CN105055038A - Toothpick capable of undergoing irreversible discoloration and preparation method thereof - Google Patents

Toothpick capable of undergoing irreversible discoloration and preparation method thereof Download PDF

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Publication number
CN105055038A
CN105055038A CN201510536866.9A CN201510536866A CN105055038A CN 105055038 A CN105055038 A CN 105055038A CN 201510536866 A CN201510536866 A CN 201510536866A CN 105055038 A CN105055038 A CN 105055038A
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China
Prior art keywords
toothpick
indicative
cream
oleum camelliae
agent
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CN201510536866.9A
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Chinese (zh)
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不公告发明人
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Foshan Hecai Technology Service Co Ltd
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Foshan Hecai Technology Service Co Ltd
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Priority to CN201510536866.9A priority Critical patent/CN105055038A/en
Publication of CN105055038A publication Critical patent/CN105055038A/en
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Abstract

Provided are a toothpick capable of undergoing irreversible discoloration and a preparation method thereof. At least one of the two ends of the toothpick is provided with an indicative hemostasis layer, and the surface of the toothpick is provided with a tea seed oil composite coating. The indicative hemostasis layer is formed by coating and solidification of indicative hemostasis cream. The indicative hemostasis cream comprises 30-50% of chitosan, 1-1.5% of compound silicate, 5-10% of borneol, 10-15% of tea saponin, 10-15% of petal leaching agent, 1-3% of preservative, 0.5-1 part of fragrance and 20-30% of solvent. The toothpick capable of undergoing irreversible discoloration has good antibacterial effect prior to use, the problem that the toothpick is subjected to bacterial pollution when unused is solved, the toothpick undergoes irreversible discoloration after use, the cross infection is avoided, the used indicative hemostasis cream and a tea seed oil composite spraying agent are easy to prepare and can be processed easily and coat the surface of the toothpick.

Description

A kind ofly there is toothpick of irreversible variable color and preparation method thereof
Technical field
The present invention relates to article of everyday use technical field, particularly relate to and a kind of toothpick of irreversible variable color and preparation method thereof occurs.
Background technology
Common toothpick is clavas that are bamboo, wooden or plastics, wherein having one or two end for most advanced and sophisticated, during for picking one's teeth, toothpick tip being stretched into teeth space, the residue in teeth space can be rejected.One toothpick, may conceal tens thousand of antibacterials, easily illness finds its way in by the mouth, such as the disease such as hepatitis B, pulmonary tuberculosis.By 2012, Chinese Consumers' Association issued warning of consumption and says, the toothpick that domestic restaurant is equipped with is many is " three nothings " products, its sanitary condition is very troubling, surface bacteria content often severe overweight, increases the risk that user periodontal disease is ill, and country is not yet for relevant criterion worked out by toothpick.Especially some illegal businessmans, can carry out collection reclaiming to the toothpick after use and produce, there is huge risk in its safe and sanitary.Therefore the current toothpick in the urgent need to there is irreversible variable color after a kind of use is avoided or prevents the pernicious recovery of illegal businessman.
Summary of the invention
The object of the invention is to propose a kind of toothpick that irreversible variable color occurs, self have good fungistatic effect before using, avoid toothpick when not using by germ contamination, use backteeth signs and issues raw irreversible variable color, avoid cross infection, also can avoid the recovery of illegal businessman simultaneously.
Another object of the present invention is to propose a kind of preparation method that the toothpick of irreversible variable color occurs, and the preparation of its indicative hemostasis cream used and the agent of Oleum Camelliae composite spraying is simple and easy, and easily processing is coated to toothpick surface.
For reaching this object, the present invention by the following technical solutions:
A toothpick for irreversible variable color occurs, and in the two ends of described toothpick, at least one end is provided with indicative hemostatic layer, and the surface of described toothpick is provided with Oleum Camelliae composite coating;
Wherein, described indicative hemostatic layer is applied to solidify by indicative hemostasis cream and is formed, and the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent;
The raw material of described Oleum Camelliae composite coating comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
Further description, described petal leachate is the leachate of Flos Chrysanthemi or Flos Rosae Rugosae.
Further description, described adjusting agent is made up of essence and binding agent, and wherein, described essence is menthol, and described binding agent is sodium carboxymethyl cellulose or edible Gelatinum oxhide.
