CN107536774B - Traditional Chinese medicine hair blackening and moistening agent and preparation method thereof - Google Patents
Traditional Chinese medicine hair blackening and moistening agent and preparation method thereof Download PDFInfo
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- CN107536774B CN107536774B CN201710739741.5A CN201710739741A CN107536774B CN 107536774 B CN107536774 B CN 107536774B CN 201710739741 A CN201710739741 A CN 201710739741A CN 107536774 B CN107536774 B CN 107536774B
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a traditional Chinese medicine hair blackening and moistening agent which is prepared from the following raw materials in parts by weight: 20-40 parts of prepared rehmannia root, 15-30 parts of prepared fleece-flower root, 22-30 parts of yerbadetajo herb, 20-30 parts of gynostemma pentaphylla, 20-30 parts of glossy privet fruit, 18-28 parts of ligusticum wallichii, 18-28 parts of angelica sinensis, 5-10 parts of dried ginger, 5-12 parts of chinaberry seed oil, 6-12 parts of lophatherum gracile, 5-10 parts of phellinus igniarius, 3-8 parts of lucid ganoderma, 5-10 parts of tuber fleeceflower root, 5-10 parts of mellea armillaria, 6-12 parts of gulfweed and 5-15 parts of black mulberry. The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent. The traditional Chinese medicine hair blackening and moistening agent has good penetration promoting capability, can enable active ingredients in the product to penetrate through fur to reach deep skin tissues more quickly, can provide sufficient nutrients for the fur, promotes metabolism, has a better product effect, and has the effects of blackening hair, nourishing hair, protecting hair, moistening and maintaining hair.
Description
Technical Field
The invention relates to the technical field of cosmetics for beauty and hairdressing, in particular to a traditional Chinese medicine hair blackening and moistening agent and a preparation method thereof.
Background
The hair quality condition of the hair is an important embodiment reflecting the physical health condition and image of modern people, and is an important mark of healthy life. With the influence of various adverse factors such as environmental pollution, hair dyeing, perm and the like, people pay more attention to hair care, at present, hair care products in the market are more and messy, not only are the price high, the effect is not ideal, some hair care products even damage scalp and hair, and the hair quality becomes worse, and the like, and the health of people is threatened.
Disclosure of Invention
The invention aims to: aiming at the problems, the traditional Chinese medicine hair blackening and moistening agent is provided, and has the effects of blackening hair, being mild to skin, nourishing and caring hair, moistening and maintaining.
In order to achieve the purpose of the invention, the technical scheme adopted by the invention is as follows:
a traditional Chinese medicine hair blackening and moistening agent is composed of the following raw materials in parts by weight: 20-40 parts of prepared rehmannia root, 15-30 parts of prepared fleece-flower root, 22-30 parts of yerbadetajo herb, 20-30 parts of gynostemma pentaphylla, 20-30 parts of glossy privet fruit, 18-28 parts of ligusticum wallichii, 18-28 parts of angelica sinensis, 5-10 parts of dried ginger, 5-12 parts of chinaberry seed oil, 6-12 parts of lophatherum gracile, 5-10 parts of phellinus igniarius, 3-8 parts of lucid ganoderma, 5-10 parts of tuber fleeceflower root, 5-10 parts of mellea armillaria, 6-12 parts of gulfweed and 5-15 parts of black mulberry.
Preferably, the traditional Chinese medicine hair blackening and moistening agent is prepared from the following raw materials in parts by weight: 35 parts of prepared rehmannia root, 25 parts of prepared fleece-flower root, 26 parts of yerbadetajo herb, 25 parts of gynostemma pentaphylla, 23 parts of glossy privet fruit, 20 parts of ligusticum wallichii, 24 parts of angelica, 6 parts of dried ginger, 10 parts of chingma chinensis seed oil, 8 parts of lophatherum gracile, 8 parts of phellinus igniarius, 5 parts of lucid ganoderma, 7 parts of tuber fleeceflower root, 6 parts of hazel mushroom, 8 parts of gulfweed and 10 parts of black mulberry.
