CN103666043A - UV printing ink having quick solidification effect and good adhesive attraction - Google Patents
UV printing ink having quick solidification effect and good adhesive attraction Download PDFInfo
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- CN103666043A CN103666043A CN201310600485.3A CN201310600485A CN103666043A CN 103666043 A CN103666043 A CN 103666043A CN 201310600485 A CN201310600485 A CN 201310600485A CN 103666043 A CN103666043 A CN 103666043A
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- printing ink
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- acetone
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- 230000008023 solidification Effects 0.000 title abstract 4
- 238000007711 solidification Methods 0.000 title abstract 4
- 239000000853 adhesive Substances 0.000 title abstract 3
- 230000001070 adhesive effect Effects 0.000 title abstract 3
- 230000000694 effects Effects 0.000 title abstract 2
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims abstract description 21
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 20
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims abstract description 14
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims abstract description 7
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920003180 amino resin Polymers 0.000 claims abstract description 7
- 239000004021 humic acid Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- JHPBZFOKBAGZBL-UHFFFAOYSA-N (3-hydroxy-2,2,4-trimethylpentyl) 2-methylprop-2-enoate Chemical compound CC(C)C(O)C(C)(C)COC(=O)C(C)=C JHPBZFOKBAGZBL-UHFFFAOYSA-N 0.000 claims abstract description 4
- PIILXFBHQILWPS-UHFFFAOYSA-N tributyltin Chemical compound CCCC[Sn](CCCC)CCCC PIILXFBHQILWPS-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 6
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims description 6
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims description 3
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 239000000654 additive Substances 0.000 abstract 2
- 230000000996 additive effect Effects 0.000 abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- XRNOKWSDVWMURZ-UHFFFAOYSA-N carbamic acid;ethenoxyethene Chemical compound NC(O)=O.C=COC=C XRNOKWSDVWMURZ-UHFFFAOYSA-N 0.000 abstract 1
- AMTWCFIAVKBGOD-UHFFFAOYSA-N dioxosilane;methoxy-dimethyl-trimethylsilyloxysilane Chemical compound O=[Si]=O.CO[Si](C)(C)O[Si](C)(C)C AMTWCFIAVKBGOD-UHFFFAOYSA-N 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 abstract 1
- 239000004814 polyurethane Substances 0.000 abstract 1
- 229940083037 simethicone Drugs 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 25
- 239000000126 substance Substances 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001723 curing Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000005283 ground state Effects 0.000 description 1
- -1 ion free radical Chemical class 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a UV printing ink having quick solidification effect and good adhesive attraction. The UV printing ink is characterized by comprising the following raw materials in parts by weight: 1-3 parts of organic pigment, 30-40 parts of polyurethane acrylate, 10-14 parts of acrylic acid ethyl ester, 10-12 parts of methyl ethyl ketone, 20-23 parts of amino resin, 4-5 parts of simethicone, 1-2 parts of humic acid, 1-2 parts of octadecanol, 3-4 parts of methacrylic ester, 20-24 parts of vinyl ether carbamate, 4-6 parts of 2-hydroxyl-2 methyl-1 phenyl-1 acetone, 2-3 parts of tributyl tin trichloride, and 4-5 parts of an additive. The additive improves the toughness of the printing ink, enables the printing ink to be dispersed uniformly, and maintains the stability of the printing ink. The printing ink can improve the solidification film flexibility while ensuring the good adhesive attraction of overprinted ink films, is fast in solidification and improves the product quality.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, UV ink that particularly a kind of quick solidifying sticking power is good and preparation method thereof.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can produce different-energy, the monomer polymerization in different ink vehicles is become to polymkeric substance, so the look film of UV ink has good machinery and chemical property.The curing mechanism of UV curable ink is, the light trigger in system directly or indirectly absorbs after ultraviolet luminous energy, from ground state transition to excited singlet, alters and jump to excited triplet state between being; After excited singlet or triplet state experience unit molecule or bimolecular chemical action, the biologically active fragment that generation can trigger monomer polymerization, these fragments can be free radical, positively charged ion, negatively charged ion or ion free radical.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, resistance to solvent, wear resisting property is good.In UV ink, light trigger is a kind of light activated compound that is subject to, and after absorb light is shone, is excited into free radical, and energy is transferred to photosensitivity molecule or photocrosslinking agent, makes UV China ink that photocuring reaction occur.UV China ink has become a kind of more ripe ink technology at present, and its pollutant emission is almost nil.Except not containing solvent, UV China ink is also just like being difficult for scumming, and site is clear, the bright-coloured light of mass colour, the advantage such as chemical resistance is excellent, low-consuming.
