CN103468402A - Essence containing natural snow pear extract and preparation method of toothpaste - Google Patents
Essence containing natural snow pear extract and preparation method of toothpaste Download PDFInfo
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- CN103468402A CN103468402A CN2013103599890A CN201310359989A CN103468402A CN 103468402 A CN103468402 A CN 103468402A CN 2013103599890 A CN2013103599890 A CN 2013103599890A CN 201310359989 A CN201310359989 A CN 201310359989A CN 103468402 A CN103468402 A CN 103468402A
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Abstract
The invention relates to an oral cleaning supply, and particularly relates to en essence containing a natural snow pear extract and preparation method of toothpaste. A preparation method of the essence containing the natural snow pear extract comprises the steps: weighing snow pears, ethanol and purified water to mix, soaking under a negative pressure condition, then heating, decocting and filtering to obtain a filtrate and a filter residue; decolouring the filtrate, and concentrating to obtain a snow pear extract; and after stirring evenly natural menthol, oleum menthae dementholatum, clove oil, eugenol, spearmint oil, ethyl butyrate, lemon oil, geraniol and the snow pear extract, standing to obtain the natural snow pear extract essence. The prepared natural snow pear extract essence has efficacies of moistening lungs, cooling heart, dissolving phlegm, reducing pathogenic-fire and removing toxicity. The prepared natural snow pear extract essence toothpaste can play roles in reducing pathogenic-fire, removing toxicity, removing halitosis and the like, and especially has a good relieving effect in allusion to oral lit and halitosis. Because the main ingredient is the natural extract, the toothpaste has the functions of reducing pathogenic-fire, removing toxicity and removing halitosis, and has no any side effects. At the same time, the toothpaste is suitable for the young, the old, women and children, and has benefits instead of harm for long-term using.
Description
Technical field
The present invention relates to dental care products, specifically relate to a kind of essence that contains the natural snow Fructus Pyri extract and toothpaste preparation method.
Background technology
Toothpaste is to be used from cleaning teeth with toothbrush one, the protection oral hygiene, and a kind of daily necessities to human-body safety, have very long history.Along with social progress, various types of toothpaste is come out one after another, and natural extract is applied in toothpaste and solves relevant oral problem, has become market mainstream focus.
The tender Bai Ruxue of snow pear meat, distinguish the flavor of sweet cold in nature, containing oxysuccinic acid, citric acid, VITMAIN B1, B2, C, carotene etc., tool promote the production of body fluid moisturize, the effect of removing heat-phlegm, be particularly suitable for autumn edible.The Compendium of Material Medica record, the pears person, also, its property is descending fluent for profit.It is medicinal can control wind-heat, moistening lung, the cool heart, dissolving phlegm, fall fire, removing toxic substances.Modern medicine study proves, pears truly have that moistening lung is dry clearly, relieving cough and reducing sputum, the effect of nourishing blood and promoting granulation.Therefore the throat patient of acute tracheitis and upper respiratory tract infection occurred does, itches, bitterly, thick, the constipation of hoarsen, phlegm, urine are red that good effect all arranged.Pears have again and reduce blood pressure and the effect of replenishing YIN and removing heat, so hypertension, hepatitis, that patient with liver cirrhosis is often eaten pears is beneficial.Pears can be eaten something rare, and also can steam, and can also make soup and custard.But Cangxi snow pear pears are cold in nature, once should not eat more.Especially insufficiency of spleen-YANG, belly crymodynia and deficiency of blood person, cannot eat more.
Summary of the invention
One of purpose of the present invention is to provide the natural snow Fructus Pyri extract essence and preparation method thereof that a kind ofly has moistening lung, the cool heart, dissolving phlegm, falls the effect of fire, removing toxic substances.
In order to realize this purpose, the technical solution adopted in the present invention is: a kind of preparation method of natural snow Fructus Pyri extract essence comprises the steps:
1., taking is snow pear by weight proportion: ethanol: pure water=0.95～1.55: 0.5～0.95: 3.7～6.5 raw material;
2., snow pear, ethanol, pure water are mixed, be-0.050 in vacuum tightness～-soak 36～48h under the condition of 0.060MPa, reheat decoction 1～2h, filter to get filtrate and filter residue;
3., by filtrate decolouring, and (for example, before concentrated, be 80～120L, concentrated then be 1L) concentrated to be by volume 80～120: 1, obtains the snow pear extract;
4., according to the weight part meter, 10～15 parts of 18～25 parts of Natural menthols, 30～36 parts of Peppermint Oils, 0.8～1.2 part of Syzygium aromaticum stem oil, 0.4～0.6 part of Eugenol, 0.5～1 part of Oleum Menthae Rotundifoliae, 0.4～0.6 part of ethyl butyrate, 0.4～0.6 part of lemon oil, 0.2～0.4 part of Geraniol and snow pear extracts are stirred, standing 12～36h, obtain natural snow Fructus Pyri extract essence.
