CN103666040B - UV curable ink of a kind of good luster that flowed and preparation method thereof - Google Patents
UV curable ink of a kind of good luster that flowed and preparation method thereof Download PDFInfo
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- CN103666040B CN103666040B CN201310600462.2A CN201310600462A CN103666040B CN 103666040 B CN103666040 B CN 103666040B CN 201310600462 A CN201310600462 A CN 201310600462A CN 103666040 B CN103666040 B CN 103666040B
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- 239000002932 luster Substances 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims description 8
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims abstract description 14
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 13
- RMVRSNDYEFQCLF-UHFFFAOYSA-N thiophenol Chemical compound SC1=CC=CC=C1 RMVRSNDYEFQCLF-UHFFFAOYSA-N 0.000 claims abstract description 12
- XMLYCEVDHLAQEL-UHFFFAOYSA-N 2-hydroxy-2-methyl-1-phenylpropan-1-one Chemical compound CC(C)(O)C(=O)C1=CC=CC=C1 XMLYCEVDHLAQEL-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- QXONIHMUSQFKJU-UHFFFAOYSA-N 2-(prop-1-enoxymethyl)oxirane Chemical compound CC=COCC1CO1 QXONIHMUSQFKJU-UHFFFAOYSA-N 0.000 claims abstract description 7
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims abstract description 7
- GWZMWHWAWHPNHN-UHFFFAOYSA-N 2-hydroxypropyl prop-2-enoate Chemical compound CC(O)COC(=O)C=C GWZMWHWAWHPNHN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 244000028419 Styrax benzoin Species 0.000 claims abstract description 7
- 235000000126 Styrax benzoin Nutrition 0.000 claims abstract description 7
- 235000008411 Sumatra benzointree Nutrition 0.000 claims abstract description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229960002130 benzoin Drugs 0.000 claims abstract description 7
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 7
- 239000011575 calcium Substances 0.000 claims abstract description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 7
- 239000001071 citrus reticulata blanco var. mandarin Substances 0.000 claims abstract description 7
- 239000007822 coupling agent Substances 0.000 claims abstract description 7
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000010459 dolomite Substances 0.000 claims abstract description 7
- 229910000514 dolomite Inorganic materials 0.000 claims abstract description 7
- 239000000975 dye Substances 0.000 claims abstract description 7
- 235000019382 gum benzoic Nutrition 0.000 claims abstract description 7
- 229910052901 montmorillonite Inorganic materials 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- 229920000570 polyether Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- -1 6-tertiary butyl-tolyl Chemical group 0.000 claims abstract description 4
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims description 3
- GTELLNMUWNJXMQ-UHFFFAOYSA-N 2-ethyl-2-(hydroxymethyl)propane-1,3-diol;prop-2-enoic acid Chemical class OC(=O)C=C.OC(=O)C=C.OC(=O)C=C.CCC(CO)(CO)CO GTELLNMUWNJXMQ-UHFFFAOYSA-N 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 2
- 239000004721 Polyphenylene oxide Substances 0.000 claims 2
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract description 5
- 229920002635 polyurethane Polymers 0.000 abstract description 5
- 239000004814 polyurethane Substances 0.000 abstract description 5
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract description 5
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract description 5
- 239000002904 solvent Substances 0.000 abstract description 5
- 238000007639 printing Methods 0.000 abstract description 2
- 238000007711 solidification Methods 0.000 abstract description 2
- 230000008023 solidification Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of UV curable ink of the good luster that flowed, it is characterized in that, be made up of the raw material of following weight part: nano-calcium carbonate calcium powder 2-3, pigment dyestuff 1-2, ground dolomite 1-2, montmorillonite 1-2, titanate coupling agent TMC-TTS? 1-2, polyurethane acroleic acid fat 20-30, 2-hydroxy-2-methyl-Propiophenone 6-8, mandarin oil 1-2, benzoin dimethylether 5-8, propenyl glycidyl ether 1-2, UV polyethers propylene 9-12, 2-hydroxypropyl acrylate 10-12, tri (propylene glycol) diacrylate 10-12, linking agent TAC1-2, 4, 4-bis-(a 6-tertiary butyl-tolyl) thiophenol 3-4, trisnonylphenyl phosphite 4-6, auxiliary agent 4-5, auxiliary agent of the present invention improves the toughness of ink, makes distributes ink even, and maintains the stability of ink, ink solidification of the present invention is fast, color is gorgeous, good luster, mobility are good, printing performance good and solvent resistant shampooing.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of UV curable ink and preparation method thereof of the good luster that flowed.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can different-energy be produced, the monomer polymerization in different ink vehicle is become polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, solvent resistant, wear resisting property is good.In UV ink, light trigger is that one is subject to light activated compound, after absorb light is shone, be excited into free radical, and energy trasfer, to photosensitivity molecule or photocrosslinking agent, makes UV ink that photocuring reaction occur.Current UV ink has become a kind of more ripe ink technology, and its pollutant emission is almost nil.Except not containing solvent, UV ink also just like not easily scumming, the advantages such as site is clear, the bright-coloured light of mass colour, and chemical resistance is excellent, low-consuming.