Further description, described emulsifying agent is sucrose ester.
Further description, described antiseptic is sodium benzoate.
Further description, described ethanol is anhydrous edible ethanol.
Further description, described toothpick is provided with one end of described indicative hemostatic layer, and it is signed body side surface and is provided with slot or position, hole, and described slot or position, described hole are for holding described indicative hemostasis cream.
Further description, the thickness of described indicative hemostatic layer is 0.1-1mm.
Further description, above-mentioned a kind of preparation method that the toothpick of irreversible variable color occurs, comprises the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick;
B, apply indicative hemostasis cream in any one end of the label body of toothpick or its two ends;
C, treat that the cream that step applies solidifies;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, carry out dry sterilization in high pressure vacuum drying equipment, and final acquisition has the toothpick of Oleum Camelliae composite coating.
Further description, the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
Further description, the preparation of described Oleum Camelliae composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain the agent of Oleum Camelliae composite spraying for subsequent use.
A kind of beneficial effect that the toothpick of irreversible variable color occurs of the present invention: self have good fungistatic effect before 1, using, avoids toothpick when not using by germ contamination; 2, use backteeth to sign and issue raw irreversible variable color, avoid cross infection, also can avoid the recovery of illegal businessman; 3, gingiva is had to hemostasis, repairs effect; 3, improve the brightness on toothpick surface, reject the bamboo woody flavour road of wooden toothpick self.
A kind of beneficial effect that the preparation method of the toothpick of irreversible variable color occurs of the present invention: 1, operation sequence is fast and simple; 2, the preparation of its indicative hemostasis cream used and the agent of Oleum Camelliae composite spraying is simple and easy, and easily processing is coated to toothpick surface.
Accompanying drawing explanation
Fig. 1 is the structural representation of one embodiment of the present of invention;
Fig. 2 is the structural representation of one embodiment of the present of invention;
Fig. 3 is the structural representation of the toothpick label body of one embodiment of the present of invention;
Fig. 4 is the partial enlargement structural representation of Fig. 3;
Fig. 5 is the structural representation of the toothpick label body of one embodiment of the present of invention.
Wherein: toothpick 1, toothpick end 11,12, indicative hemostatic layer 2, Oleum Camelliae composite coating 3, slot 101, position, hole 102.
Detailed description of the invention
Technical scheme of the present invention is further illustrated below in conjunction with accompanying drawing and specific embodiment.
As Figure 1-5, a kind of toothpick that irreversible variable color occurs, in the two ends 11,12 of described toothpick 1, at least one end is provided with indicative hemostatic layer 2, and the surface of described toothpick 1 is provided with Oleum Camelliae composite coating 3;
Wherein, described indicative hemostatic layer 2 is applied to solidify by indicative hemostasis cream and is formed, and the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent;
The raw material of described Oleum Camelliae composite coating 3 comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
The present invention is provided with indicative hemostatic layer 2 in toothpick either end, make user use toothpick pick one's teeth scratch because of carelessness time, soluble hemostyptic in its indicative hemostatic layer 2 becomes the dissolving by oral cavity endocrine liquid to be dissolved in gingival surface, injured surface is repaired, the bleeding state of effective this injury region of prevention, and in conjunction with the Oleum Camelliae antioxidant content in Oleum Camelliae composite coating 3, injury region is repaired, detumescence, pain relieving, life-time service significantly can improve the tissue on gingiva top layer, in addition, the interpolation of petal leachate makes cream frost, under PH is less than the environment of 7.1, irreversible variable color can occur, PH scope in human oral cavity is at 6.6-7.1, the toothpick divided with indicative hemostatic layer is when user uses, affect by the intraoral sour environment of user, there is the change of irreversible color in its end, when toothpick is positioned over desktop after using, other user can be avoided to use used toothpick because of carelessness, avoid cross infection, in addition, illegal businessman is also effectively avoided to recycle the toothpick after use.
