CN107446699A - A kind of jasmine green tea honeysuckle extract essence and preparation method and toothpaste and preparation method containing the essence - Google Patents
A kind of jasmine green tea honeysuckle extract essence and preparation method and toothpaste and preparation method containing the essence Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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Abstract
The present invention relates to dental care products, concretely relate to a kind of jasmine green tea honeysuckle extract essence essence and preparation method thereof, and the preparation method that essence is applied in toothpaste.The preparation method of jasmine green tea honeysuckle extract essence is soaked under condition of negative pressure to weigh jasmine, green tea, honeysuckle and pure water mixing, homogeneous, reheats decoction filtering and obtain filtrate and filter residue；Filtrate is decolourized, and is concentrated to give jasmine green tea honeysuckle extract；Stood after menthol, peppermint oil dementholized, fennel oil, propane diols, spearmint oil and jasmine green tea honeysuckle extract are stirred.Jasmine green tea honeysuckle extract essence prepared by the present invention, fragrance alcohol just, pure and fresh salubrious, and preventable disease.The toothpaste containing jasmine green tea honeysuckle extract essence prepared, the effect such as toothache caused by clearing heat and detoxicating, mitigation excessive internal heat can be played, is had no side effect.
Description
Technical field
The present invention relates to oral cleaning nursing article, concretely relates to a kind of jasmine green tea honeysuckle extract essence
And preparation method and toothpaste and preparation method containing the essence.
Background technology
Toothpaste is to be used to clean tooth together with toothbrush, protection oral hygiene, carries out daily nursing, comparatively safe to human body
A kind of daily necessities, have very long history.With the development of the society, toothpaste industry also grows with each passing hour, all kinds
Toothpaste come out one after another, common, common, conventional natural extract is applied in toothpaste and solves the problems, such as related oral,
Turn into market mainstream focus, one of important topic of toothpaste industry will be turned into.
Jasmine, alias Jasmine, Latin literary fame Jasminum sambac (L.) Ait, it is Oleaceae gelsemium evergreen shrubs
Or the general designation of liana.Jasmine is the national flower of Philippine, Tunisia, Indonesia, and in November, 2006, Jiangsu Province determined Jasmine
Spent to save.The plantation of China Jasmine at present is concentrated mainly on Hengxian County, produces more than 80,000 tons of fresh flower, Heng County Jasmine yield per year
Account for the 60% of Gross World Product.Jasmine, leaf and root are all pharmaceutically acceptable, typically uproot after autumn, and cutting into slices, it is standby to dry, and summer and autumn are picked flowers,
Dry standby.Arabian jasmine root, bitter, temperature is poisonous, anaesthetizes, analgesic, for falling damage muscles and bones, carious tooth, has a headache, insomnia.Jasmine, pungent,
It is sweet, warm, qi-regulating, open it is strongly fragrant, ward off it is dirty, and in, for diarrhea suffer from abdominal pain, red eyes swollen, sore.
Green tea is one of main teas of China, takes the young leaves or bud of tea tree, not fermented, through fixing, shaping, drying
It is made etc. technique.Green tea is not fermented manufactured tea, remains the natural materials of fresh leaf, contains more Tea Polyphenols, catechu
Element, chlorophyll, caffeine, amino acid, vitamin etc., there is special-effect to anti-aging, anti-cancer, anticancer, sterilization, anti-inflammatory etc.,
It is less than other teas.The scope of domestic product green tea is extremely wide, Zhejiang, Henan, Anhui, Jiangxi, Jiangsu, Sichuan,
Hunan, Hubei, Guangxi, Fujian, Guizhou, the green tea main product province that Hanzhong Shandong is China.
