CN105213053A - A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof - Google Patents
A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof Download PDFInfo
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- CN105213053A CN105213053A CN201510542695.0A CN201510542695A CN105213053A CN 105213053 A CN105213053 A CN 105213053A CN 201510542695 A CN201510542695 A CN 201510542695A CN 105213053 A CN105213053 A CN 105213053A
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Abstract
A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof, its preparation method comprises the following steps: A, use bamboo wood or timber processing to obtain the label body of toothpick; B, the label body of petal leachate to toothpick with acid indicator effect is used to soak; C, dry sterilization, obtain the toothpick that irreversible variable color occurs after using.The present invention proposes a kind of preparation method using the toothpick of the irreversible variable color of rear generation, by the immersion of petal leachate, make toothpick that the change of irreversible color occur under the effect of intraoral juice, avoid cross infection, also can avoid the recovery of illegal businessman simultaneously.The present invention also proposes a kind of toothpick using above-mentioned preparation method to prepare, and self has good fungistatic effect before using, and avoid toothpick when not using by germ contamination, use backteeth signs and issues raw irreversible variable color, avoids cross infection.
Description
Technical field
The present invention relates to article of everyday use technical field, particularly relate to and a kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof.
Background technology
Common toothpick is clavas that are bamboo, wooden or plastics, wherein having one or two end for most advanced and sophisticated, during for picking one's teeth, toothpick tip being stretched into teeth space, the residue in teeth space can be rejected.One toothpick, may conceal tens thousand of antibacterials, easily illness finds its way in by the mouth, such as the disease such as hepatitis B, pulmonary tuberculosis.By 2012, Chinese Consumers' Association issued warning of consumption and says, the toothpick that domestic restaurant is equipped with is many is " three nothings " products, its sanitary condition is very troubling, surface bacteria content often severe overweight, increases the risk that user periodontal disease is ill, and country is not yet for relevant criterion worked out by toothpick.Especially some illegal businessmans, can carry out collection reclaiming to the toothpick after use and produce, there is huge risk in its safe and sanitary.Therefore the current toothpick in the urgent need to there is irreversible variable color after a kind of use is avoided or prevents the pernicious recovery of illegal businessman.
Summary of the invention
The object of the invention is to propose a kind of preparation method using the toothpick of the irreversible variable color of rear generation, by the immersion of petal leachate, make toothpick that the change of irreversible color occur under the effect of intraoral juice, avoid cross infection, also can avoid the recovery of illegal businessman simultaneously.
Another object of the present invention is to propose a kind of toothpick using above-mentioned preparation method to prepare, before using, self there is good fungistatic effect, avoid toothpick when not using by germ contamination, use backteeth signs and issues raw irreversible variable color, avoids cross infection.
For reaching this object, the present invention by the following technical solutions:
Use a preparation method for the toothpick of the irreversible variable color of rear generation, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick;
B, the label body of petal leachate to toothpick with acid indicator effect is used to soak;
C, dry sterilization, obtain the toothpick that irreversible variable color occurs after using.
Further description, described petal leachate is the petal leachate of Flos Chrysanthemi or Flos Rosae Rugosae.
Further description, also comprises hemostasis property of medicine treatment step between step B and step C, described hemostasis property of medicine treatment step is apply indicative hemostasis cream in any one end of the label body of step B acquisition or its two ends, forms indicative hemostatic layer in label surface.
Further description, the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent.
Further description, the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
Further description, also comprises antibacterial medicines treatment step between step B and step C, and described antibacterial medicines treatment step is that the label surface obtained in step B sprays antibacterial composite spraying agent, forms antibacterial composite coating, enter step C in label surface.
Further description, antibacterial medicines treatment step is also comprised after described hemostasis property of medicine treatment step completes, described antibacterial medicines treatment step is that the label surface obtained in front step sprays antibacterial composite spraying agent, forms antibacterial composite coating, enter step C in label surface.
