CN106491430A - A kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof - Google Patents

A kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof Download PDF

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Publication number
CN106491430A
CN106491430A CN201611028437.1A CN201611028437A CN106491430A CN 106491430 A CN106491430 A CN 106491430A CN 201611028437 A CN201611028437 A CN 201611028437A CN 106491430 A CN106491430 A CN 106491430A
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China
Prior art keywords
parts
flos lonicerae
sorbitol solution
compound recipe
sodium
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CN201611028437.1A
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Chinese (zh)
Inventor
陈莉
侯成贤
杨燕飞
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Zunyi Medical University
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Zunyi Medical University
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Priority to CN201611028437.1A priority Critical patent/CN106491430A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Botany (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof, comprising Flos Lonicerae, Flos Chrysanthemi, green tea, Herba Menthae, Sorbitol, silicon dioxide, carrageenan, xanthan gum, sodium lauryl sulphate, sodium sulfite, vitamin C, xylitol, water solublity food coloring and sodium benzoate.Flos Lonicerae compound recipe herbaceous toothpaste of the present invention carries out water extraction with Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae as raw material, and method is simple, it is easy to implement, with low cost.The fresh Aqueous extracts of gained are directly used as solvent, do not need the processes such as concentrate drying, loss that is not only cost-effective but also being prevented effectively from effective ingredient.Preparation method has novelty, the effects such as obtained toothpaste has resolving heat and reducing pathogenic fire, anti-inflammation detumescence, pre- anti-caries, fresh breath.