Honeysuckle also known as honeysuckle, scientific name Lonicera japonica, " honeysuckle " one are come from《Compendium of Materia Medica》, due to
Honeysuckle flowers are just opened as white, after switch to yellow, hence obtain one's name honeysuckle.Medicinal material honeysuckle be Caprifoliaceae woodbine honeysuckle and
Congener dry flower or with the flower just opened.Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times, first recorded in《Mingyi Bielu》,
Top grade is classified as, it is cold in nature, it is sweet, enter lung, the heart, stomach, there is the effect of clearing heat and detoxicating, anti-inflammatory, qi-restoratives treat wind, cure mainly under turgor
The diseases such as disease, warm disease heating, heat toxin large carbuncle and tumour.For dizziness, thirst, sweating and boring, enteritis, bacillary dysentery, measles,
It is pneumonia, encephalitis, epidemic meningitis, acute mastitis, septicemia, appendicitis, skin infection, ulcer boils, erysipelas, parotitis, suppurative
The illnesss such as tonsillitis have certain curative effect.
The content of the invention
An object of the present invention be to provide a kind of fragrance alcohol just, medicine source it is abundant, safe and reliable, and mouth disease can be prevented
Jasmine green tea honeysuckle extract essence and preparation method thereof.
In order to realize the purpose, the technical solution adopted in the present invention is：
A kind of jasmine green tea honeysuckle extract essence, include the raw material of following parts by weight：
11~26 parts of menthol, 11~16 parts of peppermint oil dementholized, 1.1~1.7 parts of fennel oil, 5~10 parts of propane diols, spearmint
Oily 2.1~2.6 parts, 10~25 parts of jasmine green tea honeysuckle extract；
Described jasmine green tea honeysuckle extract by following weight than raw material be prepared：Jasmine：Green tea：Gold and silver
Flower：Pure water=1.3~1.9：1.3~1.9：1.3~1.9：5.1~9.9.
A kind of preparation method of jasmine green tea honeysuckle extract essence, comprises the following steps：
1., to weigh be jasmine by weight proportion：Green tea：Honeysuckle：Pure water=1.3~1.9：1.3~1.9：1.3~
1.9：5.1~9.9 raw material；
2., by jasmine, green tea, honeysuckle, pure water mix, soak 6~36h；
3., said mixture moved in vacuum viscolizer, vacuum be -0.05~-0.07MPa and temperature be 55~
1~3h of homogeneous under conditions of 80 DEG C, filters to get filtrate and filter residue；
4., with activated carbon filtrate is decolourized, the filtrate after decolouring is concentrated to give jasmine green tea honeysuckle extract；
5., measure according to parts by weight, by 11~26 parts of menthol, 11~16 parts of peppermint oil dementholized, 1.1~1.7 parts of fennel oil, third
10~25 parts of 5~10 parts of glycol, 2.1~2.6 parts of spearmint oil and jasmine green tea honeysuckle extract stir, and standing 12~
36h, produce jasmine green tea honeysuckle extract essence.
Preferably, 4. middle filtrate is 20~50 by volume to step:1 is concentrated, and thickening temperature is 55~80 DEG C.
Another object of the present invention is to provide a good drug efficacy, have no side effect, securely and reliably, heat-clearing solution can be played
Poison, the effect of easing toothache etc., particular for toothpaste of the toothache with good remission effect caused by excessive internal heat.
In order to realize the purpose, the technical solution adopted in the present invention is：
A kind of toothpaste of the extract of green tea honeysuckle containing jasmine essence, described toothpaste contain mass percent for 1.0~
2.0% jasmine green tea honeysuckle extract essence.
Preferably, the toothpaste also comprises the following components：
Above percentage is mass percent.
A kind of preparation method of the toothpaste of the extract of green tea honeysuckle containing jasmine essence, comprises the following steps：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1；
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2；
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, heated, form mixing
Thing D3；
D, sorbierite is well mixed with mixture D 2, heated, form mixture D 4；
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
Sky 5~10min of lower stirring, is made lotion, is filled into simultaneously sealing in multiple tube.
Preferably, heating-up temperature is 30~60 DEG C in step c, and the heat time is 3~8min.
Preferably, heating-up temperature is 30~65 DEG C in step d, and the heat time is 3~8min.
The beneficial effects of the present invention are：
1st, the jasmine green tea honeysuckle extract essence prepared, fragrance alcohol just, securely and reliably, and can prevent mouth disease.
2nd, prepare the toothpaste containing jasmine green tea honeysuckle extract essence, can play it is clearing heat and detoxicating, ease toothache
Deng effect, there is good remission effect particular for toothache caused by excessive internal heat.Because main component is natural extract, there is day
The functions such as right clearing heat and detoxicating, the caused toothache of mitigation excessive internal heat, have no side effect, long-term use of useful and harmless.
