CN106667858A - Herba ecliptae hair-blacking composition and preparation method thereof - Google Patents
Herba ecliptae hair-blacking composition and preparation method thereof Download PDFInfo
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- CN106667858A CN106667858A CN201710151237.3A CN201710151237A CN106667858A CN 106667858 A CN106667858 A CN 106667858A CN 201710151237 A CN201710151237 A CN 201710151237A CN 106667858 A CN106667858 A CN 106667858A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a herba ecliptae hair-blacking composition and a preparation method thereof. The herba ecliptae hair-blacking composition is mainly prepared from 1 to 10 parts of herba ecliptae, 1 to 10 parts of rhizoma cimicifugae, 1 to 10 parts of pine needles, 1 to 10 parts of ribes nigrum, 1 to 10 parts of herba houttuyniae and 1 to 10 parts of cortex magnoliae officinalis. The preparation method is characterized by obtaining effective ingredients by adopting yeast fermentation, decompression reflux extraction and ultrasonic extraction. The herba ecliptae hair-blacking composition disclosed by the invention is capable of directly nourishing hair roots and increasing melanin in the hair roots; meanwhile, by matching with head massage, the blood circulation is quickened, and the absorption of pores on medicine is increased, so that the effect of blacking hairs is achieved.
Description
Technical field
The present invention relates to article of everyday use or cosmetic field, more particularly to a kind of Herba Ecliptae black hair compositionss and its preparation side
Method.
Background technology
As China rapidly enters aging society, the Chinese aged is up to 300,000,000.Today's society competition simultaneously swashs
Strong, psychentonia and cause the young and the middle aged poliosis increase, black hair, the hair color market demand is increasingly increased, possess huge development
Space and market potential.
With the rapid progress of beauty science, people no longer meet the dyeing by hair dyeing product to hair, but pursue
Nutrient substance in cosmetics can participate in the metabolism of hair, pursue science nursing；Under the trend of back to nature, people compel
It is essential and wants safety non-toxic, the natural hair color hair blackening product of skin allergy will not be caused, these products should be conceived to hair sheet
The nursing and protection of matter, also makes every effort to receive certain effect in terms of skin of head, hair cell metabolism, slow down aging,
And then reach young, beautiful and pleasurable purpose.
In recent years to occurring in that special preference as black hair hair color cosmetic material using natural plants.Business both domestic and external
Family catches most of Asians to wish the pitch-black moist tradition psychology of hair, is proposed some natural black hair hair color products.Such as
The B of Chinese patent CN 103721144 disclose a kind of natural plants hair color liquid, by the hair blackening compositionss system of following weight parts
It is standby to form：Herba Ecliptae 1-20 parts, Semen Sesami Nigrum 1-20 parts, Radix Angelicae Sinensis 1-10 parts, Cacumen Platycladi 1-10 parts, Radix Rehmanniae 1-10 parts, Fructus Ligustri Lucidi
1-10 parts, Herba Ecliptae 1-10 parts, Folium Mori 1-10 parts, Radix Stemonae 1-10 parts.Chinese patent application CN106214898A discloses one kind
The Chinese medicine preparation for the treatment of poliosis, it is obtained by the medicinal raw material of following weight portion, principal agent：Rhizoma Cimicifugae 20-50 parts, Radix Rehmanniae 80-120
It is part, Herba Ecliptae 90-120 parts, Semen Cuscutae 40-80 parts, Fructus Lycii 60-120 parts, betel nut 40-60 parts, Herba Ecliptae 100-120 parts, black
Formica fusca 80-120 parts, Fructus Mori 50-120 parts, semen juglandiss 80-120 parts, Herba Houttuyniae 60-120 parts, Poria 50-100 parts, Cortex Mori
100-200 parts, Radix Paeoniae Rubra 50-80 parts, Borneolum Syntheticum 3-5 parts；Accessory drugss are glycerol, and mass concentration of the glycerol in Chinese medicine preparation is 4%-6%.
From the foregoing, active component is extracted from plant as conditioning maintenance composition for obtaining safe and reliable black hair
Class product has great importance.Based on this, the invention provides a kind of black hair compositionss unlike the prior art, the black hair
Compositionss extract active component from different types of plant, educate with significant conditioning and send out effect.
The content of the invention
Based on this, the invention provides a kind of Herba Ecliptae black hair compositionss.
Concrete technical scheme is as follows：
A kind of Herba Ecliptae black hair compositionss, its active component is prepared from by the raw material of following weight portion：Herba Ecliptae 1-10 parts, liter
Numb 1-10 parts, Folium Pini 1-10 parts, the sub- 1-10 parts of postfermented tea bit of a bridle, Herba Houttuyniae 1-10 parts, Cortex Magnoliae Officinalis 1-10 part.
Wherein in some embodiments, the Herba Ecliptae black hair compositionss, its active component by following weight portion raw material
It is prepared from：8 parts of Herba Ecliptae, 4 parts of Rhizoma Cimicifugae, 4 parts of Folium Pini, 2 parts of postfermented tea bit of a bridle, 3 parts of Herba Houttuyniae, 4 parts of Cortex Magnoliae Officinalis.
Herba Ecliptae black hair compositionss of the present invention can be used directly, and using method is：Clean hair post processing is arrived
Seventy percent is dry, takes appropriate Herba Ecliptae black hair compositionss and rubs hair root, then gently massages 3-5 minutes, with horn comb combing.