Description

A kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof
Technical field
The present invention relates to toothpaste, specially a kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof.
Background technology
Toothpaste is indispensable dental care products in people's daily life, and its product category is various, is mainly used in protecting Oral cavity and cleaning of teeth is held, is promoted breath freshening, is nursed gingiva, safeguards oral cavity good environment etc..In recent years, with toothpaste safety Problem increasingly serious, consumer healthcare's consciousness constantly strengthens, and people start to pursue pure natural, harmless raw material of toothpaste.In order to Adapt to consumer demand, the various functions tooth paste product for releasing one after another both at home and abroad has become the market mainstream, and due to Chinese medicine Active components of plants comes from natural, safe and effective, people can be allowed to feel more to trust, milder, hence with active ingredient of Chinese herbs Feature exploitation herbaceous toothpaste has become the emphasis of current field of toothpaste development.
Chinese medicinal plant wide material sources, effect are numerous, not only economic but also practicability and effectiveness.Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae It is the higher several compositions of frequency used in Chinese toothpaste, substantially all with heat-clearing and toxic substances removing, anti-inflammation detumescence, pre- anti-caries, pure and fresh mouth The effects such as gas and well-known, its effect is quite suitable for the series of products of gingiva care.And consumer is to this kind of effect demand Very big, these are made fine work toothpaste, it is believed that large quantities of high-level consumers for having natural environmental-protective thought can be attracted.By in technology It is bold in innovation with technology field, updates Flos Lonicerae compound recipe herbaceous toothpaste prescription, improve the performance evaluation to which, Flos Lonicerae is multiple Square herbaceous toothpaste will be by more consumer's recognitions and acceptances, so as to increase the demand in market.
Content of the invention
It is an object of the invention to provide a kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof.
For reaching above-mentioned purpose, the technical scheme that adopts for:
A kind of Flos Lonicerae compound recipe herbaceous toothpaste, comprising components by weight be:70% sorbitol solution A 10-40 parts, 70% Pyrusussuriensiss Alcoholic solution B 30-70 parts, silica 1 0-25 parts, carrageenan 0.2-0.6 parts, xanthan gum 0.3-0.8 parts, lauryl sulphate acid Sodium 1-3 parts, sodium sulfite 0.2-0.5 parts, vitamin C 0.5-1 parts, xylitol 0.1-0.4 parts, water solublity food coloring 0.01- 0.03 part and sodium benzoate 0.1-0.3 parts, the 70% sorbitol solution A are prepared for pure water, and the 70% sorbitol solution B is plant Thing Aqueous extracts are prepared, and the plant Aqueous extracts are by Flos Lonicerae 33.4%, Flos Chrysanthemi 22.2%, green tea 22.2%, Herba Menthae 22.2% and appropriate Water is prepared.
As the present invention preferred version described in Flos Lonicerae compound recipe herbaceous toothpaste, comprising components by weight further For:70% 25 parts of sorbitol solution A, 50 parts of 70% sorbitol solution B, 20 parts of silicon dioxide, 0.22 part of carrageenan, xanthan gum 0.5 part, 1 part of sodium lauryl sulphate, 0.5 part of sodium sulfite, 1 part of vitamin C, 0.3 part of xylitol, water solublity food coloring 0.01 part and 0.3 part of sodium benzoate.
The preparation method of above-mentioned Flos Lonicerae compound recipe herbaceous toothpaste, its step is:
1), weigh dry product Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae in proportion, add water 1000mL by three's weight and per 90g, adds The vitamin C of half, simmers 1h with small fire after boiling, soaks 2h again after truce, leaches soak, plus appropriate activated carbon, while hot Solution is taken after sucking filtration and adds remaining half vitamin C, add sodium sulfite, stir, obtain plant Aqueous extracts;
2), prepare the sorbitol solution B of 70% sorbitol solution A and 70% with pure water and above-mentioned plant Aqueous extracts respectively;
3), weigh carrageenan and xanthan gum is scattered in 70% sorbitol solution A in proportion, mix, high-speed stirred makes plastic Shape, adds 70% sorbitol solution B mixings;
4), in step 3)Silicon dioxide and sodium lauryl sulphate are added in the mixed solution of gained, in 0.096MPa vacuum bars High-speed stirred 15 ~ 20 minutes under part;
5), be eventually adding pigment, xylitol and sodium benzoate, high-speed stirred 15 minutes, fill under 0.096MPa vacuum conditions ?.
The present invention has advantages below:1st, raw material Flos Lonicerae, Flos Chrysanthemi, green tea selected by Flos Lonicerae compound recipe herbaceous toothpaste of the present invention Belong to medicinal and edible plant with Herba Menthae, wide material sources, cheap, safety is good, and its effective ingredient has resolving heat and reducing pathogenic fire, antiinflammatory The effects such as detumescence, pre- anti-caries, fresh breath.2nd, preparation method of the present invention is unique, and obtained toothpaste is light yellow, transparent exquisiteness Glossy, with the refrigerant fragrance that plant material itself has, without the need in addition adding essence.3rd, through trying brush experimental verification, this Invention product foaming abundancy, it is easy to remove, nonirritant to oral cavity, brush breath freshening.4th, the inventive method is simply unique, system Standby cost is relatively low, and composition is safe and reliable.
Specific embodiment
The present invention is further described with reference to embodiment, but the present invention is not limited only to following embodiments, it is anticipated that this In the case where prior art is combined, performance may produce many variations to art personnel.
The Flos Lonicerae compound recipe herbaceous toothpaste of the present invention, is made up of the component of following weight percentage ratio:70% sorbitol solution (Pure water is prepared, wetting agent)10-40%;70% sorbitol solution(Plant Aqueous extracts are prepared, wetting agent)30-70%;Silicon dioxide (Abrasivuss)10-25%;Carrageenan(Thickening agent)0.2-0.6%;Xanthan gum(Thickening agent)0.3-0.8%;Sodium lauryl sulphate (Foaming agent)1-3%;Sodium sulfite(Antioxidant)0.2-0.5%;Vitamin C(Antioxidant)0.5-1.0%;Xylitol(Sweet taste Agent)0.1-0.4%;Water solublity food coloring(Coloring agent)0.01-0.03%;Sodium benzoate(Preservative)0.1-0.3%.
Preferred version each component weight ratio is further:70% sorbitol solution A 25%, 70% sorbitol solution B 50%, two Silicon oxide 20%, carrageenan 0.22%, xanthan gum 0.5%, sodium lauryl sulphate 1%, sodium sulfite 0.5%, vitamin C 1%, wood Sugar alcohol 0.3%, water solublity food coloring 0.01% and sodium benzoate 0.3%.
The preparation method of above-mentioned Flos Lonicerae compound recipe herbaceous toothpaste, comprises the following steps:
1), weigh dry product Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae in proportion, add water 1000mL by three's weight and per 90g, adds The vitamin C of half, simmers 1h with small fire after boiling, soaks 2h again after truce, leaches soak, plus appropriate activated carbon, while hot Solution is taken after sucking filtration and adds remaining half vitamin C, add sodium sulfite, stir, obtain plant Aqueous extracts;
2), prepare the sorbitol solution B of 70% sorbitol solution A and 70% with pure water and above-mentioned plant Aqueous extracts respectively;
3), weigh carrageenan and xanthan gum is scattered in 70% sorbitol solution A in proportion, mix, high-speed stirred makes plastic Shape, adds 70% sorbitol solution B mixings;
4), in step 3)Silicon dioxide and sodium lauryl sulphate are added in the mixed solution of gained, in 0.096MPa vacuum bars High-speed stirred 15 ~ 20 minutes under part;
5), be eventually adding pigment, xylitol and sodium benzoate, high-speed stirred 15 minutes, fill under 0.096MPa vacuum conditions ?.
Flos Lonicerae compound recipe herbaceous toothpaste of the present invention carries out water extraction, method letter with Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae as raw material Single, it is easy to implement, with low cost.The fresh Aqueous extracts of gained are directly used as solvent, do not need the processes such as concentrate drying, both cost-effective The loss of effective ingredient can be prevented effectively from again.Preparation method has novelty, and there is obtained toothpaste resolving heat and reducing pathogenic fire, antiinflammatory to disappear The effects such as swollen, pre- anti-caries, fresh breath.