The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent, which comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to a granularity of 10-30 meshes to obtain mixed powder for later use;
(3) adding ethanol 15-20 times the weight of the mixed powder into the mixed powder in the step (2), soaking at 20-28 ℃ for 35-65h, extracting at 70-80 ℃ for 40-60min, collecting the extract, and concentrating the extract under reduced pressure to obtain a concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 3-6 times of water for 2-4 hr, separating the extractive solution with macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 70-85 deg.C water bath for 1-3 hr, stirring, reflux filtering with ethanol for 2-4 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white chinlon oil, uniformly stirring, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing, filling and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
Preferably, in the step (2) and the step (4), the microwave sterilization temperature is 80-95 ℃, the time is 15-20min, the frequency is 2200-.
Preferably, in the step (5), the concentrated solution and the mixed slurry are slowly added into the rest of the meadowfoam seed oil, and are stirred for 3-4 hours at the temperature of 55-70 ℃ to be uniformly mixed.
Preferably, the volume concentration of the ethanol is 60-80%.
Preferably, the homogenization process is carried out under a pressure condition of 25-30 MPa.
Preferably, the stirring speed at 55-70 ℃ is 150-min, and the stirring speed at above 70 ℃ is 160-180 r/min.
The raw materials of the invention are as follows:
prepared rehmannia root, radix rehmanniae Praeparata, sweet in taste and slightly warm in nature, moistens kidney, nourishes kidney yin, replenishes essence and benefits marrow, is an essential drug for tonifying kidney yin, and has the effects of benefiting essence and blood and blackening beard and hair.
The prepared fleece-flower root has the efficacies of nourishing liver, tonifying kidney, nourishing blood, blackening beard and hair, nourishing the color and dispelling wind.
Eclipta, also known as eclipta alba, is sweet and sour in nature and taste, and has the effects of cooling blood, stopping bleeding, tonifying kidney and benefiting yin. It is used to treat hematemesis, hemoptysis, epistaxis, hematuria, hematochezia, bloody flux, bleeding due to knife wound, premature gray hair, etc., and has the effects of stopping bleeding, blackening hair and beard, and relieving cough and asthma. The herbal Zhengyi states that eclipta alba enters kidney and tonifies yin to grow hair. "Ming Dynasty Miao Zhichun is highly advocated to eclipta prostrata, which is said to be: the ancient and modern whitened herbs are the wins. "he thinks that the best medicine capable of blackening white hair in Chinese herbal medicines is even eclipta alba.
Gynostemma pentaphylla, slightly sweet in taste and cool in nature. The main effective components of the health-care food comprise gypenoside, gypenoside (polysaccharide), water-soluble amino acid, flavonoid, various vitamins, trace elements, mineral substances and the like. Reducing blood lipid, regulating blood pressure, preventing and treating thrombi, preventing and treating cardiovascular diseases, regulating blood sugar, promoting sleep, delaying aging, preventing and resisting cancer, enhancing immunity, and regulating physiological function of human body. The long-term use of the hair conditioner plays a great role in promoting hair follicle growth.
The glossy privet fruit is sweet, bitter and cool in taste, is a traditional Chinese medicine for tonifying kidney, nourishing yin, nourishing liver and improving eyesight, can treat diseases such as liver and kidney deficiency, dizziness, tinnitus, early white hair and blurred vision, and can promote the generation of hair melanin and improve the effects of white hair, yellow hair and dry hair after long-term use.
Chuan Xiong, pungent and warm. It is pungent, warm, fragrant and flees in nature, and can go up and down to the vertex, go to the blood sea, go to the skin and bypass the four limbs, and is the qi-flowing medicine in the blood, so it has the actions of activating blood and qi, dispersing wind and alleviating pain, and can promote the subcutaneous blood circulation and improve the hair quality after long-term use.
Dang Gui can activate blood, promote blood circulation, and enhance hairy root and autoimmune function.
The dried ginger is warm in nature and pungent in taste, has the effects of sweating, relieving exterior syndrome, warming middle energizer, arresting vomiting, warming lung, relieving cough, relieving fish and crab toxicity, relieving drug toxicity, promoting subcutaneous blood circulation, dilating blood vessels and promoting hair follicle growth.
The meadowfoam seed oil contains more than 95 percent of long-chain fatty acid with an antioxidant effect, can effectively prolong the shelf life and stability of the product, is an excellent emollient and makes the skin soft and dry. Can be used in combination with other components to exert synergistic antioxidant effect, and protect the activity of effective components in the composition from oxidation to the maximum extent.