Present invention also offers the preparation method of above-mentioned Herba Ecliptae black hair compositionss.
Concrete technical scheme is as follows：
A kind of preparation method of above-mentioned Herba Ecliptae black hair compositionss, comprises the following steps：
（1）Weight portion as described in claim 1 or 2, raw material is mixed, and is crushed, and is sifted out, and obtains crushed mixture, then is added
Enter water and Mel, stir, heat sterilization obtains sterilized mixture；The raw material is Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle
Son, Herba Houttuyniae, Cortex Magnoliae Officinalis；
（2）Sterilized mixture is fermented with the mixture of yeast and acetic acid bacteria, fermenting mixture is obtained；
（3）Fermenting mixture is carried out at reduced pressure conditions reflux, extract, with ethanol water, then carries out microwave extraction, must be extracted
Liquid, the extracting solution is filtered, and obtains clear liquor, obtains final product the Herba Ecliptae black hair compositionss.
Wherein in some embodiments, step（1）The addition of the water is 3-5 times of the raw material gross weight, described
The addition of Mel is the 5%-10% of the raw material gross weight.
Wherein in some embodiments, step（1）The temperature of the heat sterilization is 85-90 DEG C, and sterilization time is 10-20
Minute.
Wherein in some embodiments, step（2）It is 10 that the mixture of the yeast and acetic acid bacteria is viable count8cfu/
g-1012The mixed vaccine solution of cfu/g, the acetic acid bacteria and saccharomycetic quantitative proportion are（1-10）：(1-10), the yeast
With 0.1%-1% times that the addition of the mixture of acetic acid bacteria is the raw material gross weight；The temperature of the fermentation is 25-28 DEG C,
Fermentation time is 1-3 days.
Wherein in some embodiments, step（3）The volume fraction of the ethanol water is 80%-90%, and ethanol is water-soluble
The addition of liquid is 1-3 times of the fermenting mixture gross weight.
Wherein in some embodiments, step（3）The pressure for carrying out reflux, extract, at reduced pressure conditions is 70-
80KPa, the frequency of the microwave extraction is 1000-2000MHz, and extraction time is 3-5 minutes.
Wherein in some embodiments, step（3）The filtration includes：With filter-cloth filtering, filtrate is obtained, by filtrate in 1-3
Ceramic Composite membrane filtration is used again after preserving 1-3 days at a temperature of DEG C.
Wherein in some embodiments, the aperture of the filter cloth is 200-300 mesh, and the pore footpath of the ceramic composite membrane is
90-110nm。
Present invention also offers the application of above-mentioned Herba Ecliptae black hair compositionss.
Concrete technical scheme is as follows：
Application of the above-mentioned Herba Ecliptae black hair compositionss in the hair care hair care category article of everyday use with black hair effect is prepared.It is described to support
Sending out hair care category article of everyday use includes：Hair care spraying, hair care gel, shampoo, hair care breast, hair conditioner are He hairdressing gel.
Present invention also offers a kind of breast of the hair care with black hair effect.
Concrete technical scheme is as follows：
A kind of breast of the hair care with black hair effect, its functional component includes above-mentioned Herba Ecliptae black hair compositionss.
Wherein in some embodiments, the breast of the hair care with black hair effect, by the raw material system of following mass percent
It is standby to form：
Butanediol 5-10%, glycerol 5-10%, trehalose 0.1-0.5%, 1,3- Propylene Glycol 1-3%, ethanol 1-3%, methyl hydroxybenzoate 0.1-
0.3%th, stearic acid TEA salt 0.1-0.5%, allantoin 0.1-0.3%, acrylic acid（Ester）Class/C10-30 alkylol acrylamides acid esters is handed over
It is linked polymer 0.1-0.3%, EDTA disodium 0.01-0.05%, caprylic/capric triglyceride 3-6%, hydrogenated polydecene 3-6%, poly-
The methyl distearate 1-2% of glycerol -3, polydimethylsiloxane 2-4%, cetearyl alcohol 1-3%, the poly dimethyl of ring five
Siloxanes 1-3%, glyceryl stearate 0.5-1%, C14-22 alcohol 0.5-1%, glycerol three（Thylhexoic acid）Ester 1-3%, hydrogenation lecithin
Fat 0.1-0.5%, arachidic alcohol glucoside 0.1-0.3%, stearic acid 0.1-0.3%, arginine 0.1-0.3%, above-mentioned Herba Ecliptae black hair
Compositionss 1-10%, water surplus；The Herba Ecliptae black hair compositionss are prepared from by above-mentioned preparation method.
Herba Ecliptae black hair compositionss of the present invention and its preparation method and application have advantages below and beneficial effect：
The present invention Herba Ecliptae black hair compositionss be Jing inventor it is substantial amounts of experiment and study obtain, selected Herba Ecliptae, Rhizoma Cimicifugae,
Folium Pini, postfermented tea bit of a bridle, Herba Houttuyniae, Cortex Magnoliae Officinalis carry out compatibility according to specific ratio, and draw its optimum formula composition.Wherein ink is non-irrigated
Lotus, Rhizoma Cimicifugae, Folium Pini black beard and hair liver and kidney tonifying, nutritious root of hair, promotion hair melanin are generated, cause the glossy black effect of hair；Fish
The sub- blood-nourishing hair care of raw meat grass, Cortex Magnoliae Officinalis, postfermented tea bit of a bridle removes blood stasis tissue regeneration promoting blood, expands blood capillary, promotes head blood circulation, increases hair
Nutrition supply；All medicines share can direct hairy root nourishing, increase root of hair melanin, while coordinating the massage to head to accelerate blood to follow
Ring, increases absorption of the pore to medicine, so as to reach the effect of hair blackening.The Herba Ecliptae black hair compositionss, black hair effect is good,
And safety non-toxic, without side effect such as skin allergy.The Herba Ecliptae black hair compositionss are used for into hair care hair care category article of everyday use（Such as
Hair care breast）In, make the article of everyday use that there is good black hair effect.
