CN111956568A - Shaving water with hair growing and hair loss preventing functions and preparation method thereof - Google Patents

Shaving water with hair growing and hair loss preventing functions and preparation method thereof Download PDF

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CN111956568A
CN111956568A CN202010647433.1A CN202010647433A CN111956568A CN 111956568 A CN111956568 A CN 111956568A CN 202010647433 A CN202010647433 A CN 202010647433A CN 111956568 A CN111956568 A CN 111956568A
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hair
shaving
water
hair growth
stock solution
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马鹏常
卢卓
黄小玲
赵文华
杨荟君
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Zhongshan Polytechnic
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract

The invention discloses shaving water with hair growth and hair loss prevention functions, which comprises the following components in parts by weight: 50-80 parts of shaving water stock solution, 20-50 parts of hair-growing and hair-loss-preventing plant essence, 0.5-1 part of plant preservative stock solution and 200-300 parts of purified water. The invention also provides a preparation method of the shaving water with the functions of growing hair and preventing alopecia. The shaving water prepared by the invention is green, safe, pure natural, high in activity, not going bad for a long time, obvious in hair growth and hair loss prevention effect and has hair care and shaping effects.

Description

Shaving water with hair growing and hair loss preventing functions and preparation method thereof
Technical Field
The invention relates to the technical field of daily chemical articles, in particular to shaving water with hair growing and hair loss preventing functions and a preparation method thereof.
Background
The hair plays an important role in the decoration of human instruments, the hair is concerned with the image and the quality of a person, the hair is a basic condition for obtaining the natural beauty of the instrument, meanwhile, the hair quality is also an important index for measuring the health of a human body, and the hair length is more or less concerned with the good and bad physiological functions of the person. Therefore, studies on hair loss, hair growth, hair care, and hair care have been favored in the pharmaceutical industry and the cosmetics industry. Alopecia is puzzling the lives of modern urban people and even vast rural friends. According to the statistics of the world health organization, the number of Chinese alopecia people is up to 2 hundred million, while male is about 1.3 hundred million, female is about 0.7 hundred million, and the alopecia symptom exists among 7 Chinese people on average. With the increase of working pressure, psychological pressure rises, environmental pollution aggravates and other factors, the number of alopecia people is increased at a high speed by 17.8%, and the alopecia people show a trend more and more.
For hair care, people in China often use shampoo in daily life, but the shampoo seen in daily life is mostly prepared from petrochemical products as main raw materials, most of the components of the shampoo are not harmful to human bodies but not green and healthy after being blended with water, such as mixed salt of triethanolamine of fatty sulfate alcohol and ammonium hydroxide, lauric acid isopropanolamide, formaldehyde, polyoxyethylene, lanolin, spice, pigment and the like, and the shampoo has influence on the hair of people after being used for a long time, such as poor hair quality, dependence, anaphylactic reaction of serious people and the like. Reviewing thousand years of traditional hair nourishing and protecting traditions in China, people can draw essence from the traditional hair nourishing and protecting traditions, for example, shaving water is a thousand years popular fine hair dressing and shaping product, and ancient people mostly use the comb to close hair and maintain hair. Different from the current scientific and technological development, the Chinese tradition focuses on conditioning and recuperation, the shaving water lasts for thousands of years, and the hair nourishing and caring value is further excavated and developed.
In the prior art, chinese patent application CN201811504828.5, published 2019-04-19 has disclosed a method for preparing pure natural plant shaving water, which is also a pure natural zero-burden shaving water hair styling product, but the product has a single function, has no obvious effect on hair loss and hair growth conditioning, has a high viscosity, is not easy to be absorbed by the scalp and hair, and more importantly, for hair loss (bald) users, it is more desirable to condition the scalp, hair follicles and hair roots to a healthy state. At present, some hair-nourishing and hair-growing products are often added with western medicine chemical components with hair conditioning effects, such as Minod1, which have side effects of skin irritation and the like, and also can cause drug dependence on users, and the products can not shape and protect hair.