3rd, the manufacture craft of toothpaste is simple, is adapted to industrialized production.
Embodiment
The present invention is further illustrated with reference to embodiments, it is necessary to which explanation, various raw materials are commercially available food
Grade, or be prepared according to prior art, jasmine, green tea, gold and silver Huadu be medicine source abundance source, reliable.
Embodiment 1
1st, the preparation of jasmine green tea honeysuckle extract essence
1., to weigh jasmine 130g (each half of arabian jasmine root, Jasmine, dry root, dried flower are same as below), green tea 130g (dry
Flower, similarly hereinafter), honeysuckle 130g (dried flower, similarly hereinafter) and pure water 510g are mixed, immersion 6h.
2., homogenizer homogeneous 3h is used under conditions of vacuum is -0.05MPa and homogeneous built-in temperature is 80 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), 80 DEG C of constant temperature are concentrated into 18g jasmine green tea
Honegsukle flower P.E.
4., weigh added in 10g jasmine green tea honeysuckle extracts menthol 11g, peppermint oil dementholized 11g, fennel oil 1.1g,
Propane diols 5g, spearmint oil 2.1g, stir, and stand 12h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 60 DEG C of heating 3min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,65 DEG C of heating 3min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 5min of sky, is made lotion, is filled into multiple tube and sealing.
Embodiment 2
1st, the preparation of jasmine green tea honeysuckle extract essence
1., weigh jasmine 140g, green tea 140g, honeysuckle 140g and pure water 520g mixing, soak 12h.
2., homogenizer homogeneous 2h is used under conditions of vacuum is -0.06MPa and homogeneous built-in temperature is 70 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), it is green that 70 DEG C of constant temperature are concentrated into 23.5g jasmines
Tea Honegsukle flower P.E.
4., weigh added in 20g jasmine green tea honeysuckle extracts menthol 12g, peppermint oil dementholized 12g, fennel oil 1.2g,
Propane diols 6g, spearmint oil 2.2g, stir, and stand 24h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 50 DEG C of heating 4min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,55 DEG C of heating 4min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 6min of sky, is made lotion, is filled into multiple tube and sealing.
Embodiment 3
1st, the preparation of jasmine green tea honeysuckle extract essence
1., weigh jasmine 150g, green tea 150g, honeysuckle 150g and pure water 530g mixing, soak 24h.
2., homogenizer homogeneous 1h is used under conditions of vacuum is -0.07MPa and homogeneous built-in temperature is 60 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), it is green that 60 DEG C of constant temperature are concentrated into 32.7g jasmines
Tea Honegsukle flower P.E.
4., weigh added in 21g jasmine green tea honeysuckle extracts menthol 13g, peppermint oil dementholized 13g, fennel oil 1.3g,
Propane diols 7g, spearmint oil 2.3g, stir, and stand 36h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 40 DEG C of heating 5min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,45 DEG C of heating 5min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 7min of sky, is made lotion, is filled into multiple tube and sealing.
Embodiment 4
1st, the preparation of jasmine green tea honeysuckle extract essence
1., weigh jasmine 160g, green tea 160g, honeysuckle 160g and pure water 540g mixing, soak 36h.
2., homogenizer homogeneous 3h is used under conditions of vacuum is -0.07MPa and homogeneous built-in temperature is 55 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), 55 DEG C of constant temperature are concentrated into 51g jasmine green tea
Honegsukle flower P.E.
4., weigh added in 22g jasmine green tea honeysuckle extracts menthol 14g, peppermint oil dementholized 14g, fennel oil 1.4g,
Propane diols 8g, spearmint oil 2.4g, stir, and stand 12h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 35 DEG C of heating 6min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,40 DEG C of heating 6min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 8min of sky, is made lotion, is filled into multiple tube and sealing.
Embodiment 5
1st, the preparation of jasmine green tea honeysuckle extract essence
1., weigh jasmine 170g, green tea 170g, honeysuckle 170g and pure water 550g mixing, soak 12h.
