invention
Conveniently those skilled in the art will recognize that the present invention will be further described below in conjunction with embodiment.Embodiment is only illustrating this invention, is not limitation of the invention, and the step not doing in embodiment to illustrate is all prior arts, is not described in detail at this.
Embodiment one
Raw material:
Silica 1 00kg, carrageenan 4kg, xanthan gum 5kg, sorbitol 600kg, sodium lauryl sulphate 12kg, Mentholum 0.5kg, sodium benzoate 2kg, Flos Lonicerae quintessence oil 3kg, water solublity food coloring 8kg, deionized water 50kg and Flos Lonicerae extract 40kg.
Preparation method:
By sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 20min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1000r/min, after reaction 20min, then adds aqueous solution continuation stirring 10min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 15min, then add Flos Lonicerae quintessence oil, under the vacuum state of 0.096MPa, stir 12min, last fill, obtains Flos Lonicerae odontopathy paste.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 40min of 50 DEG C, carry out decoction 2h, filter and filtrate is concentrated into the clear paste that relative density is 1.1, after clear paste and ethanol are fully mixed with the mass ratio of 20:70, reflux, extract, 1 time at the temperature of 70 DEG C, leave standstill 8h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: get 100g honeysuckle fresh flower, add 1400g water, then add 45g normal hexane, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Embodiment two
Raw material:
Silica 1 80kg, carrageenan 5kg, xanthan gum 10kg, sorbitol 800kg, sodium lauryl sulphate 18kg, Mentholum 2kg, sodium benzoate 4kg, Flos Lonicerae quintessence oil 5kg, water solublity food coloring 12kg, deionized water 80kg and Flos Lonicerae extract 60kg.
Preparation method:
By sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 60min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 2000r/min, after reaction 30min, then adds aqueous solution continuation stirring 20min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 20min, then add Flos Lonicerae quintessence oil, under the vacuum state of 0.1MPa, stir 18min, last fill, obtains Flos Lonicerae odontopathy paste.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 50min of 60 DEG C, carry out decoction 3h, filter and filtrate is concentrated into the clear paste that relative density is 1.2, after clear paste and ethanol are fully mixed with the mass ratio of 30:80, reflux, extract, 2 times at the temperature of 80 DEG C, leave standstill 10h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 7, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: get 100g honeysuckle fresh flower, add 1600g water, then add 55g normal hexane, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Embodiment three
Raw material:
Silica 1 20kg, carrageenan 4.2kg, xanthan gum 6kg, sorbitol 650kg, sodium lauryl sulphate 13kg, Mentholum 0.6kg, sodium benzoate 2.5kg, Flos Lonicerae quintessence oil 3.5kg, water solublity food coloring 9kg, deionized water 60kg and Flos Lonicerae extract 45kg.
Preparation method:
By sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 30min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1300r/min, after reaction 22min, then adds aqueous solution continuation stirring 12min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 16min, then add Flos Lonicerae quintessence oil, under the vacuum state of 0.1MPa, stir 13min, last fill, obtains Flos Lonicerae odontopathy paste.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 42min of 52 DEG C, carry out decoction 2.2h, filter and filtrate is concentrated into the clear paste that relative density is 1.1, after clear paste and ethanol are fully mixed with the mass ratio of 22:72, reflux, extract, 2 times at the temperature of 72 DEG C, leave standstill 9h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6.2, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: get 100g honeysuckle fresh flower, add 1450g water, then add 48g normal hexane, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Embodiment four
Raw material:
Silica 1 60kg, carrageenan 4.8kg, xanthan gum 9kg, sorbitol 750kg, sodium lauryl sulphate 17kg, Mentholum 1.5kg, sodium benzoate 3.5kg, Flos Lonicerae quintessence oil 4.5kg, water solublity food coloring 11kg, deionized water 70kg and Flos Lonicerae extract 55kg.
Preparation method:
By sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 50min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1800r/min, after reaction 28min, then adds aqueous solution continuation stirring 17min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 19min, then add Flos Lonicerae quintessence oil, under the vacuum state of 0.096MPa, stir 16min, last fill, obtains Flos Lonicerae odontopathy paste.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 48min of 58 DEG C, carry out decoction 2.7h, filter and filtrate is concentrated into the clear paste that relative density is 1.2, after clear paste and ethanol are fully mixed with the mass ratio of 28:78, reflux, extract, 1 time at the temperature of 78 DEG C, leave standstill 10h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6.7, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: get 100g honeysuckle fresh flower, add 1550g water, then add 52g normal hexane, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Embodiment five
Raw material:
Silica 1 40kg, carrageenan 4.4kg, xanthan gum 8kg, sorbitol 700kg, sodium lauryl sulphate 15kg, Mentholum 1kg, sodium benzoate 3kg, Flos Lonicerae quintessence oil 4kg, water solublity food coloring 10kg, deionized water 65kg and Flos Lonicerae extract 50kg.
Preparation method:
By sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 40min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1500r/min, after reaction 25min, then adds aqueous solution continuation stirring 15min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 18min, then add Flos Lonicerae quintessence oil, under the vacuum state of 0.096MPa, stir 15min, last fill, obtains Flos Lonicerae extractive solution.
The preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 45min of 55 DEG C, carry out decoction 2.5h, filter and filtrate is concentrated into the clear paste that relative density is 1.2, after clear paste and ethanol are fully mixed with the mass ratio of 25:75, reflux, extract, 2 times at the temperature of 75 DEG C, leave standstill 9h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6.5, dries to obtain Flos Lonicerae extract.