Oleum Camelliae composite coating is arranged at the surface of toothpick 1, its Oleum Camelliae and ethanol form main antibacterial bacteriostatic protective layer on the surface of toothpick 1, toothpick 1 is made to store in put procedure the impact reduced by outside unhygienic environment, can be on the defensive to the antibacterial staying in its surface or kill, reduce the quantity of toothpick 1 surface bacteria greatly, wholesomeness when effective raising toothpick 1 is deposited, in addition, the setting of Oleum Camelliae composite coating 3 effectively can improve the brightness on toothpick 1 surface, change the lacklustre characteristic on wooden toothpick surface, in conjunction with the fragrance that Oleum Camelliae carries, eliminate the taste of the bamboo wood of wooden toothpick self.
The present invention is using chitosan as main hemostatic compositions, chitosan has the effect promoting blood coagulation, natural metabolite can be generated by the lysozyme degraded in organism, have human non-toxic, the feature that can be absorbed completely by organism, its good solubility property prepares the first-class raw material of haemostatic medicament especially, use composition silicate, tea saponin and petal leachate with the use of, the cream frost system making it be prepared into there is certain fluidity and stability, and irreversible variable color can be there is be less than the environment of 7.1 at PH under in this cream frost system, this cream frost system under molten state can levelling in the surface of toothpick 1, indicative hemostatic layer 2 is formed after solidification, the levelling thickness of its single application is no more than 1mm, wherein tea saponin is except having good emulsifying, dispersion, outside moistening function, also there is antiinflammatory, the pharmacological actions such as analgesia.
It should be noted that, described composition silicate is Magnesiumaluminumsilicate, one or more mixture in lithium magnesium silicate or sodium magnesium silicate, the interpolation of composition silicate is more, the viscosity of cream is larger, mobility is lower, but the stability of cream and the effect that can realize atomization can increase with the interpolation of composition silicate and reduce, even can not pass through high temperature low tempertaure storage stability test smoothly, oil impregnate phenomenon is more easily there is in storage, be unfavorable for storage, and the too high smoothness that can affect its flowing of viscosity, be unfavorable for that the thin layer of the indicative hemostatic layer 2 in toothpick surface is formed, in addition, if when the end of toothpick 1 is provided with slot for holding described indicative hemostasis cream or position, hole, at use indicative hemostasis cream, added to toothpick surface man-hour, the auto-flowability of indicative hemostasis cream can make its slot automatically filling up end or position, hole, when user uses the toothpick after processing, soluble hemostyptic in its slot or position, hole becomes branch to be dissolved in gingival surface, and spread, gingiva is repaired, if the mobility of indicative hemostasis cream is excessive, then can not its slot or position, hole therefore, the addition of composition silicate is formed can flow and the essential condition of stability cream frost in 1%-1.5%, the emulsifying thickened systems of cream frost can be made can be held in steady statue for a long time, and certain mobility and viscosity can be kept when storing for subsequent use, make its cream can be faster and the more effective surface at toothpick forms thin layer.
Further description, described petal leachate is the leachate of Flos Chrysanthemi or Flos Rosae Rugosae.The leachate of Flos Chrysanthemi or Flos Rosae Rugosae under sour environment all colour developing be red or light red, the instruction after intraoral juice can be contacted by toothpick.
Further description, described adjusting agent is made up of essence and binding agent, and wherein, described essence is menthol, and described binding agent is sodium carboxymethyl cellulose or edible Gelatinum oxhide.Menthol is used to add as essence, when it acts on gingival surface, there is refrigerant effect, the sensation of pricking at gingival lesions place is reduced greatly, the use of binding agent can depend on the surface of toothpick 1 fast and effectively when making the agent of Oleum Camelliae composite spraying be sprayed at toothpick 1 surperficial, reduce the mobility of Oleum Camelliae composite spraying agent, make it in spraying process, not condense drippage.
Further description, described emulsifying agent is sucrose ester.Make Oleum Camelliae can more effectively be dissolved in the agent of Oleum Camelliae composite spraying, form more stable flush coater system.
Further description, described antiseptic is sodium benzoate.For the agent of Oleum Camelliae composite spraying provides a shelf-life, can deposit for subsequent use after prepared by the agent of Oleum Camelliae composite spraying within certain time limit.
Further description, described ethanol is anhydrous edible ethanol.Can effectively suppress or kill antibacterial.