2., homogenizer homogeneous 2h is used under conditions of vacuum is -0.06MPa and homogeneous built-in temperature is 60 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), it is green that 60 DEG C of constant temperature are concentrated into 42.4g jasmines
Tea Honegsukle flower P.E.
4., weigh added in 23g jasmine green tea honeysuckle extracts menthol 15g, peppermint oil dementholized 15g, fennel oil 1.5g,
Propane diols 9g, spearmint oil 2.5g, stir, and stand 24h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 30 DEG C of heating 7min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,30 DEG C of heating 7min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 9min of sky, is made lotion, is filled into multiple tube and sealing.
Embodiment 6
1st, the preparation of jasmine green tea honeysuckle extract essence
1., weigh jasmine 190g, green tea 190g, honeysuckle 190g and pure water 990g mixing, soak 36h.
2., homogenizer homogeneous 1h is used under conditions of vacuum is -0.07MPa and homogeneous built-in temperature is 80 DEG C, filter
Obtain filtrate and filter residue.
3., filtrate decolourized with activated carbon (percentage by weight be not higher than 5%), it is green that 80 DEG C of constant temperature are concentrated into 44.6g jasmines
Tea Honegsukle flower P.E.
4., weigh added in 25g jasmine green tea honeysuckle extracts menthol 26g, peppermint oil dementholized 16g, fennel oil 1.7g,
Propane diols 10g, spearmint oil 2.6g, stir, and stand 36h, produce jasmine green tea honeysuckle extract essence.
2nd, the preparation of the toothpaste of the extract of green tea honeysuckle containing jasmine essence
Composition and ratio such as following table (in terms of 100g, similarly hereinafter)
Preparation process is：
A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, sodium cellulose glycolate is scattered in silica, forms mixture D 2.
C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, 30 DEG C of heating 8min,
Form mixture D 3.
D, sorbierite is well mixed with mixture D 2,30 DEG C of heating 8min, forms mixture D 4.
E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, very
The lower stirring 10min of sky, is made lotion, is filled into multiple tube and sealing.
Comparative example 1
With differing only in for embodiment 1, jasmine green tea honeysuckle extract essence is not added when preparing toothpaste, other groups
Divide and content is (being supplied less than 100g with pure water) same as Example 1.
Clinical trial result
Test method：Choose because excessive internal heat causes the toothache people of subject 100 to be tested, each half of men and women, the age from 20~
50 years old, average age 40 years old.2 groups are randomly divided into, the toothpaste that experimental group is prepared using embodiment 1 (is added with jasmine green tea gold and silver
Flower extract essence), the toothpaste that control group is prepared using comparative example 1 (is not added with jasmine green tea honeysuckle extract perfume
Essence), every morning, noon, respectively brush teeth once at night.
Brush teeth before experiment, first unify to examine and record the toothache symptom of subject.
Brush teeth after testing fortnight, then the unified toothache symptom change for examining subject.
Criterion：Brush teeth after experiment, it is effective that subject's toothache, which is effectively alleviated or eliminated, conversely, unchanged or tooth
It is invalid that pain plus severe one are accordingly to be regarded as.
Examined after subject is using fortnight, it is as a result as follows：
In terms of the assay of subject, the toothpaste of the invention containing jasmine green tea honeysuckle extract essence, for
The effective percentage for the symptom that eases toothache is 86%, is significantly better than that the statistics of control group.Therefore, it is of the invention to contain jasmine
The toothpaste of green tea honeysuckle extract essence, there is preferably prevention and treatment effect for the toothache caused by excessive internal heat.
Above content is only to present inventive concept example and explanation, affiliated those skilled in the art couple
Described specific embodiment is made various modifications or supplement or substituted using similar mode, without departing from invention
Conceive or surmount scope defined in the claims, protection scope of the present invention all should be belonged to.
Claims (8)
- A kind of 1. jasmine green tea honeysuckle extract essence, it is characterised in that：Include the raw material of following parts by weight：11~26 parts of menthol, 11~16 parts of peppermint oil dementholized, 1.1~1.7 parts of fennel oil, 5~10 parts of propane diols, spearmint oil 2.1~2.6 parts, 10~25 parts of jasmine green tea honeysuckle extract；Described jasmine green tea honeysuckle extract by following weight than raw material be prepared：Jasmine：Green tea：Honeysuckle：It is pure Water purification=1.3~1.9：1.3~1.9：1.3~1.9：5.1~9.9.