The preparation method of the Herba Ecliptae black hair compositionss of the present invention is extracted, surpassed using yeast fermentation, reduced-pressure backflow successively
Sound wave is extracted and obtains effective ingredient, the efficiency high of this kind of method effective component extracting, the Herba Ecliptae black hair compositionss for preparing
Black hair hair color effect it is good, and process is simple is easy to operate, is adapted to large-scale production.
The preparation method of Herba Ecliptae black hair compositionss of the invention is further extracted pressure and temperature, is added by strict control
The technological parameters such as hot time, can effectively prevent the oxidation and loss of heat-sensitive materials, improve the matter of gained Herba Ecliptae black hair compositionss
Amount and black hair effect；Carried out with ceramic composite membrane microfiltration equipment filtration can the macromolecular substances such as effectively catching protein, fat, keep away
The association for exempting from macromolecular substances when product is placed for a long time produces precipitation.
Specific embodiment
More detailed are made to Herba Ecliptae black hair compositionss of the invention and its preparation method and application with reference to specific embodiment
Thin description, but embodiments of the present invention not limited to this.For especially not dated technological parameter or condition, routine is can refer to
Technology is carried out.
Each raw material involved by Herba Ecliptae black hair compositionss of the present invention is described as follows：
Herba Ecliptae, is the herb of feverfew Eclipta prostrata, medicinal, can restrain, stop blooding, invigorating the liver and kidney the effect of.《The southern regions of the Yunnan Province book on Chinese herbal medicine》Carry, ink
Fructus seu radix camptothecae acuminatae (Fructus Camptothecae Acuminatae) " teeth consolidating, black hair wash nine kinds of hemorrhoid ".《Compendium of Materia Medica》Point out, Herba Ecliptae " black beard and hair, kidney tonifying is cloudy ".
Rhizoma Cimicifugae, Chinese medicine name.For the rhizome of Ranunculaceae, Rhizoma Cimicifugae platymiscium C.heracleifolia, Cimicifuga Dahurica or Rhizoma Cimicifugae.Property is pungent,
It is sweet, it is slightly cold, return lung, spleen, large intestine, stomach, with delivering rash, heat-clearing and toxic substances removing, effect of ascending up spleen-Qi and Yang.
Folium Pini, Folium seu Strobilus Pini sibiricae, Pollen pini thunbergii in Pinaceae pine genus plant, Pinus tabuliformiss, Pinus koraiensis, Pinus armandi Franch- P. Komavovii Lavl., pinus yunnanensis faranch, Simao
The needle of pine, Pinus massoniana Lamb etc., gives birth to rich in saccharide, crude protein, crude fat, several amino acids and lot of trace ore deposit element, various dimensions
Element, bioflavonoid material, quintessence oil, chlorophyll, unsaturated fatty acid, enzyme and coenzyme isoreactivity material.Extract from pine needles can use
In expansion artery blood vessel, increase erythrocyte oxygen carrying capacity, blood circulation promoting improves the function of blood capillary, enhance immunity,
Increase hormonal secretion, strong essence makes the tissue rejuvenation of body.
Postfermented tea bit of a bridle：The undershrub of Saxifragaceae tea bit of a bridle son category ties mature fruit, also known as black currant, and trade name is black
Gallon.Fruit is small berries, and containing abundant saccharide, vitamins and other nutritious components, especially with Vc content highests, its fruit can be processed
It is also wine brewing, the good raw material of natural pigment food into fruit jam, fruit juice, fruit jelly and Fructose.The sub- fruit extract of postfermented tea bit of a bridle has medicinal
Composition, wherein flavonoid play the role of slow down aging, strengthen body immunity, blood fat reducing, improve arteriosclerosis and cancer-resisting.
Herba Houttuyniae, Chinese medicine, the dry aerial parts of saururaceae plant houttuynia cordata, acrid in the mouth is cold, return lung Jing.Can heat clearing away
Removing toxic substances, detumescence treat skin ulcer, promoting urination to remove dampness, clearing away heat to cure dysentery, invigorating the stomach and promoting digestion, with control excess-heat, pyretic toxicity, damp, disease heat be suffer from lung abscess, skin ulcer
Infectionss toxic swelling, hemorrhoidal hemorrhage, retention of heat in the spleen and stomach etc..Modern pharmacology experiment shows that this product has antibacterial, antiviral, improves immunity of organism
Power, diuresis etc. are acted on.
Cortex Magnoliae Officinalis, Chinese medicine, Cortex Magnoliae Officinalis plant is dried dried bark, root bark and branch skin, acrid in the mouth, warm in nature, stops with circulation of qi promoting removing dampness, warming middle-JIAO
Bitterly, effect of lowering the adverse QI to relieve asthma.