Preferably, described step 1. in the volumn concentration of ethanol be 40～75%.
Preferably, described step 2. middle decocting time is 1.5h, and decocting temperature is 65～80 ℃.
Preferably, described step is concentrated in 3. is to carry out at 100: 1 by volume, and thickening temperature is 70～100 ℃.
Preferably, described step 4. in time of repose be 24h.
In addition, the invention also discloses a kind of natural snow Fructus Pyri extract essence according to the described preparation of above-mentioned preparation method.
Another object of the present invention is to provide a good drug efficacy, without any side effects, can play effects such as falling fire, removing toxic substances, antihalitosis, get angry for oral cavity especially and halitosis has the toothpaste of good remission effect.
In order to realize this purpose, the technical solution adopted in the present invention is: the toothpaste that contains natural snow Fructus Pyri extract essence, the natural snow Fructus Pyri extract essence that to contain weight ratio in its lotion total composition be 1.5～2.5%.
As a kind of preferred implementation of the toothpaste that contains natural snow Fructus Pyri extract essence of the present invention, this toothpaste also comprises following component:
Three of purpose of the present invention is to provide a kind of preparation method of this toothpaste, comprises the steps:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, heat 5～10min, form mixture D 3;
D, sorbyl alcohol is mixed with mixture D 2, heat 5～10min, form mixture D 4;
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 3～5min, make lotion, be filled into multiple-unit tube.
Preferably, described step c Heating temperature is 50～70 ℃, and the steps d Heating temperature is 60～70 ℃.
The essence that the present invention contains the natural snow Fructus Pyri extract and toothpaste preparation method, its beneficial effect shows:
1, the natural snow Fructus Pyri extract essence prepared has moistening lung, the cool heart, dissolving phlegm, falls the effect of fire, removing toxic substances.
2, the toothpaste that contains natural snow Fructus Pyri extract essence of preparation, can play effects such as falling fire, removing toxic substances, antihalitosis, for oral cavity, gets angry especially and halitosis has good remission effect.Because main component is natural extract, there is natural fire, removing toxic substances, the bad breath expelling function of falling, without any side effects.Simultaneously, old and young women and children are all suitable, and life-time service is useful and harmless.
3, the manufacture craft of toothpaste is simple, is applicable to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated, it should be noted that, various raw materials are the delicatessen food level, or obtain according to the prior art preparation.
Embodiment 1
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 388g (fresh snow pear, lower with), 70% ethanol 268g and pure water 1625g mix, and under the condition that is-0.050MPa in vacuum tightness, soak 48h.
2., be heated to 75 ℃ and decoct 1.5h, filter to get filtrate and filter residue.
3., by filtrate with gac (weight percent is not higher than 5%) decolouring, 100 ℃ of constant temperature are concentrated into 20g snow pear extract.
4., add Natural menthol 33g, Peppermint Oil 48g, Syzygium aromaticum stem oil 1.6g, Eugenol 0.8g, Oleum Menthae Rotundifoliae 1.3g, ethyl butyrate 0.8g, lemon oil 0.8g and Geraniol 0.5g in the snow pear extract, stir, standing 24h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table (in 100g, lower same)
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 2.5 | Sodium monoflurophosphate | 1 |
| Sorbyl alcohol | 70 | Tertiary sodium phosphate | 0.35 |
| Silicon-dioxide | 21 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 50 ℃ of heating 10min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,70 ℃ of heating 10min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 5min, make lotion, be filled into multiple-unit tube.
Embodiment 2
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 368g, 65% ethanol 250g and pure water 1500g mixes, soak 45h under the condition that is-0.060MPa in vacuum tightness.
2., be heated to 80 ℃ and decoct 2h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 95 ℃ of constant temperature are concentrated into 19g snow pear extract.
4., add Natural menthol 31g, Peppermint Oil 46g, Syzygium aromaticum stem oil 1.5g, Eugenol 0.8g, Oleum Menthae Rotundifoliae 1.2g, ethyl butyrate 0.8g, lemon oil 0.8g and Geraniol 0.5g in the snow pear extract, stir, stir, standing 18h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 2.1 | Sodium monoflurophosphate | 0.9 |
| Sorbyl alcohol | 68 | Tertiary sodium phosphate | 0.35 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 60 ℃ of heating 7min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,65 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 4min, make lotion, be filled into multiple-unit tube.