Further description, the raw material of described antibacterial composite coating comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
Further description, the preparation of described antibacterial composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain antibacterial composite spraying agent for subsequent use.
Use the toothpick that above-mentioned preparation method prepares, in the two ends of described toothpick, at least one end is provided with indicative hemostatic layer, and the surface of described toothpick is provided with antibacterial composite coating.
A kind of beneficial effect using the preparation method of the toothpick of the irreversible variable color of rear generation of the present invention: 1, operation sequence is fast and simple; 2, by the immersion of petal leachate, make toothpick that the change of irreversible color occur under the effect of intraoral juice, avoid cross infection; 3, the preparation of its soluble hemostyptic cream frost used and antibacterial composite spraying agent is simple and easy, and easily processing is coated to toothpick surface.
The beneficial effect of the toothpick that the present invention uses said method to prepare: self have good fungistatic effect before 1, using, avoids toothpick when not using by germ contamination; 2, use backteeth to sign and issue raw irreversible variable color, avoid cross infection, also can avoid the recovery of illegal businessman; 3, gingiva is had to hemostasis, repairs effect; 3, improve the brightness on toothpick surface, reject the bamboo woody flavour road of wooden toothpick self.
Accompanying drawing explanation
Fig. 1 is the structural representation of one embodiment of the present of invention;
Fig. 2 is the structural representation of one embodiment of the present of invention;
Fig. 3 is the structural representation of the toothpick label body of one embodiment of the present of invention;
Fig. 4 is the partial enlargement structural representation of Fig. 3;
Fig. 5 is the structural representation of the toothpick label body of one embodiment of the present of invention.
Wherein: toothpick 1, toothpick end 11,12, indicative hemostatic layer 2, antibacterial composite coating 3, slot 101, position, hole 102.
Detailed description of the invention
Technical scheme of the present invention is further illustrated below in conjunction with accompanying drawing and specific embodiment.
Use a preparation method for the toothpick of the irreversible variable color of rear generation, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, the label body of petal leachate to toothpick with acid indicator effect is used to soak;
C, dry sterilization, obtain the toothpick that irreversible variable color occurs after using.
Petal leachate is used to soak toothpick, make toothpick, under PH is less than the environment of 7.1, irreversible variable color can occur, PH scope in human oral cavity is at 6.6-7.1, with there is the toothpick of acid indicative function when user uses, affect by the intraoral sour environment of user, there is the change of irreversible color in its end, when toothpick is positioned over desktop after using, other user can be avoided to use used toothpick because of carelessness, avoid cross infection, in addition, illegal businessman is also effectively avoided to recycle the toothpick after use.
Further description, described petal leachate is the petal leachate of Flos Chrysanthemi or Flos Rosae Rugosae.The leachate of Flos Chrysanthemi or Flos Rosae Rugosae under sour environment all colour developing be red or light red, the instruction after intraoral juice can be contacted by toothpick.
Further description, also comprises hemostasis property of medicine treatment step between step B and step C, described hemostasis property of medicine treatment step is apply indicative hemostasis cream in any one end of the label body of step B acquisition or its two ends, forms indicative hemostatic layer 2 in label surface.
Further description, the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent.
Further description, the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
The present invention is provided with indicative hemostatic layer 2 in toothpick either end, make user use toothpick pick one's teeth scratch because of carelessness time, soluble hemostyptic in its indicative hemostatic layer 2 becomes the dissolving by oral cavity endocrine liquid to be dissolved in gingival surface, injured surface is repaired, the effective bleeding state preventing this injury region.
More excellent, using chitosan as main hemostatic compositions, chitosan has the effect promoting blood coagulation, natural metabolite can be generated by the lysozyme degraded in organism, have human non-toxic, the feature that can be absorbed completely by organism, its good solubility property prepares the first-class raw material of haemostatic medicament especially, use composition silicate, tea saponin and petal leachate with the use of, the cream frost system making it be prepared into there is certain fluidity and stability, and irreversible variable color can be there is be less than the environment of 7.1 at PH under in this cream frost system, this cream frost system under molten state can levelling in the surface of toothpick 1, indicative hemostatic layer 2 is formed after solidification, the levelling thickness of its single application is no more than 1mm, wherein tea saponin is except having good emulsifying, dispersion, outside moistening function, also there is antiinflammatory, the pharmacological actions such as analgesia, injury region is repaired, detumescence, pain relieving, life-time service significantly can improve the tissue on gingiva top layer.