Embodiment 1
The Herba Ecliptae black hair compositionss of the present embodiment, its active component is prepared from the following materials：
Herba Ecliptae 1kg, Rhizoma Cimicifugae 10kg, Folium Pini 1kg, the sub- 10kg of postfermented tea bit of a bridle, Herba Houttuyniae 1kg, Cortex Magnoliae Officinalis 10kg.
Its preparation method is comprised the following steps：
Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle, Herba Houttuyniae, Cortex Magnoliae Officinalis are weighed by above-mentioned consumption, raw material is mixed, crushed, sieved
Son, obtains crushed mixture, adds water and Mel, and the addition of wherein water is 3 times of the raw material gross weight, the Mel
Addition be the 10% of the raw material gross weight, stir, be heated to 85 DEG C sterilize 20 minutes, obtain sterilized mixture；
Viable count is added to be 10 in sterilized mixture8The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic number
Amount ratio is 10：1, the addition of the mixture of the yeast and acetic acid bacteria is 0.1% times of the raw material gross weight, 28
DEG C condition bottom fermentation 1 day, obtains fermenting mixture；
The ethanol solution that volume fraction is 90% is added in fermenting mixture, the wherein addition of ethanol water is described
1 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 80KPa；
Then with the microwave radiation exaraction that frequency is 1000MHz 5 minutes, extracting solution is obtained；By the extracting solution with 200 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 110nm after filtrate is preserved 1 day at a temperature of 3 DEG C, clear liquor is obtained,
Obtain final product the Herba Ecliptae black hair compositionss.
Embodiment 2
The Herba Ecliptae black hair compositionss of the present embodiment, its active component is prepared from the following materials：
Herba Ecliptae 10kg, Rhizoma Cimicifugae 1kg, Folium Pini 10kg, the sub- 1kg of postfermented tea bit of a bridle, Herba Houttuyniae 10kg, Cortex Magnoliae Officinalis 1kg.
Its preparation method is comprised the following steps：
Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle, Herba Houttuyniae, Cortex Magnoliae Officinalis are weighed by above-mentioned consumption, raw material is mixed, crushed, sieved
Son, obtains crushed mixture, adds water and Mel, and the addition of wherein water is 5 times of the raw material gross weight, the Mel
Addition be the 5% of the raw material gross weight, stir, be heated to 90 DEG C sterilize 10 minutes, obtain sterilized mixture；
Viable count is added to be 10 in sterilized mixture12The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic
Quantitative proportion is 1：10, the addition of the mixture of the yeast and acetic acid bacteria is 1% times of the raw material gross weight, 25
DEG C condition bottom fermentation 3 days, obtains fermenting mixture；
The ethanol solution that volume fraction is 80% is added in fermenting mixture, the wherein addition of ethanol water is described
3 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 70KPa；
Then with the microwave radiation exaraction that frequency is 2000MHz 3 minutes, extracting solution is obtained；By the extracting solution with 300 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 90nm after filtrate is preserved 3 days at a temperature of 1 DEG C, clear liquor is obtained, i.e.,
Obtain the Herba Ecliptae black hair compositionss.
Embodiment 3
The Herba Ecliptae black hair compositionss of the present embodiment, its active component is prepared from the following materials：
Herba Ecliptae 8kg, Rhizoma Cimicifugae 4kg, Folium Pini 4kg, the sub- 2kg of postfermented tea bit of a bridle, Herba Houttuyniae 3kg, Cortex Magnoliae Officinalis 4kg.
Its preparation method is comprised the following steps：
Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle, Herba Houttuyniae, Cortex Magnoliae Officinalis are weighed by above-mentioned consumption, raw material is mixed, crushed, sieved
Son, obtains crushed mixture, adds water and Mel, and the addition of wherein water is 4 times of the raw material gross weight, the Mel
Addition be the 7% of the raw material gross weight, stir, be heated to 88 DEG C sterilize 15 minutes, obtain sterilized mixture；
Viable count is added to be 10 in sterilized mixture10The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic
Quantitative proportion is 4：7, the addition of the mixture of the yeast and acetic acid bacteria is 0.5% times of the raw material gross weight, 26
DEG C condition bottom fermentation 2 days, obtains fermenting mixture；
The ethanol solution that volume fraction is 85% is added in fermenting mixture, the wherein addition of ethanol water is described
2 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 75KPa；
Then with the microwave radiation exaraction that frequency is 1500MHz 4 minutes, extracting solution is obtained；By the extracting solution with 300 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 100nm after filtrate is preserved 2 days at a temperature of 2 DEG C, clear liquor is obtained,
Obtain final product the Herba Ecliptae black hair compositionss.
Embodiment 4
A kind of breast of the hair care with black hair effect of the present embodiment, is prepared from by the raw material of following mass percent：Butanediol
5%th, glycerol 10%, trehalose 0.1%, 1,3- Propylene Glycol 3%, ethanol 1%, methyl hydroxybenzoate 0.3%, stearic acid TEA salt 0.1%, allantois
Element 0.3%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.1%, EDTA disodiums 0.05%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 3%, hydrogenated polydecene 6%, the methyl of polyglycereol -3 distearate 1%, polydimethylsiloxane 4%, spermaceti
Stearyl alcohol 1%, ring five dimethyl silicone polymer 3%, glyceryl stearate 0.5%, C14-22 alcohol 1%, glycerol three（Thylhexoic acid）Ester
1%th, the ink drought obtained by hydrolecithin 0.5%, arachidic alcohol glucoside 0.1%, stearic acid 0.3%, arginine 0.1%, embodiment 1
Lotus black hair compositionss 10%, water surplus.
