CN105505582A - Lotus leaf and jasmine compound extract fragrance, preparing method of lotus leaf and jasmine compound extract fragrance and toothpaste containing fragrance - Google Patents
Lotus leaf and jasmine compound extract fragrance, preparing method of lotus leaf and jasmine compound extract fragrance and toothpaste containing fragrance Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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Abstract
The invention discloses a lotus leaf and jasmine compound extract fragrance, a preparing method of the lotus leaf and jasmine compound extract fragrance and toothpaste containing the fragrance. The lotus leaf and jasmine compound extract fragrance is characterized by being prepared from, by weight, 29-39 parts of lotus leaf and jasmine compound extract, 20-39 parts of menthol, 20-39 parts of peppermint oil, 0.5-2.5 parts of anise oil and 1.1-2.2 parts of spearmint oil. The lotus leaf and jasmine compound extract is prepared from lotus leaves, jasmine, purified water and alcohol at the weight ratio of (2.1-3.9):(2.1-2.9):(9.1-9.9):(6.1-6.9). According to the lotus leaf and jasmine compound extract fragrance, the preparing method of the lotus leaf and jasmine compound extract fragrance and the toothpaste containing the fragrance fragrance, lotus leaves and jasmine serve as the main raw materials of the lotus leaf and jasmine compound extract, a fresh, sweet and faint aroma is achieved, the oral cavity can diffuse a natural and faint aroma lastingly after the fragrance is applied to the toothpaste, the effects of cooling blood and stopping bleeding, treating toothache, clearing away heat, achieving freshness and the like are achieved, and a more significant treatment effect is achieved on toothache caused by firing, internal heat and excessive fatigue.
Description
Technical field
The present invention relates to consumer goods industries, particularly relate to a kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence.
Background technology
Along with expanding economy and technical progress, the requirement of people to various daily necessities also improves constantly, and especially more focuses on the medical care effect of daily necessities.And toothpaste is requisite part in daily necessities, security, both effectiveness, more graceful, more interesting, better experience sense, all will become the emerging R&D direction of toothpaste.How toothpaste industry rationally applies common Chinese medicinal materials by research tradition Chinese medicine (traditional Chinese medical science), allow human consumer in brushing teeth, enjoy more graceful and more interesting experience sense, and related oral problem can be solved, will the preferential research and development problem of toothpaste industry be become.As the Nobel laureate slaughter cry of a deer once said " Artemisinin find process in, ancient literature research the most critical moment give me inspiration.I believes, makes great efforts exploitation traditional medicine and will bring more medicine to the world.”
Summary of the invention
The object of the invention is: provide a kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence, toothpaste provided by the invention has good therapeutic action for toothache.
For achieving the above object, the invention provides following technical scheme:
A kind of lotus leaf composite jasmine extract essence, comprises the raw material of following weight part: the composite jasmine extract of lotus leaf 29 ~ 39 parts, mentha camphor 20 ~ 39 parts, Peppermint Oil 20 ~ 39 parts, olium anisi 0.5 ~ 2.5 part, Oleum Menthae Rotundifoliae 1.1 ~ 2.2 parts; Described lotus leaf composite jasmine extract is prepared from by the raw material of following weight ratio: lotus leaf: jasmine: pure water: alcohol=2.1 ~ 3.9: 2.1 ~ 2.9: 9.1 ~ 9.9: 6.1 ~ 6.9.
Preferably, the preparation method of a kind of lotus leaf composite jasmine extract essence, comprises the following steps:
(1) be lotus leaf by weight: jasmine: pure water: alcohol=2.1 ~ 3.9: the ratio of 2.1 ~ 2.9: 9.1 ~ 9.9: 6.1 ~ 6.9 soaks 12 ~ 36h by after lotus leaf, jasmine, pure water and alcohol mixing under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.050 ~-0.060MPa in vacuum tightness, temperature is homogeneous 1 ~ 3h under the condition of 50 ~ 60 DEG C, filters to get filtrate and filter residue;
(3) be to concentrate at 10 ~ 20: 1 by volume by filtrate, obtain the composite jasmine extract of lotus leaf;
(4) by proportioning composite to mentha camphor, Peppermint Oil, olium anisi and Oleum Menthae Rotundifoliae and lotus leaf jasmine extract mixed and leave standstill 12 ~ 36h after stirring, obtaining lotus leaf composite jasmine extract essence.