Therefore, the pure natural healthy shaving water which can protect and shape hair and prevent hair loss and grow hair is researched and developed, has important practical significance for satisfying people's direction of good life, and has wide application prospect.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the shaving water with the functions of growing hair and preventing alopecia, the shaving water is green, safe, pure natural, high in activity, not going bad for a long time, obvious in hair growing and preventing alopecia effect, capable of achieving the hair care and shaping effects, wide in raw material source range, low in cost and suitable for large-scale production.
The invention is realized by the following technical scheme:
a shaving water with hair growth and hair loss prevention functions is characterized by comprising the following components in parts by weight:
Figure BDA0002573665580000031
the shaving water with the functions of growing hair and preventing hair loss is characterized in that the stock solution of the shaving water is an extract of elm shaving pieces.
The shaving water with the functions of growing hair and preventing hair loss is characterized in that the plant essence for growing hair and preventing hair loss is one or more natural Chinese herbal medicine extracts.
The shaving water with the functions of growing hair and preventing hair loss is characterized in that the natural Chinese herbal medicines comprise one or more of perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, medlar, coix seed and poria cocos.
The shaving water with the functions of growing hair and preventing hair loss is characterized in that the plant preservative stock solution is one or more preservative pure natural plant extracts.
The shaving water with the functions of growing hair and preventing hair loss is characterized in that the antiseptic pure natural plant comprises one or more of bamboo leaves, ginkgo leaves, magnolia officinalis, liquorice, clove, aloe and geranium.
In addition, the invention also provides a preparation method of the shaving water with the functions of growing hair and preventing hair loss, which is characterized by comprising the following steps:
A. preparing a shaving water stock solution: slicing the sliced flos Lonicerae, granulating, performing supercritical extraction, and purifying;
B. preparing a hair-growing and anti-hair-loss plant essence: cleaning one or more natural Chinese medicinal materials, pulverizing, extracting, filtering, and purifying;
C. preparing a plant preservative stock solution: cleaning one or more antiseptic pure natural plants, pulverizing, extracting, and purifying;
D. mixing the prepared shaving water stock solution, the hair growth and hair loss prevention plant essence solution, the plant antiseptic stock solution and the purified water in proportion, and uniformly stirring to obtain the hair growth and hair loss prevention plant essence solution.
The preparation method of the shaving water with the hair growth and hair loss prevention function is characterized in that the supercritical extraction in the step A is carried out at the temperature of 25-45 ℃ and under the pressure of 25-50 Mpa for 2-10 hours.
The preparation method of the shaving water with the hair growth and hair loss prevention function is characterized in that ultrasonic extraction is adopted in the step B, the temperature is 25-60 ℃, and the time is 1-6 minutes.
The preparation method of the shaving water with the hair growth and hair loss prevention function is characterized in that ultrasonic extraction is adopted in the step C, the temperature is 25-45 ℃, and the time is 1-6 minutes.
The technical scheme of the invention is explained in detail as follows:
the shaving water with the functions of growing hair and preventing hair loss is prepared by mixing a shaving water stock solution, a hair-growing and hair-preventing plant essence solution, a plant preservative stock solution and purified water.
Wherein the stock solution of wood shavings is extract of elm wood shavings. Shavings are mostly sliced from the trunk wood of a tree in the form of rolled sheets. The elm leaves used in the invention draw traditional essence, and more elm effective components for hair care are extracted by modern means.
The hair growth and loss prevention plant essence is one or more natural Chinese herbal medicine extracts, and comprises one or more of perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus, polygonum multiflorum, sealwort, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, medlar, pearl barley, poria cocos and the like. According to the invention, 10-20 parts of purple perilla, 10-20 parts of tea, 20-35 parts of houttuynia cordata, 10-20 parts of angelica sinensis, 5-15 parts of mint, 15-30 parts of astragalus membranaceus, 20-35 parts of polygonum multiflorum, 6-15 parts of polygonatum sibiricum, 6-15 parts of eucommia ulmoides, 15-25 parts of mulberry, 10-30 parts of verbena, 10-20 parts of polygala tenuifolia, 15-30 parts of medlar, 20-35 parts of pearl barley and 15-25 parts of poria cocos are preferably selected according to the parts by weight for weighing and proportioning, and the natural Chinese herbal medicines are adopted for compounding, so that the hair can be protected, maintained and prevented from alopecia, and the nourishing components can regulate qi and blood and promote hair.