Embodiment 5
A kind of breast of the hair care with black hair effect of the present embodiment, is prepared from by the raw material of following mass percent：Butanediol
10%th, glycerol 5%, trehalose 0.5%, 1,3- Propylene Glycol 1%, ethanol 3%, methyl hydroxybenzoate 0.1%, stearic acid TEA salt 0.5%, allantois
Element 0.1%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.3%, EDTA disodiums 0.01%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 6%, hydrogenated polydecene 3%, the methyl of polyglycereol -3 distearate 2%, polydimethylsiloxane 2%, spermaceti
Stearyl alcohol 3%, ring five dimethyl silicone polymer 1%, glyceryl stearate 1%, C14-22 alcohol 0.5%, glycerol three（Thylhexoic acid）Ester
3%th, the ink drought obtained by hydrolecithin 0.1%, arachidic alcohol glucoside 0.3%, stearic acid 0.1%, arginine 0.3%, embodiment 2
Lotus black hair compositionss 1%, water surplus.
Embodiment 6
A kind of breast of the hair care with black hair effect of the present embodiment, is prepared from by the raw material of following mass percent：Butanediol
7%th, glycerol 8%, trehalose 0.3%, 1,3- Propylene Glycol 2%, ethanol 2%, methyl hydroxybenzoate 0.2%, stearic acid TEA salt 0.3%, allantois
Element 0.2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2%, EDTA disodiums 0.03%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 4%, hydrogenated polydecene 5%, the methyl of polyglycereol -3 distearate 1.5%, polydimethylsiloxane 3%, whale
Wax stearyl alcohol 2%, ring five dimethyl silicone polymer 2%, glyceryl stearate 0.7%, C14-22 alcohol 0.8%, glycerol three（Ethyl hexyl
Acid）Obtained by ester 2%, hydrolecithin 0.3%, arachidic alcohol glucoside 0.2%, stearic acid 0.2%, arginine 0.2%, embodiment 3
Herba Ecliptae black hair compositionss 5%, water surplus.
Embodiment 7
A kind of breast of the hair care with black hair effect of the present embodiment, is prepared from by the raw material of following mass percent：Butanediol
7%th, glycerol 8%, trehalose 0.3%, 1,3- Propylene Glycol 2%, ethanol 2%, methyl hydroxybenzoate 0.2%, stearic acid TEA salt 0.3%, allantois
Element 0.2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2%, EDTA disodiums 0.03%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 4%, hydrogenated polydecene 5%, the methyl of polyglycereol -3 distearate 1.5%, polydimethylsiloxane 3%, whale
Wax stearyl alcohol 2%, ring five dimethyl silicone polymer 2%, glyceryl stearate 0.7%, C14-22 alcohol 0.8%, glycerol three（Ethyl hexyl
Acid）Ester 2%, hydrolecithin 0.3%, arachidic alcohol glucoside 0.2%, stearic acid 0.2%, arginine 0.2%, Herba Ecliptae extract
1.6%th, Rhizoma Cimicifugae extract 0.8%, extract from pine needles 0.8%, postfermented tea bit of a bridle seed extract 0.4%, Herba Houttuyniae extract 0.6%, Cortex Magnoliae Officinalis are carried
Take thing 0.8%, water surplus；
Wherein, Herba Ecliptae extract, Rhizoma Cimicifugae extract, extract from pine needles, postfermented tea bit of a bridle seed extract, Herba Houttuyniae extract, Cortex Magnoliae Officinalis
The manufacturer of extract is Huzhou Jiamei.
Comparative example 1
A kind of breast of the hair care with black hair effect of this comparative example, is prepared from by the raw material of following mass percent：Butanediol
7%th, glycerol 8%, trehalose 0.3%, 1,3- Propylene Glycol 2%, ethanol 2%, methyl hydroxybenzoate 0.2%, stearic acid TEA salt 0.3%, allantois
Element 0.2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2%, EDTA disodiums 0.03%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 4%, hydrogenated polydecene 5%, the methyl of polyglycereol -3 distearate 1.5%, polydimethylsiloxane 3%, whale
Wax stearyl alcohol 2%, ring five dimethyl silicone polymer 2%, glyceryl stearate 0.7%, C14-22 alcohol 0.8%, glycerol three（Ethyl hexyl
Acid）Obtained by ester 2%, hydrolecithin 0.3%, arachidic alcohol glucoside 0.2%, stearic acid 0.2%, arginine 0.2%, comparative example 1
Herba Ecliptae black hair compositionss 5%, water surplus.
The Herba Ecliptae black hair compositionss of comparative example 1 are prepared as follows method and are obtained：
Rhizoma Cimicifugae 4kg, the sub- 2kg of postfermented tea bit of a bridle, Herba Houttuyniae 3kg, Cortex Magnoliae Officinalis 4kg are weighed, raw material is mixed, crushed, sifted out, crushed
Mixture, adds water and Mel, and the addition of wherein water is 4 times of the raw material gross weight, and the addition of the Mel is
The 7% of the raw material gross weight, stirs, and is heated to 88 DEG C and sterilizes 15 minutes, obtains sterilized mixture；
Viable count is added to be 10 in sterilized mixture10The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic
Quantitative proportion is 4：7, the addition of the mixture of the yeast and acetic acid bacteria is 0.5% times of the raw material gross weight, 26
DEG C condition bottom fermentation 2 days, obtains fermenting mixture；
The ethanol solution that volume fraction is 85% is added in fermenting mixture, the wherein addition of ethanol water is described
2 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 75KPa；
Then with the microwave radiation exaraction that frequency is 1500MHz 4 minutes, extracting solution is obtained；By the extracting solution with 300 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 100nm after filtrate is preserved 2 days at a temperature of 2 DEG C, clear liquor is obtained,
Obtain final product the Herba Ecliptae black hair compositionss.