Further description, described toothpick 1 is provided with one end of described indicative hemostatic layer 2, and it is signed body side surface and is provided with slot 101 or position, hole 102, and described slot 101 or position, described hole 102 are for holding described indicative hemostasis cream.Separately be provided with slot 101 or position, hole 102 for holding indicative hemostasis cream, increase the saturation of hemostatic compositions medicine in toothpick 1, and the solubility of hemostatic compositions, make cream in slot 101 and position, hole 102 under the effect of intraoral juice, be dissolvable in water gingival surface, spread at gingival surface, the periphery of gingival lesions place and injury region is carried out to the reparation on top layer, improve the health of gingiva.
Further description, the thickness of described indicative hemostatic layer 2 is 0.1-1mm.Because it has solubility, can not have influence on the actual size of the end of toothpick 1, but preferred thickness is 0.1-1mm, the pharmacology effective ingredient of its indicative hemostatic layer 2 can meet the reparation of general injury region, avoids unnecessary waste.
Further description, the above-mentioned preparation method that the toothpick of irreversible variable color occurs, comprises the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, carry out dry sterilization in high pressure vacuum drying equipment, and final acquisition has the toothpick 1 of Oleum Camelliae composite coating 3.
Further description, the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
Further description, the preparation of described Oleum Camelliae composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain the agent of Oleum Camelliae composite spraying for subsequent use.
It should be noted that, being prepared as of Oleum Camelliae: Semen Camelliae is peeled off through conventional method, dry, pulverize, steam and fry after, adopt milling process to extract Oleum Camelliae, obtain through alkali refining, washing, decolouring, deodorize, winterization the refine Oleum Camelliae meeting the edible one-level Oleum Brassicae campestris standard of country.
Embodiment 1
Indicative hemostasis cream and the agent of Oleum Camelliae composite spraying is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 30% chitosan, 1.5% composition silicate, 10% Borneolum Syntheticum, 15% tea saponin, 10% petal leachate, 3% sodium benzoate, 0.5% essence and 30% pure water;
The raw material of Oleum Camelliae composite coating comprises following composition: 45% Oleum Camelliae, 2.5% menthol, 0.5% sodium carboxymethyl cellulose, 20% ethanol, 10% emulsifying agent, 1% antiseptic, 22% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and the agent of Oleum Camelliae composite spraying to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.1mm;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by Oleum Camelliae composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of Oleum Camelliae composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g.
Embodiment 2
Indicative hemostasis cream and the agent of Oleum Camelliae composite spraying is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 45% chitosan, 1% composition silicate, 5% Borneolum Syntheticum, 10% tea saponin, 15% petal leachate, 1% sodium benzoate, 1% essence and 22% pure water;
The raw material of Oleum Camelliae composite coating comprises following composition: 30% Oleum Camelliae, 7% menthol, 3% edible Gelatinum oxhide, 30% ethanol, 5% emulsifying agent, 3% antiseptic, 22% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and the agent of Oleum Camelliae composite spraying to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.5mm;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by Oleum Camelliae composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of Oleum Camelliae composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g.
Embodiment 3
Indicative hemostasis cream and the agent of Oleum Camelliae composite spraying is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 50% chitosan, 1% composition silicate, 5% Borneolum Syntheticum, 10% tea saponin, 12% petal leachate, 1% sodium benzoate, 1% essence and 20% pure water;
The raw material of Oleum Camelliae composite coating comprises following composition: 40% Oleum Camelliae, 5% menthol, 2% sodium carboxymethyl cellulose, 27% ethanol, 8% emulsifying agent, 3% antiseptic, 15% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and the agent of Oleum Camelliae composite spraying to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.8mm;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by Oleum Camelliae composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of Oleum Camelliae composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g.
Embodiment 4
Indicative hemostasis cream and the agent of Oleum Camelliae composite spraying is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 40% chitosan, 1% composition silicate, 8% Borneolum Syntheticum, 12% tea saponin, 11% petal leachate, 2% sodium benzoate, 1% essence and 25% pure water;
The raw material of Oleum Camelliae composite coating comprises following composition: 35% Oleum Camelliae, 5% menthol, 2% edible Gelatinum oxhide, 22% ethanol, 5% emulsifying agent, 1% antiseptic, 30% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and the agent of Oleum Camelliae composite spraying to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 1mm;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by Oleum Camelliae composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of Oleum Camelliae composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g.