Wherein the plant antiseptic stock solution is one or more antiseptic pure natural plant extracts, and comprises one or more of folium Bambusae, folium Ginkgo, cortex Magnolia officinalis, Glycyrrhrizae radix, flos Caryophylli, Aloe, and flos Pelargonii Hortori. The bamboo leaf and aloe composite material is prepared by preferably weighing and proportioning 2-15 parts of bamboo leaves, 0-5 parts of ginkgo leaves, 0-5 parts of mangnolia officinalis, 0-5 parts of liquorice, 0-3 parts of clove, 0-3 parts of aloe and 0-3 parts of geranium according to parts by weight, and the pure natural plants are compounded to achieve the effects of oxidation resistance and corrosion resistance, so that the effective components of elm and hair growth and hair loss prevention components are not damaged, and the bamboo leaf and aloe composite material is green, healthy, safe and reliable. Preferably, the plant preservative stock solution comprises 2-12 parts of bamboo leaves, 0-4 parts of ginkgo leaves, 0-4 parts of mangnolia officinalis, 0-4 parts of liquorice, 0-2 parts of clove, 0-2 parts of aloe and 0-2 parts of geranium; more preferably, the plant preservative stock solution comprises 2-10 parts of bamboo leaves, 0-2 parts of ginkgo leaves, 0-2 parts of mangnolia officinalis, 0-2 parts of liquorice, 0-1 part of clove, 0-1 part of aloe and 0-1 part of geranium.
The preparation method of the shaving water comprises the following steps:
A. preparing a stock solution of wood shaving water;
B. preparing a hair-growing and anti-hair-loss plant essence;
C. preparing a plant antiseptic stock solution;
D. mixing the prepared shaving water stock solution, the hair growth and hair loss prevention plant essence solution, the plant antiseptic stock solution and the purified water in proportion, and uniformly stirring to obtain the hair growth and hair loss prevention plant essence solution.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: pulverizing the sliced shavings and sieving;
3. and (3) extraction: adding 50-100 times of the mixture of purified water and ethanol into the wood shaving particles, and passing through supercritical CO2The extraction process carries out extraction at a certain temperature and pressure;
4. and (3) purification: decoloring and filtering the active carbon, and then distilling the active carbon at the temperature of 30-45 ℃ under reduced pressure to remove ethanol to obtain the shaving water stock solution.
The thickness of the wood shaving pieces is 0.2-1.5 mm, preferably 0.4-1.2 mm, and more preferably 0.5-1 mm.
The particle size of the wood shavings is 15-100 meshes, preferably 20-85 meshes, and more preferably 25-60 meshes;
the volume ratio of the mixture of the purified water and the ethanol is (3-10): (7-0), preferably (4-10): (7-0), more preferably (5-10): (5-0).
The supercritical CO2Temperature of extractionIs 25 to 45 ℃, preferably 28 to 42 ℃, and more preferably 35 to 40 ℃.
The extraction pressure is 25-50 Mpa, preferably 30-45 Mpa, and more preferably 30-40 Mpa.