- A kind of 2. preparation method of jasmine green tea honeysuckle extract essence, it is characterised in that：Comprise the following steps：1., to weigh be jasmine by weight proportion：Green tea：Honeysuckle：Pure water=1.3~1.9：1.3~1.9：1.3~1.9： 5.1~9.9 raw material；2., by jasmine, green tea, honeysuckle, pure water mix, soak 6~36h；3., said mixture moved in vacuum viscolizer, in vacuum be -0.05~-0.07MPa and temperature is 55~80 DEG C Under conditions of 1~3h of homogeneous, filter to get filtrate and filter residue；4., with activated carbon filtrate is decolourized, the filtrate after decolouring is concentrated to give jasmine green tea honeysuckle extract；5., measure according to parts by weight, by 11~26 parts of menthol, 11~16 parts of peppermint oil dementholized, 1.1~1.7 parts of fennel oil, propane diols 10~25 parts of 5~10 parts, 2.1~2.6 parts of spearmint oil and jasmine green tea honeysuckle extract stir, and stand 12~36h, Produce jasmine green tea honeysuckle extract essence.
- 3. the preparation method of jasmine green tea honeysuckle extract essence according to claim 2, it is characterised in that：Step is 4. Middle filtrate is 20~50 by volume:1 is concentrated, and thickening temperature is 55~80 DEG C.
- A kind of 4. toothpaste of the extract of green tea honeysuckle containing jasmine essence, it is characterised in that：Described toothpaste contains quality percentage Number is 1.0~2.0% jasmine green tea honeysuckle extract essence.
- 5. the toothpaste of the extract of green tea honeysuckle containing jasmine essence according to claim 4, it is characterised in that：The toothpaste is also Including following component：Above percentage is mass percent.
- 6. the preparation method of the toothpaste of the extract of green tea honeysuckle containing jasmine essence according to claim 5, its feature exist In：Comprise the following steps：A, laruyl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1；B, sodium cellulose glycolate is scattered in silica, forms mixture D 2；C, tertiary sodium phosphate, saccharin sodium, titanium dioxide, sodium monofluorophosphate and mixture D 1 are well mixed, heated, form mixture D3；D, sorbierite is well mixed with mixture D 2, heated, form mixture D 4；E, mixture D 3, D4 are added in emulsification pot, adds jasmine green tea honeysuckle extract essence and be well mixed, under vacuum 5~10min is stirred, lotion is made, is filled into simultaneously sealing in multiple tube.
- 7. the preparation method of the toothpaste of the extract of green tea honeysuckle containing jasmine essence according to claim 6, its feature exist In：Heating-up temperature is 30~60 DEG C in step c, and the heat time is 3~8min.
- 8. the preparation method of the toothpaste of the extract of green tea honeysuckle containing jasmine essence according to claim 6, its feature exist In：Heating-up temperature is 30~65 DEG C in step d, and the heat time is 3~8min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710792304.XA CN107446699A (en) | 2017-09-05 | 2017-09-05 | A kind of jasmine green tea honeysuckle extract essence and preparation method and toothpaste and preparation method containing the essence |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109609267A (en) * | 2019-01-10 | 2019-04-12 | 德利宝(广州)香料有限公司 | A kind of preparation method of Artemisinin essence and dentifrice composition containing the essence |
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| CN103451017A (en) * | 2013-08-16 | 2013-12-18 | 德利宝(广州)香料有限公司 | Preparation methods of essence and toothpaste containing natural green tea extract |
| CN104940060A (en) * | 2015-06-08 | 2015-09-30 | 德利宝(广州)香料有限公司 | Toothpaste containing jasmine compounded green tea extract essence and preparation method of toothpaste |
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| CN109609267A (en) * | 2019-01-10 | 2019-04-12 | 德利宝(广州)香料有限公司 | A kind of preparation method of Artemisinin essence and dentifrice composition containing the essence |
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Application publication date: 20171208 |