Summary of the invention
The object of this invention is to provide UV ink that a kind of quick solidifying sticking power is good and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
The UV ink that quick solidifying sticking power is good, is made by the raw material of following weight part: pigment dyestuff 1-3, urethane acrylate 30-40, ethyl propenoate 10-14, methylethylketone 10-12, aminoresin 20-23, dimethyl silicone oil 4-5, humic acid 1-2, stearyl alcohol 1-2, methacrylic ester 3-4, vinyl ether type carbamate 20-24, phenyl-1, methyl-1,2-hydroxyl-2 acetone 4-6, tributyl tin trichloride 2-3, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, morpholine 1-2, neopentyl glycol 3-4, oxidation inhibitor 1035 1-2, linking agent TAC2-3, tri (propylene glycol) diacrylate 10-12,1-Methoxy-2-propyl acetate 5-10, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
The UV ink that quick solidifying sticking power of the present invention is good, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, ethyl propenoate, methylethylketone, aminoresin, dimethyl silicone oil, humic acid, stearyl alcohol stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except the acetone of phenyl-1, methyl-1,2-hydroxyl-2, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add phenyl-1, methyl-1,2-hydroxyl-2 acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even, and maintained the stability of ink; The present invention has improved the snappiness of cured film, guarantees the good adhesion of double exposure ink film, solidifies rapidly, has promoted quality product.
Specific embodiments
Below by specific examples, the present invention is described in detail.
The UV ink that quick solidifying sticking power is good, by following weight part (kilogram) raw material make: pigment dyestuff 1, urethane acrylate 30, ethyl propenoate 10, methylethylketone 10, aminoresin 20, dimethyl silicone oil 4, humic acid 1, stearyl alcohol 1, methacrylic ester 3, vinyl ether type carbamate 20, phenyl-1, methyl-1,2-hydroxyl-2 acetone 4, tributyl tin trichloride 2, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, silane resin acceptor kh-550 2, morpholine 1, neopentyl glycol 3, oxidation inhibitor 1,035 1, linking agent TAC2, tri (propylene glycol) diacrylate 10,1-Methoxy-2-propyl acetate 5, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
The UV ink that quick solidifying sticking power of the present invention is good, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, ethyl propenoate, methylethylketone, aminoresin, dimethyl silicone oil, humic acid, stearyl alcohol stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except the acetone of phenyl-1, methyl-1,2-hydroxyl-2, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add phenyl-1, methyl-1,2-hydroxyl-2 acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. the UV ink that quick solidifying sticking power is good, it is characterized in that, by the raw material of following weight part, made: pigment dyestuff 1-3, urethane acrylate 30-40, ethyl propenoate 10-14, methylethylketone 10-12, aminoresin 20-23, dimethyl silicone oil 4-5, humic acid 1-2, stearyl alcohol 1-2, methacrylic ester 3-4, vinyl ether type carbamate 20-24, phenyl-1, methyl-1,2-hydroxyl-2 acetone 4-6, tributyl tin trichloride 2-3, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, morpholine 1-2, neopentyl glycol 3-4, oxidation inhibitor 1035 1-2, linking agent TAC2-3, tri (propylene glycol) diacrylate 10-12,1-Methoxy-2-propyl acetate 5-10, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. the UV ink that quick solidifying sticking power is good according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, ethyl propenoate, methylethylketone, aminoresin, dimethyl silicone oil, humic acid, stearyl alcohol stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except the acetone of phenyl-1, methyl-1,2-hydroxyl-2, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add phenyl-1, methyl-1,2-hydroxyl-2 acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600485.3A CN103666043B (en) | 2013-11-25 | 2013-11-25 | UV ink that a kind of quick solidifying sticking power is good and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600485.3A CN103666043B (en) | 2013-11-25 | 2013-11-25 | UV ink that a kind of quick solidifying sticking power is good and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666043A true CN103666043A (en) | 2014-03-26 |