Embodiment 3
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 350g, 60% ethanol 240g and pure water 1400g mixes, soak 40h under the condition that is-0.060MPa in vacuum tightness.
2., be heated to 75 ℃ and decoct 1h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 90 ℃ of constant temperature are concentrated into 18g snow pear extract.
4., add Natural menthol 30g, Peppermint Oil 43g, Syzygium aromaticum stem oil 1.4g, Eugenol 0.7g, Oleum Menthae Rotundifoliae 1.3g, ethyl butyrate 0.7g, lemon oil 0.7g and Geraniol 0.5g in the snow pear extract, stir, standing 30h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 1.8 | Sodium monoflurophosphate | 0.8 |
| Sorbyl alcohol | 67 | Tertiary sodium phosphate | 0.35 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 65 ℃ of heating 5min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,60 ℃ of heating 10min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 3min, make lotion, be filled into multiple-unit tube.
Embodiment 4
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 320g, 50% ethanol 230g and pure water 1300g mixes, soak 38h under the condition that is-0.050MPa in vacuum tightness.
2., be heated to 65 ℃ and decoct 1h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into 17g snow pear extract.
4., add Natural menthol 28g, Peppermint Oil 41g, Syzygium aromaticum stem oil 1.4g, Eugenol 0.7g, Oleum Menthae Rotundifoliae 1.1g, ethyl butyrate 0.7g, lemon oil 0.7g and Geraniol 0.4g in the snow pear extract, stir, standing 12h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 1.7 | Sodium monoflurophosphate | 0.7 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.2 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 70 ℃ of heating 8min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,70 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 3min, make lotion, be filled into multiple-unit tube.
Embodiment 5
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 300g, 45% ethanol 210g and pure water 1250g mixes, soak 37h under the condition that is-0.055MPa in vacuum tightness.
2., be heated to 70 ℃ and decoct 2h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into 16g snow pear extract.
4., add Natural menthol 26g, Peppermint Oil 38g, Syzygium aromaticum stem oil 1.2g, Eugenol 0.6g, Oleum Menthae Rotundifoliae 1g, ethyl butyrate 0.6g, lemon oil 0.6g and Geraniol 0.4g in the snow pear extract, stir, standing 36h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 1.6 | Sodium monoflurophosphate | 0.6 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.15 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 55 ℃ of heating 5min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,60 ℃ of heating 8min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 4min, make lotion, be filled into multiple-unit tube.
Embodiment 6
1, the preparation of natural snow Fructus Pyri extract essence
1., get snow pear 280g, 40% ethanol 190g and pure water 1100g mixes, soak 36h under the condition that is-0.055MPa in vacuum tightness.
2., be heated to 75 ℃ and decoct 1.5h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into 15g snow pear extract.
4., add Natural menthol 25g, Peppermint Oil 36g, Syzygium aromaticum stem oil 1.2g, Eugenol 0.6g, Oleum Menthae Rotundifoliae 1g, ethyl butyrate 0.6g, lemon oil 0.6g and Geraniol 0.4g in the snow pear extract, stir, standing 25h, obtain natural snow Fructus Pyri extract essence.
The preparation of the toothpaste that 2, contains natural snow Fructus Pyri extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural snow Fructus Pyri extract essence | 1.5 | Sodium monoflurophosphate | 0.55 |
| Sorbyl alcohol | 50 | Tertiary sodium phosphate | 0.1 |
| Silicon-dioxide | 21 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 65 ℃ of heating 9min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,65 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 5min, make lotion, be filled into multiple-unit tube.
The comparative example 1
Only be with the difference of embodiment 1, do not add natural snow Fructus Pyri extract essence while preparing toothpaste, other component and content identical with embodiment 1 (not enough 100g supplies with pure water).
Clinical trial result
Test method: choose and have that get angry in oral cavity, halitosis symptom experimenter 90 people are tested, men and women each half, the age is from 18～59 years old, 30 years old mean age.Be divided at random 2 groups, experimental group is used the toothpaste (being added with natural snow Fructus Pyri extract essence) of embodiment 1 preparation, control group is used the toothpaste (not adding natural snow Fructus Pyri extract essence) of comparative example's 1 preparation, and every morning, evening respectively brush teeth once.
Brush teeth before test, get angry in the oral cavity of first recording the experimenter, the halitosis symptom.
Brush teeth test after the 7th day, then get angry in unified check experimenter's oral cavity, the halitosis symptom variation.