Lophatherum gracile of Gramineae belongs to perennial herb. Cold in nature, sweet and bland in flavor, can clear heat, relieve restlessness and induce diuresis, and is mainly used for treating: chest heat, cough, dyspnea, hematemesis, toxic heat, wind, diabetes, etc. The lophatherum gracile leaves are rich in chlorophyll, flavone, phenolic acid compounds, amino acids, manganese, zinc and other trace elements. Can effectively remove active oxygen free radicals in human body and enhance the anti-stress and anti-fatigue capability of the body; the invention uses the lophatherum gracile to remove free radicals, improve the oxidation resistance of hair and delay the anti-aging capability of scalp and hair quality.
Phellinus linteus is known as "forest gold". The sporocarp is slightly bitter in taste, can benefit five internal organs, soften hard mass, expel toxin, stop bleeding and activate blood, has the functions of resisting oxidation stress, resisting bacteria, viruses and aging and promoting the generation of immune cell factors, and can assist in removing grease and bacteria on scalp, delaying the aging of hair quality and moistening the hair quality after long-term use.
The ganoderma lucidum is sweet in nature and taste, has the effects of tonifying qi and soothing nerves, relieving cough and asthma, is rich in nutritional ingredients, mainly contains amino acids, polypeptides, proteins, fungal lysozyme, saccharides, ergosterol, triterpenes, coumarins, volatile oil, stearic acid, benzoic acid, alkaloids, vitamin B2, vitamin C and the like, and has the effects of quickly improving the human immune function and delaying cell aging.
The tremellodon gelatinosum has the advantages of mild nature and sweet taste, has the effects of expelling wind and cold, relaxing muscles and tendons and activating blood circulation, can improve the immunity of a human body, can promote subcutaneous blood circulation, dilate blood vessels and keep hair glossy and elastic.
The mellea armillaria sporophore is sporophore of Armillariella mellea of Eumycota, and has effects of delaying hair aging, preventing and treating scalp angiosclerosis, and moistening skin and hair quality.
Black mulberry, being slightly cold in nature, enters heart, liver and kidney meridians, is a good fruit for nourishing and strengthening, nourishing heart and promoting intelligence. Has effects in replenishing blood, nourishing yin, promoting salivation, quenching thirst, moistening intestine, resisting aging, promoting generation of hair melanin, and improving white hair, yellow hair, and dry hair.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that:
(1) the traditional Chinese medicine hair blackening and conditioning agent disclosed by the invention is reasonable and scientific in compatibility of components, mutually cooperated, has natural nutritional ingredients, can effectively protect hair from being injured, and can effectively improve the hair care effect of the nutritional ingredients in the hair conditioning agent by extracting and separating the essential ingredients in the traditional Chinese medicine. Through repeated tests, the product efficacy can be maximized by the raw material component ratio of the invention. After the hair moistening agent is continuously used for 10-15 days, the hair is gradually blackish, bright, soft and smooth, and after 1 month, dandruff, hair oil and head itch are greatly reduced, so that the hair is bright, glossy and elastic.
(2) The traditional Chinese medicine hair blackening and moistening agent has good penetration promoting capability, can enable active ingredients in the product to penetrate through fur to reach deep skin tissues more quickly, can provide sufficient nutrients for the fur, promotes metabolism, has a better product effect, and has the effects of blackening hair, nourishing hair, protecting hair, moistening and maintaining hair. Meanwhile, all the raw materials provided by the invention are natural in source, green and environment-friendly, do not add preservatives and antibiotics, are mild and not irritate, and accord with the trend of hair care product development.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail below with reference to preferred embodiments. It should be noted, however, that the numerous details set forth in the description are merely for the purpose of providing the reader with a thorough understanding of one or more aspects of the present invention, which may be practiced without these specific details.
The raw materials and equipment used in the invention can be purchased from the market.