The preparation method of described Flos Lonicerae quintessence oil is: get 100g honeysuckle fresh flower, add 1500g water, then add 50g normal hexane, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
Effect of the present invention is verified below with test example:
Test example
Choose 100 consumers of often getting angry, men and women half and half.Use freely to by this Flos Lonicerae odontopathy paste above-mentioned consumer, after half a year, allow these 100 consumers be described the situation after this Flos Lonicerae odontopathy paste of use.Survey result shows: the consumer of 100% all thinks that this Flos Lonicerae odontopathy paste has good cleaning oral cavity effect, and feel oral cavity refreshing after brushing teeth, the consumer of 98% is after this Flos Lonicerae odontopathy paste of use, there is not the situation of getting angry, the consumer of 2% is during this Flos Lonicerae odontopathy paste of use, also occur the situation of getting angry, but also represent that degree of getting angry is less than in the past, and frequency is lower than in the past.Known by above-mentioned survey result, this Flos Lonicerae odontopathy paste has the effect of good cleaning oral cavity, cleaning implication and resolving heat and reducing pathogenic fire.
The above, it is only better example of the present invention, not any pro forma restriction is done to the present invention, anyly do not depart from technical solution of the present invention content, the any simple modification done above example according to technical spirit of the present invention, coversion material equivalent variations and modification, all still belong in the scope of technical solution of the present invention.
Claims (9)
1. a Flos Lonicerae odontopathy paste, is characterized in that, is prepared from by the raw material of following weight portion:
2. Flos Lonicerae odontopathy paste as claimed in claim 1, is characterized in that, be prepared from by the raw material of following weight portion:
3. Flos Lonicerae odontopathy paste as claimed in claim 1, is characterized in that, be prepared from by the raw material of following weight portion:
4. the preparation method of the Flos Lonicerae odontopathy paste as described in claim 1,2,3 any one, is characterized in that, first by sodium benzoate, deionized water, Mentholum and after water solublity food coloring mix and blend a period of time, obtains aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, a period of time is stirred under certain rotating speed, after adding aqueous solution continuation stirring a period of time, add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions with after certain rotating speed stirring reaction a period of time, then add quintessence oil, stir a period of time with certain rotating speed under vacuum conditions, last fill, to obtain final product.
5. the preparation method of Flos Lonicerae odontopathy paste as claimed in claim 4, is characterized in that, by sodium benzoate, deionized water, Mentholum and water solublity food coloring mix and blend 20 ~ 60min, obtain aqueous solution; Carrageenan, xanthan gum and sorbitol are mixed, adjusting rotary speed is 1000 ~ 2000r/min, after reaction 20 ~ 30min, then adds aqueous solution continuation stirring 10 ~ 20min; Then add silicon dioxide, Flos Lonicerae extract and sodium lauryl sulphate, under vacuum conditions stirring reaction 15 ~ 20min, then add quintessence oil, stir 12 ~ 18min under vacuum conditions, last fill, to obtain final product.
6. the preparation method of the Flos Lonicerae odontopathy paste as described in claim 4 or 5, is characterized in that, the vacuum under described vacuum state is more than 0.096MPa.
7. the Flos Lonicerae odontopathy paste as described in claim 1,2,3 any one, is characterized in that, described quintessence oil is Flos Lonicerae quintessence oil.
8. as claim 1, 2, Flos Lonicerae odontopathy paste described in 3 any one, it is characterized in that, the preparation method of described Flos Lonicerae extract is: after Flos Lonicerae being added the warm water lixiviate 40 ~ 50min of 50 ~ 60 DEG C, carry out decoction 2 ~ 3h, filter and filtrate is concentrated into the clear paste that relative density is 1.1 ~ 1.2, by clear paste and ethanol with (20 ~ 30): after the mass ratio of (70 ~ 80) fully mixes, reflux, extract, 1 ~ 2 time at the temperature of 70 ~ 80 DEG C, leave standstill 8 ~ 10h, crossing leaching supernatant sodium hydroxide solution adjust ph is after 6 ~ 7, dry to obtain Flos Lonicerae extract.
9. the Flos Lonicerae odontopathy paste as described in claim 1,2,3 any one, it is characterized in that, the preparation method of described Flos Lonicerae quintessence oil is: with parts by weight, get 100 parts of honeysuckle fresh flowers, add 1400 ~ 1600 parts of water, add 45 ~ 55 parts of normal hexane again, be heated to liquid boiling, collect distillate, and normal hexane layer is separated from distillate, by the extracted with diethyl ether 3 times of water layer same volume obtained, isolate ether layer, merge normal hexane layer and ether layer, with filter paper filtering after centrifugal, after volatilizing organic reagent, obtain Flos Lonicerae quintessence oil.
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| CN108420781A (en) * | 2018-04-24 | 2018-08-21 | 纯美生物医药科技（上海）有限公司 | A kind of toothpaste |
| CN109464319A (en) * | 2018-11-02 | 2019-03-15 | 东莞波顿香料有限公司 | Breath freshening capsule and preparation method thereof |
| CN109223650A (en) * | 2018-11-12 | 2019-01-18 | 魏楚杰 | A kind of clearing heat and removing internal heat toothpaste |
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Application publication date: 20150909 |