Criterion: after the test of brushing teeth, subject oral cavity get angry reduce or eliminate, halitosis alleviates or eliminates be effective, otherwise, unchanged or oral cavity get angry increase and halitosis add severe one all be considered as invalid.
Check after the experimenter uses seven days, result is as follows:
From experimenter's assay, the toothpaste that contains natural snow Fructus Pyri extract essence of the present invention, for alleviating, the oral cavity symptom of getting angry is efficient 73.3%, for alleviating the halitosis symptom efficient, is 82.2%, all obviously is better than the statistic data of control group.Therefore, the toothpaste that contains natural snow Fructus Pyri extract essence of the present invention, for oral cavity get angry, halitosis all has good prevention and result for the treatment of.
Above content is only that the present invention is conceived to example and explanation; affiliated those skilled in the art make various modifications to described specific embodiment or supplement or adopt similar mode to substitute; only otherwise depart from the design of invention or surmount this scope as defined in the claims, all should belong to protection scope of the present invention.
Claims (10)
1. the preparation method of a natural snow Fructus Pyri extract essence, is characterized in that comprising the steps:
1., taking is snow pear by weight proportion: ethanol: pure water=0.95～1.55: 0.5～0.95: 3.7～6.5 raw material;
2., snow pear, ethanol, pure water are mixed, be-0.050 in vacuum tightness～-soak 36～48h under the condition of 0.060MPa, reheat decoction 1～2h, filter to get filtrate and filter residue;
3., by filtrate decolouring, and concentrated at 80～120: 1, obtain the snow pear extract;
4., according to the weight part meter, 10～15 parts of 18～25 parts of Natural menthols, 30～36 parts of Peppermint Oils, 0.8～1.2 part of Syzygium aromaticum stem oil, 0.4～0.6 part of Eugenol, 0.5～1 part of Oleum Menthae Rotundifoliae, 0.4～0.6 part of ethyl butyrate, 0.4～0.6 part of lemon oil, 0.2～0.4 part of Geraniol and snow pear extracts are stirred, standing 12～36h, obtain natural snow Fructus Pyri extract essence.
2. the preparation method of natural snow Fructus Pyri extract essence according to claim 1, is characterized in that, the described step 1. volumn concentration of middle ethanol is 40～75%.
3. the preparation method of natural snow Fructus Pyri extract essence according to claim 1, is characterized in that, described step 2. middle decocting time is 1.5h, and decocting temperature is 65～80 ℃.
4. the preparation method of natural snow Fructus Pyri extract essence according to claim 1, is characterized in that, described step is concentrated in 3. is to carry out at 100: 1 by volume, and thickening temperature is 70～100 ℃.
5. the preparation method of natural snow Fructus Pyri extract essence according to claim 1, is characterized in that, described step 4. middle time of repose is 24h.
6. the natural snow Fructus Pyri extract essence prepared as preparation method as described in claim 1～5 any one.
7. one kind contains the toothpaste of natural snow Fructus Pyri extract essence as claimed in claim 6, it is characterized in that, the natural snow Fructus Pyri extract essence that to contain weight ratio in the lotion of toothpaste total composition be 1.5～2.5%.
8. the toothpaste that contains natural snow Fructus Pyri extract essence according to claim 7, is characterized in that, also comprises following component:
9. the preparation method of toothpaste as claimed in claim 8, is characterized in that, comprises the steps:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, heat 5～10min, form mixture D 3;
D, sorbyl alcohol is mixed with mixture D 2, heat 5～10min, form mixture D 4;
E, mixture D 3, D4 are added in the emulsification pot, add natural snow Fructus Pyri extract essence and mix, under vacuum, stir 3～5min, make lotion, be filled into multiple-unit tube.
10. preparation method according to claim 9, is characterized in that, described step c Heating temperature is 50～70 ℃, and the steps d Heating temperature is 60～70 ℃.
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| CN106974845A (en) * | 2017-03-21 | 2017-07-25 | 广州满庭芳实业有限公司 | Essence combination and preparation method and application |
| CN107365629A (en) * | 2017-09-05 | 2017-11-21 | 德利宝(广州)香料有限公司 | A kind of spearmint oil bay extract essence and preparation method and toothpaste and preparation method containing the essence |
| CN108553398A (en) * | 2018-06-14 | 2018-09-21 | 王建林 | A kind of snow pear juice, the mothproof strong tooth whitening toothpaste of cider nutrition and preparation method |
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| CN107365629A (en) * | 2017-09-05 | 2017-11-21 | 德利宝(广州)香料有限公司 | A kind of spearmint oil bay extract essence and preparation method and toothpaste and preparation method containing the essence |
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