The toothpick of above-described embodiment 1 is used below in comparative example's group.
Comparative example organizes 1
After sterilizing, open type toothpick is used to store classifiedly without the toothpick of fungistatic effect and the toothpick that irreversible variable color occurs of the present invention by existing, respectively with or without processed group toothpick and antibacterial improvement group toothpick, being positioned over respectively, the different dining tables in same restaurant uncap for people fetches toothpick and carries out, after one week, recovery is carried out to remaining toothpick and detects.
Respectively microorganism detection test is carried out to the toothpick in non-processor group toothpick and antibacterial improvement group toothpick, its total number of bacterial colonies average out to of toothpick in non-processor group toothpick is 76cfu/g, its total number of bacterial colonies average out to of toothpick 8cfu/g in antibacterial improvement group toothpick, the Disposable Sanitary Accessory sanitary standard of China, its standard is that total number of bacterial colonies is less than 20cfu/g, the visible toothpick with Oleum Camelliae composite coating 3 of the present invention effectively can suppress or kill the antibacterial staying in its surface in certain useful life, guarantee that the total number of bacterial colonies on toothpick surface meets the Disposable Sanitary Accessory sanitary standard of China, effectively avoid the bacteriological infection at gingival lesions place, reduce the risk that the oral problem such as periodontal disease occur.
Comparative example organizes 2
Having random selecting 200 in the student using toothpick custom in certain university, stochastic averagina grouping being carried out to these 200 students, is respectively existing group and improvement group, often organizing each 100 students, the toothpick that it uses after the meal is specified.
The existing group of toothpick used is the toothpick without hemostasia effect in prior art, the toothpick with antibacterial anastalsis after improvement group uses the present invention to improve, and carries out record registration and statistical analysis, three weeks by a definite date to their using state.
The student of existing group generally represents that the use of toothpick uses similar with usual toothpick, and when puncturing gingiva, in oral cavity, the smell of blood is heavier, feels to have significantly hemorrhage, and minority student represents and easily causes gingiva problem to occur.
The student of improvement group generally represents toothpick in use, the toothpick that feel uses comparatively before will be got well, and there is effect of cool pain-alleviating, when puncturing gingiva especially because of carelessness, its intraoral smell of blood is lighter, substantially do not have bleeding subsequently, minority student represents original oral problem, and the situation as implication, gingival swelling and pain etc. is improved comparatively before.
Subjective appreciation after toothpick being used by existing group and improvement group student, can know that the toothpick with antibacterial anastalsis can effectively be repaired injured surface, it can prevent the bleeding state of this injury region, and can repair injury region, subside a swelling, pain relieving, life-time service significantly can improve the tissue on gingiva top layer, can solve part oral problem, as removed implication or alleviating gingival swelling and pain.
After contrast test terminates, the student of existing group is carried out to the test of next round, be three weeks by a definite date equally, change after the meal and use the toothpick with antibacterial anastalsis of the present invention, represent after test, comparatively, the toothpick of test is compared, it is fragrant that the toothpick that new test uses has light tea, and gingiva feels obvious refrigerant effect, even if pierce through gingiva because of carelessness, also can not feel the obvious smell of blood, the pain of gingiva significantly weakens.
Below know-why of the present invention is described in conjunction with specific embodiments.These describe just in order to explain principle of the present invention, and can not be interpreted as limiting the scope of the invention by any way.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other detailed description of the invention of the present invention, and these modes all will fall within protection scope of the present invention.

Claims (10)

1. a toothpick for irreversible variable color can occur, it is characterized in that: in the two ends of described toothpick, at least one end is provided with indicative hemostatic layer, the surface of described toothpick is provided with Oleum Camelliae composite coating;
Wherein, described indicative hemostatic layer is applied to solidify by indicative hemostasis cream and is formed, and the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent;
The raw material of described Oleum Camelliae composite coating comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
2. a kind of toothpick that irreversible variable color occurs according to claim 1, is characterized in that: described petal leachate is the leachate of Flos Chrysanthemi or Flos Rosae Rugosae.
3. a kind of toothpick that irreversible variable color occurs according to claim 1, is characterized in that: described emulsifying agent is sucrose ester.