Summary of the invention
The object of this invention is to provide UV curable ink of a kind of good luster that flowed and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of UV curable ink of the good luster that flowed, be made up of the raw material of following weight part: nano-calcium carbonate calcium powder 2-3, pigment dyestuff 1-2, ground dolomite 1-2, montmorillonite 1-2, titanate coupling agent TMC-TTS1-2, polyurethane acroleic acid fat 20-30, 2-hydroxy-2-methyl-Propiophenone 6-8, mandarin oil 1-2, benzoin dimethylether 5-8, propenyl glycidyl ether 1-2, UV polyethers propylene 9-12, 2-hydroxypropyl acrylate 10-12, tri (propylene glycol) diacrylate 10-12, linking agent TAC1-2, 4, 4-bis-(a 6-tertiary butyl-tolyl) thiophenol 3-4, trisnonylphenyl phosphite 4-6, auxiliary agent 4-5,
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, tea-polyphenol 2-3, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, oxidation inhibitor 10351-2,2-butoxy-ethanol 3-4, linking agent TAC2-3, ethoxylated trimethylolpropane triacrylate 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curable ink of the good luster that flowed of the present invention, be made up of following concrete steps: first add nano-calcium carbonate calcium powder, pigment dyestuff, ground dolomite, montmorillonite, titanate coupling agent TMC-TTS, polyurethane acroleic acid fat, mandarin oil, benzoin dimethylether, propenyl glycidyl ether, UV polyethers propylene, 2-hydroxypropyl acrylate, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 2-hydroxy-2-methyl-Propiophenone are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 2-hydroxy-2-methyl-Propiophenone, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The invention has the beneficial effects as follows: auxiliary agent of the present invention improves the toughness of ink, make distributes ink even, and maintain the stability of ink; Ink solidification of the present invention is fast, color is gorgeous, good luster, mobility are good, printing performance good and solvent resistant shampooing.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of UV curable ink of the good luster that flowed, be made up of the raw material of following weight part: nano-calcium carbonate calcium powder 2-3, pigment dyestuff 1-2, ground dolomite 1-2, montmorillonite 1-2, titanate coupling agent TMC-TTS1-2, polyurethane acroleic acid fat 20-30, 2-hydroxy-2-methyl-Propiophenone 6-8, mandarin oil 1-2, benzoin dimethylether 5-8, propenyl glycidyl ether 1-2, UV polyethers propylene 9-12, 2-hydroxypropyl acrylate 10-12, tri (propylene glycol) diacrylate 10-12, linking agent TAC1-2, 4, 4-bis-(a 6-tertiary butyl-tolyl) thiophenol 3-4, trisnonylphenyl phosphite 4-6, auxiliary agent 4-5,
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2, nano mica powder 0.2, silane resin acceptor kh-550 2, tea-polyphenol 2, neopentyl glycol 5, p-tert-butyl benzoic acid 1, oxidation inhibitor 10351,2-butoxy-ethanol 3, linking agent TAC2, ethoxylated trimethylolpropane triacrylate 10, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curable ink of the good luster that flowed of the present invention, be made up of following concrete steps: first add nano-calcium carbonate calcium powder, pigment dyestuff, ground dolomite, montmorillonite, titanate coupling agent TMC-TTS, polyurethane acroleic acid fat, mandarin oil, benzoin dimethylether, propenyl glycidyl ether, UV polyethers propylene, 2-hydroxypropyl acrylate, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 2-hydroxy-2-methyl-Propiophenone are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 2-hydroxy-2-methyl-Propiophenone, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, 100% attachment; Use the spirituous cotton balls of leaching, 300 grams of pressure wipings 50 times, are as good as shape; To be soaked in salad oil (normal temperature) 8 hours, to be as good as shape; Use and be soaked with the cotton balls of salt solution, 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. the UV curable ink of the good luster that flowed, it is characterized in that, be prepared from by the raw material of following weight part: nano-calcium carbonate calcium powder 2-3, pigment dyestuff 1-2, ground dolomite 1-2, montmorillonite 1-2, titanate coupling agent TMC-TTS1-2, urethane acrylate 20-30, 2-hydroxy-2-methyl Propiophenone 6-8, mandarin oil 1-2, benzoin dimethylether 5-8, propenyl glycidyl ether 1-2, UV polyether acrylate 9-12, 2-hydroxypropyl acrylate 10-12, tri (propylene glycol) diacrylate 10-12, linking agent TAC1-2, 4, 4-bis-(a 6-tertiary butyl-tolyl) thiophenol 3-4, trisnonylphenyl phosphite 4-6, auxiliary agent 4-5,