Example 1
A traditional Chinese medicine hair blackening and moistening agent is composed of the following raw materials in parts by weight: 35 parts of prepared rehmannia root, 25 parts of prepared fleece-flower root, 26 parts of yerbadetajo herb, 25 parts of gynostemma pentaphylla, 23 parts of glossy privet fruit, 20 parts of ligusticum wallichii, 24 parts of angelica, 6 parts of dried ginger, 10 parts of chingma chinensis seed oil, 8 parts of lophatherum gracile, 8 parts of phellinus igniarius, 5 parts of lucid ganoderma, 7 parts of tuber fleeceflower root, 6 parts of hazel mushroom, 8 parts of gulfweed and 10 parts of black mulberry.
The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent, which comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to 20 meshes, thus obtaining mixed powder for later use;
(3) adding ethanol with the volume concentration of 70 percent which is 18 times the weight of the mixed powder into the mixed powder in the step (2), soaking for 40h at 25 ℃, extracting for 50min at 75 ℃, collecting extract liquor, and concentrating the extract liquor under reduced pressure to obtain concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 5 times of water in a cooking pot for 3 hr, extracting, purifying the extractive solution with macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 80 deg.C water bath for 2 hr while stirring at 170r/min, reflux-filtering with ethanol for 3 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white pond flower seed oil, stirring for 3 hours at the temperature of 60 ℃ and uniformly mixing, wherein the stirring speed is 140r/min, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing under the pressure of 28MPa, filling and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
In the step (2) and the step (4), the microwave sterilization temperature is 90 ℃, the time is 18min, the frequency is 2400MHz, and the power is 7 kw.
Example 2
A traditional Chinese medicine hair blackening and moistening agent is composed of the following raw materials in parts by weight: 20 parts of prepared rehmannia root, 15 parts of prepared fleece-flower root, 22 parts of yerbadetajo herb, 20 parts of gynostemma pentaphylla, 20 parts of glossy privet fruit, 18 parts of ligusticum wallichii, 18 parts of angelica, 5 parts of dried ginger, 5 parts of chingma chinensis seed oil, 6 parts of lophatherum gracile, 5 parts of phellinus igniarius, 3 parts of lucid ganoderma, 5 parts of tuber fleeceflower root, 5 parts of hazel mushroom, 6 parts of gulfweed and 5 parts of black mulberry.
The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent, which comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to 20 meshes, thus obtaining mixed powder for later use;
(3) adding ethanol with volume concentration of 60% which is 15 times of the weight of the mixed powder into the mixed powder in the step (2), soaking at 20 ℃ for 65h, then extracting at 70 ℃ for 40min, collecting extract liquor, and concentrating the extract liquor under reduced pressure to obtain concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 3 times of water in a cooking pot for 4 hr, extracting, subjecting the extractive solution to macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 70 deg.C water bath for 1 hr, stirring at 180r/min, reflux-filtering with ethanol for 4 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white pond flower seed oil, stirring for 3 hours at 70 ℃, uniformly mixing, stirring at the speed of 120r/min, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing under the pressure of 25MPa, filling, and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
In the step (2) and the step (4), the microwave sterilization temperature is 80 ℃, the time is 15min, the frequency is 2200MHz, and the power is 6 kw.
Example 3
A traditional Chinese medicine hair blackening and moistening agent is composed of the following raw materials in parts by weight: 40 parts of prepared rehmannia root, 30 parts of prepared fleece-flower root, 30 parts of yerbadetajo herb, 30 parts of gynostemma pentaphylla, 30 parts of glossy privet fruit, 28 parts of ligusticum wallichii, 28 parts of angelica, 10 parts of dried ginger, 12 parts of chingma chinensis seed oil, 12 parts of lophatherum gracile, 10 parts of phellinus igniarius, 8 parts of lucid ganoderma, 10 parts of tuber fleeceflower root, 10 parts of hazel mushroom, 12 parts of gulfweed and 15 parts of black mulberry.
The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent, which comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to 30 meshes, thus obtaining mixed powder for later use;
(3) adding ethanol with volume concentration of 60% which is 15 times of the weight of the mixed powder into the mixed powder in the step (2), soaking at 20 ℃ for 65h, then extracting at 70 ℃ for 40min, collecting extract liquor, and concentrating the extract liquor under reduced pressure to obtain concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 3 times of water in a cooking pot for 4 hr, extracting, subjecting the extractive solution to macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 70 deg.C water bath for 1 hr, stirring at 180r/min, reflux-filtering with ethanol for 4 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white pond flower seed oil, stirring for 3 hours at 70 ℃, uniformly mixing, stirring at the speed of 120r/min, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing under the pressure of 25MPa, filling, and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
In the step (2) and the step (4), the microwave sterilization temperature is 80 ℃, the time is 15min, the frequency is 2200MHz, and the power is 6 kw.