Comparative example 2
A kind of breast of the hair care with black hair effect of this comparative example, is prepared from by the raw material of following mass percent：Butanediol
7%th, glycerol 8%, trehalose 0.3%, 1,3- Propylene Glycol 2%, ethanol 2%, methyl hydroxybenzoate 0.2%, stearic acid TEA salt 0.3%, allantois
Element 0.2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2%, EDTA disodiums 0.03%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 4%, hydrogenated polydecene 5%, the methyl of polyglycereol -3 distearate 1.5%, polydimethylsiloxane 3%, whale
Wax stearyl alcohol 2%, ring five dimethyl silicone polymer 2%, glyceryl stearate 0.7%, C14-22 alcohol 0.8%, glycerol three（Ethyl hexyl
Acid）Obtained by ester 2%, hydrolecithin 0.3%, arachidic alcohol glucoside 0.2%, stearic acid 0.2%, arginine 0.2%, comparative example 1
Herba Ecliptae black hair compositionss 5%, water surplus.
The Herba Ecliptae black hair compositionss of comparative example 1 are prepared as follows method and are obtained：
Herba Ecliptae 8kg, Folium Pini 4kg, Herba Houttuyniae 3kg, Cortex Magnoliae Officinalis 4kg are weighed, raw material is mixed, crushed, sifted out, obtained and crush mixed
Compound, adds water and Mel, and the addition of wherein water is 4 times of the raw material gross weight, and the addition of the Mel is institute
The 7% of raw material gross weight is stated, is stirred, be heated to 88 DEG C and sterilize 15 minutes, obtain sterilized mixture；
Viable count is added to be 10 in sterilized mixture10The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic
Quantitative proportion is 4：7, the addition of the mixture of the yeast and acetic acid bacteria is 0.5% times of the raw material gross weight, 26
DEG C condition bottom fermentation 2 days, obtains fermenting mixture；
The ethanol solution that volume fraction is 85% is added in fermenting mixture, the wherein addition of ethanol water is described
2 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 75KPa；
Then with the microwave radiation exaraction that frequency is 1500MHz 4 minutes, extracting solution is obtained；By the extracting solution with 300 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 100nm after filtrate is preserved 2 days at a temperature of 2 DEG C, clear liquor is obtained,
Obtain final product the Herba Ecliptae black hair compositionss.
Comparative example 3
A kind of breast of the hair care with black hair effect of this comparative example, is prepared from by the raw material of following mass percent：Butanediol
7%th, glycerol 8%, trehalose 0.3%, 1,3- Propylene Glycol 2%, ethanol 2%, methyl hydroxybenzoate 0.2%, stearic acid TEA salt 0.3%, allantois
Element 0.2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2%, EDTA disodiums 0.03%, the octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester 4%, hydrogenated polydecene 5%, the methyl of polyglycereol -3 distearate 1.5%, polydimethylsiloxane 3%, whale
Wax stearyl alcohol 2%, ring five dimethyl silicone polymer 2%, glyceryl stearate 0.7%, C14-22 alcohol 0.8%, glycerol three（Ethyl hexyl
Acid）Obtained by ester 2%, hydrolecithin 0.3%, arachidic alcohol glucoside 0.2%, stearic acid 0.2%, arginine 0.2%, comparative example 1
Herba Ecliptae black hair compositionss 5%, water surplus.
The Herba Ecliptae black hair compositionss of comparative example 1 are prepared as follows method and are obtained：
Herba Ecliptae 8kg, Rhizoma Cimicifugae 4kg, Folium Pini 4kg, the sub- 2kg of postfermented tea bit of a bridle are weighed, is mixed, crushed, sifted out, be pulverized and mixed
Thing, adds water and Mel, and the addition of wherein water is 4 times of the raw material gross weight, and the addition of the Mel is described
The 7% of raw material gross weight, stirs, and is heated to 88 DEG C and sterilizes 15 minutes, obtains sterilized mixture；
Viable count is added to be 10 in sterilized mixture10The mixed vaccine solution of cfu/g, wherein the acetic acid bacteria and saccharomycetic
Quantitative proportion is 4：7, the addition of the mixture of the yeast and acetic acid bacteria is 0.5% times of the raw material gross weight, 26
DEG C condition bottom fermentation 2 days, obtains fermenting mixture；
The ethanol solution that volume fraction is 85% is added in fermenting mixture, the wherein addition of ethanol water is described
2 times of ferment total weight of the mixture；After mixing, extract in reduced-pressure backflow tank, wherein the air pressure in reduced-pressure backflow tank is 75KPa；
Then with the microwave radiation exaraction that frequency is 1500MHz 4 minutes, extracting solution is obtained；By the extracting solution with 300 mesh filter-cloth filterings,
Filtrate is obtained, again with the Ceramic Composite membrane filtration that aperture is 100nm after filtrate is preserved 2 days at a temperature of 2 DEG C, clear liquor is obtained,
Obtain final product the Herba Ecliptae black hair compositionss.