It should be noted that, described composition silicate is Magnesiumaluminumsilicate, one or more mixture in lithium magnesium silicate or sodium magnesium silicate, the interpolation of composition silicate is more, the viscosity of cream is larger, mobility is lower, but the stability of cream and the effect that can realize atomization can increase with the interpolation of composition silicate and reduce, even can not pass through high temperature low tempertaure storage stability test smoothly, oil impregnate phenomenon is more easily there is in storage, be unfavorable for storage, and the too high smoothness that can affect its flowing of viscosity, be unfavorable for that the thin layer of the indicative hemostatic layer 2 in toothpick surface is formed, in addition, if when the end of toothpick 1 is provided with slot for holding described indicative hemostasis cream or position, hole, at use indicative hemostasis cream, added to toothpick surface man-hour, the auto-flowability of indicative hemostasis cream can make its slot automatically filling up end or position, hole, when user uses the toothpick after processing, soluble hemostyptic in its slot or position, hole becomes branch to be dissolved in gingival surface, and spread, gingiva is repaired, if the mobility of indicative hemostasis cream is excessive, then can not its slot or position, hole therefore, the addition of composition silicate is formed can flow and the essential condition of stability cream frost in 1%-1.5%, the emulsifying thickened systems of cream frost can be made can be held in steady statue for a long time, and certain mobility and viscosity can be kept when storing for subsequent use, make its cream can be faster and the more effective surface at toothpick forms thin layer.
Further description, also comprises antibacterial medicines treatment step between step B and step C, and described antibacterial medicines treatment step is that the label surface obtained in step B sprays antibacterial composite spraying agent, forms antibacterial composite coating 3, enter step C in label surface.
Further description, antibacterial medicines treatment step is also comprised after described hemostasis property of medicine treatment step completes, described antibacterial medicines treatment step is that the label surface obtained in front step sprays antibacterial composite spraying agent, forms antibacterial composite coating 3, enter step C in label surface.Toothpick either end is provided with indicative hemostatic layer 2, make user use toothpick pick one's teeth scratch because of carelessness time, soluble hemostyptic in its indicative hemostatic layer 2 becomes the dissolving by oral cavity endocrine liquid to be dissolved in gingival surface, injured surface is repaired, the bleeding state of effective this injury region of prevention, and in conjunction with the Oleum Camelliae antioxidant content in antibacterial composite coating 3, injury region repaired, subside a swelling, pain relieving, life-time service significantly can improve the tissue on gingiva top layer.
Further description, the raw material of described antibacterial composite coating comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
Further description, described adjusting agent is made up of essence and binding agent, and wherein, described essence is menthol, and described binding agent is sodium carboxymethyl cellulose or edible Gelatinum oxhide.Menthol is used to add as essence, when it acts on gingival surface, there is refrigerant effect, the sensation of pricking at gingival lesions place is reduced greatly, the use of binding agent can depend on the surface of toothpick 1 fast and effectively when making antibacterial composite spraying agent be sprayed at toothpick 1 surperficial, reduce the mobility of antibacterial composite spraying agent, make it in spraying process, not condense drippage.
Further description, described emulsifying agent is sucrose ester.Make Oleum Camelliae can more effectively be dissolved in antibacterial composite spraying agent, form more stable flush coater system.
Further description, described antiseptic is sodium benzoate.For antibacterial composite spraying agent provides a shelf-life, can deposit for subsequent use after prepared by antibacterial composite spraying agent within certain time limit.
Further description, described ethanol is anhydrous edible ethanol.Can effectively suppress or kill antibacterial.