Example 4
A traditional Chinese medicine hair blackening and moistening agent is composed of the following raw materials in parts by weight: 35 parts of prepared rehmannia root, 25 parts of prepared fleece-flower root, 26 parts of yerbadetajo herb, 25 parts of gynostemma pentaphylla, 23 parts of glossy privet fruit, 20 parts of ligusticum wallichii, 24 parts of angelica, 6 parts of dried ginger, 10 parts of chingma chinensis seed oil, 8 parts of lophatherum gracile, 8 parts of phellinus igniarius, 5 parts of lucid ganoderma, 7 parts of tuber fleeceflower root, 6 parts of hazel mushroom, 8 parts of gulfweed and 10 parts of black mulberry.
The invention also provides a preparation method of the traditional Chinese medicine hair blackening and moistening agent, which comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to 10 meshes, thus obtaining mixed powder for later use;
(3) adding ethanol with the volume concentration of 80 percent which is 20 times the weight of the mixed powder into the mixed powder in the step (2), soaking for 35 hours at the temperature of 28 ℃, extracting for 60 minutes at the temperature of 80 ℃, collecting extract liquor, and concentrating the extract liquor under reduced pressure to obtain concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 6 times of water in a cooking pot for 2 hr, extracting, purifying the extractive solution with macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 85 deg.C water bath for 1 hr, stirring at 180r/min, reflux-filtering with ethanol for 4 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white pond flower seed oil, stirring for 1h at 85 ℃ and uniformly mixing, wherein the stirring speed is 180r/min, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing under the pressure of 25MPa, filling and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
In the step (2) and the step (4), the microwave sterilization temperature is 95 ℃, the time is 20min, the frequency is 2500MHz, and the power is 8 kw.
The application method of the traditional Chinese medicine hair blackening and moistening agent comprises the following steps: cleaning hair, uniformly smearing an appropriate amount of the Chinese medicinal hair blackening and moistening agent from tail to root, gently massaging until the root is reached, standing for 3-5min, wrapping the hair with a bath cap or a hot towel, standing for 15-20min, and washing with warm water. It is recommended to use 1 time every 3 days.
Clinical experiments are carried out on the traditional Chinese medicine hair blackening and moisturizing agent and the sea-fly scurf removing hair conditioner. After the hair conditioner is used for 7 days, the hair conditioner prepared by the embodiment of the invention has better effect than the Haifeisu hair conditioner, after the hair conditioner is continuously used for 10-15 days, the hair is gradually blackish and bright, soft and smooth, and after 1 month, dandruff, hair oil and head itch are greatly reduced, and the hair is bright and glossy and rich in elasticity. The effect of example 2 and example 3 is lower than that of example 1 and example 4, with the conditioner of example 1 being the most effective.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that those skilled in the art can make various improvements and modifications without departing from the principle of the present invention, and these improvements and modifications should also be construed as the protection scope of the present invention.