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, tea-polyphenol 2-3, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, oxidation inhibitor 10351-2, butoxy ethanol 3-4, linking agent TAC2-3, ethoxylated trimethylolpropane triacrylate 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
2. the UV curable ink of the good luster that flowed according to claim 1, it is characterized in that, be made up of following concrete steps: first add nano-calcium carbonate calcium powder, pigment dyestuff, ground dolomite, montmorillonite, titanate coupling agent TMC-TTS, urethane acrylate, mandarin oil, benzoin dimethylether, propenyl glycidyl ether, UV polyether acrylate, 2-hydroxypropyl acrylate, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 2-hydroxy-2-methyl Propiophenone are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 2-hydroxy-2-methyl-Propiophenone, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600462.2A CN103666040B (en) | 2013-11-25 | 2013-11-25 | UV curable ink of a kind of good luster that flowed and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600462.2A CN103666040B (en) | 2013-11-25 | 2013-11-25 | UV curable ink of a kind of good luster that flowed and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666040A CN103666040A (en) | 2014-03-26 |
| CN103666040B true CN103666040B (en) | 2016-04-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310600462.2A Active CN103666040B (en) | 2013-11-25 | 2013-11-25 | UV curable ink of a kind of good luster that flowed and preparation method thereof |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101291816A (en) * | 2005-10-21 | 2008-10-22 | 爱克发印艺公司 | Set of curable liquids and methods for inkjet printing |
| CN101292000A (en) * | 2005-10-21 | 2008-10-22 | 爱克发印艺公司 | Curable inkjet ink set and inkjet printing method |
| CN102369248A (en) * | 2009-04-08 | 2012-03-07 | 大日精化工业株式会社 | Color composition for pixel-forming ink, pigment dispersion liquid, pixel-forming ink, color filter, and production methods thereof |
| CN102993824A (en) * | 2011-09-14 | 2013-03-27 | 中国科学院化学研究所 | UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103160168A (en) * | 2011-12-12 | 2013-06-19 | 中国科学院化学研究所 | Waterborne UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103232751A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | UV (ultraviolet) curing ink and application thereof |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
-
2013
- 2013-11-25 CN CN201310600462.2A patent/CN103666040B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101291816A (en) * | 2005-10-21 | 2008-10-22 | 爱克发印艺公司 | Set of curable liquids and methods for inkjet printing |
| CN101292000A (en) * | 2005-10-21 | 2008-10-22 | 爱克发印艺公司 | Curable inkjet ink set and inkjet printing method |
| CN102369248A (en) * | 2009-04-08 | 2012-03-07 | 大日精化工业株式会社 | Color composition for pixel-forming ink, pigment dispersion liquid, pixel-forming ink, color filter, and production methods thereof |
| CN102993824A (en) * | 2011-09-14 | 2013-03-27 | 中国科学院化学研究所 | UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103160168A (en) * | 2011-12-12 | 2013-06-19 | 中国科学院化学研究所 | Waterborne UV-curable ink used in inkjet printing direct-to-plate, and preparation method and application thereof |
| CN103232751A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | UV (ultraviolet) curing ink and application thereof |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
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| CN103666040A (en) | 2014-03-26 |
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