Further description, the preparation of described antibacterial composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain antibacterial composite spraying agent for subsequent use.
Antibacterial composite coating is arranged at the surface of toothpick 1, its Oleum Camelliae and ethanol form main antibacterial bacteriostatic protective layer on the surface of toothpick 1, toothpick 1 is made to store in put procedure the impact reduced by outside unhygienic environment, can be on the defensive to the antibacterial staying in its surface or kill, reduce the quantity of toothpick 1 surface bacteria greatly, wholesomeness when effective raising toothpick 1 is deposited, in addition, the setting of antibacterial composite coating 3 effectively can improve the brightness on toothpick 1 surface, change the lacklustre characteristic on wooden toothpick surface, in conjunction with the fragrance that Oleum Camelliae carries, eliminate the taste of the bamboo wood of wooden toothpick self.
It should be noted that, being prepared as of Oleum Camelliae: Semen Camelliae is peeled off through conventional method, dry, pulverize, steam and fry after, adopt milling process to extract Oleum Camelliae, obtain through alkali refining, washing, decolouring, deodorize, winterization the refine Oleum Camelliae meeting the edible one-level Oleum Brassicae campestris standard of country.
As shown in Figure 1-2, in the two ends 11,12 of described toothpick, at least one end is provided with indicative hemostatic layer 2, and the surface of described toothpick is provided with antibacterial composite coating 3.
Further description, described toothpick 1 is provided with one end of described indicative hemostatic layer 2, and as shown in Fig. 3 or Fig. 4 or Fig. 5, it is signed body side surface and is provided with slot 101 or position, hole 102, and described slot 101 or position, described hole 102 are for holding described indicative hemostasis cream.Separately be provided with slot 101 or position, hole 102 for holding indicative hemostasis cream, increase the saturation of hemostatic compositions medicine in toothpick 1, and the solubility of hemostatic compositions, make cream in slot 101 and position, hole 102 under the effect of intraoral juice, be dissolvable in water gingival surface, spread at gingival surface, the periphery of gingival lesions place and injury region is carried out to the reparation on top layer, improve the health of gingiva.
Embodiment 1-1
Indicative hemostasis cream is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 30% chitosan, 1.5% composition silicate, 10% Borneolum Syntheticum, 15% tea saponin, 10% petal leachate, 3% sodium benzoate, 0.5% essence and 30% pure water;
Use the indicative hemostasis cream of above-mentioned preparation to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1, carry out Flos Chrysanthemi leachate soak 3h to label body;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.5mm;
D, in high pressure vacuum drying equipment, carry out dry sterilization, finally obtain toothpick 1.
After using, the end colour developing that it uses is redness, and lasting one week also colour-fast; In use, lessly there is bleeding in the more sensitive user of gingiva, even if occurred, its intraoral smell of blood does not also weigh.
After toothpick deposits one month, its total number of bacterial colonies is 45cfu/g.
Embodiment 1-2
Antibacterial composite spraying agent is prepared by following ingredients:
The raw material of antibacterial composite coating comprises following composition: 45% Oleum Camelliae, 2.5% menthol, 0.5% sodium carboxymethyl cellulose, 20% ethanol, 10% emulsifying agent, 1% antiseptic, 22% pure water.
Use the antibacterial composite spraying agent of above-mentioned preparation to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1, carry out Flos Chrysanthemi leachate soak 3h to label body;
B, to signing the antibacterial composite spraying agent of surface spraying of body, wherein, the equipment that spraying uses is spraying nozzle equipment, by antibacterial composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of antibacterial composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies lower than 15cfu/g, after using, the end colour developing that it uses is redness, and lasting one week also colour-fast, and the more sensitive user of gingiva in use, easily occur bleeding, hemorrhage more, in oral cavity, the smell of blood is denseer.