Embodiment 4-7 comprises the steps with the preparation method of the hair care breast with black hair effect described in comparative example 1-3：
（1）By butanediol, glycerol, trehalose, 1,3- Propylene Glycol, ethanol, methyl hydroxybenzoate, stearic acid TEA salt, allantoin, acrylic acid
（Ester）Class/C10-30 alkylol acrylamide acid esters cross linked polymers, EDTA disodiums, water input emulsifying pot, stir, and are heated to 85
DEG C, it is obtained water phase, insulation 20 minutes is standby；（2）By caprylic/capric triglyceride, hydrogenated polydecene, the methyl of polyglycereol -3 Portugal
Sugared distearate, polydimethylsiloxane, cetearyl alcohol, ring five dimethyl silicone polymer, glyceryl stearate, C14-22
Alcohol, glycerol three（Thylhexoic acid）Ester, hydrolecithin, arachidic alcohol glucoside, stearic acid input oil phase pot, stir, and heat
To 85 DEG C, oil phase is obtained；（3）Homogenizing is opened, oil phase suction emulsifying pot, homogenizing 5 minutes, insulated and stirred 20 minutes are cooled to
45℃；（4）By arginine, Herba Ecliptae black hair compositionss input emulsifying pot, stir, verification is qualified can discharging.
The efficacy test of embodiment 8
To obtained by embodiment 4-7 and comparative example 1-4/the hair care breast with black hair effect buied carries out effect test and appraisal（Contrast
Example 4 is a commercially available hair care breast declared with hair color black hair effect）.
Concrete method of testing is as follows：Each experimental group chooses 30 volunteers, age 30-60 year, there are poliosis；Use
Method：Clean hair post processing is dry to seventy percent, takes appropriate hair care breast and rubs hair root, then gently massages 3-5 minutes, uses Cornu Bovis seu Bubali
Comb combing, 1 evening 1 time, continuous on probation 12 weeks, mug, and trier is paid a return visit.Evaluation methodology：Contrast the 0th day
With the 12nd week photo, wherein poliosis substantially tailed off, hair becomes glossy black for effective；Poliosis slightly reduce for effective；Poliosis
Phenomenon be not changed in for invalid.Concrete test result such as table 1.Trier is paid a return visit after on probation 12 weeks, do not occurred
The phenomenon of skin allergy, shows the hair care breast safety non-toxic.
The test result log of table 1
| It is effective | Effectively | It is invalid | |
| Embodiment 4 | 16 | 11 | 3 |
| Embodiment 5 | 12 | 13 | 5 |
| Embodiment 6 | 17 | 11 | 2 |
| Embodiment 7 | 8 | 12 | 10 |
| Comparative example 1 | 1 | 13 | 16 |
| Comparative example 2 | 0 | 14 | 16 |
| Comparative example 3 | 1 | 14 | 15 |
| Comparative example 4 | 1 | 11 | 18 |
From the result of table 1：
Embodiment 4-7 contrasts visible with comparative example 1-4, the breast black hair hair color effect of the hair care with black hair effect obtained by the present invention
Fruit is considerably better than comparative example；
Embodiment 6 contrasts visible with embodiment 7, with Herba Ecliptae black hair compositionss obtained in preparation method disclosed in this invention,
Its black hair effect is than marketable material more preferably；
Embodiment 6 contrasts visible with comparative example 1-3, Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle, Herba Houttuyniae, the Cortex Magnoliae Officinalis of the present invention
Black hair hair color is better when sharing, and each plant component after specific ratio compatibility according to playing the role of Synergistic.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality
Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, the scope of this specification record is all considered to be.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more concrete and detailed, but and
Can not therefore be construed as limiting the scope of the patent.It should be pointed out that for one of ordinary skill in the art comes
Say, without departing from the inventive concept of the premise, some deformations and improvement can also be made, these belong to present invention protection model
Enclose.Therefore, the protection domain of patent of the present invention should be defined by claims.
Claims (10)
1. a kind of Herba Ecliptae black hair compositionss, it is characterised in that its active component is prepared from by the raw material of following weight portion：Ink
Fructus seu radix camptothecae acuminatae (Fructus Camptothecae Acuminatae) 1-10 parts, Rhizoma Cimicifugae 1-10 parts, Folium Pini 1-10 parts, the sub- 1-10 parts of postfermented tea bit of a bridle, Herba Houttuyniae 1-10 parts, Cortex Magnoliae Officinalis 1-10 part.
2. Herba Ecliptae black hair compositionss according to claim 1, it is characterised in that the Herba Ecliptae black hair compositionss, its
Active component is prepared from by the raw material of following weight portion：8 parts of Herba Ecliptae, 4 parts of Rhizoma Cimicifugae, 4 parts of Folium Pini, postfermented tea bit of a bridle son 2 parts, fish raw meat
Careless 3 parts, 4 parts of Cortex Magnoliae Officinalis.
3. the preparation method of the Herba Ecliptae black hair compositionss described in any one of claim 1 or 2, it is characterised in that including following
Step：
（1）Weight portion as described in claim 1 or 2, raw material is mixed, and is crushed, and is sifted out, and obtains crushed mixture, then is added
Enter water and Mel, stir, heat sterilization obtains sterilized mixture；The raw material is Herba Ecliptae, Rhizoma Cimicifugae, Folium Pini, postfermented tea bit of a bridle
Son, Herba Houttuyniae, Cortex Magnoliae Officinalis；
（2）Sterilized mixture is fermented with the mixture of yeast and acetic acid bacteria, fermenting mixture is obtained；
（3）Fermenting mixture is carried out at reduced pressure conditions reflux, extract, with ethanol water, then carries out microwave extraction, must be extracted
Liquid, the extracting solution is filtered, and obtains clear liquor, obtains final product the Herba Ecliptae black hair compositionss.