| CN103666043B CN103666043B (en) | 2016-04-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201310600485.3A Active CN103666043B (en) | 2013-11-25 | 2013-11-25 | UV ink that a kind of quick solidifying sticking power is good and preparation method thereof |
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| Country | Link |
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| CN (1) | CN103666043B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194471A (en) * | 2014-07-28 | 2014-12-10 | 蚌埠首创滤清器有限公司 | Printing ink prepared by modifying waste powdered ink |
| CN104263062A (en) * | 2014-09-03 | 2015-01-07 | 安徽雅美油墨有限公司 | High-adsorption wear-resistant water-based environment-friendly photocuring tin printing ink |
| CN104312265A (en) * | 2014-11-11 | 2015-01-28 | 合肥皖为电气设备工程有限责任公司 | Environmentally friendly alcohol soluble anti-yellowing plastic printing ink and preparation method thereof |
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| CN1339054A (en) * | 1999-01-29 | 2002-03-06 | 日清制油株式会社 | Coating material or ink compositions |
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN102321407A (en) * | 2011-09-06 | 2012-01-18 | 南昌航空大学 | Electron beam cured tin printing ink |
| CN102433044A (en) * | 2011-11-02 | 2012-05-02 | 广东新中源陶瓷有限公司 | Ink for 3D digital ink-jet ceramic tile |
| CN102993824A (en) * | 2011-09-14 | 2013-03-27 | 中国科学院化学研究所 | UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103160168A (en) * | 2011-12-12 | 2013-06-19 | 中国科学院化学研究所 | Waterborne UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
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2013
- 2013-11-25 CN CN201310600485.3A patent/CN103666043B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1339054A (en) * | 1999-01-29 | 2002-03-06 | 日清制油株式会社 | Coating material or ink compositions |
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN102321407A (en) * | 2011-09-06 | 2012-01-18 | 南昌航空大学 | Electron beam cured tin printing ink |
| CN102993824A (en) * | 2011-09-14 | 2013-03-27 | 中国科学院化学研究所 | UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
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| CN103160168A (en) * | 2011-12-12 | 2013-06-19 | 中国科学院化学研究所 | Waterborne UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194471A (en) * | 2014-07-28 | 2014-12-10 | 蚌埠首创滤清器有限公司 | Printing ink prepared by modifying waste powdered ink |
| CN104194471B (en) * | 2014-07-28 | 2016-06-15 | 蚌埠首创滤清器有限公司 | A kind of printing-ink being modifiied preparation by wasted ink powder |
| CN104263062A (en) * | 2014-09-03 | 2015-01-07 | 安徽雅美油墨有限公司 | High-adsorption wear-resistant water-based environment-friendly photocuring tin printing ink |
| CN104263062B (en) * | 2014-09-03 | 2016-04-27 | 安徽雅美油墨有限公司 | A kind of high absorption abrasion-resistance water environmental protection photocuring tin printing ink |
| CN104312265A (en) * | 2014-11-11 | 2015-01-28 | 合肥皖为电气设备工程有限责任公司 | Environmentally friendly alcohol soluble anti-yellowing plastic printing ink and preparation method thereof |
| CN104312265B (en) * | 2014-11-11 | 2016-04-27 | 合肥皖为电气设备工程有限责任公司 | Molten color inhibition plastic printing ink of a kind of environment-friendly type alcohol and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103666043B (en) | 2016-04-13 |
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