Preferably, in step (3), filtrate is to concentrate at 20: 1 by volume, and thickening temperature is 70 ~ 90 DEG C.
Preferably, in step (4), time of repose is 36h.
Preferably, a kind of toothpaste containing lotus leaf composite jasmine extract essence, comprises the raw material of following weight part: toothpaste main body 96.0 ~ 99.5 parts, 0.5 ~ 4.0 part, lotus leaf composite jasmine extract essence.
Preferably, described toothpaste main body comprises the raw material of following weight part: silicon-dioxide 2 ~ 25 parts, 0.01 ~ 55 part, calcium carbonate, sorbyl alcohol 15 ~ 65 parts, lauryl alcohol sodium sulfovinate 1.5 ~ 3.0 parts, tertiary sodium phosphate 0.1 ~ 0.3 part, Xylo-Mucine 0.5 ~ 1.5 part, titanium dioxide 0.1 ~ 0.5 part, soluble saccharin 0.1 ~ 0.3 part, sodium monoflurophosphate 0.55 ~ 1 part, surplus is pure water, and the total amount of toothpaste main body is 96.0-99.5 part.
Preferably, the preparation method of the described toothpaste containing lotus leaf composite jasmine extract essence, comprises the following steps:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 1 ~ 6min, and Heating temperature is 30 ~ 50 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 10 ~ 15min, and Heating temperature is 50 ~ 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
Beneficial effect of the present invention is: the present invention adds lotus leaf composite jasmine extract essence in toothpaste, and the main raw material of lotus leaf composite jasmine extract essence is lotus leaf and jasmine.Compendium of Material Medica records " dental pain.With Lotus leaf base seven, enriching vinegar one bowl, decocts into half bowl, removes slag, be boiled into cream, wipe tooth constantly, and effectively ", " Chinese Pharmacopoeia " then records lotus leaf " cooling blood for hemostasis, removing blood stasis and hemostasis "." Root of Arabian Jasmine cures mainly: pain relieving; control carious tooth ", " Flower of Arabian Jasmine cures mainly: regulate the flow of vital energy; control sore " is recited as in " Chinese medicine voluminous dictionary ", " Root of Arabian Jasmine cures mainly: analgesia; wound ", " Flower of Arabian Jasmine, leaf cure mainly: relieving superficies by cooling; control conjunctival congestion with pain and swelling of the eye " is recited as in " national herbal medicine compilation ", " Flower of Arabian Jasmine cures mainly: regulating QI to relieve pain ", " leaf of Arabian Jasmine cures mainly: expelling wind to resolve the exterior; swelling and pain relieving ", " Root of Arabian Jasmine cures mainly: anesthesia; pain relieving " is recited as in " China's book on Chinese herbal medicine ", lotus leaf and jasmine are all modal Chinese medicinal materialss, abundance, inexpensive.Lotus leaf and jasmine composite be traditional Chinese medical science traditional classical arranging scheme, except playing the stronger analgesic efficacy of lotus leaf, the herbal mixture system of hemostasis and pain-relieving can also be formed, to toothache, there is good treatment, remission effect.The present invention make toothpaste safely, have no side effect, old and young women and children are all suitable, and life-time service is useful and harmless.
Embodiment
Below in conjunction with the embodiment of the present invention, carry out clear, intactly describe the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 1min, and Heating temperature is 30 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 10min, and Heating temperature is 50 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 15min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 210g (dry lotus leaf, comprises root, leaf, rhizoma nelumbinis, lower same), jasmine 210g (dry jasmine, lower same) mixes with pure water 910g, alcohol 690g, and soak 12h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.060MPa in vacuum tightness, temperature is homogeneous 1h under the condition of 50 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 101g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 29g lotus leaf, and add mentha camphor 20g, Peppermint Oil 39g, olium anisi 2.5g, Oleum Menthae Rotundifoliae 1.1g, leave standstill 12h after stirring, obtain lotus leaf composite jasmine extract essence.