The extraction time is 2-10 hours, preferably 3-8 hours, and more preferably 3-6 hours.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning raw materials of purple perilla, tea, houttuynia cordata, angelica sinensis, mint, astragalus membranaceus, polygonum multiflorum, sealwort, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, medlar, pearl barley, poria cocos and the like with purified water for three times in an ultrasonic mode until the raw materials are clean;
2. preparing plant medicinal material powder: smashing and grinding the medicinal materials in the step 1;
3. and (3) extraction and filtration: adding a mixture of purified water and ethanol in an amount which is 5-50 times the weight of the medicinal powder into the medicinal powder, soaking for 3-8 hours, extracting at a certain temperature by using an ultrasonic synergistic extraction process, and then decolorizing and filtering to obtain a filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
The size of the medicinal powder is 100-400 meshes, preferably 150-350 meshes, and more preferably 200-300 meshes;
the volume ratio of the mixture of the purified water and the ethanol is (1-5): (5-10), preferably (1-4): (6-10), more preferably (1-3): (7 to 10)
The ultrasonic extraction temperature is 25-60 ℃, preferably 30-55 ℃, and more preferably 35-50 ℃;
the extraction time is 1-6 minutes, preferably 2-6 minutes, and more preferably 2-4 minutes.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning raw materials of bamboo leaves, ginkgo leaves, mangnolia officinalis, liquorice, clove, aloe and geranium with purified water in an ultrasonic wave for three times until the bamboo leaves, the ginkgo leaves, the mangnolia officinalis, the liquorice, the clove, the aloe and the geranium are clean;
2. preparing plant preservative medicinal material powder: smashing and grinding the medicinal materials in the step 1;
3. and (3) extraction: adding a mixture of purified water and ethanol in an amount which is 5-50 times the weight of the medicinal powder into the medicinal powder, soaking for 3-8 hours, extracting at a certain temperature by using an ultrasonic synergistic extraction process, and then decolorizing and filtering to obtain a filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
The size of the medicinal powder is 100-400 meshes, preferably 150-350 meshes, and more preferably 200-300 meshes;
the ultrasonic extraction temperature is 25-45 ℃, preferably 28-42 ℃, and more preferably 35-40 ℃;
the extraction time is 1-6 minutes, preferably 2-6 minutes, and more preferably 2-4 minutes.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
Mixing the wood shaving water stock solution prepared by the first method, the hair-growing and hair-loss preventing plant essence prepared by the second method and the plant preservative stock solution prepared by the third method according to a certain proportion, adding a certain amount of purified water at room temperature to adjust viscosity, and uniformly stirring to obtain the wood shaving water with the hair-growing and hair-loss preventing functions.
The ratio of the wood shaving water stock solution, the hair growth and hair loss prevention plant essence solution, the plant anticorrosion stock solution and the purified water is 50-80 parts of the wood shaving water stock solution, 20-50 parts of the hair growth and hair loss prevention plant essence solution and 0.5-1 part of the plant anticorrosion stock solution; 200-300 parts of purified water. Preferably, the ratio of the plant preservative solution to the wood shaving water is 60-70 parts of shaving water stock solution, 30-40 parts of hair growth and hair loss prevention plant essence solution and 0.8-1 part of plant preservative stock solution; 200 parts of purified water; more preferably, the ratio of the plant preservative solution to the wood shaving water stock solution is 60 parts, the hair growth and loss prevention plant essence solution is 40 parts, and the plant preservative stock solution is 1 part; 200 parts of purified water.
The viscosity of the prepared hair-growing and hair-loss preventing shaving water is preferably 2000-7500 mPa.s, more preferably 2500-7000 mPa.s, and most preferably 3000-6000 mPa.s.
Compared with the prior art, the invention has the beneficial effects that:
1. the shaving water disclosed by the invention is green, safe, pure natural, high in activity, not going bad for a long time, obvious in hair growth and hair loss prevention effect and has hair care and shaping effects.
2. According to the characteristics of elm wood shavings and medicinal materials, the supercritical CO2 extraction process and the ultrasonic synergistic extraction process are respectively adopted, so that the content of active ingredients is greatly improved, the activity of each active ingredient is not damaged, and meanwhile, the introduction of a chemical preservative is avoided by combining the preparation and addition processes of a natural preservative, and the pure natural characteristics of the product are ensured.
3. The preparation method provided by the invention optimizes the component proportion of the medicinal materials and the compounding proportion of the shaving water stock solution and the hair growth and hair loss prevention plant essence solution, is safe and reliable, has small environmental pollution, and is suitable for large-scale production and application and popularization.
Detailed Description
The present invention will be further described with reference to the following examples for facilitating understanding of those skilled in the art, and the description of the embodiments is not intended to limit the present invention.