4. the preparation method of Herba Ecliptae black hair compositionss according to claim 3, it is characterised in that step（1）The water
Addition be 3-5 times of the raw material gross weight, the addition of the Mel is the 5%-10% of the raw material gross weight；Step
（1）The temperature of the heat sterilization is 85-90 DEG C, and sterilization time is 10-20 minutes.
5. the preparation method of Herba Ecliptae black hair compositionss according to claim 3, it is characterised in that step（2）The ferment
It is 10 that the mixture of female bacterium and acetic acid bacteria is viable count8cfu/g-1012The mixed vaccine solution of cfu/g, the acetic acid bacteria and yeast
The quantitative proportion of bacterium is（1-10）：(1-10), the addition of the mixture of the yeast and acetic acid bacteria is the raw material gross weight
0.1%-1% times of amount；The temperature of the fermentation is 25-28 DEG C, and fermentation time is 1-3 days.
6. the preparation method of Herba Ecliptae black hair compositionss according to claim 3, it is characterised in that step（3）The second
The volume fraction of alcohol-water solution is 80%-90%, and the addition of ethanol water is 1-3 times of the fermenting mixture gross weight；
Step（3）The pressure for carrying out reflux, extract, at reduced pressure conditions is 70-80KPa, and the frequency of the microwave extraction is 1000-
2000MHz, extraction time is 3-5 minutes.
7. the preparation method of Herba Ecliptae black hair compositionss according to claim 3, it is characterised in that step（3）The mistake
Filter includes：With filter-cloth filtering, filtrate is obtained, after filtrate is preserved 1-3 days at a temperature of 1-3 DEG C Ceramic Composite membrane filtration is used again；
The aperture of the filter cloth is 200-300 mesh, and the pore footpath of the ceramic composite membrane is 90-110nm.
8. application of the Herba Ecliptae black hair compositionss described in claim 1 or 2 in hair care hair care category article of everyday use is prepared.
9. a kind of hair care with black hair effect is newborn, it is characterised in that its functional component includes the ink described in claim 1 or 2
Fructus seu radix camptothecae acuminatae (Fructus Camptothecae Acuminatae) black hair compositionss.
10. the hair care with hair color effect according to claim 9 is newborn, it is characterised in that by following mass percent
Raw material is prepared from：
Butanediol 5-10%, glycerol 5-10%, trehalose 0.1-0.5%, 1,3- Propylene Glycol 1-3%, ethanol 1-3%, methyl hydroxybenzoate 0.1-
0.3%th, stearic acid TEA salt 0.1-0.5%, allantoin 0.1-0.3%, acrylic acid（Ester）Class/C10-30 alkylol acrylamides acid esters is handed over
It is linked polymer 0.1-0.3%, EDTA disodium 0.01-0.05%, caprylic/capric triglyceride 3-6%, hydrogenated polydecene 3-6%, poly-
The methyl distearate 1-2% of glycerol -3, polydimethylsiloxane 2-4%, cetearyl alcohol 1-3%, the poly dimethyl of ring five
Siloxanes 1-3%, glyceryl stearate 0.5-1%, C14-22 alcohol 0.5-1%, glycerol three（Thylhexoic acid）Ester 1-3%, hydrogenation lecithin
Fat 0.1-0.5%, arachidic alcohol glucoside 0.1-0.3%, stearic acid 0.1-0.3%, arginine 0.1-0.3%, the institute of claim 1 or 2
Herba Ecliptae black hair compositionss 1-10%, the water surplus stated；The Herba Ecliptae black hair compositionss are by any one of claim 3-7 institute
The preparation method stated is prepared from.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581647A (en) * | 2022-10-19 | 2023-01-10 | 聚华生物科技(广州)有限公司 | Natural hair dyeing composition and application thereof in hair dye |
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|---|---|---|---|---|
| CN1543925A (en) * | 2003-11-20 | 2004-11-10 | 李明劲 | Shampoo cream containing Yerbadetajo Herb and method for preparing the same |
| CN103239559A (en) * | 2012-02-02 | 2013-08-14 | 徐建人 | White hair blacking liquid and preparation method thereof |
| CN104840778A (en) * | 2015-04-01 | 2015-08-19 | 徐凌川 | Traditional Chinese medicine fermented hair-blacking preparation, preparation method and purpose thereof |
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2017
- 2017-03-14 CN CN201710151237.3A patent/CN106667858A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1543925A (en) * | 2003-11-20 | 2004-11-10 | 李明劲 | Shampoo cream containing Yerbadetajo Herb and method for preparing the same |
| CN103239559A (en) * | 2012-02-02 | 2013-08-14 | 徐建人 | White hair blacking liquid and preparation method thereof |
| CN104840778A (en) * | 2015-04-01 | 2015-08-19 | 徐凌川 | Traditional Chinese medicine fermented hair-blacking preparation, preparation method and purpose thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581647A (en) * | 2022-10-19 | 2023-01-10 | 聚华生物科技(广州)有限公司 | Natural hair dyeing composition and application thereof in hair dye |
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