Embodiment 2
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
| Raw material | Weight/g | Raw material | Weight/g |
| Lotus leaf composite jasmine extract essence | 0.95 | Sodium monoflurophosphate | 0.9 |
| Sorbyl alcohol | 20 | Tertiary sodium phosphate | 0.1 |
| Silicon-dioxide | 25 | Xylo-Mucine | 1.4 |
| Lauryl alcohol sodium sulfovinate | 2.5 | Soluble saccharin | 0.3 |
| Titanium dioxide | 0.4 | Pure water | Complement to 100 |
| Calcium carbonate | 0.01 |
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 3min, and Heating temperature is 40 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 11min, and Heating temperature is 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 14min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 230g, jasmine 220g mixes with pure water 920g, alcohol 680g, and soak 24h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.050MPa in vacuum tightness, temperature is homogeneous 2h under the condition of 60 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 121g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 33g lotus leaf, and add mentha camphor 22g, Peppermint Oil 37g, olium anisi 2.3g, Oleum Menthae Rotundifoliae 1.3g, leave standstill 24h after stirring, obtain lotus leaf composite jasmine extract essence.
Embodiment 3
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
| Raw material | Weight/g | Raw material | Weight/g |
| Lotus leaf composite jasmine extract essence | 1.1 | Sodium monoflurophosphate | 0.7 |
| Sorbyl alcohol | 30 | Tertiary sodium phosphate | 0.2 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.0 |
| Lauryl alcohol sodium sulfovinate | 2.0 | Soluble saccharin | 0.2 |
| Titanium dioxide | 0.3 | Pure water | Complement to 100 |
| Calcium carbonate | 0.01 |
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 5min, and Heating temperature is 45 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 12min, and Heating temperature is 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 13min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 260g, jasmine 230g mixes with pure water 930g, alcohol 670g, and soak 24h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.055MPa in vacuum tightness, temperature is homogeneous 3h under the condition of 55 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 135g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 35g lotus leaf, and add mentha camphor 29g, Peppermint Oil 35g, olium anisi 2.1g, Oleum Menthae Rotundifoliae 1.5g, leave standstill 36h after stirring, obtain lotus leaf composite jasmine extract essence.
Embodiment 4
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
| Raw material | Weight/g | Raw material | Weight/g |
| Lotus leaf composite jasmine extract essence | 2.3 | Sodium monoflurophosphate | 0.6 |
| Sorbyl alcohol | 40 | Tertiary sodium phosphate | 0.3 |
| Silicon-dioxide | 18 | Xylo-Mucine | 0.9 |
| Lauryl alcohol sodium sulfovinate | 1.9 | Soluble saccharin | 0.2 |
| Titanium dioxide | 0.2 | Pure water | Complement to 100 |
| Calcium carbonate | 0.01 |
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 6min, and Heating temperature is 50 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 13min, and Heating temperature is 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 12min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 290g, jasmine 260g mixes with pure water 960g, alcohol 650g, and soak 24h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.050MPa in vacuum tightness, temperature is homogeneous 1h under the condition of 50 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 216g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 39g lotus leaf, and add mentha camphor 39g, Peppermint Oil 20g, olium anisi 2.0g, Oleum Menthae Rotundifoliae 1.7g, leave standstill 24h after stirring, obtain lotus leaf composite jasmine extract essence.
Embodiment 5
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
| Raw material | Weight/g | Raw material | Weight/g |
| Lotus leaf composite jasmine extract essence | 3.0 | Sodium monoflurophosphate | 0.55 |
| Sorbyl alcohol | 55 | Tertiary sodium phosphate | 0.2 |
| Silicon-dioxide | 15 | Xylo-Mucine | 0.7 |
| Lauryl alcohol sodium sulfovinate | 1.8 | Soluble saccharin | 0.1 |
| Titanium dioxide | 0.3 | Pure water | Complement to 100 |
| Calcium carbonate | 0.01 |
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 5min, and Heating temperature is 50 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 14min, and Heating temperature is 50 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 11min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 350g, jasmine 270g mixes with pure water 970g, alcohol 630g, and soak 12h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.055MPa in vacuum tightness, temperature is homogeneous 3h under the condition of 50 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 196g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 35g lotus leaf, and add mentha camphor 36g, Peppermint Oil 25g, olium anisi 1.9g, Oleum Menthae Rotundifoliae 1.9g, leave standstill 12h after stirring, obtain lotus leaf composite jasmine extract essence.