Example 1
The raw materials comprise the following components:
preparing elm wood shavings original slices; purple perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, Chinese wolfberry, coix seed and poria cocos; bamboo leaf, ginkgo leaf, magnolia bark, liquorice, clove, aloe and geranium.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: crushing the shavings slices, and weighing 100g of shavings particles of 15-100 meshes;
3. and (3) extraction: adding 5Kg of mixture of purified water and ethanol in a volume ratio of 5:1 into the wood shaving particles, and passing through supercritical CO2The extraction process is used for extracting for 2-10 hours at the temperature of 25-45 ℃ and under the pressure of 25-50 Mpa;
4. and (3) purification: adding 50g of activated carbon into the extracted mixture for decolorization, filtering, and then carrying out reduced pressure distillation at the temperature of 30-45 ℃ to remove ethanol, thereby obtaining the wood shaving water stock solution.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning 10g of purple perilla, 10g of tea, 20g of houttuynia cordata, 15g of angelica sinensis, 5g of mint, 20g of astragalus membranaceus, 25g of polygonum multiflorum, 6g of rhizoma polygonati, 6g of eucommia ulmoides, 20g of mulberry, 15g of verbena, 15g of polygala tenuifolia, 20g of medlar, 20g of coix seed and 15g of poria cocos by using purified water in ultrasonic waves for three times until the purple perilla, the tea leaves, the houttuynia cordata, the angelica sinensis, the mint;
2. preparing plant medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder within 100-400 meshes;
3. and (3) extraction and filtration: adding 2.5Kg of mixture of purified water and ethanol with the volume ratio of 2:5, soaking for 3-8 hours, extracting for 1-6 minutes at 25-60 ℃ by using an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning raw materials of 2g of bamboo leaves, 5g of ginkgo leaves, 5g of mangnolia officinalis, 5g of liquorice, 3g of clove, 3g of aloe and 3g of geranium with purified water in ultrasonic waves for three times until the raw materials are clean;
2. preparing plant preservative medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder within 100-400 meshes;
3. and (3) extraction: adding 0.8Kg of mixture of purified water and ethanol with a volume ratio of 1:2 into the medicinal material powder, soaking for 3-8 hours, then extracting for 1-6 minutes at 25-45 ℃ by an ultrasonic synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
And (3) mixing 50g of the wood shaving water stock solution prepared by the first method, 20g of the hair-growing and hair-loss-preventing plant essence prepared by the second method and 0.5g of the plant preservative stock solution prepared by the third method, adding 200g of purified water at room temperature, and uniformly stirring and mixing to obtain the wood shaving water with the hair-growing and hair-loss-preventing functions, wherein the viscosity is 2000 mPa.s.
Example 2
The raw materials comprise the following components:
preparing elm wood shavings original slices; purple perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, Chinese wolfberry, coix seed and poria cocos; bamboo leaf, licorice, clove, aloe and geranium.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: crushing the shavings slices, and weighing 100g of 20-85-mesh shavings particles;
3. and (3) extraction: adding the wood shaving particles with the volume ratio of 10: 3 mixture of purified water and ethanol 5Kg, then passing through supercritical CO2The extraction process is used for extracting for 3-8 hours at the temperature of 28-42 ℃ and under the pressure of 30-45 Mpa;
4. and (3) purification: adding 50g of activated carbon into the extracted mixture for decolorization, filtering, and then carrying out reduced pressure distillation at the temperature of 30-45 ℃ to remove ethanol, thereby obtaining the wood shaving water stock solution.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning 15g of perilla, 15g of tea, 30g of houttuynia cordata, 10g of angelica sinensis, 10g of mint, 15g of astragalus membranaceus, 20g of polygonum multiflorum, 10g of rhizoma polygonati, 10g of eucommia ulmoides, 15g of mulberry, 10g of verbena, 10g of polygala tenuifolia, 15g of medlar, 25g of pearl barley and 20g of poria cocos by using purified water in ultrasonic waves for three times until the mixture is clean;
2. preparing plant medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction and filtration: adding the mixture in a volume ratio of 1:2, soaking 2.5Kg of mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 30-55 ℃ by using an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning raw materials of 15g of bamboo leaves, 2g of liquorice, 1g of clove, 2g of aloe and 2g of geranium in purified water for three times in an ultrasonic mode until the raw materials are clean;
2. preparing plant preservative medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction: adding the medicinal material powder into a mixture with a volume ratio of 1:2, soaking 0.8Kg of a mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 28-42 ℃ by using an ultrasonic synergistic extraction process, and then decoloring and filtering to obtain a filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
60g of the shaving water stock solution prepared by the first method, 30g of the hair growth and hair loss prevention plant essence solution prepared by the second method and 0.6g of the plant preservative stock solution prepared by the third method are mixed, 200g of purified water is added at room temperature, the shaving water with the hair growth and hair loss prevention functions is obtained by stirring and mixing uniformly, and the viscosity is measured to be 3500 mPa.s.