Claims (6)
1. A traditional Chinese medicine hair blackening and moistening agent is characterized in that: the feed is prepared from the following raw materials in parts by weight: 20-40 parts of prepared rehmannia root, 15-30 parts of prepared fleece-flower root, 22-30 parts of yerbadetajo herb, 20-30 parts of gynostemma pentaphylla, 20-30 parts of glossy privet fruit, 18-28 parts of ligusticum wallichii, 18-28 parts of angelica sinensis, 5-10 parts of dried ginger, 5-12 parts of chinaberry seed oil, 6-12 parts of lophatherum gracile, 5-10 parts of phellinus igniarius, 3-8 parts of lucid ganoderma, 5-10 parts of tuber fleeceflower root, 5-10 parts of mellea armillaria, 6-12 parts of gulfweed and 5-15 parts of black mulberry;
the preparation method of the traditional Chinese medicine hair blackening and conditioning agent comprises the following steps:
(1) weighing the following raw materials in parts by weight: radix rehmanniae Preparata, radix Polygoni Multiflori Preparata, Ecliptae herba, herba Gynostemmatis, fructus Ligustri Lucidi, rhizoma Ligustici Chuanxiong, radix Angelicae sinensis, Zingiberis rhizoma, BAIJIHUA seed oil, folium Bambusae, Phellinus Linteus, Ganoderma, Tremella, Corylus heterophylla, Sargassum, and Mori fructus;
(2) respectively sterilizing the weighed prepared rehmannia root, prepared fleece-flower root, yerbadetajo herb, fiveleaf gynostemma herb, glossy privet fruit, szechuan lovage rhizome and Chinese angelica by microwave, and then feeding the materials into a pulverizer to pulverize the materials to a granularity of 10-30 meshes to obtain mixed powder for later use;
(3) adding ethanol 15-20 times the weight of the mixed powder into the mixed powder in the step (2), soaking at 20-28 ℃ for 35-65h, extracting at 70-80 ℃ for 40-60min, collecting the extract, and concentrating the extract under reduced pressure to obtain a concentrated solution;
(4) cleaning rhizoma Zingiberis, herba Lophatheri, Phellinus Linteus, Ganoderma, Tremella fuciformis, Corylus millettii, Sargassum, and Mori fructus, air drying, microwave sterilizing, pulverizing, decocting in 3-6 times of water for 2-4 hr, separating the extractive solution with macroporous resin column, gradient eluting with ethanol, concentrating the eluate, adding 1/2 weight of white Potentilla chinensis seed oil, heating in 70-85 deg.C water bath for 1-3 hr, stirring, reflux filtering with ethanol for 2-4 times to obtain mixed slurry;
(5) slowly pouring the concentrated solution obtained in the step (2) and the mixed slurry obtained in the step (3) into the residual white chinlon oil, uniformly stirring, sterilizing by a low-temperature instantaneous sterilizer, and then homogenizing, filling and inspecting to be qualified to obtain the traditional Chinese medicine hair blackening and moistening agent.
2. The traditional Chinese medicine hair blackening and conditioning agent according to claim 1, which is characterized in that: the feed is prepared from the following raw materials in parts by weight: 35 parts of prepared rehmannia root, 25 parts of prepared fleece-flower root, 26 parts of yerbadetajo herb, 25 parts of gynostemma pentaphylla, 23 parts of glossy privet fruit, 20 parts of ligusticum wallichii, 24 parts of angelica, 6 parts of dried ginger, 10 parts of chingma chinensis seed oil, 8 parts of lophatherum gracile, 8 parts of phellinus igniarius, 5 parts of lucid ganoderma, 7 parts of tuber fleeceflower root, 6 parts of hazel mushroom, 8 parts of gulfweed and 10 parts of black mulberry.
3. The traditional Chinese medicine hair blackening and conditioning agent according to claim 1, which is characterized in that: in the step (2) and the step (4), the temperature of the microwave sterilization is 80-95 ℃, the time is 15-20min, the frequency is 2200-.
4. The traditional Chinese medicine hair blackening and conditioning agent according to claim 1, which is characterized in that: and (5) slowly adding the concentrated solution and the mixed slurry into the rest of the white Poissa japonica seed oil, stirring for 3-4h at the temperature of 55-70 ℃, and uniformly mixing.
5. The traditional Chinese medicine hair blackening and conditioning agent according to claim 1, which is characterized in that: the volume concentration of the ethanol is 60-80%.
6. The traditional Chinese medicine hair blackening and conditioning agent according to claim 1, which is characterized in that: the homogenizing process is carried out under the pressure condition of 25-30 MPa.
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| CN102772496B (en) * | 2012-07-18 | 2013-09-11 | 赤壁本草药材农民专业合作社 | Folium mori hair blackening particles and preparation method thereof |
| CN103340995A (en) * | 2013-07-19 | 2013-10-09 | 苏州市天灵中药饮片有限公司 | Preparation method of traditional Chinese medicine additive for treating alopecia |
| CN103877549A (en) * | 2014-04-01 | 2014-06-25 | 邓林生 | Hair growth liquid taking fresh gingers as main component |
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