Embodiment 6
A kind of lotus leaf composite jasmine extract essence and preparation method thereof and the toothpaste containing this essence:
The composition and ratio of toothpaste is as following table (in 100g)
| Raw material | Weight/g | Raw material | Weight/g |
| Lotus leaf composite jasmine extract essence | 4.0 | Sodium monoflurophosphate | 0.55 |
| Sorbyl alcohol | 65 | Tertiary sodium phosphate | 0.1 |
| Silicon-dioxide | 25 | Xylo-Mucine | 0.5 |
| Lauryl alcohol sodium sulfovinate | 1.5 | Soluble saccharin | 0.1 |
| Titanium dioxide | 0.1 | Pure water | Complement to 100 |
| Calcium carbonate | 0.01 |
The concrete preparation process of toothpaste is as follows:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 6min, and Heating temperature is 50 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 15min, and Heating temperature is 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, stir 10min under mixing final vacuum, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
In the present embodiment, described lotus leaf composite jasmine extract essence, its preparation method is as follows:
(1) get lotus leaf 390g, jasmine 290g mixes with pure water 990g, alcohol 610g, and soak 36h under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.060MPa in vacuum tightness, temperature is homogeneous 3h under the condition of 60 DEG C, filters to get filtrate and filter residue;
(3) filtrate is concentrated into 114g, obtains the composite jasmine extract of lotus leaf;
(4) take the composite jasmine extract of 39g lotus leaf, and add mentha camphor 39g, Peppermint Oil 20g, olium anisi 2.5g, Oleum Menthae Rotundifoliae 1.1g, leave standstill 36h after stirring, obtain lotus leaf composite jasmine extract essence.
Comparative example 1
Comparative example 1 is only with the difference of embodiment any one of above-described embodiment 1-6, does not add lotus leaf composite jasmine extract essence, other component and content (supplying less than 100g pure water) same as the previously described embodiments when preparing toothpaste.
Clinical trial result
Test method: choose and there is toothache symptom experimenter 96 people test, each half of men and women, the age from 30 ~ 60 years old, 45 years old mean age.Be divided into 2 groups at random, experimental group uses the toothpaste (being added with lotus leaf composite jasmine extract essence) that any one of above-described embodiment 1-6 item prepared by embodiment, the toothpaste (not adding lotus leaf composite jasmine extract essence) that control group uses comparative example 6 to prepare, every morning, evening respectively brush teeth once (brushes teeth general lasting three minutes at every turn, general 3 grams of toothpaste dosage, brushes teeth with the warm water of 29-39 DEG C).
Brush teeth before test, first unification is checked and is recorded the toothache symptom of experimenter.
To brush teeth test the 15th day, then the toothache symptom variation of unified inspection experimenter.
Criterion: after test of brushing teeth, experimenter's toothache alleviates or eliminates and is effectively, otherwise, unchanged or have a toothache add severe one be all considered as invalid.
Inspection in the 15th day after experimenter uses, result is as follows:
From the assay of experimenter, the present invention make containing the toothpaste of lotus leaf composite jasmine extract essence, for ease toothache efficient be 89.58%, be all obviously better than the statistic data of control group.Therefore, the toothpaste containing lotus leaf composite jasmine extract essence of the present invention, has good prevention and therapy effect for toothache.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (7)
1. a lotus leaf composite jasmine extract essence, is characterized in that: the raw material comprising following weight part: the composite jasmine extract of lotus leaf 29 ~ 39 parts, mentha camphor 20 ~ 39 parts, Peppermint Oil 20 ~ 39 parts, olium anisi 0.5 ~ 2.5 part, Oleum Menthae Rotundifoliae 1.1 ~ 2.2 parts; Described lotus leaf composite jasmine extract is prepared from by the raw material of following weight ratio: lotus leaf: jasmine: pure water: alcohol=2.1 ~ 3.9: 2.1 ~ 2.9: 9.1 ~ 9.9: 6.1 ~ 6.9.