Example 3
The raw materials comprise the following components:
preparing elm wood shavings original slices; purple perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, Chinese wolfberry, coix seed and poria cocos; bamboo leaf, ginkgo leaf, magnolia bark and licorice.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: crushing the shavings slices, and weighing 100g of shavings particles of 25-60 meshes;
3. and (3) extraction: adding 5Kg of mixture of purified water and ethanol in a volume ratio of 7:3 into the wood shaving particles, and passing through supercritical CO2The extraction process is used for extracting for 3-6 hours at the temperature of 35-40 ℃ and under the pressure of 30-40 Mpa;
4. and (3) purification: adding 50g of activated carbon into the extracted mixture for decolorization, filtering, and then carrying out reduced pressure distillation at the temperature of 30-45 ℃ to remove ethanol, thereby obtaining the wood shaving water stock solution.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning 10g of perilla, 15g of tea, 35g of houttuynia cordata, 15g of angelica sinensis, 15g of mint, 25g of astragalus membranaceus, 30g of polygonum multiflorum, 15g of rhizoma polygonati, 15g of eucommia ulmoides, 15g of mulberry, 20g of verbena, 20g of polygala tenuifolia, 25g of medlar, 30g of coix seed and 25g of poria cocos by using purified water in ultrasonic waves for three times until the mixture is clean;
2. preparing plant medicinal material powder: smashing and grinding the medicinal materials in the step 1, and keeping the size of medicinal material powder within 200-300 meshes;
3. and (3) extraction and filtration: adding 3Kg of mixture of purified water and ethanol in a volume ratio of 3:5, soaking for 3-8 hours, extracting for 2-4 minutes at 35-50 ℃ by using an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning 15g of bamboo leaves, 3g of ginkgo leaves, 3g of mangnolia officinalis and 3g of liquorice which are used as raw materials in ultrasonic waves for three times until the raw materials are clean;
2. preparing plant preservative medicinal material powder: smashing and grinding the medicinal materials in the step 1, and keeping the size of medicinal material powder within 200-300 meshes;
3. and (3) extraction: adding 1Kg of mixture of purified water and ethanol with a volume ratio of 1:2 into the medicinal material powder, soaking for 3-8 hours, then extracting for 2-4 minutes at 35-40 ℃ by using an ultrasonic synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
70g of the shaving water stock solution prepared by the first method, 40g of the hair growth and hair loss prevention plant essence solution prepared by the second method and 1g of the plant preservative stock solution prepared by the third method are mixed, 300g of purified water is added at room temperature, the shaving water with the hair growth and hair loss prevention functions is obtained by stirring and mixing uniformly, and the viscosity of the shaving water is 4500 mPa.s.