Embodiment 1-3
Indicative hemostasis cream and antibacterial composite spraying agent is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 30% chitosan, 1.5% composition silicate, 10% Borneolum Syntheticum, 15% tea saponin, 10% petal leachate, 3% sodium benzoate, 0.5% essence and 30% pure water;
The raw material of antibacterial composite coating comprises following composition: 45% Oleum Camelliae, 2.5% menthol, 0.5% sodium carboxymethyl cellulose, 20% ethanol, 10% emulsifying agent, 1% antiseptic, 22% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and antibacterial composite spraying agent to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1, carry out Flos Chrysanthemi leachate soak 3h to label body;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.5mm;
D, the antibacterial composite spraying agent of the surface spraying with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by antibacterial composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of antibacterial composite coating 3.
After using, end colour developing that it uses is redness, continue one week also colour-fast, in use, lessly there is bleeding in the more sensitive user of gingiva, even if occurred, its intraoral smell of blood does not also weigh;
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g.
Embodiment 2
Indicative hemostasis cream and antibacterial composite spraying agent is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 45% chitosan, 1% composition silicate, 5% Borneolum Syntheticum, 10% tea saponin, 15% petal leachate, 1% sodium benzoate, 1% essence and 22% pure water;
The raw material of antibacterial composite coating comprises following composition: 30% Oleum Camelliae, 7% menthol, 3% edible Gelatinum oxhide, 30% ethanol, 5% emulsifying agent, 3% antiseptic, 22% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and antibacterial composite spraying agent to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.1mm;
D, the antibacterial composite spraying agent of the surface spraying with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by antibacterial composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of antibacterial composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g, and after using, the end colour developing that it uses is redness, and lasting one week also colour-fast.
Embodiment 3
Indicative hemostasis cream and antibacterial composite spraying agent is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 50% chitosan, 1% composition silicate, 5% Borneolum Syntheticum, 10% tea saponin, 12% petal leachate, 1% sodium benzoate, 1% essence and 20% pure water;
The raw material of antibacterial composite coating comprises following composition: 40% Oleum Camelliae, 5% menthol, 2% sodium carboxymethyl cellulose, 27% ethanol, 8% emulsifying agent, 3% antiseptic, 15% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and antibacterial composite spraying agent to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 0.8mm;
D, the antibacterial composite spraying agent of the surface spraying with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by antibacterial composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of antibacterial composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g, and after using, the end colour developing that it uses is redness, and lasting one week also colour-fast.
Embodiment 4
Indicative hemostasis cream and antibacterial composite spraying agent is prepared by following ingredients:
The raw material of indicative hemostasis cream comprises following composition: 40% chitosan, 1% composition silicate, 8% Borneolum Syntheticum, 12% tea saponin, 11% petal leachate, 2% sodium benzoate, 1% essence and 25% pure water;
The raw material of antibacterial composite coating comprises following composition: 35% Oleum Camelliae, 5% menthol, 2% edible Gelatinum oxhide, 22% ethanol, 5% emulsifying agent, 1% antiseptic, 30% pure water.
Use the indicative hemostasis cream of above-mentioned preparation and antibacterial composite spraying agent to process toothpick, comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick 1;
B, apply indicative hemostasis cream in any one end of the label body of toothpick 1 or its two ends;
C, treat that the cream that step applies solidifies, the indicative hemostatic layer thickness of acquisition is 1mm;
D, the antibacterial composite spraying agent of the surface spraying with the label body of cream obtained in step C, wherein, the equipment that spraying uses is spraying nozzle equipment, by antibacterial composite spraying agent atomizing spraying in toothpick surface, in high pressure vacuum drying equipment, carry out dry sterilization, final acquisition has the toothpick 1 of antibacterial composite coating 3.
After toothpick deposits one month, its total number of bacterial colonies is lower than 15cfu/g, and after using, the end colour developing that it uses is redness, and lasting one week also colour-fast.
The toothpick of above-described embodiment 1-3 is used below in comparative example's group.