Claims (3)

1. a kind of Flos Lonicerae compound recipe herbaceous toothpaste, comprising components by weight be characterised by:70% sorbitol solution A 10-40 parts, 70% sorbitol solution B 30-70 parts, silica 1 0-25 parts, carrageenan 0.2-0.6 parts, xanthan gum 0.3-0.8 parts, dodecane Base sodium sulfate 1-3 parts, sodium sulfite 0.2-0.5 parts, vitamin C 0.5-1 parts, xylitol 0.1-0.4 parts, the edible color of water solublity Plain 0.01-0.03 parts and sodium benzoate 0.1-0.3 parts, the 70% sorbitol solution A are prepared for pure water, and 70% Sorbitol is molten Liquid B is prepared for plant Aqueous extracts, and the plant Aqueous extracts are by Flos Lonicerae 33.4%, Flos Chrysanthemi 22.2%, green tea 22.2%, Herba Menthae 22.2% Prepare with suitable quantity of water.
2. Flos Lonicerae compound recipe herbaceous toothpaste according to claim 1, comprising components by weight be characterised by:70% Pyrusussuriensiss 25 parts of alcoholic solution A, 50 parts of 70% sorbitol solution B, 20 parts of silicon dioxide, 0.22 part of carrageenan, 0.5 part of xanthan gum, dodecane 1 part of base sodium sulfate, 0.5 part of sodium sulfite, 1 part of vitamin C, 0.3 part of xylitol, 0.01 part of water solublity food coloring and benzene first 0.3 part of sour sodium.
3. the preparation method of Flos Lonicerae compound recipe herbaceous toothpaste according to claim 1 and 2, its steps characteristic are:
1), weigh dry product Flos Lonicerae, Flos Chrysanthemi, green tea and Herba Menthae in proportion, add water 1000mL by three's weight and per 90g, then plus Enter the vitamin C of half, 1h is simmered with small fire after boiling, soak 2h again after truce, leach soak, plus appropriate activated carbon, take advantage of Solution is taken after hot sucking filtration and adds remaining half vitamin C, add sodium sulfite, stir, obtain plant Aqueous extracts;
2), prepare the sorbitol solution B of 70% sorbitol solution A and 70% with pure water and above-mentioned plant Aqueous extracts respectively;
3), weigh carrageenan and xanthan gum is scattered in 70% sorbitol solution A in proportion, mix, high-speed stirred makes plastic Shape, adds 70% sorbitol solution B mixings;
4), in step 3)Silicon dioxide and sodium lauryl sulphate are added in the mixed solution of gained, in 0.096MPa vacuum bars High-speed stirred 15 ~ 20 minutes under part;
5), be eventually adding pigment, xylitol and sodium benzoate, high-speed stirred 15 minutes, fill under 0.096MPa vacuum conditions ?.
CN201611028437.1A 2016-11-22 2016-11-22 A kind of Flos Lonicerae compound recipe herbaceous toothpaste and preparation method thereof Pending CN106491430A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111110602A (en) * 2020-01-19 2020-05-08 广东立爽生物科技有限公司 Anti-inflammatory analgesic toothpaste and preparation method thereof
CN111991289A (en) * 2020-08-26 2020-11-27 广东工业大学 Antibacterial and anti-inflammatory formula and antibacterial and anti-inflammatory toothpaste
CN113057922A (en) * 2021-04-08 2021-07-02 许耿防 Toothpaste capable of efficiently removing tooth stains, whitening teeth, and refreshing breath and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104586708A (en) * 2013-10-31 2015-05-06 孙铭 Caries prevention toothpaste
CN104887555A (en) * 2015-05-06 2015-09-09 绥阳县吉帮金银花科技发展有限公司 Honeysuckle flower toothpaste and preparation method thereof
CN105434309A (en) * 2015-12-24 2016-03-30 青岛克立克信息技术有限公司 Toothpaste with functions of clearing fire and preventing halitosis
CN105534828A (en) * 2016-03-01 2016-05-04 程艳青 Toothpaste with efficacy of hemostasis, detoxification, care and refreshing and preparation method of toothpaste

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104586708A (en) * 2013-10-31 2015-05-06 孙铭 Caries prevention toothpaste
CN104887555A (en) * 2015-05-06 2015-09-09 绥阳县吉帮金银花科技发展有限公司 Honeysuckle flower toothpaste and preparation method thereof
CN105434309A (en) * 2015-12-24 2016-03-30 青岛克立克信息技术有限公司 Toothpaste with functions of clearing fire and preventing halitosis
CN105534828A (en) * 2016-03-01 2016-05-04 程艳青 Toothpaste with efficacy of hemostasis, detoxification, care and refreshing and preparation method of toothpaste

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Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111110602A (en) * 2020-01-19 2020-05-08 广东立爽生物科技有限公司 Anti-inflammatory analgesic toothpaste and preparation method thereof
CN111991289A (en) * 2020-08-26 2020-11-27 广东工业大学 Antibacterial and anti-inflammatory formula and antibacterial and anti-inflammatory toothpaste
CN113057922A (en) * 2021-04-08 2021-07-02 许耿防 Toothpaste capable of efficiently removing tooth stains, whitening teeth, and refreshing breath and preparation method thereof

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