2. a preparation method for lotus leaf composite jasmine extract essence, is characterized in that: comprise the following steps:
(1) be lotus leaf by weight: jasmine: pure water: alcohol=2.1 ~ 3.9: the ratio of 2.1 ~ 2.9: 9.1 ~ 9.9: 6.1 ~ 6.9 soaks 12 ~ 36h by after lotus leaf, jasmine, pure water and alcohol mixing under the condition of normal temperature, normal pressure;
(2), after immersion terminates, make soak solution be-0.050 ~-0.060MPa in vacuum tightness, temperature is homogeneous 1 ~ 3h under the condition of 50 ~ 60 DEG C, filters to get filtrate and filter residue;
(3) be to concentrate at 10 ~ 20: 1 by volume by filtrate, obtain the composite jasmine extract of lotus leaf;
(4) by proportioning composite to mentha camphor, Peppermint Oil, olium anisi and Oleum Menthae Rotundifoliae and lotus leaf jasmine extract mixed and leave standstill 12 ~ 36h after stirring, obtaining lotus leaf composite jasmine extract essence.
3. the preparation method of lotus leaf according to claim 2 composite jasmine extract essence, is characterized in that: in step (3), and filtrate is to concentrate at 20: 1 by volume, and thickening temperature is 70 ~ 90 DEG C.
4. the preparation method of lotus leaf according to claim 2 composite jasmine extract essence, is characterized in that: in step (4), and time of repose is 36h.
5. the toothpaste containing lotus leaf composite jasmine extract essence, is characterized in that: the raw material comprising following weight part: toothpaste main body 96.0 ~ 99.5 parts, 0.5 ~ 4.0 part, lotus leaf composite jasmine extract essence.
6. the toothpaste containing lotus leaf composite jasmine extract essence according to claim 5, it is characterized in that: described toothpaste main body comprises the raw material of following weight part: silicon-dioxide 2 ~ 25 parts, 0.01 ~ 55 part, calcium carbonate, sorbyl alcohol 15 ~ 65 parts, lauryl alcohol sodium sulfovinate 1.5 ~ 3.0 parts, tertiary sodium phosphate 0.1 ~ 0.3 part, Xylo-Mucine 0.5 ~ 1.5 part, titanium dioxide 0.1 ~ 0.5 part, soluble saccharin 0.1 ~ 0.3 part, sodium monoflurophosphate 0.55 ~ 1 part, surplus is pure water, and the total amount of toothpaste main body is 96.0-99.5 part.
7. the preparation method of the toothpaste containing lotus leaf composite jasmine extract essence according to claim 6, is characterized in that: comprise the following steps:
(1) lauryl alcohol sodium sulfovinate is dissolved in the water, forms mixture D 1;
(2) Xylo-Mucine is scattered in silicon-dioxide, calcium carbonate, forms mixture D 2;
(3) heat after tertiary sodium phosphate, soluble saccharin, titanium dioxide, sodium monoflurophosphate and mixture D 1 being mixed, heat-up time is 1 ~ 6min, and Heating temperature is 30 ~ 50 DEG C, forms mixture D 3;
(4) heat after being mixed with mixture D 2 by sorbyl alcohol, heat-up time is 10 ~ 15min, and Heating temperature is 50 ~ 55 DEG C, forms mixture D 4;
(5) mixture D 3, D4 being added in emulsification pot and to add lotus leaf composite jasmine extract essence, make lotion, gained lotion is the toothpaste containing lotus leaf composite jasmine extract essence.
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| CN113384492A (en) * | 2021-06-04 | 2021-09-14 | 上海应用技术大学 | Cool and refreshing mint-flavored toothpaste essence and preparation method thereof |
| CN113444574A (en) * | 2021-07-03 | 2021-09-28 | 广州芬豪香精有限公司 | Preparation method of water-soluble essence |
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