4. a kind of toothpick that irreversible variable color occurs according to claim 1, is characterized in that: described adjusting agent is made up of essence and binding agent, and wherein, described essence is menthol, and described binding agent is sodium carboxymethyl cellulose or edible Gelatinum oxhide.
5. a kind of toothpick that irreversible variable color occurs according to claim 1, is characterized in that: described ethanol is anhydrous edible ethanol.
6. a kind of toothpick that irreversible variable color occurs according to claim 1, it is characterized in that: described toothpick is provided with one end of described indicative hemostatic layer, it is signed body side surface and is provided with slot or position, hole, and described slot or position, described hole are for holding described indicative hemostasis cream.
7. a kind of toothpick that irreversible variable color occurs according to claim 1, is characterized in that: the thickness of described indicative hemostatic layer is 0.1-1mm.
8. a kind of preparation method that the toothpick of irreversible variable color occurs according to claim 1, is characterized in that: comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick;
B, apply indicative hemostasis cream in any one end of the label body of toothpick or its two ends;
C, treat that the cream that step applies solidifies;
D, the surface spraying Oleum Camelliae composite spraying agent with the label body of cream obtained in step C, carry out dry sterilization in high pressure vacuum drying equipment, and final acquisition has the toothpick of Oleum Camelliae composite coating.
9. a kind of preparation method that the toothpick of irreversible variable color occurs according to claim 8, is characterized in that: the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
10. a kind of preparation method that the toothpick of irreversible variable color occurs according to claim 8, is characterized in that: the preparation of described Oleum Camelliae composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain the agent of Oleum Camelliae composite spraying for subsequent use.
CN201510536866.9A 2015-08-27 2015-08-27 Toothpick capable of undergoing irreversible discoloration and preparation method thereof Pending CN105055038A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3806686A4 (en) * 2018-06-12 2022-03-23 Buzzelet Development And Technologies Ltd Dental care cannabis device and use thereof

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CN2051856U (en) * 1989-06-14 1990-01-31 金鸿伟 Medicine toothpick
CN1045526A (en) * 1990-02-27 1990-09-26 邱石玉 Make toothpick have the ingredients manufacture method of health care
US5393229A (en) * 1993-06-14 1995-02-28 Ram; Zeev Dental cleaning implement including toothpick, and method of cleaning teeth therewith
US20040202981A1 (en) * 2002-12-31 2004-10-14 Luettgen Harold A. Whitening tip for dental flossing device
CN103690257A (en) * 2013-12-17 2014-04-02 江苏科技大学 Novel plant toothpick and preparation method thereof
CN103989532A (en) * 2014-05-21 2014-08-20 孙明杰 Edible toothpick for relieving pain, stopping bleeding and preventing and treating odontopathy
CN104013547A (en) * 2014-05-26 2014-09-03 皖南医学院 Toothpaste for stopping bleeding, brightening and refreshing breath and preparation method thereof
US20140263718A1 (en) * 2013-03-15 2014-09-18 Kathie Ann Marouthis Straw with hygiene pick

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2051856U (en) * 1989-06-14 1990-01-31 金鸿伟 Medicine toothpick
CN1045526A (en) * 1990-02-27 1990-09-26 邱石玉 Make toothpick have the ingredients manufacture method of health care
US5393229A (en) * 1993-06-14 1995-02-28 Ram; Zeev Dental cleaning implement including toothpick, and method of cleaning teeth therewith
US20040202981A1 (en) * 2002-12-31 2004-10-14 Luettgen Harold A. Whitening tip for dental flossing device
US20140263718A1 (en) * 2013-03-15 2014-09-18 Kathie Ann Marouthis Straw with hygiene pick
CN103690257A (en) * 2013-12-17 2014-04-02 江苏科技大学 Novel plant toothpick and preparation method thereof
CN103989532A (en) * 2014-05-21 2014-08-20 孙明杰 Edible toothpick for relieving pain, stopping bleeding and preventing and treating odontopathy
CN104013547A (en) * 2014-05-26 2014-09-03 皖南医学院 Toothpaste for stopping bleeding, brightening and refreshing breath and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3806686A4 (en) * 2018-06-12 2022-03-23 Buzzelet Development And Technologies Ltd Dental care cannabis device and use thereof

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