Example 4
The raw materials comprise the following components:
preparing elm wood shavings original slices; purple perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, Chinese wolfberry, coix seed and poria cocos; bamboo leaf, ginkgo leaf, magnolia bark, clove, aloe and geranium.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: crushing the shavings slices, and weighing 100g of 20-85-mesh shavings particles;
3. and (3) extraction: adding the wood shaving particles with the volume ratio of 5:1, 5Kg of mixture of purified water and ethanol, and passing through supercritical CO2The extraction process is used for extracting for 3-8 hours at the temperature of 28-42 ℃ and under the pressure of 30-45 Mpa;
4. and (3) purification: adding 60g of activated carbon into the extracted mixture for decolorization, filtering, and then carrying out reduced pressure distillation at the temperature of 30-45 ℃ to remove ethanol, thereby obtaining the wood shaving water stock solution.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning 20g of perilla, 20g of tea, 20g of houttuynia cordata, 20g of angelica sinensis, 10g of mint, 30g of astragalus membranaceus, 35g of polygonum multiflorum, 10g of rhizoma polygonati, 10g of eucommia ulmoides, 25g of mulberry, 30g of verbena, 10g of polygala tenuifolia, 30g of medlar, 35g of coix seed and 20g of poria cocos by using purified water in ultrasonic waves for three times until the mixture is clean;
2. preparing plant medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction and filtration: adding the mixture in a volume ratio of 3:5, soaking 2.5Kg of mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 30-55 ℃ by using an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning 10g of bamboo leaves, 2g of ginkgo leaves, 2g of mangnolia officinalis, 2g of clove, 2g of aloe and 2g of geranium with purified water in an ultrasonic wave for three times until the raw materials are clean;
2. preparing plant preservative medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction: adding the medicinal material powder into a mixture with a volume ratio of 3:5, soaking 1Kg of mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 28-42 ℃ by an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
And (3) mixing 80g of the shaving water stock solution prepared by the first method, 40g of the hair-growing and hair-loss preventing plant essence prepared by the second method and 0.8g of the plant preservative stock solution prepared by the third method, adding 300g of purified water at room temperature, and uniformly stirring and mixing to obtain the shaving water with the hair-growing and hair-loss preventing functions, wherein the viscosity is 5500 mPa.s.
Example 5
The raw materials comprise the following components:
preparing elm wood shavings original slices; purple perilla, tea, houttuynia cordata, Chinese angelica, mint, astragalus mongholicus, polygonum multiflorum, rhizoma polygonati, eucommia ulmoides, mulberry, verbena, polygala tenuifolia, Chinese wolfberry, coix seed and poria cocos; bamboo leaf, ginkgo leaf, magnolia bark, liquorice, clove, aloe and geranium.
Preparation of wood shaving water stock solution
1. Shaving pieces: preparing a dry elm wood shaving piece, anchoring the elm wood shaving piece in a longitudinal direction, controlling the thickness of the elm wood shaving piece to be 0.2-1.5 mm, and storing the elm wood shaving piece in a drying vacuum cabinet at the temperature of 2-10 ℃ to avoid moisture absorption, mildew and worm damage;
2. preparing wood shaving particles: crushing the shavings slices, and weighing 100g of shavings particles of 25-60 meshes;
3. and (3) extraction: adding the volume ratio of 4: 1, 5Kg of mixture of purified water and ethanol, and passing through supercritical CO2The extraction process is used for extracting for 3-8 hours at the temperature of 28-42 ℃ and under the pressure of 30-45 Mpa;
4. and (3) purification: adding 60g of activated carbon into the extracted mixture for decolorization, filtering, and then carrying out reduced pressure distillation at the temperature of 30-45 ℃ to remove ethanol, thereby obtaining the wood shaving water stock solution.
Second, preparation of hair-growing and anti-hair loss plant essence
1. Cleaning: cleaning 15g of perilla, 15g of tea, 25g of houttuynia cordata, 15g of angelica sinensis, 10g of mint, 20g of astragalus membranaceus, 30g of polygonum multiflorum, 10g of rhizoma polygonati, 6g of eucommia ulmoides, 15g of mulberry, 20g of verbena, 15g of polygala tenuifolia, 20g of medlar, 20g of coix seed and 20g of poria cocos by using purified water in ultrasonic waves for three times until the mixture is clean;
2. preparing plant medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction and filtration: adding the mixture in a volume ratio of 2:5, soaking 2.5Kg of mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 30-55 ℃ by using an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 40-50 ℃ under reduced pressure to remove ethanol to obtain the plant essence.