Comparative example organizes 1
After sterilizing, open type toothpick is used to store classifiedly without the toothpick of fungistatic effect and the toothpick that irreversible variable color occurs of the present invention by existing, respectively with or without processed group toothpick and antibacterial improvement group toothpick, being positioned over respectively, the different dining tables in same restaurant uncap for people fetches toothpick and carries out, after one week, recovery is carried out to remaining toothpick and detects.
Respectively microorganism detection test is carried out to the toothpick in non-processor group toothpick and antibacterial improvement group toothpick, its total number of bacterial colonies average out to of toothpick in non-processor group toothpick is 76cfu/g, its total number of bacterial colonies average out to of toothpick 8cfu/g in antibacterial improvement group toothpick, the Disposable Sanitary Accessory sanitary standard of China, its standard is that total number of bacterial colonies is less than 20cfu/g, the visible toothpick with antibacterial composite coating 3 of the present invention effectively can suppress or kill the antibacterial staying in its surface in certain useful life, guarantee that the total number of bacterial colonies on toothpick surface meets the Disposable Sanitary Accessory sanitary standard of China, effectively avoid the bacteriological infection at gingival lesions place, reduce the risk that the oral problem such as periodontal disease occur.
Comparative example organizes 2
Having random selecting 200 in the student using toothpick custom in certain university, stochastic averagina grouping being carried out to these 200 students, is respectively existing group and improvement group, often organizing each 100 students, the toothpick that it uses after the meal is specified.
The existing group of toothpick used is the toothpick without hemostasia effect in prior art, the toothpick with antibacterial anastalsis after improvement group uses the present invention to improve, and carries out record registration and statistical analysis, three weeks by a definite date to their using state.
The student of existing group generally represents that the use of toothpick uses similar with usual toothpick, and when puncturing gingiva, in oral cavity, the smell of blood is heavier, feels to have significantly hemorrhage, and minority student represents and easily causes gingiva problem to occur.
The student of improvement group generally represents toothpick in use, the toothpick that feel uses comparatively before will be got well, and there is effect of cool pain-alleviating, when puncturing gingiva especially because of carelessness, its intraoral smell of blood is lighter, substantially do not have bleeding subsequently, minority student represents original oral problem, and the situation as implication, gingival swelling and pain etc. is improved comparatively before.
Subjective appreciation after toothpick being used by existing group and improvement group student, can know that the toothpick with antibacterial anastalsis can effectively be repaired injured surface, it can prevent the bleeding state of this injury region, and can repair injury region, subside a swelling, pain relieving, life-time service significantly can improve the tissue on gingiva top layer, can solve part oral problem, as removed implication or alleviating gingival swelling and pain.
After contrast test terminates, the student of existing group is carried out to the test of next round, be three weeks by a definite date equally, change after the meal and use the toothpick with antibacterial anastalsis of the present invention, represent after test, comparatively, the toothpick of test is compared, it is fragrant that the toothpick that new test uses has light tea, and gingiva feels obvious refrigerant effect, even if pierce through gingiva because of carelessness, also can not feel the obvious smell of blood, the pain of gingiva significantly weakens.
Below know-why of the present invention is described in conjunction with specific embodiments.These describe just in order to explain principle of the present invention, and can not be interpreted as limiting the scope of the invention by any way.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other detailed description of the invention of the present invention, and these modes all will fall within protection scope of the present invention.
Claims (10)
1. there is a preparation method for the toothpick of irreversible variable color after using, it is characterized in that: comprise the following steps:
A, use bamboo wood or timber processing obtain the label body of toothpick;
B, the label body of petal leachate to toothpick with acid indicator effect is used to soak;
C, dry sterilization, obtain the toothpick that irreversible variable color occurs after using.
2. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 1, is characterized in that: described petal leachate is the petal leachate of Flos Chrysanthemi or Flos Rosae Rugosae.
3. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 1, it is characterized in that: between step B and step C, also comprise hemostasis property of medicine treatment step, described hemostasis property of medicine treatment step is apply indicative hemostasis cream in any one end of the label body of step B acquisition or its two ends, forms indicative hemostatic layer in label surface.
4. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 3, is characterized in that: the raw material of described indicative hemostasis cream comprises following composition: 30-50% chitosan, 1-1.5% composition silicate, 5-10% Borneolum Syntheticum, 10-15% tea saponin, 10-15% petal leachate, 1-3% antiseptic, 0.5-1% essence and 20-30% solvent.
5. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 1, is characterized in that: the preparation of described indicative hemostasis cream comprises following operation:
(1) weighing: according to the dissolution characteristics of material, presses oil phase by all materials or aqueous phase classification weighs, and wherein tea saponin joins oil phase, and composition silicate joins aqueous phase, and antiseptic and essence independently weigh;
(2) dissolve, heating: be dissolved in by oil phase material in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
(3) emulsifying: the aqueous phase that hydration is good in step (2) is pumped in emulsifying pot, and 80 DEG C of insulations, start stirring, homogenizing in emulsifying pot, oil phase component is pumped in emulsifying pot, homogenizing 3-5 minute, stirs cooling, is cooled to add antiseptic when 60 DEG C until cream;
(4) discharging, obtains indicative hemostasis cream for subsequent use.
6. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 1, it is characterized in that: between step B and step C, also comprise antibacterial medicines treatment step, described antibacterial medicines treatment step is that the label surface obtained in step B sprays antibacterial composite spraying agent, form antibacterial composite coating in label surface, enter step C.
7. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 3, it is characterized in that: after described hemostasis property of medicine treatment step completes, also comprise antibacterial medicines treatment step, described antibacterial medicines treatment step is that the label surface obtained in front step sprays antibacterial composite spraying agent, form antibacterial composite coating in label surface, enter step C.
8. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 6 or 7, is characterized in that: the raw material of described antibacterial composite coating comprises following composition: 30-45% Oleum Camelliae, 3-10% adjusting agent, 20-30% ethanol, 5-10% emulsifying agent, 1-3% antiseptic, 15-30% pure water.
9. a kind of preparation method using the toothpick of the irreversible variable color of rear generation according to claim 8, is characterized in that: the preparation of described antibacterial composite spraying agent comprises following operation:
A, weighing: each component is independently weighed;
B, mixing, stirring and emulsifying: in Oleum Camelliae, add ethanol, emulsifying agent and adjusting agent, and add pure water and be uniformly mixed, and be heated to 70 DEG C of insulated and stirred homogenizing;
C, homogenizing, after 10 minutes, stir cooling, are cooled to add antiseptic when 60 DEG C until system;
D, discharging, obtain antibacterial composite spraying agent for subsequent use.
10. the toothpick using the preparation method of claim 7 to prepare, is characterized in that: in the two ends of described toothpick, at least one end is provided with indicative hemostatic layer, and the surface of described toothpick is provided with antibacterial composite coating.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510542695.0A CN105213053A (en) | 2015-08-27 | 2015-08-27 | A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510542695.0A CN105213053A (en) | 2015-08-27 | 2015-08-27 | A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105213053A true CN105213053A (en) | 2016-01-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510542695.0A Pending CN105213053A (en) | 2015-08-27 | 2015-08-27 | A kind ofly use toothpick of the irreversible variable color of rear generation and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3806686A4 (en) * | 2018-06-12 | 2022-03-23 | Buzzelet Development And Technologies Ltd | Dental care cannabis device and use thereof |
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| CN1045526A (en) * | 1990-02-27 | 1990-09-26 | 邱石玉 | Make toothpick have the ingredients manufacture method of health care |
| US5393229A (en) * | 1993-06-14 | 1995-02-28 | Ram; Zeev | Dental cleaning implement including toothpick, and method of cleaning teeth therewith |
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| EP3806686A4 (en) * | 2018-06-12 | 2022-03-23 | Buzzelet Development And Technologies Ltd | Dental care cannabis device and use thereof |
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Application publication date: 20160106 |