Preparation of plant antiseptic stock solution
1. Cleaning: cleaning 10g of bamboo leaves, 2g of ginkgo leaves, 2g of mangnolia officinalis, 2g of liquorice, 2g of clove, 2g of aloe and 2g of geranium with purified water in ultrasonic waves for three times until the raw materials are clean;
2. preparing plant preservative medicinal material powder: smashing the medicinal materials in the step 1, and grinding, and keeping the size of medicinal material powder at 150-350 meshes;
3. and (3) extraction: adding the medicinal material powder into the mixture according to the volume ratio of 2:5, soaking 1Kg of mixture of purified water and ethanol for 3-8 hours, then extracting for 2-6 minutes at 28-42 ℃ by an ultrasonic wave synergistic extraction process, and then decoloring and filtering to obtain filtrate;
4. and (3) purification: and distilling the obtained filtrate at 35-45 ℃ under reduced pressure, and removing ethanol to obtain the plant preservative extract.
Preparation of shaving liquid for promoting hair growth and preventing hair loss
Mixing 80g of the shaving water stock solution prepared by the first method, 50g of the hair growth and hair loss prevention plant essence solution prepared by the second method and 1g of the plant preservative stock solution prepared by the third method, adding 200g of purified water at room temperature, stirring and mixing uniformly to obtain the shaving water with the hair growth and hair loss prevention functions, and measuring the viscosity of the shaving water to be 7000mPa.s
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.

Claims (10)

1. A shaving water with hair growth and hair loss prevention functions is characterized by comprising the following components in parts by weight:
Figure FDA0002573665570000011
2. the shaving water with hair growth promoting and hair loss preventing functions as claimed in claim 1, wherein the shaving water stock solution is elm shaving slice extract.
3. The shaving water with hair growth and loss prevention functions as claimed in claim 1, wherein the hair growth and loss prevention plant essence is one or more natural Chinese herbal medicine extracts.
4. The water with hair growth promoting and hair loss preventing functions of claim 3, wherein the natural Chinese herbal medicines comprise one or more of perilla, tea, houttuynia, angelica, mint, astragalus, polygonum multiflorum, polygonatum, eucommia, mulberry, verbena, polygala tenuifolia, medlar, coix seed and poria cocos.
5. The shaving water with hair growth and loss prevention functions as claimed in claim 1, wherein the plant preservative stock solution is one or more preservative pure natural plant extracts.
6. The shaving water with hair growth and loss prevention functions as claimed in claim 5, wherein the antiseptic pure natural plants comprise one or more of bamboo leaves, ginkgo leaves, magnolia officinalis, liquorice, clove, aloe and geranium.
7. A method for preparing shaving water with hair growth and loss prevention functions as claimed in any one of claims 1 to 6, comprising the following steps:
A. preparing a shaving water stock solution: slicing the sliced flos Lonicerae, granulating, performing supercritical extraction, and purifying;
B. preparing a hair-growing and anti-hair-loss plant essence: cleaning one or more natural Chinese medicinal materials, pulverizing, extracting, filtering, and purifying;
C. preparing a plant preservative stock solution: cleaning one or more antiseptic pure natural plants, pulverizing, extracting, and purifying;
D. mixing the prepared shaving water stock solution, the hair growth and hair loss prevention plant essence solution, the plant antiseptic stock solution and the purified water in proportion, and uniformly stirring to obtain the hair growth and hair loss prevention plant essence solution.
8. The method for preparing water with hair growth promoting and hair loss preventing effects as claimed in claim 7, wherein the supercritical extraction in step A is carried out at 25-45 deg.C under 25-50 MPa for 2-10 hr.
9. The method for preparing water with hair growth and loss prevention functions according to claim 7, wherein the ultrasonic extraction is adopted in the step B, the temperature is 25-60 ℃, and the time is 1-6 minutes.
10. The method for preparing water with hair growth and loss prevention functions according to claim 7, wherein the ultrasonic extraction is adopted in the step C, the temperature is 25-45 ℃, and the time is 1-6 minutes.
CN202010647433.1A 2020-07-07 2020-07-07 Shaving water with hair growing and hair loss preventing functions and preparation method thereof Pending CN111956568A (en)

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CN117598954A (en) * 2023-12-14 2024-02-27 中国中医科学院中医药健康产业研究所 Elm wood shavings glue and preparation method and application thereof

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